DTA measure 2pb_updown_4 Date: 2025108:1031 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1724.06 s Mass = 1355.100 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4676 0.1503 231.5150 231.3647 217.8373 4.0768 0.1594 231.4993 231.3399 217.5425 5.6813 0.1686 231.5054 231.3368 217.2257 7.2809 0.1715 231.5246 231.3531 216.9313 8.8856 0.1774 231.5697 231.3923 216.6225 10.4845 0.1852 231.5831 231.3979 216.3527 12.0941 0.1968 231.5843 231.3875 216.1088 13.6989 0.2037 231.5917 231.3881 215.8876 15.3029 0.2098 231.6309 231.4210 215.7101 16.9125 0.2193 231.6742 231.4549 215.6832 18.5173 0.2251 231.6799 231.4548 215.7102 20.1265 0.2362 231.7027 231.4665 215.7759 21.7309 0.2406 231.7325 231.4919 215.9253 23.3408 0.2394 231.7491 231.5097 216.2001 24.9603 0.2409 231.7897 231.5488 216.5338 26.5646 0.2481 231.7917 231.5436 217.0139 28.1796 0.2517 231.8106 231.5588 217.5329 29.7684 0.2548 231.7947 231.5399 218.1305 31.3984 0.2610 231.8528 231.5918 218.7099 32.9878 0.2654 231.8341 231.5687 219.2913 34.5971 0.2643 231.8780 231.6137 219.8270 36.2014 0.2690 231.8987 231.6297 220.3449 37.8266 0.2662 231.9415 231.6753 220.8173 39.4205 0.2625 231.9661 231.7035 221.2408 41.0095 0.2632 231.9786 231.7153 221.5522 42.6143 0.2596 231.9482 231.6885 221.8095 44.2131 0.2574 231.9403 231.6829 222.0496 45.8228 0.2562 231.9760 231.7198 222.2074 47.4326 0.2529 232.0189 231.7661 222.3221 49.0366 0.2532 232.0225 231.7693 222.3442 50.6360 0.2446 232.0405 231.7959 222.3017 52.2561 0.2395 232.0504 231.8109 222.2420 53.8655 0.2395 232.0410 231.8014 222.1766 55.4698 0.2444 232.0476 231.8032 222.1019 57.0796 0.2427 232.1010 231.8583 221.9993 58.6690 0.2404 232.1561 231.9157 221.9427 60.2738 0.2423 232.2001 231.9578 221.9135 61.8883 0.2381 232.2021 231.9640 221.9126 63.4925 0.2301 232.1915 231.9613 221.9619 65.1178 0.2280 232.1973 231.9693 222.0821 66.7225 0.2191 232.2078 231.9887 222.2589 68.3323 0.2133 232.2140 232.0007 222.5108 69.9259 0.2198 232.2334 232.0135 222.7628 71.5255 0.2210 232.2518 232.0308 223.1120 73.1354 0.2194 232.3012 232.0817 223.5547 74.7346 0.2169 232.3004 232.0835 223.9923 76.3541 0.2152 232.3358 232.1206 224.4596 77.9486 0.2108 232.3290 232.1182 224.9094 79.5533 0.2074 232.3763 232.1689 225.3653 81.1623 0.2037 232.4128 232.2091 225.8079 82.7670 0.1973 232.4182 232.2209 226.2228 84.3716 0.1913 232.4660 232.2747 226.5934 85.9858 0.1874 232.4968 232.3094 226.9198 87.5905 0.1815 232.5284 232.3468 227.1569 89.2158 0.1742 232.5319 232.3577 227.3412 90.8200 0.1671 232.5696 232.4025 227.5598 92.4294 0.1649 232.6132 232.4482 227.7111 94.0341 0.1607 232.6218 232.4611 227.8056 95.6440 0.1614 232.6867 232.5253 227.8567 97.2485 0.1607 232.7780 232.6173 227.8435 98.8525 0.1562 232.7921 232.6359 227.7949 100.4829 0.1499 232.8437 232.6938 227.8145 102.0825 0.1462 232.9265 232.7803 227.8365 103.6870 0.1454 232.9435 232.7982 227.7953 105.2859 0.1440 232.9685 232.8244 227.8172 106.8753 0.1356 233.0534 232.9179 227.8615 108.4800 0.1319 233.0543 232.9223 227.9570 110.0839 0.1301 233.0190 232.8888 228.1089 111.6885 0.1268 233.0645 232.9376 228.3224 113.3135 0.1270 233.1174 232.9905 228.6100 114.9021 0.1285 233.1677 233.0392 228.8679 116.5223 0.1234 233.1784 233.0551 229.2631 118.1270 0.1139 233.2499 233.1360 229.6434 119.7309 0.1109 233.3228 233.2119 230.0519 121.3253 0.1052 233.3837 233.2786 230.4865 122.9300 0.1022 233.4199 233.3177 230.9696 124.5393 0.1013 233.4755 233.3742 231.3875 126.1590 0.1023 233.5172 233.4149 231.7415 127.7689 0.0997 233.5454 233.4457 232.1054 129.3736 0.0968 233.6151 233.5183 232.3942 130.9884 0.0938 233.6997 233.6060 232.6422 132.5924 0.0906 233.8018 233.7112 232.8587 134.1920 0.0920 233.8382 233.7462 233.0253 135.7814 0.0841 233.8947 233.8105 233.1639 137.3860 0.0819 233.9658 233.8839 233.2297 139.0001 0.0803 234.0247 233.9444 233.2701 140.6100 0.0791 234.1182 234.0391 233.3057 142.1994 0.0766 234.1809 234.1043 233.3075 143.8088 0.0673 234.2852 234.2178 233.3250 145.4130 0.0623 234.3187 234.2564 233.3708 147.0178 0.0609 234.3759 234.3150 233.4373 148.6276 0.0584 234.4224 234.3640 233.5121 150.2324 0.0507 234.5028 234.4521 233.5964 151.8569 0.0446 234.5433 234.4987 233.7319 153.4614 0.0490 234.6211 234.5720 233.9066 155.0713 0.0507 234.6575 234.6068 234.1089 156.6760 0.0476 234.7591 234.7116 234.4160 158.2856 0.0446 234.8441 234.7995 234.7373 159.8948 0.0448 234.9570 234.9123 235.0720 161.4995 0.0441 235.0666 235.0224 235.4729 163.1248 0.0398 235.1933 235.1535 235.8232 164.7295 0.0385 235.2966 235.2581 236.2460 166.3385 0.0425 235.3857 235.3432 236.6499 167.9175 0.0423 235.4529 235.4106 237.0123 169.5223 0.0418 235.4889 235.4471 237.3504 171.1214 0.0326 235.5601 235.5275 237.6838 172.7256 0.0304 235.6601 235.6297 237.9631 174.3304 0.0281 235.7638 235.7357 238.2051 175.9555 0.0265 235.8716 235.8451 238.4320 177.5594 0.0253 235.9891 235.9638 238.5546 179.1693 0.0179 236.0787 236.0608 238.6633 180.7740 0.0179 236.1395 236.1216 238.7992 182.3624 0.0160 236.2238 236.2078 238.8814 183.9723 0.0162 236.3086 236.2925 238.9020 185.5770 0.0172 236.3843 236.3671 238.9092 187.1861 0.0215 236.4872 236.4658 238.8937 188.8060 0.0214 236.6173 236.5959 238.9336 190.4159 0.0178 236.7418 236.7240 238.9828 192.0206 0.0166 236.8968 236.8803 239.1051 193.6251 0.0158 236.9711 236.9553 239.2248 195.2189 0.0168 237.0671 237.0503 239.4070 196.8236 0.0105 237.1713 237.1608 239.6375 198.4335 0.0066 237.2706 237.2640 239.9104 200.0329 0.0071 237.3892 237.3820 240.1918 201.6369 0.0075 237.5039 237.4964 240.4966 203.2416 0.0057 237.6724 237.6667 240.8960 204.8464 0.0008 237.7822 237.7814 241.2944 206.4555 0.0058 237.8622 237.8565 241.6819 208.0600 0.0020 237.9437 237.9417 242.1057 209.6648 0.0012 238.0190 238.0178 242.4674 211.2588 -0.0038 238.1620 238.1657 242.8015 212.8630 -0.0035 238.2726 238.2761 243.1061 214.4729 0.0017 238.4164 238.4147 243.4243 216.0930 0.0040 238.5922 238.5882 243.6878 217.7071 0.0038 238.6399 238.6361 243.8698 219.3118 -0.0012 238.7415 238.7426 244.0470 220.9216 -0.0046 238.8681 238.8726 244.1334 222.5258 -0.0126 239.0331 239.0458 244.2239 224.1301 -0.0158 239.1730 239.1888 244.2956 225.7400 -0.0134 239.3127 239.3261 244.3413 227.3648 -0.0072 239.4521 239.4593 244.3735 228.9741 -0.0032 239.5945 239.5977 244.4051 230.5789 -0.0091 239.7065 239.7157 244.4690 232.1785 -0.0079 239.8089 239.8168 244.5368 233.7824 -0.0026 239.9407 239.9433 244.6333 235.3665 0.0008 240.0744 240.0736 244.7761 236.9764 -0.0017 240.1973 240.1989 244.9852 238.5805 0.0044 240.2900 240.2856 245.2076 240.2003 0.0105 240.4112 240.4007 245.4746 241.8101 0.0138 240.5649 240.5510 245.7703 243.3991 0.0104 240.7069 240.6965 246.0782 245.0238 0.0093 240.8464 240.8371 246.3999 246.6131 0.0096 240.9821 240.9725 246.7547 248.2384 0.0120 241.1479 241.1359 247.1594 249.8269 0.0139 241.2903 241.2764 247.5421 251.4366 0.0131 241.4163 241.4032 247.9237 253.0619 0.0141 241.5281 241.5140 248.2904 254.6659 0.0187 241.6896 241.6709 248.6019 256.2806 0.0213 241.8282 241.8068 248.8784 257.8854 0.0187 241.9730 241.9543 249.0897 259.4945 0.0130 242.0722 242.0592 249.2884 261.0888 0.0131 242.2228 242.2097 249.4420 262.6986 0.0143 242.3772 242.3629 249.5559 264.2981 0.0097 242.5328 242.5231 249.6555 265.8969 0.0083 242.7101 242.7019 249.7597 267.5016 0.0051 242.8600 242.8548 249.7916 269.1064 0.0037 243.0348 243.0311 249.8500 270.7050 0.0069 243.2045 243.1976 249.8898 272.3149 0.0108 243.4120 243.4012 249.8913 273.9196 0.0165 243.5511 243.5346 249.9708 275.5136 0.0206 243.6332 243.6127 250.1157 277.1179 0.0204 243.7901 243.7698 250.3001 278.7278 0.0198 243.9798 243.9600 250.5337 280.3479 0.0199 244.1484 244.1285 250.7882 281.9516 0.0228 244.2750 244.2522 251.0724 283.5615 0.0228 244.4264 244.4036 251.3978 285.1663 0.0214 244.5746 244.5532 251.7473 286.7755 0.0207 244.6723 244.6517 252.1177 288.3799 0.0181 244.8430 244.8249 252.4915 289.9898 0.0235 245.0227 244.9992 252.8477 291.6099 0.0218 245.2088 245.1870 253.2030 293.2195 0.0200 245.3794 245.3594 253.5565 294.8235 0.0214 245.5131 245.4917 253.8562 296.4283 0.0238 245.6747 245.6509 254.1201 298.0125 0.0260 245.8334 245.8073 254.3573 299.6173 0.0252 245.9974 245.9722 254.5210 301.2210 0.0262 246.1574 246.1312 254.6938 302.8258 0.0276 246.3218 246.2942 254.8201 304.4459 0.0267 246.5348 246.5081 254.8920 306.0506 0.0294 246.6944 246.6650 254.9466 307.6605 0.0275 246.8675 246.8400 254.9997 309.2644 0.0287 247.0591 247.0304 255.0493 310.8741 0.0329 247.2171 247.1842 255.1583 312.4789 0.0377 247.3675 247.3297 255.2226 314.0888 0.0409 247.4962 247.4554 255.3272 315.7079 0.0415 247.6682 247.6268 255.4277 317.3126 0.0375 247.8359 247.7983 255.5834 318.9225 0.0379 248.0382 248.0003 255.7925 320.5273 0.0385 248.1879 248.1494 256.0733 322.1361 0.0425 248.3319 248.2894 256.4025 323.7460 0.0438 248.5001 248.4563 256.7214 325.3559 0.0423 248.7013 248.6590 257.0764 326.9603 0.0451 248.9009 248.8558 257.4577 328.5593 0.0470 249.0668 249.0198 257.8052 330.1691 0.0437 249.2285 249.1848 258.1640 331.7683 0.0470 249.4169 249.3698 258.5201 333.3725 0.0459 249.5774 249.5314 258.8486 334.9773 0.0434 249.7374 249.6940 259.1381 336.5611 0.0431 249.9074 249.8643 259.4133 338.1704 0.0389 250.0976 250.0586 259.6583 339.7751 0.0364 250.3057 250.2692 259.8543 341.3951 0.0379 250.5482 250.5103 260.0119 343.0041 0.0417 250.7110 250.6693 260.1147 344.6089 0.0426 250.9230 250.8804 260.2165 346.2188 0.0443 251.1006 251.0563 260.3050 347.8125 0.0428 251.2731 251.2303 260.3438 349.4221 0.0421 251.4386 251.3965 260.4163 351.0269 0.0429 251.5969 251.5540 260.4751 352.6358 0.0455 251.8190 251.7735 260.5549 354.2559 0.0481 251.9853 251.9372 260.6746 355.8504 0.0477 252.1455 252.0977 260.7356 357.4603 0.0483 252.3836 252.3353 260.8882 359.0698 0.0504 252.5854 252.5350 261.1171 360.6688 0.0493 252.7866 252.7373 261.3562 362.2735 0.0512 253.0531 253.0019 261.6392 363.8731 0.0515 253.2751 253.2236 261.9955 365.4779 0.0562 253.4065 253.3503 262.3892 367.0971 0.0547 253.5749 253.5202 262.7440 368.7069 0.0551 253.7884 253.7334 263.1207 370.3116 0.0554 254.0006 253.9452 263.4905 371.9001 0.0532 254.1725 254.1193 263.8815 373.5099 0.0516 254.3734 254.3218 264.2180 375.1146 0.0410 254.5688 254.5279 264.4853 376.7236 0.0410 254.7213 254.6803 264.7584 378.3283 0.0349 254.9402 254.9053 264.9633 379.9535 0.0373 255.1485 255.1112 265.1308 381.5583 0.0401 255.3302 255.2901 265.2981 383.1676 0.0373 255.5111 255.4738 265.4259 384.7770 0.0420 255.7075 255.6654 265.5243 386.3818 0.0439 255.8680 255.8241 265.5408 387.9916 0.0442 256.0715 256.0273 265.5746 389.5956 0.0445 256.2834 256.2390 265.6101 391.2206 0.0420 256.5163 256.4743 265.6937 392.8151 0.0429 256.7465 256.7036 265.7937 394.4199 0.0397 256.8571 256.8175 265.8969 396.0246 0.0367 256.9938 256.9571 266.0294 397.6130 0.0351 257.2260 257.1909 266.1992 399.2178 0.0389 257.4453 257.4064 266.3924 400.8225 0.0449 257.6392 257.5943 266.6837 402.4265 0.0462 257.8419 257.7957 267.0346 404.0515 0.0427 258.0414 257.9987 267.3488 405.6563 0.0468 258.2440 258.1972 267.7000 407.2608 0.0507 258.4349 258.3842 268.1356 408.8699 0.0500 258.6088 258.5588 268.5101 410.4746 0.0512 258.8406 258.7894 268.9018 412.0691 0.0463 259.0680 259.0217 269.2534 413.6736 0.0400 259.2971 259.2571 269.5959 415.2981 0.0430 259.4815 259.4385 269.9143 416.9183 0.0386 259.6645 259.6259 270.1537 418.5230 0.0354 259.8665 259.8310 270.3237 420.1329 0.0327 260.0736 260.0409 270.4871 421.7368 0.0223 260.3039 260.2817 270.6292 423.3465 0.0268 260.5315 260.5047 270.7131 424.9513 0.0331 260.7339 260.7008 270.7690 426.5509 0.0348 260.9976 260.9628 270.8000 428.1546 0.0315 261.1860 261.1545 270.8251 429.7594 0.0369 261.3914 261.3545 270.8851 431.3693 0.0362 261.5700 261.5338 270.9656 432.9740 0.0399 261.7592 261.7193 271.0801 434.5779 0.0390 261.9912 261.9523 271.1708 436.1876 0.0358 262.2054 262.1695 271.2646 437.7924 0.0419 262.3883 262.3465 271.4527 439.4169 0.0450 262.6305 262.5855 271.6942 441.0214 0.0417 262.8360 262.7943 272.0166 442.6313 0.0432 263.0177 262.9745 272.3483 444.2359 0.0440 263.1942 263.1502 272.7027 445.8398 0.0406 263.4270 263.3864 273.0996 447.4496 0.0348 263.6091 263.5743 273.5284 449.0544 0.0284 263.8362 263.8078 273.9266 450.6845 0.0279 264.1051 264.0772 274.3585 452.2885 0.0297 264.3109 264.2812 274.7279 453.8984 0.0295 264.5346 264.5051 275.0491 455.5031 0.0261 264.7095 264.6834 275.3134 457.1120 0.0281 264.8985 264.8704 275.5195 458.7783 0.0321 265.1208 265.0887 275.7456 460.3779 0.0325 265.3590 265.3265 275.8653 461.9826 0.0300 265.5703 265.5404 275.9724 463.5768 0.0238 265.7449 265.7211 276.0214 465.1809 0.0255 265.9322 265.9066 276.0501 466.7908 0.0280 266.1332 266.1052 276.0586 468.4109 0.0255 266.3314 266.3059 276.0866 470.0150 0.0214 266.5939 266.5725 276.1459 471.6245 0.0223 266.8630 266.8406 276.2004 473.2293 0.0249 267.0569 267.0320 276.2432 474.8438 0.0204 267.2852 267.2648 276.3590 476.4480 0.0192 267.5082 267.4891 276.5509 478.0579 0.0204 267.7394 267.7190 276.7765 479.6780 0.0245 267.9681 267.9437 276.9956 481.2870 0.0228 268.1475 268.1247 277.2835 482.8916 0.0252 268.3867 268.3615 277.5996 484.4964 0.0254 268.5775 268.5521 278.0099 486.1063 0.0231 268.8062 268.7831 278.4671 487.7105 0.0269 269.0338 269.0069 278.9010 489.3199 0.0264 269.1984 269.1720 279.3243 490.9349 0.0262 269.4405 269.4143 279.7095 492.5345 0.0284 269.6630 269.6345 280.1023 494.1438 0.0246 269.8890 269.8644 280.4175 495.7481 0.0217 270.1321 270.1104 280.6872 497.3375 0.0173 270.3641 270.3468 280.9402 498.9416 0.0098 270.5556 270.5458 281.0886 500.5460 0.0091 270.8084 270.7993 281.2204 502.1559 0.0071 271.0046 270.9975 281.3096 503.7756 0.0009 271.2096 271.2087 281.3410 505.3849 0.0009 271.4516 271.4507 281.3677 506.9896 -0.0080 271.6332 271.6412 281.3212 508.5940 -0.0080 271.8648 271.8728 281.3338 510.2033 -0.0045 272.0734 272.0779 281.3650 511.8080 -0.0076 272.3079 272.3155 281.4531 513.4333 -0.0098 272.5205 272.5303 281.5560 515.0421 -0.0058 272.7550 272.7608 281.7068 516.6520 0.0008 272.9981 272.9973 281.8779 518.2721 -0.0035 273.2180 273.2215 282.0938 519.8814 -0.0059 273.4467 273.4526 282.3689 521.4806 -0.0012 273.6944 273.6956 282.7057 523.0649 0.0003 273.8773 273.8770 283.0751 524.6744 -0.0015 274.0685 274.0700 283.4523 526.2888 -0.0020 274.2801 274.2821 283.8822 527.8935 -0.0028 274.4914 274.4943 284.2913 529.5030 -0.0064 274.7033 274.7096 284.7130 531.1071 -0.0069 274.9293 274.9362 285.0968 532.7016 -0.0105 275.1533 275.1638 285.4234 534.3064 -0.0145 275.3421 275.3566 285.7368 535.9111 -0.0211 275.5175 275.5386 286.0295 537.5206 -0.0244 275.7632 275.7876 286.2806 539.1401 -0.0281 275.9743 276.0023 286.4385 540.7500 -0.0307 276.2200 276.2508 286.5048 542.3540 -0.0320 276.4866 276.5186 286.5627 543.9688 -0.0333 276.7268 276.7602 286.5582 545.5735 -0.0370 276.9957 277.0327 286.5592 547.1825 -0.0365 277.2391 277.2756 286.5601 548.7871 -0.0346 277.4404 277.4749 286.5546 550.4073 -0.0401 277.6668 277.7070 286.5497 552.0065 -0.0431 277.8912 277.9343 286.6396 553.6055 -0.0380 278.1199 278.1579 286.7841 555.2205 -0.0358 278.3658 278.4016 286.9555 556.8253 -0.0324 278.5700 278.6024 287.1608 558.4091 -0.0307 278.7512 278.7820 287.3929 560.0184 -0.0328 278.9659 278.9987 287.6738 561.6231 -0.0353 279.1773 279.2126 288.0475 563.2433 -0.0355 279.3921 279.4277 288.4259 564.8524 -0.0338 279.6204 279.6542 288.8793 566.4569 -0.0393 279.8349 279.8743 289.2904 568.0668 -0.0420 280.0716 280.1136 289.7100 569.6706 -0.0428 280.3320 280.3749 290.1070 571.2701 -0.0413 280.5620 280.6033 290.4750 572.8749 -0.0437 280.8254 280.8691 290.8642 574.4839 -0.0484 281.0783 281.1266 291.1722 576.1039 -0.0539 281.3399 281.3938 291.4054 577.7086 -0.0590 281.5526 281.6116 291.5344 579.3179 -0.0658 281.7840 281.8498 291.6690 580.9223 -0.0680 281.9964 282.0643 291.7660 582.5373 -0.0727 282.2147 282.2875 291.8011 584.1419 -0.0748 282.4675 282.5423 291.8389 585.7463 -0.0747 282.6559 282.7306 291.8343 587.3608 -0.0734 282.8817 282.9551 291.7919 588.9604 -0.0747 283.0768 283.1515 291.8228 590.5703 -0.0790 283.3110 283.3900 291.8128 592.1693 -0.0802 283.5108 283.5910 291.8757 593.7736 -0.0795 283.7355 283.8150 292.0077 595.3835 -0.0813 284.0125 284.0938 292.1981 596.9883 -0.0822 284.2066 284.2887 292.4608 598.6129 -0.0806 284.4001 284.4807 292.7556 600.2173 -0.0787 284.6457 284.7244 293.1067 601.8220 -0.0803 284.8859 284.9662 293.4856 603.4319 -0.0850 285.1198 285.2048 293.8777 605.0359 -0.0898 285.3539 285.4437 294.3440 606.6455 -0.0961 285.5529 285.6490 294.8028 608.2503 -0.1000 285.7994 285.8994 295.2299 609.8804 -0.1052 286.0572 286.1624 295.6137 611.4844 -0.1086 286.2772 286.3858 295.9544 613.0943 -0.1110 286.4902 286.6012 296.2803 614.6990 -0.1142 286.6766 286.7908 296.5310 616.3084 -0.1172 286.8824 286.9997 296.7187 617.8973 -0.1174 287.1467 287.2641 296.8725 619.5020 -0.1146 287.4258 287.5404 296.9881 621.1068 -0.1167 287.6356 287.7523 297.0616 622.7261 -0.1250 287.8570 287.9820 297.0072 624.3255 -0.1273 288.0867 288.2140 296.9548 625.9354 -0.1276 288.3141 288.4417 296.9558 627.5401 -0.1285 288.5333 288.6618 296.9624 629.1495 -0.1337 288.7900 288.9237 296.9848 630.7538 -0.1389 289.0125 289.1514 297.0235 632.3585 -0.1377 289.2616 289.3993 297.1246 633.9833 -0.1362 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