DTA measure 3f Date: 20251125:1751 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 453.74 s Mass = 100.000 mg data_number = 1129 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 0.7225 -4.4803 454.8412 459.3215 433.1642 1.0750 -4.4870 454.8655 459.3525 433.2212 1.4480 -4.4914 454.8797 459.3711 433.3088 1.8825 -4.4941 454.8976 459.3917 433.3821 2.3170 -4.4951 454.9309 459.4260 433.4519 2.6695 -4.4979 454.9389 459.4368 433.5181 3.0425 -4.4997 454.9480 459.4477 433.5719 3.5380 -4.5034 454.9674 459.4708 433.6211 3.8900 -4.5063 454.9589 459.4653 433.6622 4.2630 -4.5067 454.9556 459.4622 433.7124 4.6975 -4.5078 454.9830 459.4908 433.7298 5.1320 -4.5075 455.0220 459.5295 433.7693 5.4845 -4.5109 455.0470 459.5579 433.7609 5.8575 -4.5151 455.0641 459.5791 433.7803 6.3535 -4.5176 455.0761 459.5936 433.7967 6.7060 -4.5203 455.0929 459.6132 433.8041 7.0790 -4.5204 455.1183 459.6387 433.8044 7.5135 -4.5249 455.1423 459.6672 433.8037 7.9470 -4.5279 455.1577 459.6856 433.7996 8.2995 -4.5282 455.1718 459.7000 433.7770 8.6725 -4.5308 455.2060 459.7368 433.7444 9.1685 -4.5348 455.2393 459.7741 433.7093 9.5210 -4.5382 455.2617 459.7998 433.6620 9.8940 -4.5384 455.2757 459.8141 433.6242 10.3285 -4.5391 455.2971 459.8363 433.5722 10.7630 -4.5395 455.3353 459.8748 433.5146 11.1155 -4.5414 455.3609 459.9023 433.4469 11.4885 -4.5450 455.3716 459.9166 433.3589 11.9220 -4.5462 455.4141 459.9604 433.2782 12.3360 -4.5501 455.4313 459.9814 433.2008 12.7090 -4.5530 455.4454 459.9985 433.1295 13.0820 -4.5582 455.4458 460.0040 433.0375 13.5780 -4.5591 455.4671 460.0262 432.9729 13.9305 -4.5608 455.4737 460.0344 432.8899 14.3035 -4.5659 455.4969 460.0628 432.8024 14.7380 -4.5683 455.5201 460.0885 432.7068 15.1515 -4.5706 455.5259 460.0965 432.5957 15.5240 -4.5705 455.5203 460.0908 432.5000 15.8970 -4.5708 455.5323 460.1031 432.3860 16.3930 -4.5745 455.5560 460.1305 432.2464 16.7660 -4.5777 455.5741 460.1518 432.1311 17.1185 -4.5787 455.5846 460.1633 432.0298 17.5530 -4.5820 455.5970 460.1790 431.9156 17.9875 -4.5810 455.6181 460.1991 431.7866 18.3400 -4.5820 455.6324 460.2144 431.6824 18.7125 -4.5804 455.6433 460.2237 431.5662 19.2080 -4.5786 455.6725 460.2511 431.3991 19.5810 -4.5797 455.6899 460.2696 431.2915 19.9335 -4.5818 455.7071 460.2889 431.2023 20.3680 -4.5825 455.7504 460.3329 431.0546 20.8025 -4.5840 455.7486 460.3326 430.9121 21.1550 -4.5833 455.7661 460.3494 430.8139 21.5280 -4.5813 455.7704 460.3516 430.6844 22.0240 -4.5814 455.7925 460.3739 430.5364 22.3970 -4.5831 455.8006 460.3837 430.4251 22.7485 -4.5870 455.7970 460.3840 430.3372 23.1215 -4.5887 455.8208 460.4095 430.2288 23.6175 -4.5908 455.8523 460.4431 430.0847 23.9700 -4.5931 455.8697 460.4628 429.9780 24.3430 -4.5935 455.8928 460.4862 429.8517 24.8390 -4.5928 455.9217 460.5146 429.7260 25.2120 -4.5939 455.9277 460.5217 429.6401 25.5645 -4.5955 455.9297 460.5252 429.5568 25.9370 -4.5959 455.9587 460.5545 429.4423 26.4325 -4.5940 455.9774 460.5715 429.3342 26.7850 -4.5929 455.9928 460.5858 429.2541 27.1580 -4.5925 455.9937 460.5862 429.1740 27.5925 -4.5919 456.0257 460.6176 429.0541 28.0270 -4.5926 456.0477 460.6403 428.9579 28.3795 -4.5925 456.0552 460.6477 428.8815 28.7525 -4.5930 456.0642 460.6572 428.8242 29.2480 -4.5955 456.0739 460.6695 428.7470 29.6000 -4.5961 456.0980 460.6941 428.6838 29.9730 -4.5982 456.1173 460.7154 428.6183 30.4075 -4.5971 456.1295 460.7266 428.5272 30.8420 -4.5999 456.1174 460.7173 428.4478 31.1945 -4.6001 456.1245 460.7246 428.3945 31.5675 -4.6008 456.1059 460.7067 428.3603 32.0635 -4.5981 456.1007 460.6988 428.2909 32.4160 -4.5978 456.1100 460.7078 428.2528 32.7890 -4.6009 456.1012 460.7021 428.2264 33.2230 -4.6030 456.0970 460.7001 428.1812 33.6570 -4.6029 456.0918 460.6947 428.1404 34.0095 -4.6005 456.0951 460.6956 428.1046 34.3825 -4.5979 456.0925 460.6904 428.0709 34.8785 -4.5960 456.0881 460.6841 428.0353 35.2310 -4.5974 456.1008 460.6982 428.0323 35.6040 -4.5984 456.1131 460.7115 427.9986 36.0385 -4.6028 456.1129 460.7158 427.9714 36.4730 -4.6001 456.0965 460.6966 427.9630 36.8255 -4.5999 456.1106 460.7105 427.9372 37.1980 -4.6011 456.1307 460.7318 427.9271 37.6730 -4.6044 456.0970 460.7014 427.9265 38.0460 -4.6048 456.0858 460.6905 427.9198 38.4190 -4.6055 456.0961 460.7016 427.9114 38.8535 -4.6065 456.0887 460.6951 427.9343 39.2675 -4.6077 456.1080 460.7158 427.9578 39.6405 -4.6089 456.1204 460.7292 427.9545 39.9930 -4.6094 456.1122 460.7216 427.9642 40.4890 -4.6101 456.1198 460.7299 427.9679 40.8615 -4.6093 456.1420 460.7513 427.9656 41.2135 -4.6110 456.1589 460.7699 427.9769 41.6480 -4.6158 456.1771 460.7929 427.9636 42.0620 -4.6180 456.1895 460.8074 427.9614 42.4350 -4.6190 456.1649 460.7838 427.9615 42.8080 -4.6211 456.1670 460.7881 427.9391 43.3040 -4.6203 456.1971 460.8174 427.9341 43.6565 -4.6209 456.2000 460.8209 427.9304 44.0295 -4.6197 456.2027 460.8224 427.9292 44.4025 -4.6181 456.1965 460.8146 427.9185 44.8770 -4.6241 456.1928 460.8169 427.9031 45.2500 -4.6287 456.1995 460.8283 427.8596 45.6230 -4.6281 456.1999 460.8280 427.8539 46.0370 -4.6303 456.1993 460.8295 427.8446 46.4715 -4.6291 456.1968 460.8259 427.8320 46.8445 -4.6292 456.1859 460.8151 427.8236 47.1970 -4.6312 456.1822 460.8134 427.8027 47.6930 -4.6353 456.1984 460.8337 427.7710 48.0660 -4.6352 456.1971 460.8322 427.7237 48.4380 -4.6362 456.1940 460.8302 427.6956 48.8520 -4.6373 456.2066 460.8439 427.6336 49.2865 -4.6380 456.2175 460.8555 427.6101 49.6390 -4.6413 456.2200 460.8613 427.5851 50.0120 -4.6452 456.2283 460.8734 427.5450 50.5080 -4.6467 456.2063 460.8530 427.4833 50.8810 -4.6467 456.2054 460.8521 427.4522 51.2335 -4.6493 456.2147 460.8640 427.4199 51.6680 -4.6540 456.2145 460.8685 427.3802 52.1025 -4.6540 456.2181 460.8720 427.3525 52.4540 -4.6555 456.2331 460.8886 427.3023 52.8270 -4.6581 456.2465 460.9046 427.2464 53.3230 -4.6588 456.2611 460.9199 427.1906 53.6960 -4.6601 456.2529 460.9130 427.1352 54.0485 -4.6574 456.2418 460.8993 427.0846 54.4215 -4.6588 456.2449 460.9037 427.0301 54.9175 -4.6616 456.2439 460.9055 426.9428 55.2700 -4.6625 456.2376 460.9001 426.8876 55.6420 -4.6619 456.2465 460.9084 426.8124 56.0765 -4.6625 456.2518 460.9143 426.7452 56.5110 -4.6628 456.2424 460.9052 426.6542 56.8635 -4.6644 456.2420 460.9064 426.5996 57.2365 -4.6668 456.2642 460.9310 426.5313 57.7120 -4.6682 456.2698 460.9380 426.4353 58.0850 -4.6707 456.2619 460.9326 426.3726 58.4580 -4.6736 456.2431 460.9167 426.2983 58.8925 -4.6734 456.2341 460.9075 426.2039 59.3055 -4.6752 456.2519 460.9271 426.1272 59.6785 -4.6747 456.2391 460.9138 426.0588 60.0515 -4.6743 456.2525 460.9268 425.9805 60.5270 -4.6766 456.2440 460.9206 425.8924 60.9000 -4.6791 456.2360 460.9151 425.7967 61.2730 -4.6793 456.2345 460.9139 425.7114 61.7075 -4.6796 456.2398 460.9194 425.5962 62.1215 -4.6796 456.2399 460.9195 425.5044 62.4945 -4.6801 456.2376 460.9177 425.4074 62.8675 -4.6821 456.2432 460.9253 425.3353 63.3420 -4.6820 456.2377 460.9197 425.2292 63.7150 -4.6855 456.2491 460.9345 425.1691 64.0880 -4.6845 456.2587 460.9431 425.0899 64.5225 -4.6854 456.2662 460.9517 425.0215 64.9365 -4.6853 456.2639 460.9493 424.9376 65.3095 -4.6869 456.2593 460.9462 424.8548 65.6825 -4.6866 456.2593 460.9460 424.7923 66.1580 -4.6878 456.2545 460.9423 424.6930 66.5310 -4.6861 456.2578 460.9439 424.6175 66.9035 -4.6882 456.2508 460.9390 424.5537 67.3375 -4.6875 456.2282 460.9157 424.4740 67.7515 -4.6885 456.1986 460.8871 424.4065 68.1245 -4.6861 456.1919 460.8780 424.3456 68.4975 -4.6840 456.1786 460.8626 424.2714 68.9730 -4.6837 456.1561 460.8399 424.1833 69.3460 -4.6856 456.1576 460.8431 424.0985 69.7190 -4.6867 456.1416 460.8283 424.0194 70.1535 -4.6846 456.1278 460.8124 423.9379 70.5675 -4.6853 456.1280 460.8132 423.8568 70.9400 -4.6868 456.1267 460.8135 423.8061 71.3125 -4.6889 456.0979 460.7868 423.7626 71.7880 -4.6893 456.0782 460.7675 423.6998 72.1610 -4.6892 456.0701 460.7593 423.6147 72.5340 -4.6895 456.0619 460.7514 423.5710 72.9685 -4.6903 456.0395 460.7297 423.5296 73.3825 -4.6918 456.0315 460.7233 423.4762 73.7555 -4.6920 456.0044 460.6964 423.4287 74.1285 -4.6927 455.9961 460.6888 423.3864 74.6040 -4.6941 455.9851 460.6793 423.3219 74.9770 -4.6966 455.9718 460.6684 423.2719 75.3490 -4.6963 455.9656 460.6619 423.2200 75.7835 -4.6971 455.9584 460.6555 423.1596 76.1975 -4.6963 455.9520 460.6483 423.1149 76.5705 -4.6968 455.9489 460.6457 423.0786 76.9435 -4.6998 455.9347 460.6345 423.0274 77.4190 -4.7023 455.9319 460.6342 422.9825 77.7920 -4.7010 455.9246 460.6256 422.9615 78.1650 -4.6999 455.9386 460.6384 422.9219 78.5995 -4.7009 455.9174 460.6183 422.8839 79.0135 -4.7001 455.8990 460.5991 422.8284 79.3865 -4.7005 455.8830 460.5835 422.8120 79.7585 -4.7027 455.8781 460.5808 422.7979 80.2340 -4.7042 455.8640 460.5681 422.7442 80.6070 -4.7044 455.8469 460.5513 422.7155 80.9800 -4.7056 455.8382 460.5438 422.6725 81.4145 -4.7046 455.8238 460.5284 422.6371 81.8490 -4.7022 455.8036 460.5058 422.6041 82.2015 -4.7008 455.7915 460.4923 422.5791 82.5745 -4.7013 455.7917 460.4929 422.5567 83.0705 -4.7041 455.7676 460.4717 422.5312 83.4230 -4.7033 455.7593 460.4626 422.5067 83.7960 -4.7049 455.7399 460.4448 422.4928 84.2295 -4.7081 455.7330 460.4411 422.4696 84.6640 -4.7104 455.7003 460.4107 422.4411 85.0165 -4.7115 455.6688 460.3804 422.4146 85.3895 -4.7123 455.6668 460.3791 422.3622 85.8855 -4.7134 455.6603 460.3737 422.3092 86.2380 -4.7168 455.6763 460.3932 422.2842 86.6110 -4.7170 455.6554 460.3724 422.2690 87.0455 -4.7162 455.6361 460.3523 422.2200 87.4795 -4.7159 455.6224 460.3383 422.1868 87.8315 -4.7183 455.6176 460.3359 422.1765 88.2045 -4.7165 455.6141 460.3306 422.1487 88.7005 -4.7153 455.5812 460.2965 422.1032 89.0530 -4.7159 455.5895 460.3054 422.0833 89.4260 -4.7168 455.5747 460.2915 422.0452 89.8605 -4.7167 455.5455 460.2622 421.9761 90.2950 -4.7175 455.5377 460.2552 421.9361 90.6675 -4.7185 455.5213 460.2398 421.8794 91.0195 -4.7201 455.5075 460.2275 421.8420 91.5155 -4.7211 455.4865 460.2076 421.7995 91.8885 -4.7231 455.4696 460.1927 421.7764 92.2410 -4.7261 455.4636 460.1896 421.7500 92.6755 -4.7301 455.4428 460.1729 421.7129 93.1100 -4.7369 455.4090 460.1459 421.6685 93.4830 -4.7343 455.3774 460.1117 421.6172 93.8355 -4.7345 455.3511 460.0856 421.5951 94.3310 -4.7347 455.3253 460.0599 421.5729 94.7035 -4.7339 455.3197 460.0536 421.5443 95.0765 -4.7355 455.2977 460.0332 421.4959 95.4905 -4.7351 455.3061 460.0412 421.4428 95.9250 -4.7339 455.3057 460.0397 421.3869 96.2980 -4.7330 455.2859 460.0188 421.3399 96.6710 -4.7338 455.2714 460.0052 421.3018 97.1465 -4.7336 455.2442 459.9778 421.2321 97.5190 -4.7334 455.2099 459.9433 421.1782 97.8915 -4.7310 455.1840 459.9151 421.1228 98.3055 -4.7326 455.1618 459.8944 421.0434 98.7400 -4.7330 455.1450 459.8780 420.9619 99.1130 -4.7331 455.1289 459.8620 420.8977 99.4860 -4.7329 455.1218 459.8547 420.8244 99.9615 -4.7366 455.1037 459.8403 420.7301 100.3345 -4.7381 455.0909 459.8290 420.6821 100.7075 -4.7398 455.0713 459.8111 420.6242 101.1205 -4.7411 455.0564 459.7975 420.5568 101.5550 -4.7425 455.0465 459.7890 420.4810 101.9280 -4.7419 455.0445 459.7864 420.4217 102.3010 -4.7394 455.0216 459.7609 420.3593 102.7150 -4.7375 454.9965 459.7340 420.3098 103.1495 -4.7376 454.9604 459.6980 420.2368 103.5020 -4.7367 454.9418 459.6786 420.1851 103.8750 -4.7373 454.9207 459.6580 420.1216 104.3710 -4.7420 454.8910 459.6330 420.0389 104.7440 -4.7446 454.8705 459.6151 419.9636 105.0955 -4.7466 454.8612 459.6078 419.9016 105.5300 -4.7459 454.8421 459.5880 419.8135 105.9440 -4.7469 454.8119 459.5588 419.7384 106.3170 -4.7509 454.7880 459.5389 419.6790 106.6900 -4.7524 454.7631 459.5155 419.5979 107.1245 -4.7509 454.7301 459.4810 419.5264 107.5385 -4.7528 454.7064 459.4592 419.4564 107.9110 -4.7517 454.7016 459.4533 419.3995 108.2835 -4.7539 454.6869 459.4407 419.3375 108.7590 -4.7561 454.6618 459.4179 419.2796 109.1320 -4.7576 454.6383 459.3959 419.2115 109.5050 -4.7561 454.6385 459.3946 419.1463 109.9190 -4.7571 454.6426 459.3997 419.0787 110.3535 -4.7579 454.6156 459.3734 418.9812 110.7060 -4.7582 454.5778 459.3360 418.9257 111.0785 -4.7592 454.5680 459.3271 418.8516 111.5740 -4.7574 454.5536 459.3110 418.8023 111.9470 -4.7574 454.5262 459.2836 418.7570 112.2995 -4.7564 454.5033 459.2597 418.6925 112.7340 -4.7571 454.4804 459.2375 418.6303 113.1480 -4.7584 454.4732 459.2317 418.5760 113.5210 -4.7583 454.4450 459.2033 418.5229 113.8940 -4.7605 454.4382 459.1986 418.4882 114.3900 -4.7614 454.4118 459.1732 418.4424 114.7425 -4.7599 454.4002 459.1601 418.3846 115.1155 -4.7583 454.3902 459.1484 418.3191 115.4875 -4.7593 454.3635 459.1228 418.2693 115.9630 -4.7599 454.3501 459.1100 418.2060 116.3360 -4.7607 454.3437 459.1045 418.1501 116.7090 -4.7606 454.3187 459.0793 418.0874 117.1435 -4.7639 454.2906 459.0545 418.0317 117.5575 -4.7660 454.2501 459.0162 417.9773 117.9305 -4.7667 454.2391 459.0058 417.9289 118.3035 -4.7655 454.2213 458.9868 417.8910 118.7790 -4.7648 454.1869 458.9516 417.8344 119.1515 -4.7648 454.1603 458.9251 417.7961 119.5240 -4.7659 454.1372 458.9031 417.7584 119.9585 -4.7668 454.1081 458.8749 417.7130 120.3725 -4.7675 454.0773 458.8449 417.6598 120.7455 -4.7664 454.0454 458.8118 417.6052 121.1185 -4.7651 454.0025 458.7676 417.5637 121.5940 -4.7616 453.9685 458.7300 417.5256 121.9670 -4.7609 453.9370 458.6979 417.4791 122.3400 -4.7637 453.9259 458.6896 417.4342 122.7125 -4.7672 453.9158 458.6830 417.3903 123.1875 -4.7689 453.9002 458.6691 417.3309 123.5605 -4.7684 453.8795 458.6479 417.2781 123.9335 -4.7716 453.8422 458.6138 417.2321 124.3475 -4.7718 453.8297 458.6015 417.1940 124.7820 -4.7703 453.8085 458.5788 417.1500 125.1550 -4.7694 453.7585 458.5279 417.0982 125.5280 -4.7693 453.7227 458.4920 417.0657 126.0035 -4.7673 453.7245 458.4918 417.0256 126.3765 -4.7686 453.7051 458.4737 416.9764 126.7490 -4.7690 453.6803 458.4492 416.9404 127.1625 -4.7694 453.6462 458.4156 416.9037 127.5970 -4.7710 453.6402 458.4112 416.8490 127.9700 -4.7734 453.6338 458.4072 416.8261 128.3430 -4.7729 453.6065 458.3794 416.7866 128.8185 -4.7728 453.5988 458.3716 416.7418 129.1915 -4.7694 453.5685 458.3380 416.7000 129.5645 -4.7679 453.5342 458.3021 416.6768 129.9785 -4.7674 453.5129 458.2803 416.6270 130.4130 -4.7657 453.4728 458.2385 416.5871 130.7850 -4.7654 453.4389 458.2042 416.5553 131.1580 -4.7671 453.4184 458.1855 416.5143 131.5925 -4.7677 453.3847 458.1524 416.4807 132.0065 -4.7664 453.3576 458.1240 416.4365 132.3795 -4.7660 453.3197 458.0857 416.3966 132.7525 -4.7670 453.2909 458.0579 416.3540 133.2280 -4.7677 453.2445 458.0122 416.3151 133.6010 -4.7648 453.2150 457.9798 416.2758 133.9740 -4.7689 453.2102 457.9791 416.2321 134.4080 -4.7686 453.1845 457.9530 416.1896 134.8215 -4.7672 453.1505 457.9177 416.1519 135.1945 -4.7676 453.1225 457.8901 416.1049 135.5675 -4.7670 453.0946 457.8616 416.0541 136.0430 -4.7698 453.0849 457.8547 415.9936 136.4160 -4.7694 453.0679 457.8373 415.9470 136.7890 -4.7699 453.0279 457.7978 415.8870 137.2235 -4.7716 452.9878 457.7595 415.8382 137.6375 -4.7705 452.9590 457.7295 415.7980 138.0095 -4.7694 452.9178 457.6872 415.7639 138.3825 -4.7716 452.8937 457.6652 415.7231 138.8580 -4.7700 452.8403 457.6103 415.6517 139.2310 -4.7706 452.8206 457.5912 415.5949 139.6040 -4.7673 452.7768 457.5442 415.5474 140.0385 -4.7674 452.7460 457.5134 415.4958 140.4525 -4.7674 452.7259 457.4933 415.4620 140.8255 -4.7669 452.6972 457.4642 415.4156 141.1985 -4.7713 452.6758 457.4471 415.3602 141.6740 -4.7738 452.6658 457.4396 415.3026 142.0460 -4.7768 452.6384 457.4152 415.2590 142.4190 -4.7779 452.6138 457.3918 415.2063 142.7920 -4.7810 452.5954 457.3764 415.1580 143.2880 -4.7820 452.5587 457.3407 415.0906 143.6405 -4.7818 452.5132 457.2950 415.0487 144.0135 -4.7823 452.4930 457.2754 414.9829 144.4480 -4.7840 452.4749 457.2589 414.9085 144.8620 -4.7834 452.4278 457.2112 414.8566 145.2350 -4.7862 452.4108 457.1971 414.7882 145.6080 -4.7851 452.3756 457.1607 414.7269 146.1040 -4.7880 452.3520 457.1401 414.6386 146.4760 -4.7878 452.3237 457.1115 414.5647 146.8285 -4.7879 452.2845 457.0724 414.5244 147.2630 -4.7878 452.2458 457.0337 414.4553 147.6975 -4.7878 452.1981 456.9859 414.3674 148.0500 -4.7893 452.1624 456.9516 414.3177 148.4230 -4.7911 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