DTA measure 1pb_updown_3 Date: 2025108:917 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1018.90 s Mass = 1355.100 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3133 -0.2492 229.4220 229.6712 276.4792 2.1408 -0.2448 229.6933 229.9381 276.7321 2.9065 -0.2383 229.9790 230.2173 276.9335 3.7648 -0.2385 230.2778 230.5163 277.0981 4.5203 -0.2371 230.5404 230.7775 277.1991 5.3580 -0.2342 230.8456 231.0798 277.3239 6.1445 -0.2321 231.1192 231.3513 277.3331 6.9408 -0.2328 231.4133 231.6461 277.3174 7.7683 -0.2359 231.6905 231.9264 277.2956 8.5343 -0.2354 231.9585 232.1939 277.2668 9.3615 -0.2301 232.2281 232.4583 277.1859 10.1378 -0.2312 232.4990 232.7302 277.0924 10.9753 -0.2303 232.7791 233.0094 276.9404 11.7305 -0.2267 233.0251 233.2518 276.8070 12.5990 -0.2240 233.3481 233.5721 276.6319 13.3548 -0.2214 233.6075 233.8289 276.4878 14.1920 -0.2203 233.8904 234.1107 276.3018 14.9785 -0.2176 234.1161 234.3337 276.1200 15.7855 -0.2152 234.3921 234.6073 275.9292 16.6023 -0.2121 234.6493 234.8614 275.7982 17.3683 -0.2082 234.9049 235.1131 275.6818 18.2265 -0.2022 235.2070 235.4092 275.4890 18.9923 -0.1991 235.4708 235.6699 275.3880 19.8198 -0.1966 235.7278 235.9245 275.3112 20.6060 -0.1914 236.0023 236.1936 275.2496 21.4128 -0.1856 236.2895 236.4751 275.2050 22.2303 -0.1848 236.5516 236.7364 275.1724 23.0060 -0.1809 236.7767 236.9576 275.1855 23.8540 -0.1767 236.9882 237.1649 275.2685 24.6303 -0.1786 237.2198 237.3984 275.3566 25.4470 -0.1796 237.4830 237.6626 275.5279 26.2438 -0.1765 237.7578 237.9343 275.7231 27.0403 -0.1770 237.9940 238.1710 275.9588 27.8573 -0.1741 238.2473 238.4214 276.2451 28.6233 -0.1660 238.4774 238.6434 276.5779 29.4815 -0.1633 238.7422 238.9055 276.9523 30.2368 -0.1603 238.9875 239.1478 277.3385 31.0643 -0.1591 239.2446 239.4037 277.7656 31.8608 -0.1586 239.5279 239.6865 278.2317 32.6573 -0.1574 239.7803 239.9378 278.7062 33.4845 -0.1527 240.0028 240.1554 279.2168 34.2403 -0.1460 240.2484 240.3944 279.7166 35.1085 -0.1429 240.5215 240.6643 280.2117 35.8640 -0.1411 240.7469 240.8880 280.6188 36.6915 -0.1447 240.9829 241.1275 281.0873 37.4880 -0.1436 241.2311 241.3747 281.4781 38.2848 -0.1443 241.5007 241.6450 281.8681 39.1123 -0.1436 241.7407 241.8844 282.2508 39.8778 -0.1457 241.9715 242.1172 282.5690 40.7360 -0.1486 242.2465 242.3952 282.8993 41.5020 -0.1503 242.4736 242.6239 283.1086 42.3290 -0.1486 242.7010 242.8496 283.3545 43.1155 -0.1494 242.9488 243.0981 283.5124 43.9225 -0.1469 243.2532 243.4000 283.6142 44.7393 -0.1446 243.4852 243.6298 283.7227 45.5155 -0.1443 243.6985 243.8428 283.7818 46.3635 -0.1436 243.9401 244.0837 283.7934 47.1393 -0.1547 244.1875 244.3422 283.7246 47.9565 -0.1608 244.4657 244.6265 283.6792 48.7533 -0.1631 244.7297 244.8928 283.6368 49.5495 -0.1627 244.9732 245.1359 283.5589 50.3873 -0.1641 245.2010 245.3651 283.4530 51.1430 -0.1638 245.4065 245.5703 283.3212 52.0008 -0.1629 245.6740 245.8369 283.2048 52.7668 -0.1653 245.9162 246.0815 283.0525 53.6045 -0.1647 246.1763 246.3410 282.8731 54.3598 -0.1655 246.4166 246.5821 282.7309 55.1870 -0.1691 246.6755 246.8446 282.5950 55.9838 -0.1645 246.9247 247.0892 282.4775 56.7905 -0.1632 247.1646 247.3277 282.3159 57.6075 -0.1630 247.3944 247.5574 282.1956 58.3633 -0.1588 247.6092 247.7681 282.0975 59.2315 -0.1554 247.8556 248.0110 282.0132 59.9873 -0.1567 248.0914 248.2481 281.9474 60.8045 -0.1554 248.3464 248.5018 281.8965 61.6113 -0.1541 248.5928 248.7469 281.8668 62.3975 -0.1565 248.8009 248.9574 281.8872 63.1943 -0.1551 249.0101 249.1651 281.9474 63.9908 -0.1566 249.2215 249.3781 282.0508 64.8180 -0.1558 249.4467 249.6025 282.1703 65.5840 -0.1550 249.7072 249.8622 282.3513 66.4318 -0.1544 249.9538 250.1082 282.6320 67.2080 -0.1565 250.1521 250.3086 282.8994 68.0250 -0.1605 250.3742 250.5347 283.2110 68.8213 -0.1587 250.6371 250.7958 283.5485 69.6183 -0.1565 250.8537 251.0102 283.9165 70.4148 -0.1531 251.0978 251.2510 284.3258 71.2113 -0.1530 251.3251 251.4782 284.7326 72.0385 -0.1570 251.5375 251.6945 285.1674 72.8353 -0.1593 251.7561 251.9154 285.5997 73.6318 -0.1551 251.9938 252.1489 286.0574 74.4183 -0.1540 252.2052 252.3592 286.4758 75.2558 -0.1578 252.4366 252.5944 286.9191 76.0215 -0.1610 252.6202 252.7812 287.3079 76.8798 -0.1607 252.8375 252.9982 287.7250 77.6353 -0.1695 253.0528 253.2223 288.1004 78.4728 -0.1739 253.3014 253.4753 288.4987 79.2695 -0.1769 253.5070 253.6840 288.8078 80.0660 -0.1782 253.7236 253.9018 289.0956 80.8525 -0.1792 253.9519 254.1311 289.3246 81.6595 -0.1783 254.2057 254.3841 289.5467 82.4865 -0.1779 254.3853 254.5633 289.7521 83.2525 -0.1787 254.5770 254.7557 289.8869 84.1005 -0.1819 254.8387 255.0206 290.0451 84.8765 -0.1826 255.0634 255.2459 290.1537 85.6938 -0.1851 255.2872 255.4722 290.2073 86.5005 -0.1833 255.4921 255.6754 290.2418 87.2870 -0.1841 255.6831 255.8672 290.2326 88.1248 -0.1862 255.9111 256.0973 290.1550 88.8800 -0.1904 256.1129 256.3034 290.0811 89.7385 -0.1952 256.3454 256.5406 289.9803 90.5043 -0.1951 256.5971 256.7921 289.8766 91.3215 -0.1993 256.8512 257.0505 289.7680 92.0773 -0.2009 257.0913 257.2922 289.6463 92.9145 -0.2040 257.2938 257.4978 289.5425 93.6808 -0.2072 257.5297 257.7368 289.4370 94.5285 -0.2097 257.7547 257.9644 289.2607 95.3043 -0.2094 257.9495 258.1589 289.1581 96.1215 -0.2095 258.1590 258.3685 289.0563 96.9183 -0.2100 258.3790 258.5891 288.9109 97.7145 -0.2064 258.5553 258.7617 288.8016 98.5420 -0.2072 258.7760 258.9832 288.7017 99.3080 -0.2118 258.9524 259.1642 288.6255 100.1248 -0.2136 259.1753 259.3889 288.5754 100.9010 -0.2138 259.3845 259.5984 288.5587 101.7490 -0.2177 259.6406 259.8582 288.5306 102.5145 -0.2211 259.8772 260.0983 288.5752 103.3420 -0.2238 260.1090 260.3329 288.5913 104.1388 -0.2286 260.3414 260.5700 288.7700 104.9350 -0.2321 260.5552 260.7873 288.9520 105.7523 -0.2330 260.7408 260.9739 289.1606 106.5285 -0.2311 260.9399 261.1710 289.4046 107.3763 -0.2328 261.1652 261.3979 289.7095 108.1423 -0.2355 261.3404 261.5759 289.9917 108.9695 -0.2349 261.5500 261.7849 290.3248 109.7660 -0.2343 261.7244 261.9588 290.7034 110.5630 -0.2358 261.9283 262.1641 291.1389 111.3798 -0.2360 262.1407 262.3767 291.5982 112.1560 -0.2378 262.3585 262.5963 292.0252 113.0038 -0.2383 262.5854 262.8237 292.4984 113.7695 -0.2389 262.8049 263.0439 292.9415 114.5968 -0.2402 263.0395 263.2797 293.3834 115.3935 -0.2388 263.2563 263.4951 293.7642 116.1900 -0.2354 263.4587 263.6941 294.1620 117.0173 -0.2392 263.6674 263.9066 294.5970 117.7833 -0.2419 263.8548 264.0967 294.9575 118.6413 -0.2445 264.1064 264.3509 295.2771 119.4073 -0.2471 264.2835 264.5306 295.5721 120.2348 -0.2490 264.4985 264.7474 295.8253 121.0310 -0.2512 264.7147 264.9660 296.0831 121.8278 -0.2549 264.8955 265.1504 296.2897 122.6550 -0.2594 265.0858 265.3452 296.4635 123.4105 -0.2619 265.2510 265.5129 296.6122 124.2685 -0.2626 265.4874 265.7500 296.7366 125.0345 -0.2641 265.6952 265.9592 296.7581 125.8515 -0.2684 265.9063 266.1747 296.7594 126.6278 -0.2772 266.1029 266.3801 296.7324 127.4450 -0.2819 266.2978 266.5797 296.6852 128.2310 -0.2850 266.4913 266.7764 296.6395 129.0380 -0.2879 266.6905 266.9784 296.6070 129.8553 -0.2914 266.8818 267.1731 296.5278 130.6208 -0.2885 267.0864 267.3749 296.4267 131.4790 -0.2916 267.3319 267.6235 296.2689 132.2450 -0.2958 267.5421 267.8379 296.1266 133.0723 -0.2980 267.7432 268.0412 295.9722 133.8690 -0.2969 267.9541 268.2510 295.8440 134.6655 -0.3003 268.1604 268.4607 295.7059 135.4928 -0.3030 268.3752 268.6782 295.5570 136.2585 -0.3036 268.5828 268.8864 295.4257 137.1065 -0.3029 268.8248 269.1277 295.3193 137.8823 -0.3014 269.0152 269.3165 295.2442 138.6995 -0.3034 269.2328 269.5362 295.1548 139.4963 -0.3097 269.4239 269.7335 295.1015 140.2928 -0.3123 269.6198 269.9322 295.0869 141.0995 -0.3121 269.7987 270.1109 295.1042 141.8860 -0.3124 269.9854 270.2978 295.1231 142.7235 -0.3113 270.1694 270.4807 295.2271 143.4790 -0.3128 270.3444 270.6572 295.3416 144.3475 -0.3134 270.5869 270.9003 295.5197 145.1028 -0.3142 270.7644 271.0786 295.7176 145.9303 -0.3128 270.9636 271.2765 295.9563 146.7270 -0.3089 271.1467 271.4556 296.2028 147.5335 -0.3106 271.3393 271.6499 296.5095 148.3508 -0.3120 271.5120 271.8240 296.8575 149.1168 -0.3148 271.7131 272.0280 297.1954 149.9748 -0.3130 271.8812 272.1942 297.6404 150.7508 -0.3120 272.0728 272.3848 298.0390 151.5680 -0.3101 272.2884 272.5985 298.4927 152.3643 -0.3078 272.4671 272.7749 298.9361 153.1713 -0.3076 272.6591 272.9667 299.4105 153.9578 -0.3073 272.8258 273.1332 299.8339 154.7848 -0.3052 273.0397 273.3449 300.2640 155.5815 -0.3041 273.2629 273.5670 300.6709 156.3680 -0.3106 273.4500 273.7605 301.0678 157.1848 -0.3141 273.6522 273.9663 301.4398 157.9610 -0.3182 273.8603 274.1786 301.7772 158.8090 -0.3237 274.0575 274.3812 302.0617 159.5745 -0.3276 274.2339 274.5615 302.2707 160.4020 -0.3293 274.4331 274.7624 302.5148 161.1988 -0.3282 274.6417 274.9700 302.7275 161.9848 -0.3305 274.8043 275.1348 302.8648 162.8125 -0.3327 275.0535 275.3862 302.9966 163.5885 -0.3366 275.2373 275.5739 303.0824 164.4260 -0.3410 275.4058 275.7469 303.1399 165.1920 -0.3430 275.5758 275.9188 303.1546 166.0500 -0.3482 275.7542 276.1025 303.1778 166.8055 -0.3485 275.9181 276.2666 303.1351 167.6433 -0.3511 276.1346 276.4857 303.0535 168.4295 -0.3527 276.3452 276.6979 302.9814 169.2263 -0.3542 276.5586 276.9128 302.9030 170.0538 -0.3581 276.7519 277.1100 302.7701 170.8295 -0.3590 276.9536 277.3126 302.6879 171.6470 -0.3612 277.1712 277.5324 302.5669 172.4128 -0.3601 277.3890 277.7491 302.4448 173.2708 -0.3584 277.6193 277.9776 302.2869 174.0368 -0.3591 277.8089 278.1680 302.1749 174.8640 -0.3589 278.0006 278.3595 302.0534 175.6505 -0.3568 278.1545 278.5113 301.9299 176.4575 -0.3603 278.3111 278.6715 301.8742 177.2745 -0.3634 278.4892 278.8526 301.8294 178.0405 -0.3629 278.6368 278.9997 301.7730 178.8985 -0.3637 278.8116 279.1752 301.7193 179.6645 -0.3595 279.0136 279.3731 301.6935 180.4920 -0.3616 279.2271 279.5887 301.6863 181.2780 -0.3612 279.4374 279.7986 301.7086 182.0853 -0.3609 279.6179 279.9788 301.8099 182.9023 -0.3669 279.8107 280.1776 301.9793 183.6783 -0.3705 280.0055 280.3759 302.1552 184.5263 -0.3726 280.2272 280.5998 302.4006 185.3023 -0.3721 280.4210 280.7931 302.6155 186.1193 -0.3735 280.5934 280.9669 302.8705 186.9160 -0.3736 280.7713 281.1449 303.2054 187.7125 -0.3710 280.9658 281.3368 303.5349 188.5295 -0.3706 281.1471 281.5177 303.8974 189.2855 -0.3755 281.2909 281.6663 304.2297 190.1535 -0.3800 281.4867 281.8667 304.6633 190.9093 -0.3827 281.6779 282.0605 305.0316 191.7265 -0.3828 281.8679 282.2507 305.4612 192.5330 -0.3819 282.0887 282.4706 305.9073 193.3195 -0.3867 282.2916 282.6783 306.3003 194.1163 -0.3905 282.4720 282.8626 306.7024 194.9125 -0.3881 282.6645 283.0526 307.1184 195.7398 -0.3803 282.8511 283.2313 307.5150 196.5058 -0.3830 283.0299 283.4129 307.8536 197.3535 -0.3841 283.2059 283.5900 308.1534 198.1295 -0.3826 283.3909 283.7734 308.4269 198.9470 -0.3785 283.5712 283.9498 308.6981 199.7433 -0.3807 283.7529 284.1336 308.9335 200.5400 -0.3860 283.9458 284.3318 309.1450 201.3675 -0.3905 284.1402 284.5306 309.2659 202.1330 -0.3964 284.3124 284.7087 309.3741 202.9503 -0.3994 284.4814 284.8808 309.4358 203.7265 -0.4007 284.6405 285.0412 309.4924 204.5740 -0.4026 284.8046 285.2072 309.5455 205.3403 -0.4047 284.9786 285.3833 309.5345 206.1675 -0.4070 285.1794 285.5865 309.4951 206.9743 -0.4052 285.3763 285.7815 309.4493 207.7610 -0.4088 285.5594 285.9682 309.3711 208.5880 -0.4081 285.7286 286.1367 309.3094 209.3543 -0.4089 285.8463 286.2552 309.2095 210.2225 -0.4110 286.0672 286.4782 309.0857 210.9780 -0.4111 286.2533 286.6643 308.9779 211.8055 -0.4131 286.4759 286.8889 308.8521 212.6020 -0.4118 286.6533 287.0651 308.7453 213.4090 -0.4137 286.8457 287.2594 308.6148 214.2263 -0.4164 287.0118 287.4282 308.5168 214.9918 -0.4204 287.1909 287.6113 308.3644 215.8503 -0.4199 287.3659 287.7857 308.2586 216.5955 -0.4214 287.5404 287.9619 308.1879 217.4433 -0.4309 287.7264 288.1573 308.1393 218.2093 -0.4327 287.8935 288.3262 308.1566 219.0365 -0.4305 288.0507 288.4812 308.1589 219.8330 -0.4308 288.2196 288.6504 308.1739 220.6298 -0.4320 288.4224 288.8544 308.2581 221.4468 -0.4327 288.6160 289.0488 308.3786 222.2128 -0.4310 288.8076 289.2386 308.5113 223.0710 -0.4276 289.0206 289.4483 308.7008 223.8263 -0.4259 289.2043 289.6303 308.8931 224.6538 -0.4280 289.3810 289.8090 309.1442 225.4095 -0.4279 289.5258 289.9536 309.4700 226.2573 -0.4297 289.6832 290.1130 309.8336 227.0233 -0.4281 289.8636 290.2918 310.1804 227.8505 -0.4271 290.0272 290.4543 310.5672 228.6470 -0.4297 290.2002 290.6299 310.9437 229.4438 -0.4376 290.3810 290.8186 311.3642 230.2608 -0.4399 290.5315 290.9714 311.8046 231.0368 -0.4383 290.7103 291.1487 312.2060 231.8848 -0.4414 290.9024 291.3438 312.6570 232.6505 -0.4430 291.0949 291.5379 313.0665 233.4778 -0.4440 291.2757 291.7197 313.4707 234.2743 -0.4425 291.4368 291.8793 313.8244 235.0710 -0.4459 291.5780 292.0239 314.1837 235.8878 -0.4462 291.7761 292.2223 314.5395 236.6640 -0.4475 291.9643 292.4118 314.8307 237.5120 -0.4513 292.1298 292.5812 315.1419 238.2775 -0.4546 292.3317 292.7862 315.3589 239.1053 -0.4612 292.4829 292.9441 315.5725 239.9018 -0.4655 292.6952 293.1607 315.7285 240.6983 -0.4682 292.8734 293.3415 315.8217 241.5155 -0.4741 293.0404 293.5145 315.8590 242.2915 -0.4751 293.2217 293.6968 315.9088 243.1393 -0.4778 293.4431 293.9208 315.9570 243.9050 -0.4805 293.5969 294.0774 315.9579 244.7325 -0.4795 293.7671 294.2466 315.9120 245.5288 -0.4802 293.9339 294.4140 315.8825 246.3255 -0.4780 294.0733 294.5513 315.8351 247.1530 -0.4810 294.2354 294.7164 315.7381 247.9185 -0.4836 294.4584 294.9421 315.6550 248.7768 -0.4823 294.6301 295.1124 315.5347 249.5428 -0.4776 294.8104 295.2880 315.4251 250.3698 -0.4791 295.0071 295.4863 315.3010 251.1665 -0.4846 295.1948 295.6795 315.1637 252.0248 -0.4857 295.3853 295.8710 315.0439 252.8930 -0.4886 295.5839 296.0726 314.9475 253.6693 -0.4859 295.7336 296.2195 314.8396 254.5170 -0.4914 295.8972 296.3885 314.7327 255.2725 -0.4947 296.0769 296.5717 314.6757 256.1103 -0.4972 296.2768 296.7740 314.6304 256.8965 -0.4972 296.4379 296.9351 314.6139 257.6930 -0.4966 296.6066 297.1032 314.5795 258.4898 -0.4994 296.7520 297.2514 314.6337 259.2863 -0.5001 296.9316 297.4317 314.7076 260.1135 -0.5016 297.1227 297.6243 314.8376 260.8695 -0.5016 297.3273 297.8289 314.9767 261.7375 -0.5019 297.5540 298.0559 315.1842 262.4935 -0.4991 297.7037 298.2027 315.4007 263.3208 -0.4999 297.8923 298.3922 315.6592 264.1173 -0.4953 298.0004 298.4956 315.9469 264.9140 -0.4949 298.1685 298.6633 316.2780 265.7413 -0.4949 298.3880 298.8829 316.6057 266.5070 -0.4930 298.5281 299.0211 316.9230 267.3653 -0.4953 298.7306 299.2259 317.3322 268.1310 -0.4943 298.9026 299.3969 317.7253 268.9583 -0.4936 299.0737 299.5673 318.1697 269.7448 -0.4965 299.2288 299.7252 318.5839 270.5515 -0.4986 299.4037 299.9023 318.9946 271.3685 -0.4975 299.5746 300.0721 319.4167 272.1450 -0.4979 299.7423 300.2402 319.8047 272.9925 -0.4989 299.9324 300.4312 320.2063 273.7688 -0.4994 300.0947 300.5941 320.5367 274.5860 -0.4985 300.2558 300.7543 320.8687 275.3823 -0.4990 300.3974 300.8964 321.1363 276.1790 -0.5024 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