DTA measure 1lassumeres1 Date: 2026915:1633 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.34 s Mass = 1184.100 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1590 -2.4436 212.8639 215.3075 248.1556 1.9460 -2.4543 213.1351 215.5894 248.0356 2.7740 -2.4479 213.1854 215.6333 248.0139 3.5405 -2.4133 213.2777 215.6910 248.1538 4.3993 -2.3987 213.4014 215.8001 247.9998 5.1660 -2.4038 213.4824 215.8862 248.0674 5.9845 -2.4135 213.5103 215.9237 248.0752 6.7920 -2.4083 213.5733 215.9817 248.0638 7.5790 -2.4142 213.8004 216.2146 248.2285 8.3763 -2.4285 213.9745 216.4031 248.1358 9.1735 -2.4365 214.0169 216.4534 247.8822 10.0015 -2.4400 214.0384 216.4784 247.8774 10.7680 -2.4570 214.0561 216.5131 247.8719 11.6165 -2.4774 214.2091 216.6865 247.6553 12.3933 -2.4427 214.5285 216.9712 247.8095 13.2110 -2.4241 214.6838 217.1079 247.8884 14.0083 -2.4293 214.8924 217.3217 247.9836 14.8055 -2.4358 214.8914 217.3271 247.7033 15.6335 -2.4653 214.7643 217.2296 247.5508 16.4000 -2.4632 214.8965 217.3597 247.4816 17.2488 -2.4805 214.9593 217.4399 247.4549 18.0263 -2.4610 215.1341 217.5951 247.3234 18.8440 -2.4557 215.5381 217.9938 247.4058 19.6413 -2.4586 215.7143 218.1729 247.1882 20.4385 -2.4536 216.0855 218.5391 247.2594 21.2665 -2.4655 216.2781 218.7436 247.2958 22.0330 -2.4149 216.4010 218.8159 247.4047 22.8815 -2.3814 216.5074 218.8888 247.3069 23.6378 -2.4137 216.6021 219.0157 247.3846 24.4965 -2.4163 216.7772 219.1935 247.3606 25.2220 -2.4395 216.9287 219.3682 247.2750 26.0705 -2.4446 217.1033 219.5478 247.4591 26.8473 -2.4037 217.2097 219.6134 247.6956 27.6650 -2.3694 217.4674 219.8368 247.6664 28.4520 -2.3756 217.4711 219.8467 247.5922 29.2493 -2.4170 217.4571 219.8741 247.5765 30.0673 -2.4202 217.6925 220.1127 247.6696 30.8345 -2.3859 217.8143 220.2002 247.8429 31.6830 -2.3875 217.8772 220.2647 248.0591 32.4495 -2.3770 218.0423 220.4192 248.1445 33.2775 -2.4139 218.1427 220.5566 248.1917 34.0645 -2.4075 218.4067 220.8141 248.2157 34.8618 -2.3594 218.7817 221.1412 248.0410 35.6898 -2.3279 218.6454 220.9733 248.1389 36.4563 -2.3213 218.6179 220.9392 248.3556 37.3048 -2.3086 218.6708 220.9794 248.3610 38.0713 -2.3257 218.8064 221.1321 248.4510 38.8993 -2.3580 219.0409 221.3988 248.4381 39.6963 -2.3627 219.2011 221.5639 248.5900 40.4835 -2.3499 219.3705 221.7204 248.9342 41.3115 -2.3488 219.3007 221.6495 248.9720 42.0780 -2.3490 219.3271 221.6761 249.0698 42.9265 -2.3397 219.5868 221.9265 249.0928 43.6725 -2.3384 219.7729 222.1113 249.1198 44.5313 -2.3195 220.0450 222.3645 249.3946 45.2978 -2.2922 220.0384 222.3306 249.5902 46.1155 -2.3005 219.9513 222.2518 249.7902 46.9230 -2.3163 220.1623 222.4786 249.6557 47.7100 -2.3351 220.1363 222.4714 249.8186 48.5380 -2.3480 220.0726 222.4206 250.0908 49.3045 -2.3486 220.2848 222.6334 250.0482 50.1633 -2.2895 220.3726 222.6621 250.0733 50.9298 -2.2560 220.4326 222.6885 250.2109 51.7475 -2.2613 220.5660 222.8273 250.4412 52.5243 -2.2754 220.8728 223.1481 250.5459 53.3423 -2.2648 221.0625 223.3272 250.6436 54.1400 -2.2612 221.2618 223.5230 250.4751 54.9375 -2.2541 221.4009 223.6550 250.6026 55.7758 -2.2209 221.6467 223.8676 250.8720 56.5320 -2.2239 221.7828 224.0067 251.0942 57.3908 -2.2386 221.7981 224.0367 251.0921 58.1573 -2.2283 222.0553 224.2835 251.0448 58.9955 -2.2135 222.1536 224.3671 251.2312 59.7825 -2.2115 222.2582 224.4697 251.5904 60.5798 -2.2003 222.3657 224.5660 251.8142 61.4078 -2.2137 222.4924 224.7062 251.9404 62.1743 -2.2276 222.4858 224.7134 252.1610 63.0330 -2.2353 222.5403 224.7757 252.4091 63.7585 -2.2254 222.7477 224.9730 252.5504 64.6275 -2.1956 222.9941 225.1897 252.5813 65.3838 -2.2137 222.9701 225.1838 252.4846 66.2220 -2.2503 223.1807 225.4310 252.4245 67.0090 -2.2642 223.4866 225.7508 252.5944 67.8168 -2.2850 223.5707 225.8556 252.8626 68.6455 -2.2833 223.5978 225.8811 253.0973 69.4120 -2.2722 223.5001 225.7723 253.1844 70.2605 -2.2875 223.5875 225.8750 253.2221 71.0373 -2.2925 223.6947 225.9872 253.2817 71.8550 -2.2924 223.9705 226.2629 253.4226 72.6523 -2.2863 224.2643 226.5505 253.4991 73.4495 -2.2534 224.2236 226.4770 253.5618 74.2775 -2.2689 224.2739 226.5427 253.7676 75.0440 -2.2576 224.5094 226.7669 254.1068 75.8925 -2.2328 224.6366 226.8694 254.0157 76.6385 -2.1957 224.9260 227.1218 254.1222 77.5085 -2.1905 225.0882 227.2787 254.3642 78.2648 -2.1867 225.1921 227.3788 254.5144 79.1030 -2.1538 225.4155 227.5692 254.7089 79.8900 -2.1468 225.4803 227.6271 254.7253 80.6975 -2.1598 225.4891 227.6490 254.7676 81.5153 -2.1752 225.6570 227.8322 254.9304 82.2818 -2.1687 225.7989 227.9676 255.1049 83.1405 -2.1960 225.9651 228.1612 255.3025 83.9070 -2.2132 226.1220 228.3352 255.5147 84.7350 -2.2112 226.0578 228.2690 255.5822 85.5220 -2.2073 226.0950 228.3023 255.9033 86.3198 -2.2057 226.1027 228.3084 255.8683 87.1073 -2.1827 226.2530 228.4357 255.9423 87.9045 -2.1953 226.4856 228.6810 255.9204 88.7325 -2.2136 226.7842 228.9978 255.9221 89.4888 -2.1935 227.0529 229.2464 256.0938 90.3475 -2.1868 227.0019 229.1887 256.2362 91.1038 -2.1801 226.9312 229.1113 256.4410 91.9318 -2.1642 227.3033 229.4674 256.5518 92.7290 -2.1728 227.4791 229.6519 256.8114 93.5160 -2.1796 227.4725 229.6522 256.8641 94.3338 -2.1806 227.4091 229.5897 256.8609 95.1105 -2.1763 227.5533 229.7296 257.1020 95.9590 -2.1380 227.4344 229.5724 257.2629 96.6845 -2.1356 227.4575 229.5930 257.3838 97.5535 -2.1254 227.6353 229.7607 257.4245 98.3098 -2.1205 227.7478 229.8684 257.4757 99.1378 -2.1062 227.8939 230.0001 257.5838 99.9350 -2.0890 228.1586 230.2476 257.6645 100.7220 -2.1003 228.2302 230.3306 257.7897 101.5500 -2.1184 228.3134 230.4318 257.8894 102.3165 -2.1099 228.6161 230.7260 257.8978 103.1650 -2.1245 228.6472 230.7718 258.0949 103.9315 -2.1309 228.8445 230.9754 258.3651 104.7595 -2.1485 229.0204 231.1689 258.4565 105.5260 -2.1541 229.1371 231.2912 258.2934 106.3848 -2.1404 229.3214 231.4618 258.6488 107.1205 -2.1430 229.4545 231.5976 258.7177 107.9793 -2.1545 229.5399 231.6945 258.7291 108.7458 -2.1671 229.6165 231.7836 258.9256 109.5635 -2.1520 229.7098 231.8618 258.8665 110.3710 -2.1395 229.7616 231.9012 258.7980 111.1580 -2.1244 229.8253 231.9497 258.9220 111.9860 -2.1458 229.7613 231.9071 258.9758 112.7525 -2.1556 229.6903 231.8458 259.2739 113.6113 -2.1584 229.7789 231.9373 259.4790 114.3783 -2.1718 230.1132 232.2849 259.5417 115.1965 -2.1959 230.4045 232.6004 259.5598 116.0040 -2.2313 230.5826 232.8139 259.6185 116.7910 -2.2311 230.7698 233.0008 259.8067 117.5883 -2.2015 230.7454 232.9469 259.9105 118.3855 -2.1834 230.7340 232.9175 260.0640 119.2135 -2.1989 230.7727 232.9716 259.9848 119.9800 -2.1688 230.9979 233.1667 260.0690 120.8285 -2.1643 231.0664 233.2308 260.3997 121.6053 -2.1497 231.0684 233.2182 260.6011 122.4230 -2.1343 231.4017 233.5359 260.6348 123.2203 -2.1130 231.6838 233.7968 260.4937 124.0175 -2.1046 231.8671 233.9717 260.4175 124.8455 -2.1164 231.9916 234.1079 260.4074 125.6120 -2.1211 231.8267 233.9478 260.5516 126.4608 -2.1172 231.8529 233.9701 260.7397 127.2383 -2.1096 231.9677 234.0773 260.7994 128.0560 -2.1086 232.2228 234.3314 260.9521 128.8533 -2.1265 232.5746 234.7011 261.1432 129.6505 -2.1232 232.8049 234.9281 261.4296 130.4785 -2.1515 233.1668 235.3183 261.6985 131.2450 -2.1608 233.2863 235.4472 261.9683 132.0935 -2.1391 233.4189 235.5580 262.2741 132.8703 -2.1626 233.6113 235.7739 262.2370 133.6880 -2.1643 233.5770 235.7412 262.2419 134.4853 -2.1688 233.6558 235.8246 262.4275 135.2825 -2.1571 233.7474 235.9045 262.6501 136.1925 -2.1503 233.9339 236.0842 262.5715 137.1025 -2.1645 233.8496 236.0142 262.7751 137.8895 -2.1635 233.8990 236.0624 262.9994 138.7278 -2.1778 233.8892 236.0670 262.9105 139.4840 -2.1913 233.8139 236.0052 263.0029 140.3428 -2.1542 233.8866 236.0408 263.0980 141.1093 -2.1586 234.0438 236.2025 263.2367 141.9373 -2.1869 233.9524 236.1393 263.2631 142.7345 -2.1660 233.8710 236.0371 263.4083 143.5215 -2.1501 233.8543 236.0044 263.4877 144.3600 -2.1601 234.1072 236.2673 263.4213 145.1273 -2.1360 234.2678 236.4038 263.4910 145.9860 -2.1457 234.4314 236.5770 263.5854 146.7423 -2.1353 234.7016 236.8368 263.6153 147.5805 -2.1308 234.9459 237.0767 263.7681 148.3778 -2.1179 235.0725 237.1904 263.5973 149.1750 -2.1129 235.4340 237.5469 263.5222 149.9928 -2.1256 235.4231 237.5487 263.7420 150.7593 -2.1368 235.5960 237.7328 263.8812 151.5770 -2.1275 235.7091 237.8366 264.0021 152.3435 -2.1382 235.7997 237.9379 264.0753 153.1920 -2.1378 235.9610 238.0988 264.0051 153.9585 -2.1226 236.1832 238.3058 264.1822 154.7865 -2.0952 236.2833 238.3785 264.4672 155.5735 -2.0652 236.2493 238.3145 264.6290 156.3708 -2.0789 236.4374 238.5162 264.7184 157.1783 -2.0903 236.5232 238.6135 264.7143 157.9755 -2.0985 236.5976 238.6961 264.9418 158.7625 -2.0792 236.8398 238.9191 265.0019 159.5505 -2.1044 236.9083 239.0127 265.2271 160.3785 -2.0998 236.9324 239.0323 265.1265 161.1450 -2.0861 236.9820 239.0681 265.2426 161.9935 -2.0867 237.1337 239.2204 265.4918 162.7600 -2.0933 237.1341 239.2274 265.4793 163.5778 -2.0745 237.1202 239.1947 265.6225 164.3750 -2.0825 237.4201 239.5026 265.8588 165.1723 -2.0772 237.8196 239.8968 265.8649 165.9900 -2.0651 237.8626 239.9277 265.8919 166.7565 -2.0556 238.0182 240.0738 265.9287 167.5948 -2.0121 238.1783 240.1904 266.2308 168.3510 -2.0383 238.2001 240.2384 266.1943 169.2098 -2.0695 238.1749 240.2444 266.3202 169.9763 -2.0682 238.2703 240.3385 266.4803 170.8043 -2.0603 238.3037 240.3640 266.5661 171.6015 -2.0738 238.5987 240.6725 266.5296 172.3885 -2.0722 238.8997 240.9719 266.4982 173.2268 -2.0760 239.0184 241.0944 266.5654 173.9830 -2.0870 238.9510 241.0380 266.6628 174.8315 -2.1162 239.1037 241.2198 266.9643 175.6083 -2.1146 239.2207 241.3353 267.0536 176.4260 -2.1129 239.0702 241.1831 267.0077 177.2238 -2.1215 239.1018 241.2233 267.1699 178.0215 -2.1330 239.1282 241.2612 267.4387 178.8495 -2.1147 239.2200 241.3347 267.5158 179.6160 -2.0763 239.3970 241.4732 267.5542 180.4440 -2.0697 239.6158 241.6855 267.6691 181.2105 -2.0704 239.7759 241.8464 267.7164 182.0693 -2.0567 239.8184 241.8750 267.9064 182.8358 -2.0471 240.0761 242.1232 267.9572 183.6535 -2.0694 240.3667 242.4361 268.0880 184.4610 -2.0531 240.3784 242.4315 268.2014 185.2480 -2.0414 240.3975 242.4389 268.3746 186.0760 -2.0519 240.4197 242.4716 268.4771 186.8425 -2.0591 240.5082 242.5673 268.7652 187.6500 -2.0646 240.6421 242.7067 268.8414 188.4985 -2.0868 240.8679 242.9546 268.6809 189.2753 -2.0811 241.1735 243.2546 268.6927 190.0930 -2.0701 241.4241 243.4942 269.0531 190.8903 -2.0366 241.4820 243.5186 269.2582 191.6875 -2.0118 241.7020 243.7138 269.1603 192.5155 -2.0220 241.7360 243.7580 269.1398 193.2820 -2.0243 241.6220 243.6462 269.1564 194.1305 -2.0054 241.6903 243.6957 269.4439 194.9073 -2.0064 241.9579 243.9642 269.5933 195.7250 -2.0097 242.2179 244.2276 269.7088 196.5018 -2.0094 242.2911 244.3005 269.8738 197.3200 -2.0414 242.4105 244.4519 270.0680 198.1280 -2.0405 242.2800 244.3205 270.2385 198.9150 -2.0347 242.2579 244.2925 270.6551 199.7430 -2.0264 242.2498 244.2761 270.7430 200.5095 -2.0136 242.4006 244.4142 270.6725 201.3683 -2.0150 242.4276 244.4426 270.9051 202.1348 -2.0320 242.6170 244.6490 271.0217 202.9525 -2.0310 242.8909 244.9219 271.0580 203.7600 -2.0144 243.2627 245.2771 271.0634 204.5470 -2.0110 243.3633 245.3743 271.2958 205.3750 -2.0142 243.5482 245.5624 271.3679 206.1415 -2.0154 243.5484 245.5638 271.5022 207.0003 -2.0218 243.5998 245.6215 271.6000 207.7565 -2.0215 243.5534 245.5749 271.5865 208.5850 -2.0288 243.5570 245.5858 271.6771 209.3725 -2.0233 243.7714 245.7947 271.6667 210.2108 -2.0268 244.0368 246.0636 271.8083 210.9670 -2.0236 244.1257 246.1493 271.8413 211.8258 -2.0311 244.1247 246.1559 271.8604 212.5923 -2.0134 244.1956 246.2090 272.0399 213.4203 -1.9927 244.1283 246.1210 272.0356 214.1765 -1.9932 244.2224 246.2157 272.0893 215.0045 -1.9925 244.4375 246.4300 272.0076 215.8223 -1.9919 244.6937 246.6856 272.1243 216.5785 -2.0014 244.8553 246.8567 272.2204 217.4065 -2.0048 244.9541 246.9589 272.4484 218.1833 -2.0358 245.1128 247.1486 272.5086 219.0113 -2.0324 245.2790 247.3114 272.6644 219.7675 -2.0258 245.6023 247.6281 272.8279 220.6265 -2.0254 245.8754 247.9007 272.8808 221.3835 -2.0074 245.8254 247.8329 273.1622 222.2115 -2.0066 245.9505 247.9570 273.2779 223.0088 -2.0154 246.1455 248.1610 273.1954 223.7958 -2.0026 246.1893 248.1920 273.3492 224.6238 -1.9868 246.2112 248.1980 273.3476 225.3800 -1.9940 246.0809 248.0749 273.3553 226.2388 -1.9741 246.1154 248.0896 273.4311 226.9745 -1.9705 246.1873 248.1579 273.8114 227.8333 -1.9417 246.1187 248.0604 274.0369 228.5895 -1.9331 246.3265 248.2596 274.1566 229.4175 -1.9268 246.5015 248.4283 274.2809 230.2148 -1.9426 246.6928 248.6354 274.4027 231.0120 -1.9570 246.8662 248.8232 274.4441 231.8298 -1.9715 246.8414 248.8129 274.4374 232.6065 -1.9820 246.7582 248.7402 274.5429 233.4550 -2.0125 246.8901 248.9026 274.7226 234.2215 -2.0220 247.1864 249.2084 274.7638 235.0495 -2.0291 247.5734 249.6024 274.8034 235.8468 -2.0311 247.7571 249.7881 274.9199 236.6440 -2.0117 247.9449 249.9566 275.0888 237.4618 -2.0139 248.2235 250.2374 275.1476 238.2385 -2.0217 248.1959 250.2176 275.5012 239.0870 -2.0330 248.0945 250.1275 275.7119 239.8535 -2.0261 248.2483 250.2745 275.7211 240.6815 -2.0121 248.3665 250.3786 275.7808 241.4788 -2.0401 248.3347 250.3748 275.6880 242.2760 -2.0330 248.5803 250.6133 275.9242 243.0938 -2.0193 248.7355 250.7548 276.0037 243.8705 -2.0115 248.7174 250.7288 275.9529 244.7190 -2.0350 248.8592 250.8942 276.0921 245.4855 -2.0203 248.9796 251.0000 276.2181 246.3135 -2.0118 249.0600 251.0719 276.2122 247.1108 -2.0215 249.1615 251.1830 276.3527 247.9080 -2.0458 249.3096 251.3554 276.5546 248.7053 -2.0421 249.5202 251.5623 276.5234 249.5025 -2.0517 249.5936 251.6454 276.6741 250.3305 -2.0631 249.7406 251.8038 277.0001 251.0970 -2.0738 249.8074 251.8813 277.2145 251.9455 -2.1057 250.1585 252.2642 277.3699 252.7223 -2.0788 250.4186 252.4974 277.4164 253.5400 -2.0574 250.4675 252.5249 277.5756 254.3373 -2.0268 250.4871 252.5140 277.4647 255.1345 -2.0097 250.4158 252.4255 277.5049 255.9625 -1.9973 250.5077 252.5050 277.5219 256.7290 -2.0109 250.5899 252.6008 277.5309 257.5775 -2.0347 250.7362 252.7709 277.5168 258.3543 -2.0351 250.8841 252.9193 277.5396 259.1720 -2.0268 250.9388 252.9656 277.6466 259.9693 -2.0314 251.0307 253.0621 277.8251 260.7665 -2.0337 251.1346 253.1683 278.0163 261.6048 -2.0372 251.2394 253.2767 277.9717 262.3610 -2.0431 251.2215 253.2645 277.8928 263.2198 -2.0591 251.5562 253.6153 278.0031 263.9863 -2.0455 251.6881 253.7336 278.2149 264.8143 -2.0542 251.7081 253.7622 278.2981 265.6115 -2.0446 251.8913 253.9359 278.5107 266.3985 -2.0564 252.0291 254.0855 278.5503 267.2368 -2.0516 252.1200 254.1716 278.5472 268.0033 -2.0772 252.1440 254.2212 278.6234 268.8620 -2.0684 252.3280 254.3964 278.8784 269.5875 -2.0570 252.6230 254.6800 279.1417 270.4565 -2.0579 252.6610 254.7188 279.1957 271.2128 -2.0757 252.6830 254.7587 279.2876 272.0408 -2.0743 252.7032 254.7775 279.3146 272.8380 -2.0537 252.6564 254.7101 279.3578 273.6355 -2.0406 252.8330 254.8736 279.3406 274.4643 -2.0384 253.0056 255.0440 279.5648 275.2205 -2.0258 253.0907 255.1165 279.7294 276.0895 -2.0355 253.3389 255.3744 279.7308 276.8458 -2.0392 253.3502 255.3894 279.7425 277.6738 -2.0431 253.5057 255.5488 279.9281 278.4710 -2.0495 253.4288 255.4783 279.9280 279.2683 -2.0495 253.5805 255.6300 280.1221 280.0860 -2.0536 253.7641 255.8177 280.1924 280.8525 -2.0388 253.9395 255.9783 280.1839 281.7010 -2.0456 253.9947 256.0403 280.3746 282.4675 -2.0291 254.2447 256.2738 280.5003 283.2955 -2.0341 254.3253 256.3594 280.5104 284.0518 -2.0343 254.5647 256.5990 280.6041 284.8695 -2.0481 254.7000 256.7482 280.8081 285.6770 -2.0608 254.8517 256.9125 280.9440 286.4640 -2.0531 254.8542 256.9073 280.9503 287.2818 -2.0473 254.9036 256.9509 281.1349 288.0585 -2.0260 254.9010 256.9270 281.1834 288.9070 -2.0302 254.9577 256.9880 281.4190 289.6735 -2.0154 255.1799 257.1953 281.6274 290.5015 -2.0126 255.2444 257.2570 281.6572 291.2680 -2.0276 255.4167 257.4443 281.7014 292.0960 -2.0437 255.3577 257.4015 281.7636 292.8830 -2.0334 255.4576 257.4909 281.6519 293.6905 -2.0101 255.5531 257.5632 281.7400 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