DTA measure 2pb_updown_3 Date: 2025108:947 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.49 s Mass = 1355.100 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3684 -2.8168 459.4406 462.2574 434.4974 3.9819 -2.8266 459.4390 462.2656 434.8392 5.5854 -2.8338 459.5037 462.3375 435.0807 7.1941 -2.8408 459.5260 462.3668 435.1552 8.8178 -2.8460 459.6012 462.4472 435.1298 10.4265 -2.8520 459.6767 462.5287 434.9904 12.0299 -2.8600 459.7119 462.5719 434.7692 13.6434 -2.8714 459.7612 462.6326 434.4438 15.2469 -2.8756 459.8427 462.7183 434.0183 16.8500 -2.8791 459.9059 462.7850 433.4859 18.4484 -2.8814 459.9391 462.8204 432.9950 20.0364 -2.8877 459.9971 462.8848 432.4328 21.6499 -2.8903 460.0380 462.9283 431.8423 23.2585 -2.8916 460.1099 463.0014 431.2824 24.8618 -2.8880 460.0949 462.9829 430.7182 26.4703 -2.8867 460.0479 462.9345 430.1846 28.0633 -2.8903 460.0500 462.9403 429.7307 29.6716 -2.8930 460.0910 462.9841 429.3327 31.2751 -2.8898 460.0758 462.9656 429.0244 32.8834 -2.8900 460.0808 462.9707 428.7201 34.5075 -2.8945 460.0393 462.9337 428.5411 36.1159 -2.8924 460.0541 462.9465 428.4232 37.7090 -2.8907 460.0818 462.9725 428.3979 39.3178 -2.8914 460.0675 462.9589 428.3983 40.9261 -2.8919 460.0403 462.9322 428.4257 42.5398 -2.8892 460.0275 462.9167 428.4654 44.1433 -2.8909 460.0266 462.9176 428.5557 45.7518 -2.8890 460.0674 462.9564 428.6100 47.3550 -2.8909 460.0896 462.9804 428.6494 48.9534 -2.8897 460.0840 462.9737 428.6328 50.5619 -2.8913 460.0993 462.9906 428.5871 52.1653 -2.8995 460.0760 462.9755 428.4368 53.7636 -2.9049 460.0606 462.9655 428.2681 55.3720 -2.9097 460.0082 462.9178 428.0228 56.9754 -2.9088 459.9779 462.8866 427.7268 58.5736 -2.9078 459.9814 462.8892 427.3806 60.1770 -2.9107 459.9406 462.8514 426.9596 61.8010 -2.9163 459.9146 462.8309 426.5690 63.4044 -2.9192 459.8137 462.7329 426.1816 65.0129 -2.9205 459.7860 462.7065 425.7885 66.6164 -2.9204 459.7312 462.6516 425.4251 68.2249 -2.9113 459.7100 462.6213 425.0684 69.8334 -2.9117 459.6850 462.5967 424.6779 71.4521 -2.9112 459.6527 462.5638 424.3203 73.0759 -2.9140 459.6035 462.5175 424.0442 74.6793 -2.9112 459.5459 462.4571 423.8139 76.2929 -2.9111 459.4624 462.3735 423.6206 77.8961 -2.9113 459.4003 462.3116 423.4517 79.5048 -2.9139 459.3759 462.2899 423.2703 81.1080 -2.9153 459.3349 462.2503 423.1604 82.7218 -2.9159 459.2683 462.1842 423.1027 84.3304 -2.9181 459.1955 462.1136 423.0165 85.9131 -2.9158 459.1258 462.0416 422.9350 87.5218 -2.9148 459.0751 461.9898 422.9036 89.1251 -2.9119 459.0343 461.9462 422.8321 90.7284 -2.9130 459.0061 461.9191 422.7236 92.3370 -2.9136 458.9928 461.9064 422.6137 93.9404 -2.9161 458.9456 461.8618 422.4814 95.5489 -2.9184 458.8599 461.7783 422.3226 97.1524 -2.9192 458.7687 461.6879 422.0949 98.7658 -2.9232 458.6517 461.5749 421.8549 100.3693 -2.9249 458.5200 461.4449 421.5859 101.9779 -2.9304 458.4031 461.3335 421.3338 103.5811 -2.9300 458.3471 461.2771 421.0524 105.1949 -2.9352 458.2173 461.1525 420.8004 106.7984 -2.9333 458.1495 461.0827 420.5031 108.4068 -2.9317 458.0885 461.0202 420.1526 110.0154 -2.9275 458.0279 460.9554 419.8011 111.6240 -2.9233 457.9700 460.8933 419.4634 113.2273 -2.9195 457.8958 460.8153 419.1612 114.8308 -2.9165 457.8028 460.7193 418.8777 116.4343 -2.9172 457.7016 460.6188 418.6100 118.0375 -2.9106 457.6119 460.5224 418.3723 119.6410 -2.9084 457.5310 460.4394 418.2021 121.2340 -2.9107 457.4039 460.3145 418.0093 122.8528 -2.9132 457.2644 460.1776 417.8713 124.4613 -2.9166 457.1632 460.0798 417.7658 126.0696 -2.9230 457.0627 459.9857 417.5899 127.6781 -2.9179 456.9833 459.9012 417.4643 129.2713 -2.9179 456.8723 459.7901 417.3646 130.8796 -2.9126 456.7394 459.6520 417.2729 132.4883 -2.9075 456.6156 459.5231 417.1435 134.0966 -2.9071 456.4863 459.3934 416.9967 135.7154 -2.9114 456.3880 459.2994 416.8405 137.3239 -2.9066 456.2764 459.1830 416.6956 138.9426 -2.8988 456.1647 459.0635 416.5048 140.5563 -2.8973 456.0578 458.9551 416.2826 142.1596 -2.8955 455.9432 458.8386 416.0560 143.7681 -2.9054 455.7633 458.6686 415.7867 145.3870 -2.9113 455.6586 458.5699 415.5154 146.9851 -2.9145 455.5639 458.4784 415.2227 148.5784 -2.9154 455.4675 458.3829 414.9576 150.1818 -2.9162 455.3339 458.2501 414.6550 151.7851 -2.9140 455.2043 458.1183 414.3820 153.3936 -2.9112 455.0796 457.9908 414.0869 154.9818 -2.9128 454.9777 457.8905 413.8296 156.5901 -2.9122 454.8962 457.8084 413.5796 158.1936 -2.9146 454.8019 457.7165 413.3419 159.8228 -2.9133 454.6476 457.5609 413.1274 161.4260 -2.9113 454.5120 457.4233 412.9115 163.0346 -2.9079 454.3870 457.2949 412.7095 164.6278 -2.9009 454.2430 457.1439 412.5164 166.2361 -2.8983 454.0884 456.9868 412.3242 167.8396 -2.9032 453.9952 456.8984 412.1895 169.4530 -2.8976 453.8694 456.7669 412.0627 171.0514 -2.8967 453.6946 456.5913 411.8949 172.6598 -2.8988 453.5015 456.4003 411.7135 174.2836 -2.8907 453.3646 456.2553 411.5642 175.8923 -2.8845 453.1983 456.0828 411.3845 177.4801 -2.8848 453.0451 455.9300 411.2412 179.0733 -2.8872 452.8896 455.7768 411.0928 180.6818 -2.8867 452.7635 455.6502 410.9152 182.2850 -2.8894 452.5934 455.4829 410.7123 183.8936 -2.8882 452.4399 455.3281 410.4889 185.4969 -2.8863 452.3364 455.2226 410.2145 187.1055 -2.8853 452.1701 455.0554 409.9319 188.7141 -2.8858 452.0338 454.9196 409.6512 190.3174 -2.8875 451.9061 454.7936 409.3941 191.9260 -2.8883 451.7446 454.6329 409.1789 193.5295 -2.8881 451.5833 454.4713 408.9312 195.1379 -2.8878 451.4194 454.3071 408.6733 196.7413 -2.8853 451.2645 454.1499 408.4619 198.3499 -2.8772 451.1275 454.0048 408.2794 199.9686 -2.8767 450.9889 453.8656 408.0730 201.5824 -2.8730 450.8326 453.7056 407.8401 203.1855 -2.8687 450.7066 453.5753 407.6076 204.7993 -2.8677 450.5309 453.3985 407.3920 206.4028 -2.8628 450.3518 453.2146 407.1843 208.0110 -2.8682 450.2348 453.1030 407.0119 209.6145 -2.8675 450.0756 452.9431 406.8130 211.2330 -2.8616 449.9189 452.7806 406.6099 212.8364 -2.8581 449.7459 452.6040 406.3831 214.4396 -2.8561 449.5661 452.4221 406.1427 216.0225 -2.8540 449.4019 452.2559 405.9358 217.6465 -2.8471 449.2286 452.0757 405.7566 219.2343 -2.8425 449.0774 451.9199 405.5119 220.8429 -2.8421 448.9340 451.7761 405.2979 222.4464 -2.8456 448.7772 451.6228 405.1119 224.0649 -2.8411 448.6008 451.4419 404.9519 225.6735 -2.8369 448.4057 451.2426 404.7852 227.2769 -2.8369 448.2439 451.0809 404.5935 228.8905 -2.8350 448.0772 450.9122 404.4143 230.4940 -2.8371 447.8909 450.7280 404.2136 232.1025 -2.8399 447.6805 450.5203 404.0218 233.7059 -2.8372 447.5321 450.3693 403.8366 235.3349 -2.8333 447.3866 450.2199 403.5942 236.9380 -2.8296 447.2512 450.0808 403.3793 238.5466 -2.8310 447.0779 449.9088 403.1439 240.1395 -2.8297 446.9123 449.7419 402.8967 241.7480 -2.8261 446.7300 449.5561 402.6571 243.3461 -2.8197 446.5432 449.3628 402.3974 244.9494 -2.8123 446.3776 449.1899 402.1640 246.5428 -2.8110 446.2070 449.0181 401.9272 248.1459 -2.8087 446.0377 448.8464 401.7189 249.7596 -2.8030 445.9063 448.7093 401.4635 251.3681 -2.7996 445.6745 448.4740 401.2573 252.9715 -2.7936 445.5058 448.2994 401.0594 254.5699 -2.7906 445.3095 448.1002 400.8480 256.1733 -2.7904 445.1335 447.9239 400.6595 257.7818 -2.7922 444.9265 447.7188 400.4508 259.3853 -2.7887 444.7285 447.5172 400.2948 260.9989 -2.7856 444.6233 447.4089 400.1206 262.6176 -2.7872 444.4593 447.2465 399.9230 264.2263 -2.7860 444.2158 447.0018 399.7383 265.8296 -2.7835 444.0163 446.7998 399.5513 267.4431 -2.7837 443.8454 446.6291 399.3604 269.0466 -2.7778 443.6853 446.4632 399.1666 270.6604 -2.7714 443.4865 446.2579 398.9170 272.2650 -2.7708 443.2870 446.0577 398.6813 273.8586 -2.7671 443.1204 445.8875 398.4570 275.4736 -2.7648 442.9498 445.7146 398.2351 277.0776 -2.7578 442.7381 445.4958 398.0088 278.6770 -2.7529 442.5481 445.3010 397.7902 280.2864 -2.7528 442.3533 445.1061 397.5877 281.8855 -2.7457 442.1649 444.9106 397.3790 283.4954 -2.7390 442.0131 444.7521 397.0887 285.0991 -2.7412 441.8452 444.5865 396.8941 286.7193 -2.7367 441.6701 444.4068 396.7019 288.3285 -2.7326 441.4831 444.2157 396.5167 289.9329 -2.7309 441.3360 444.0669 396.3494 291.5425 -2.7286 441.1592 443.8879 396.1565 293.1465 -2.7229 440.9335 443.6564 395.9569 294.7564 -2.7226 440.7301 443.4527 395.7684 296.3653 -2.7211 440.5429 443.2640 395.5576 297.9905 -2.7138 440.3752 443.0890 395.3164 299.5948 -2.7099 440.1967 442.9066 395.1166 301.1990 -2.7083 440.0164 442.7246 394.9201 302.8138 -2.7012 439.8178 442.5190 394.7056 304.4178 -2.7011 439.6185 442.3196 394.4306 306.0070 -2.6936 439.4127 442.1063 394.1821 307.6109 -2.6873 439.1895 441.8768 393.9380 309.2105 -2.6824 439.0016 441.6840 393.7009 310.8300 -2.6781 438.7703 441.4484 393.4997 312.4344 -2.6756 438.5643 441.2399 393.3013 314.0179 -2.6691 438.4067 441.0758 393.0924 315.6275 -2.6656 438.2497 440.9153 392.8418 317.2319 -2.6625 438.0776 440.7402 392.6649 318.8411 -2.6553 437.8802 440.5355 392.4870 320.4458 -2.6524 437.6778 440.3302 392.3090 322.0548 -2.6484 437.5053 440.1537 392.1142 323.6749 -2.6529 437.3260 439.9788 391.9350 325.2638 -2.6501 437.0984 439.7485 391.7144 326.8731 -2.6415 436.8325 439.4740 391.5540 328.4779 -2.6372 436.6154 439.2526 391.3907 330.0868 -2.6364 436.4389 439.0753 391.1666 331.6915 -2.6312 436.2302 438.8614 390.9132 333.3006 -2.6273 436.0597 438.6870 390.6916 334.9103 -2.6227 435.8740 438.4967 390.4703 336.5353 -2.6217 435.6718 438.2935 390.2821 338.1444 -2.6180 435.4911 438.1091 390.0674 339.7389 -2.6155 435.3190 437.9345 389.8548 341.3480 -2.6069 435.1447 437.7515 389.6023 342.9474 -2.6050 434.9761 437.5811 389.3732 344.5468 -2.5979 434.7291 437.3270 389.1328 346.1405 -2.5956 434.5351 437.1307 388.8944 347.7451 -2.5914 434.3123 436.9037 388.6025 349.3593 -2.5909 434.0908 436.6817 388.3712 350.9691 -2.5954 433.8635 436.4589 388.1865 352.5733 -2.5913 433.6953 436.2866 387.9747 354.1828 -2.5911 433.5075 436.0986 387.7757 355.7875 -2.5882 433.2392 435.8274 387.5277 357.3966 -2.5826 433.0676 435.6502 387.3152 359.0011 -2.5772 432.9093 435.4865 387.1038 360.6308 -2.5761 432.7209 435.2970 386.8705 362.2353 -2.5750 432.5341 435.1091 386.6757 363.8395 -2.5710 432.3625 434.9335 386.5502 365.4540 -2.5640 432.1592 434.7232 386.3774 367.0586 -2.5603 431.9464 434.5066 386.1700 368.6676 -2.5565 431.7349 434.2914 385.9797 370.2724 -2.5540 431.5494 434.1034 385.7672 371.8921 -2.5459 431.3551 433.9010 385.5767 373.4911 -2.5475 431.1554 433.7029 385.3821 375.0856 -2.5457 430.9512 433.4969 385.1686 376.6894 -2.5434 430.7440 433.2874 384.9573 378.2941 -2.5377 430.5485 433.0862 384.7261 379.9035 -2.5366 430.3678 432.9044 384.5125 381.5078 -2.5336 430.1758 432.7094 384.3236 383.1125 -2.5351 429.9177 432.4528 384.1011 384.7063 -2.5327 429.6911 432.2237 383.8706 386.3261 -2.5250 429.4675 431.9926 383.6711 387.9354 -2.5156 429.2848 431.8004 383.4720 389.5398 -2.5084 429.0644 431.5728 383.2487 391.1495 -2.5003 428.8452 431.3456 383.0334 392.7380 -2.4992 428.6180 431.1172 382.8537 394.3428 -2.4929 428.4590 430.9519 382.5890 395.9573 -2.4865 428.2759 430.7624 382.3516 397.5615 -2.4832 428.0670 430.5502 382.1650 399.1866 -2.4792 427.8830 430.3621 381.9513 400.7956 -2.4779 427.6686 430.1465 381.7600 402.3901 -2.4764 427.4685 429.9449 381.5393 403.9889 -2.4712 427.2323 429.7035 381.3136 405.5986 -2.4688 427.0538 429.5226 381.0830 407.1975 -2.4621 426.8538 429.3158 380.8509 408.8020 -2.4614 426.6289 429.0903 380.6263 410.4115 -2.4580 426.4325 428.8904 380.3892 412.0310 -2.4511 426.2412 428.6923 380.2014 413.6306 -2.4487 426.0077 428.4564 380.0036 415.2401 -2.4424 425.7992 428.2415 379.8262 416.8443 -2.4332 425.6195 428.0527 379.6129 418.4541 -2.4332 425.4430 427.8762 379.3916 420.0583 -2.4272 425.2416 427.6688 379.1948 421.6678 -2.4243 425.0626 427.4869 378.9597 423.2879 -2.4205 424.8499 427.2705 378.7170 424.8918 -2.4198 424.5873 427.0071 378.5191 426.5015 -2.4163 424.3890 426.8052 378.3109 428.1059 -2.4096 424.1966 426.6062 378.1419 429.7151 -2.4068 423.9700 426.3768 377.9333 431.3196 -2.3974 423.7058 426.1032 377.7194 432.9288 -2.3898 423.5003 425.8901 377.5014 434.5538 -2.3841 423.3052 425.6894 377.2691 436.1526 -2.3890 423.1443 425.5333 377.0579 437.7573 -2.3863 422.9522 425.3386 376.8712 439.3611 -2.3826 422.7663 425.1488 376.6966 440.9608 -2.3763 422.5294 424.9057 376.4856 442.5700 -2.3720 422.3392 424.7112 376.2771 444.1590 -2.3683 422.1300 424.4983 376.0891 445.7688 -2.3617 421.9120 424.2737 375.9038 447.3880 -2.3617 421.6967 424.0584 375.6974 448.9979 -2.3585 421.4850 423.8435 375.5091 450.6018 -2.3540 421.2810 423.6350 375.2813 452.2064 -2.3502 421.0738 423.4241 375.0368 453.8158 -2.3440 420.8339 423.1779 374.7745 455.4200 -2.3437 420.6346 422.9783 374.5133 457.0298 -2.3451 420.4150 422.7601 374.3287 458.6490 -2.3450 420.2003 422.5453 374.1209 460.2743 -2.3401 419.9705 422.3106 373.8875 461.8781 -2.3307 419.7622 422.0928 373.6504 463.4930 -2.3225 419.5595 421.8821 373.4071 465.0975 -2.3194 419.3587 421.6781 373.1454 466.7015 -2.3153 419.1318 421.4471 372.9358 468.3216 -2.3160 418.9515 421.2675 372.7345 469.9254 -2.3101 418.7422 421.0523 372.5228 471.5096 -2.3032 418.5172 420.8204 372.3349 473.1188 -2.2954 418.2636 420.5590 372.1100 474.7233 -2.2922 418.0419 420.3340 371.8909 476.3276 -2.2955 417.8527 420.1482 371.7369 477.9318 -2.2882 417.6624 419.9506 371.5839 479.5364 -2.2782 417.4451 419.7232 371.3940 481.1608 -2.2744 417.3034 419.5778 371.2017 482.7655 -2.2741 417.1082 419.3823 371.0383 484.3748 -2.2731 416.9004 419.1735 370.8344 485.9791 -2.2711 416.6957 418.9667 370.5881 487.5888 -2.2668 416.4421 418.7089 370.3638 489.1979 -2.2630 416.2789 418.5419 370.1690 490.8078 -2.2670 416.0648 418.3318 369.9718 492.4273 -2.2592 415.8128 418.0721 369.7576 494.0316 -2.2527 415.5857 417.8384 369.5351 495.6415 -2.2508 415.3465 417.5973 369.2937 497.2453 -2.2463 415.1843 417.4306 369.0148 498.8551 -2.2475 414.9651 417.2126 368.8061 500.4593 -2.2429 414.7563 416.9992 368.6003 502.0534 -2.2400 414.5068 416.7468 368.3954 503.6684 -2.2350 414.2662 416.5013 368.1995 505.2728 -2.2251 414.0442 416.2693 367.9914 506.8769 -2.2218 413.8220 416.0439 367.7775 508.4868 -2.2213 413.5868 415.8081 367.5394 510.0751 -2.2151 413.4166 415.6317 367.3362 511.6748 -2.2092 413.2431 415.4523 367.1408 513.2839 -2.2077 413.0020 415.2096 366.9391 514.8884 -2.2017 412.7813 414.9831 366.7254 516.5130 -2.2020 412.5996 414.8016 366.5219 518.1174 -2.2012 412.4172 414.6184 366.2857 519.7270 -2.1983 412.2134 414.4117 366.0830 521.3310 -2.1928 412.0152 414.2079 365.8908 522.9358 -2.1881 411.8169 414.0050 365.6686 524.5498 -2.1792 411.6172 413.7964 365.4503 526.1545 -2.1755 411.3886 413.5641 365.2736 527.7794 -2.1721 411.1748 413.3469 365.0346 529.3886 -2.1658 410.9518 413.1176 364.7782 530.9933 -2.1598 410.7048 412.8646 364.5400 532.5869 -2.1584 410.4665 412.6249 364.3215 534.1968 -2.1610 410.2295 412.3904 364.0993 535.7956 -2.1643 410.0232 412.1875 363.9208 537.3796 -2.1618 409.8161 411.9778 363.7167 538.9888 -2.1565 409.6092 411.7657 363.5328 540.5881 -2.1526 409.4221 411.5748 363.3274 542.2078 -2.1442 409.1942 411.3385 363.1744 543.8171 -2.1347 408.9775 411.1123 362.9663 545.4216 -2.1305 408.7834 410.9139 362.7344 547.0308 -2.1250 408.5690 410.6940 362.4963 548.6355 -2.1228 408.3320 410.4547 362.2766 550.2495 -2.1233 408.1286 410.2518 362.0520 551.8543 -2.1228 407.8809 410.0037 361.8379 553.4840 -2.1214 407.6864 409.8078 361.6180 555.0884 -2.1140 407.4717 409.5857 361.4142 556.6983 -2.1110 407.2704 409.3814 361.2291 558.3020 -2.1052 407.0513 409.1566 361.0568 559.9170 -2.1032 406.8540 408.9572 360.8251 561.5211 -2.1021 406.6413 408.7435 360.6242 563.1306 -2.1045 406.4693 408.5738 360.3602 564.7353 -2.1002 406.2447 408.3449 360.1674 566.3340 -2.0948 405.9973 408.0921 359.9623 567.9439 -2.0875 405.8078 407.8953 359.7700 569.5378 -2.0886 405.6054 407.6940 359.5795 571.1575 -2.0849 405.3618 407.4467 359.4099 572.7623 -2.0801 405.1834 407.2634 359.2154 574.3716 -2.0726 404.9773 407.0500 359.0183 575.9759 -2.0702 404.7636 406.8339 358.8158 577.5858 -2.0648 404.5607 406.6256 358.5912 579.1896 -2.0655 404.3526 406.4181 358.3761 580.8045 -2.0622 404.1400 406.2022 358.1500 582.4086 -2.0556 403.9025 405.9582 357.8877 584.0130 -2.0516 403.6836 405.7351 357.6512 585.6225 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