DTA measure 2f Date: 20251125:1742 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.27 s Mass = 100.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1280 0.3864 243.0042 242.6179 275.2261 1.8938 0.3873 243.2155 242.8282 275.2290 2.7525 0.3884 243.4685 243.0801 275.2067 3.5088 0.3929 243.6959 243.3030 275.1269 4.3368 0.3935 243.9237 243.5302 275.0506 5.1340 0.3940 244.1561 243.7621 274.9483 5.9313 0.3970 244.3906 243.9935 274.8425 6.7285 0.4010 244.6272 244.2262 274.7146 7.5150 0.4017 244.8449 244.4432 274.5984 8.3528 0.4030 245.0690 244.6661 274.4868 9.1090 0.4018 245.2546 244.8528 274.3539 9.9575 0.4055 245.4719 245.0664 274.2368 10.7343 0.4085 245.6852 245.2767 274.1022 11.5520 0.4101 245.9301 245.5200 274.0511 12.3490 0.4129 246.1608 245.7479 273.9861 13.1455 0.4136 246.3831 245.9694 273.9357 13.9735 0.4145 246.5987 246.1842 273.9158 14.7400 0.4183 246.7892 246.3709 273.9217 15.5885 0.4256 247.0258 246.6003 273.9407 16.3653 0.4303 247.2603 246.8300 274.0020 17.1830 0.4314 247.4888 247.0574 274.0542 17.9803 0.4319 247.6899 247.2580 274.1451 18.7768 0.4332 247.8799 247.4467 274.2925 19.6045 0.4344 248.0941 247.6597 274.4828 20.3710 0.4386 248.2819 247.8433 274.6780 21.2195 0.4401 248.5040 248.0640 274.9483 21.9963 0.4422 248.6931 248.2509 275.2103 22.8140 0.4428 248.8975 248.4547 275.5420 23.5703 0.4441 249.0913 248.6472 275.8635 24.4383 0.4451 249.3411 248.8959 276.2411 25.2048 0.4453 249.5650 249.1197 276.5645 26.0225 0.4440 249.8001 249.3561 276.9563 26.8300 0.4435 250.0061 249.5626 277.3399 27.6170 0.4423 250.2179 249.7755 277.7099 28.4450 0.4443 250.4338 249.9895 278.1082 29.2115 0.4428 250.6473 250.2045 278.4594 30.0703 0.4395 250.8654 250.4258 278.8480 30.8368 0.4377 251.0531 250.6154 279.1653 31.6535 0.4382 251.2705 250.8324 279.4995 32.4610 0.4370 251.4947 251.0577 279.7917 33.2583 0.4317 251.7144 251.2827 280.0525 34.0453 0.4235 251.9298 251.5063 280.3208 34.8835 0.4251 252.1077 251.6826 280.5407 35.6703 0.4272 252.2646 251.8374 280.7176 36.4668 0.4244 252.4560 252.0315 280.8991 37.2948 0.4211 252.6785 252.2575 281.0610 38.0715 0.4186 252.9085 252.4898 281.1872 38.9200 0.4152 253.1510 252.7358 281.2540 39.6865 0.4174 253.3569 252.9395 281.3482 40.5145 0.4175 253.5525 253.1350 281.3807 41.3110 0.4149 253.7602 253.3453 281.3761 42.1080 0.4102 253.9626 253.5524 281.3767 42.9258 0.4059 254.1687 253.7627 281.3531 43.7025 0.3998 254.3737 253.9739 281.3235 44.5510 0.3982 254.5672 254.1690 281.2665 45.3175 0.3944 254.7675 254.3731 281.1977 46.1453 0.3938 254.9699 254.5761 281.1320 46.9418 0.3910 255.1832 254.7921 281.0645 47.7390 0.3882 255.3796 254.9914 280.9816 48.5670 0.3860 255.5627 255.1766 280.8945 49.3335 0.3861 255.7443 255.3582 280.8238 50.1923 0.3817 255.9497 255.5681 280.7815 50.9588 0.3788 256.1586 255.7799 280.7451 51.7755 0.3766 256.3670 255.9903 280.6843 52.5830 0.3799 256.5706 256.1907 280.6522 53.3700 0.3786 256.7915 256.4129 280.6616 54.2083 0.3758 257.0188 256.6430 280.7068 54.9645 0.3753 257.1745 256.7992 280.7417 55.8335 0.3748 257.3648 256.9900 280.8064 56.5888 0.3740 257.5449 257.1710 280.8950 57.4065 0.3743 257.7442 257.3699 281.0247 58.2038 0.3698 257.9441 257.5743 281.1830 59.0010 0.3667 258.1284 257.7617 281.3658 59.8188 0.3621 258.3420 257.9799 281.5759 60.5853 0.3595 258.5484 258.1889 281.7951 61.4028 0.3561 258.7492 258.3930 282.0626 62.1685 0.3568 258.9137 258.5569 282.3358 63.0273 0.3554 259.1400 258.7846 282.6603 63.7835 0.3532 259.3337 258.9806 282.9223 64.6115 0.3534 259.5288 259.1753 283.2436 65.4088 0.3501 259.7151 259.3649 283.5704 66.2060 0.3497 259.9117 259.5621 283.8668 67.0235 0.3458 260.1031 259.7573 284.2120 67.7995 0.3391 260.2732 259.9341 284.5297 68.6173 0.3360 260.4622 260.1262 284.8787 69.3735 0.3341 260.6622 260.3280 285.1637 70.2425 0.3307 260.8719 260.5412 285.4662 70.9988 0.3272 261.0637 260.7365 285.7106 71.8265 0.3202 261.2828 260.9626 286.0081 72.6230 0.3137 261.4925 261.1788 286.2576 73.4203 0.3083 261.6699 261.3616 286.4868 74.2483 0.3048 261.8917 261.5869 286.6944 75.0045 0.3033 262.0730 261.7697 286.8491 75.8325 0.2936 262.2618 261.9682 286.9953 76.5990 0.2905 262.4044 262.1139 287.1290 77.4475 0.2906 262.6127 262.3221 287.2623 78.2238 0.2849 262.8063 262.5214 287.3379 79.0513 0.2760 263.0257 262.7497 287.3987 79.8383 0.2726 263.2120 262.9394 287.4502 80.6355 0.2677 263.3985 263.1307 287.4806 81.4635 0.2629 263.5903 263.3274 287.4849 82.2300 0.2608 263.7328 263.4720 287.4970 83.0785 0.2531 263.9220 263.6689 287.4892 83.8235 0.2500 264.1042 263.8542 287.4691 84.6720 0.2475 264.3035 264.0560 287.4355 85.4385 0.2449 264.4889 264.2440 287.4219 86.2665 0.2387 264.6857 264.4470 287.3980 87.0638 0.2356 264.8677 264.6321 287.3861 87.8608 0.2337 265.0824 264.8487 287.3610 88.6778 0.2292 265.2569 265.0277 287.3241 89.4545 0.2234 265.4526 265.2293 287.3036 90.3030 0.2205 265.6488 265.4282 287.2898 91.0695 0.2189 265.8480 265.6292 287.2827 91.8975 0.2140 266.0507 265.8367 287.2830 92.6948 0.2113 266.2122 266.0009 287.3151 93.4918 0.2074 266.3833 266.1759 287.3790 94.2883 0.2033 266.5534 266.3502 287.4885 95.0855 0.1998 266.7402 266.5403 287.5986 95.9135 0.1960 266.9357 266.7396 287.7122 96.6800 0.1923 267.1191 266.9268 287.8524 97.5285 0.1885 267.3088 267.1203 287.9985 98.3053 0.1844 267.4776 267.2932 288.1829 99.1228 0.1810 267.6589 267.4780 288.3949 99.9193 0.1794 267.8394 267.6600 288.6168 100.7165 0.1758 268.0150 267.8391 288.8433 101.5445 0.1732 268.1980 268.0247 289.1201 102.3110 0.1686 268.3651 268.1965 289.3800 103.1595 0.1604 268.5617 268.4013 289.6691 103.9360 0.1583 268.7435 268.5852 289.9333 104.7633 0.1514 268.9442 268.7928 290.2304 105.5605 0.1474 269.1544 269.0070 290.5338 106.3475 0.1472 269.3377 269.1905 290.8076 107.1858 0.1451 269.5125 269.3674 291.1032 107.9420 0.1414 269.6907 269.5493 291.3600 108.8008 0.1358 269.8603 269.7245 291.6482 109.5365 0.1272 270.0299 269.9027 291.8742 110.3953 0.1191 270.2346 270.1155 292.1415 111.1613 0.1167 270.4149 270.2983 292.3451 111.9888 0.1156 270.5955 270.4799 292.5656 112.7860 0.1083 270.7583 270.6500 292.7656 113.5833 0.1066 270.9378 270.8312 292.9159 114.4113 0.1035 271.1449 271.0414 293.0697 115.1675 0.0957 271.3279 271.2322 293.1922 116.0363 0.0900 271.5238 271.4337 293.3266 116.7918 0.0834 271.7026 271.6191 293.4207 117.6300 0.0760 271.9094 271.8334 293.5407 118.4170 0.0713 272.0657 271.9944 293.6126 119.2245 0.0646 272.2517 272.1871 293.6867 120.0423 0.0583 272.4387 272.3804 293.7371 120.7975 0.0543 272.5934 272.5390 293.7576 121.6665 0.0508 272.8022 272.7515 293.7910 122.4228 0.0461 272.9681 272.9219 293.8060 123.2405 0.0437 273.1190 273.0753 293.7999 124.0070 0.0417 273.2903 273.2486 293.8062 124.8248 0.0370 273.4883 273.4514 293.7743 125.6525 0.0334 273.7032 273.6698 293.7843 126.4183 0.0303 273.8832 273.8529 293.8057 127.2360 0.0238 274.0453 274.0215 293.8247 128.0025 0.0178 274.2066 274.1888 293.8341 128.8613 0.0133 274.3914 274.3781 293.8243 129.6175 0.0099 274.5508 274.5409 293.8556 130.4455 0.0053 274.7281 274.7227 293.9086 131.2428 -0.0003 274.9037 274.9039 293.9527 132.0400 -0.0057 275.0679 275.0736 294.0077 132.8568 -0.0096 275.2590 275.2686 294.0771 133.6335 -0.0182 275.4282 275.4464 294.2162 134.4820 -0.0199 275.6097 275.6296 294.3313 135.2485 -0.0216 275.7797 275.8013 294.4621 136.0765 -0.0209 275.9694 275.9903 294.6487 136.8735 -0.0247 276.1427 276.1674 294.8077 137.6700 -0.0294 276.3319 276.3614 295.0043 138.4878 -0.0375 276.5017 276.5391 295.2174 139.2645 -0.0416 276.6686 276.7102 295.4193 140.1130 -0.0472 276.8620 276.9092 295.6542 140.8795 -0.0515 277.0308 277.0823 295.8774 141.7075 -0.0547 277.1933 277.2480 296.1398 142.5045 -0.0598 277.3445 277.4043 296.3828 143.3010 -0.0628 277.5312 277.5940 296.6363 144.1188 -0.0631 277.6888 277.7519 296.8937 144.8955 -0.0694 277.8665 277.9360 297.1344 145.7440 -0.0758 278.0566 278.1324 297.4076 146.5105 -0.0817 278.2343 278.3160 297.6513 147.3385 -0.0821 278.4217 278.5038 297.9036 148.1350 -0.0834 278.6012 278.6845 298.1361 148.9320 -0.0885 278.7413 278.8298 298.3643 149.7498 -0.0956 278.9158 279.0114 298.5735 150.5265 -0.1008 279.0946 279.1954 298.7500 151.3750 -0.1088 279.2521 279.3608 298.9318 152.1413 -0.1163 279.4085 279.5249 299.0674 152.9685 -0.1229 279.5675 279.6904 299.2222 153.7658 -0.1280 279.7252 279.8531 299.3832 154.5630 -0.1313 279.8936 280.0249 299.5152 155.3808 -0.1345 280.0928 280.2273 299.6564 156.1575 -0.1367 280.2809 280.4176 299.7747 157.0060 -0.1420 280.4507 280.5927 299.8736 157.7513 -0.1484 280.6161 280.7645 299.9443 158.5995 -0.1556 280.7651 280.9207 299.9960 159.3763 -0.1581 280.9588 281.1170 300.0261 160.1940 -0.1615 281.1649 281.3264 300.0518 160.9913 -0.1661 281.3583 281.5245 300.0674 161.7885 -0.1698 281.5418 281.7116 300.1015 162.6160 -0.1763 281.7165 281.8928 300.1011 163.3820 -0.1800 281.8797 282.0597 300.1046 164.2305 -0.1836 282.0622 282.2458 300.1506 165.0073 -0.1879 282.2212 282.4091 300.1534 165.8250 -0.1888 282.3614 282.5502 300.1862 166.6223 -0.1910 282.5266 282.7175 300.2218 167.4195 -0.1970 282.6833 282.8803 300.2646 168.2475 -0.2030 282.8510 283.0540 300.2904 169.0138 -0.2072 283.0302 283.2374 300.3244 169.8615 -0.2137 283.2131 283.4268 300.4005 170.6383 -0.2169 283.3910 283.6079 300.4947 171.4560 -0.2183 283.5713 283.7896 300.6206 172.2533 -0.2198 283.7233 283.9431 300.7340 173.0505 -0.2217 283.8897 284.1114 300.8717 173.8785 -0.2286 284.0608 284.2895 301.0361 174.6450 -0.2333 284.2401 284.4734 301.1861 175.4930 -0.2426 284.4208 284.6634 301.3607 176.2693 -0.2472 284.5861 284.8334 301.5541 177.0870 -0.2515 284.7487 285.0001 301.7761 177.8843 -0.2571 284.9307 285.1877 301.9935 178.6815 -0.2620 285.0929 285.3549 302.2203 179.5095 -0.2685 285.2855 285.5540 302.4414 180.2760 -0.2719 285.4447 285.7166 302.6754 181.1245 -0.2761 285.6251 285.9012 302.9451 181.9003 -0.2825 285.7856 286.0681 303.1764 182.7180 -0.2872 285.9640 286.2512 303.4354 183.5153 -0.2909 286.1208 286.4117 303.6489 184.3125 -0.2924 286.2773 286.5697 303.8678 185.1405 -0.2960 286.4385 286.7345 304.0983 185.8968 -0.2990 286.6036 286.9025 304.3033 186.7243 -0.3040 286.7918 287.0958 304.4989 187.4800 -0.3076 286.9414 287.2489 304.6609 188.3388 -0.3181 287.1160 287.4341 304.8234 189.1053 -0.3221 287.2765 287.5986 304.9830 189.9230 -0.3277 287.4411 287.7688 305.1762 190.7203 -0.3322 287.6029 287.9351 305.3376 191.5175 -0.3442 287.7590 288.1032 305.4759 192.3143 -0.3517 287.9166 288.2683 305.6198 193.1008 -0.3549 288.0780 288.4329 305.7398 193.9288 -0.3602 288.2591 288.6193 305.8602 194.6953 -0.3635 288.4156 288.7791 305.9603 195.5438 -0.3720 288.5757 288.9477 306.0111 196.3103 -0.3752 288.7177 289.0928 306.0465 197.1383 -0.3753 288.8951 289.2705 306.1137 197.9348 -0.3740 289.0386 289.4126 306.1770 198.7215 -0.3761 289.1919 289.5680 306.2393 199.5495 -0.3779 289.3550 289.7329 306.2928 200.3160 -0.3865 289.4871 289.8736 306.3423 201.1645 -0.3912 289.6649 290.0560 306.3696 201.9410 -0.3968 289.8357 290.2326 306.3976 202.7580 -0.4024 290.0374 290.4398 306.4394 203.5245 -0.4045 290.2041 290.6085 306.4571 204.3525 -0.4076 290.3882 290.7958 306.5119 205.1498 -0.4107 290.5549 290.9656 306.5687 205.9470 -0.4148 290.7354 291.1502 306.6245 206.7643 -0.4189 290.9179 291.3368 306.7204 207.5405 -0.4233 291.0706 291.4939 306.7953 208.3890 -0.4280 291.2409 291.6689 306.8900 209.1555 -0.4365 291.3665 291.8030 306.9988 209.9835 -0.4439 291.5670 292.0110 307.1280 210.7808 -0.4475 291.7698 292.2174 307.2474 211.5775 -0.4570 291.9287 292.3857 307.3599 212.3948 -0.4601 292.1015 292.5616 307.5417 213.1715 -0.4619 292.2798 292.7417 307.7072 214.0200 -0.4668 292.4636 292.9304 307.9028 214.7660 -0.4719 292.6124 293.0843 308.0494 215.6143 -0.4749 292.7738 293.2487 308.2393 216.3903 -0.4751 292.9520 293.4271 308.4456 217.2080 -0.4778 293.1283 293.6061 308.6620 218.0053 -0.4778 293.2792 293.7570 308.8683 218.8025 -0.4808 293.4539 293.9347 309.0917 219.6305 -0.4859 293.6363 294.1223 309.3032 220.3968 -0.4910 293.7788 294.2698 309.5220 221.2445 -0.4973 293.9139 294.4112 309.7623 222.0213 -0.5001 294.0724 294.5726 309.9993 222.8390 -0.5032 294.2519 294.7551 310.2034 223.6465 -0.5098 294.4350 294.9448 310.4056 224.4335 -0.5129 294.5942 295.1071 310.5743 225.2710 -0.5170 294.7394 295.2564 310.7454 226.0270 -0.5212 294.8801 295.4013 310.9488 226.8858 -0.5295 295.0381 295.5676 311.1552 227.6215 -0.5318 295.1593 295.6911 311.3146 228.4803 -0.5417 295.3120 295.8537 311.4606 229.2460 -0.5480 295.4656 296.0137 311.5804 230.0635 -0.5550 295.6343 296.1893 311.7305 230.8710 -0.5590 295.8120 296.3710 311.8678 231.6580 -0.5629 295.9972 296.5602 311.9683 232.4860 -0.5672 296.1577 296.7249 312.0556 233.2525 -0.5693 296.3111 296.8804 312.1428 234.1208 -0.5708 296.5033 297.0741 312.2056 234.8768 -0.5735 296.6602 297.2337 312.2967 235.7048 -0.5765 296.8312 297.4077 312.3761 236.5020 -0.5807 296.9836 297.5643 312.4263 237.2993 -0.5843 297.1486 297.7329 312.5112 238.1273 -0.5879 297.3154 297.9033 312.5200 238.8935 -0.5893 297.4813 298.0706 312.5573 239.7208 -0.5934 297.6375 298.2310 312.6318 240.4873 -0.5976 297.7848 298.3824 312.6934 241.3460 -0.6030 297.9742 298.5772 312.7732 242.1023 -0.6070 298.1445 298.7515 312.8576 242.9405 -0.6131 298.2834 298.8965 312.9268 243.7373 -0.6189 298.4291 299.0481 312.9877 244.5340 -0.6206 298.6086 299.2292 313.0641 245.3518 -0.6241 298.7806 299.4047 313.1653 246.1285 -0.6293 298.9443 299.5736 313.2930 246.9770 -0.6310 299.1158 299.7468 313.4030 247.7435 -0.6373 299.2994 299.9367 313.4954 248.5715 -0.6406 299.4662 300.1068 313.6206 249.3683 -0.6441 299.6297 300.2738 313.7522 250.1548 -0.6476 299.7718 300.4194 313.9086 250.9828 -0.6518 299.9004 300.5523 314.0685 251.7390 -0.6557 300.0423 300.6980 314.2041 252.5670 -0.6581 300.2347 300.8928 314.3938 253.3335 -0.6638 300.3862 301.0501 314.5879 254.1820 -0.6633 300.5715 301.2348 314.7697 254.9478 -0.6677 300.7433 301.4109 314.9474 255.7755 -0.6719 300.8900 301.5620 315.1326 256.5625 -0.6781 301.0680 301.7461 315.3186 257.3598 -0.6795 301.2028 301.8823 315.5469 258.1878 -0.6838 301.3497 302.0334 315.7711 258.9543 -0.6904 301.5199 302.2104 315.9662 259.8025 -0.6933 301.6921 302.3854 316.1762 260.5683 -0.6972 301.8645 302.5617 316.3581 261.3963 -0.7035 302.0281 302.7316 316.5525 262.1935 -0.7082 302.1721 302.8802 316.7597 262.9805 -0.7112 302.3293 303.0404 316.9507 263.8085 -0.7175 302.4944 303.2120 317.1013 264.5740 -0.7245 302.6592 303.3837 317.2695 265.4225 -0.7284 302.8369 303.5654 317.4428 266.1993 -0.7347 303.0040 303.7387 317.5978 267.0170 -0.7413 303.1630 303.9044 317.7661 267.8143 -0.7426 303.3018 304.0445 317.9478 268.6115 -0.7467 303.4681 304.2148 318.0744 269.4393 -0.7530 303.6387 304.3917 318.2038 270.2050 -0.7589 303.7617 304.5207 318.3148 271.0228 -0.7649 303.9076 304.6724 318.4335 271.7995 -0.7687 304.0756 304.8443 318.5093 272.6480 -0.7664 304.2585 305.0250 318.6128 273.4145 -0.7723 304.4144 305.1867 318.6712 274.2415 -0.7794 304.5505 305.3299 318.7584 275.0388 -0.7861 304.7313 305.5173 318.8287 275.8360 -0.7857 304.8700 305.6557 318.9129 276.6538 -0.7860 305.0125 305.7985 318.9659 277.4305 -0.7894 305.1739 305.9633 319.0005 278.2788 -0.7933 305.3386 306.1319 319.0504 279.0445 -0.7961 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