DTA measure 1lassu Date: 202633:1154 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.92 s Mass = 1163.800 mg data_number = 1067 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4099 -0.2170 242.0425 242.2595 221.6325 4.0390 -0.2065 242.0511 242.2576 221.3570 5.6426 -0.1949 242.0205 242.2153 221.0907 7.2510 -0.1866 242.0470 242.2337 220.7882 8.8545 -0.1777 242.0412 242.2188 220.4776 10.4583 -0.1692 242.0100 242.1792 220.1891 12.0669 -0.1590 242.0072 242.1661 219.9473 13.6701 -0.1512 241.9881 242.1393 219.6558 15.2891 -0.1423 241.9455 242.0878 219.3817 16.8773 -0.1335 241.8947 242.0283 219.1115 18.4758 -0.1301 241.8683 241.9984 218.8360 20.0843 -0.1250 241.8440 241.9690 218.5815 21.6879 -0.1235 241.8147 241.9382 218.3226 23.2965 -0.1164 241.7768 241.8932 218.1200 24.9000 -0.1128 241.7332 241.8460 217.8892 26.4934 -0.1031 241.7329 241.8360 217.7165 28.1019 -0.1006 241.6987 241.7993 217.5707 29.7209 -0.0993 241.6098 241.7091 217.4861 31.3295 -0.0971 241.5778 241.6749 217.4914 32.9379 -0.0909 241.5193 241.6102 217.5542 34.5465 -0.0873 241.4583 241.5456 217.6995 36.1399 -0.0852 241.4151 241.5003 217.9047 37.7486 -0.0830 241.3539 241.4369 218.1774 39.3523 -0.0826 241.3046 241.3872 218.5437 40.9760 -0.0841 241.2799 241.3640 218.9686 42.5849 -0.0865 241.2387 241.3253 219.4234 44.1940 -0.0851 241.1978 241.2829 219.8760 45.7988 -0.0861 241.1261 241.2122 220.3685 47.3933 -0.0867 241.0436 241.1303 220.8485 49.0030 -0.0829 241.0038 241.0867 221.3679 50.6018 -0.0862 240.9675 241.0537 221.8365 52.2014 -0.0957 240.9207 241.0165 222.2369 53.8266 -0.1024 240.8092 240.9116 222.5600 55.4308 -0.1092 240.7564 240.8656 222.8598 57.0403 -0.1109 240.7060 240.8169 223.0870 58.6450 -0.1147 240.6634 240.7782 223.2496 60.2496 -0.1205 240.6275 240.7480 223.4292 61.8586 -0.1289 240.6178 240.7468 223.5471 63.4634 -0.1417 240.6169 240.7586 223.6186 65.0886 -0.1420 240.6075 240.7495 223.6481 66.6926 -0.1492 240.5186 240.6678 223.6572 68.3023 -0.1536 240.4860 240.6396 223.6839 69.9070 -0.1578 240.4356 240.5934 223.6966 71.5165 -0.1616 240.4148 240.5764 223.7350 73.1258 -0.1644 240.3856 240.5499 223.7841 74.7356 -0.1657 240.3293 240.4950 223.8504 76.3404 -0.1697 240.2945 240.4642 223.9258 77.9648 -0.1709 240.2529 240.4238 224.0418 79.5591 -0.1778 240.1604 240.3382 224.1919 81.1485 -0.1877 240.1285 240.3162 224.3728 82.7579 -0.1958 240.0977 240.2935 224.5657 84.3570 -0.2022 240.0727 240.2749 224.8133 85.9566 -0.2042 240.0800 240.2842 225.0896 87.5664 -0.2106 240.0576 240.2681 225.3900 89.1754 -0.2109 240.0031 240.2140 225.7115 90.7801 -0.2150 239.9844 240.1994 226.0622 92.3900 -0.2216 239.9295 240.1511 226.4379 93.9998 -0.2279 239.9328 240.1606 226.7888 95.6036 -0.2342 239.8672 240.1014 227.1475 97.2135 -0.2425 239.8348 240.0773 227.4868 98.8183 -0.2492 239.8356 240.0847 227.7728 100.4281 -0.2546 239.7844 240.0390 228.0540 102.0328 -0.2547 239.7603 240.0150 228.2727 103.6264 -0.2557 239.7457 240.0015 228.4774 105.2311 -0.2589 239.7357 239.9945 228.6912 106.8564 -0.2622 239.7273 239.9895 228.9137 108.4663 -0.2725 239.7434 240.0159 229.0460 110.0710 -0.2805 239.7454 240.0259 229.1985 111.6748 -0.2859 239.7467 240.0326 229.3238 113.2795 -0.2891 239.7382 240.0272 229.4271 114.8638 -0.2970 239.7018 239.9988 229.4949 116.4731 -0.2997 239.7077 240.0074 229.5903 118.0723 -0.3053 239.7030 240.0083 229.6517 119.6821 -0.3087 239.7078 240.0164 229.7749 121.2869 -0.3074 239.6979 240.0052 229.8640 122.8910 -0.3100 239.7197 240.0297 230.0467 124.5005 -0.3141 239.7302 240.0443 230.2500 126.1053 -0.3205 239.7412 240.0617 230.4030 127.7151 -0.3232 239.7059 240.0291 230.5772 129.3189 -0.3228 239.7023 240.0251 230.7686 130.9134 -0.3239 239.7171 240.0410 230.9884 132.5181 -0.3258 239.7319 240.0577 231.2325 134.1378 -0.3293 239.7358 240.0651 231.5723 135.7471 -0.3345 239.7641 240.0986 231.8543 137.3519 -0.3384 239.7531 240.0914 232.1637 138.9618 -0.3378 239.7546 240.0924 232.4861 140.5658 -0.3418 239.7441 240.0859 232.7914 142.1805 -0.3454 239.7500 240.0954 233.1397 143.7801 -0.3439 239.7999 240.1438 233.4180 145.3951 -0.3440 239.8461 240.1901 233.7149 147.0043 -0.3440 239.8760 240.2201 233.9631 148.6088 -0.3447 239.9063 240.2510 234.1873 150.2084 -0.3544 239.9312 240.2857 234.3743 151.8029 -0.3635 239.9645 240.3279 234.5689 153.4066 -0.3644 239.9974 240.3619 234.7333 155.0165 -0.3681 240.0239 240.3920 234.8795 156.6213 -0.3709 240.0704 240.4413 234.9808 158.2463 -0.3687 240.1199 240.4885 235.1155 159.8503 -0.3701 240.1525 240.5226 235.1996 161.4550 -0.3727 240.2286 240.6014 235.3404 163.0649 -0.3744 240.2758 240.6503 235.4742 164.6691 -0.3756 240.2897 240.6654 235.5945 166.2785 -0.3785 240.2885 240.6670 235.7410 167.8833 -0.3717 240.3226 240.6943 235.9360 169.5085 -0.3758 240.3853 240.7610 236.1447 171.1286 -0.3773 240.4109 240.7882 236.3718 172.7378 -0.3730 240.4466 240.8196 236.5785 174.3423 -0.3710 240.5073 240.8783 236.8111 175.9419 -0.3722 240.5503 240.9224 237.1032 177.5364 -0.3707 240.5864 240.9571 237.3889 179.1401 -0.3690 240.6776 241.0467 237.6689 180.7603 -0.3691 240.7404 241.1096 237.9156 182.3701 -0.3760 240.8429 241.2189 238.1902 183.9544 -0.3769 240.9152 241.2921 238.4599 185.5638 -0.3827 240.9709 241.3536 238.7553 187.1680 -0.3785 241.0315 241.4100 239.0257 188.7728 -0.3766 241.0757 241.4523 239.2631 190.3826 -0.3801 241.1021 241.4822 239.5281 191.9873 -0.3783 241.1471 241.5254 239.7721 193.6116 -0.3727 241.1923 241.5650 239.9119 195.2010 -0.3703 241.3138 241.6841 240.0743 196.8109 -0.3692 241.3638 241.7330 240.2421 198.4150 -0.3714 241.4317 241.8031 240.3895 200.0194 -0.3696 241.5316 241.9012 240.5512 201.6293 -0.3689 241.6109 241.9799 240.6972 203.2340 -0.3683 241.7265 242.0948 240.8248 204.8490 -0.3651 241.8176 242.1827 240.9633 206.4686 -0.3647 241.9305 242.2953 241.0775 208.0575 -0.3626 242.0289 242.3915 241.2563 209.6623 -0.3647 242.1315 242.4963 241.4390 211.2619 -0.3651 242.1688 242.5339 241.6478 212.8711 -0.3648 242.2257 242.5905 241.8587 214.4601 -0.3625 242.3400 242.7025 242.0794 216.0598 -0.3591 242.4392 242.7983 242.3325 217.6690 -0.3600 242.5034 242.8634 242.5691 219.2734 -0.3612 242.5773 242.9386 242.7940 220.8986 -0.3658 242.6850 243.0508 243.0725 222.5031 -0.3629 242.7705 243.1334 243.3421 224.1123 -0.3569 242.8456 243.2025 243.6115 225.7016 -0.3535 242.9671 243.3205 243.8567 227.3064 -0.3492 243.0445 243.3937 244.1246 228.9160 -0.3498 243.1127 243.4625 244.3816 230.5200 -0.3500 243.2194 243.5695 244.6271 232.1299 -0.3491 243.3355 243.6845 244.9035 233.7500 -0.3480 243.4522 243.8002 245.1426 235.3598 -0.3495 243.5506 243.9002 245.3522 236.9636 -0.3464 243.6301 243.9765 245.5424 238.5684 -0.3455 243.7352 244.0807 245.7248 240.1731 -0.3437 243.8887 244.2324 245.9291 241.7779 -0.3453 243.9928 244.3381 246.0986 243.3765 -0.3501 244.0713 244.4214 246.2487 244.9966 -0.3453 244.1819 244.5272 246.3911 246.6014 -0.3490 244.3045 244.6535 246.5795 248.2113 -0.3442 244.4301 244.7743 246.7177 249.7954 -0.3372 244.5652 244.9024 246.8470 251.3993 -0.3326 244.6820 245.0146 247.0206 253.0091 -0.3314 244.8070 245.1383 247.1862 254.6139 -0.3301 244.9191 245.2492 247.3822 256.2238 -0.3268 245.0446 245.3714 247.5450 257.8433 -0.3284 245.1788 245.5072 247.7527 259.4425 -0.3206 245.2782 245.5988 247.9774 261.0575 -0.3170 245.3722 245.6892 248.2118 262.6674 -0.3158 245.5075 245.8233 248.4791 264.2768 -0.3089 245.6321 245.9410 248.7500 265.8861 -0.3070 245.7828 246.0898 248.9955 267.4909 -0.3050 245.9213 246.2262 249.2918 269.1008 -0.3033 246.0379 246.3412 249.5553 270.7203 -0.2981 246.1720 246.4700 249.7945 272.3195 -0.2970 246.2862 246.5832 250.0883 273.9243 -0.2992 246.4137 246.7129 250.3389 275.5236 -0.2972 246.5507 246.8479 250.5575 277.1276 -0.2973 246.6810 246.9782 250.7983 278.7324 -0.2969 246.8036 247.1005 251.0462 280.3371 -0.2933 246.9441 247.2375 251.2747 281.9563 -0.2986 247.1221 247.4207 251.4422 283.5508 -0.2995 247.2567 247.5562 251.6090 285.1555 -0.2983 247.4038 247.7021 251.8048 286.7648 -0.2970 247.5459 247.8429 251.9682 288.3691 -0.2917 247.6986 247.9904 252.1394 289.9841 -0.2936 247.8328 248.1264 252.2888 291.5889 -0.2916 247.9710 248.2626 252.4155 293.1984 -0.2852 248.0960 248.3812 252.5819 294.8025 -0.2848 248.2318 248.5166 252.7120 296.4124 -0.2779 248.3817 248.6595 252.8659 298.0223 -0.2728 248.5366 248.8094 253.0878 299.6269 -0.2690 248.6816 248.9505 253.2617 301.2359 -0.2677 248.7957 249.0634 253.4744 302.8406 -0.2636 248.9775 249.2411 253.7164 304.4454 -0.2623 249.1155 249.3779 253.9497 306.0288 -0.2646 249.2805 249.5451 254.1984 307.6334 -0.2638 249.4414 249.7052 254.4580 309.2535 -0.2669 249.6166 249.8834 254.7441 310.8583 -0.2661 249.7712 250.0372 255.0226 312.4471 -0.2656 249.8727 250.1383 255.2821 314.0565 -0.2605 250.0248 250.2853 255.5501 315.6613 -0.2612 250.1724 250.4336 255.7792 317.2711 -0.2637 250.3216 250.5853 256.0182 318.8750 -0.2596 250.4724 250.7320 256.2770 320.4848 -0.2553 250.6584 250.9138 256.4967 322.1049 -0.2508 250.8057 251.0565 256.7175 323.6943 -0.2491 251.0003 251.2494 256.9535 325.3039 -0.2509 251.1532 251.4041 257.1761 326.9079 -0.2464 251.3143 251.5607 257.3467 328.5178 -0.2487 251.4856 251.7343 257.5000 330.1225 -0.2443 251.6245 251.8688 257.6437 331.7314 -0.2448 251.8128 252.0577 257.8270 333.3361 -0.2507 251.9957 252.2464 257.9826 334.9563 -0.2475 252.1741 252.4217 258.1703 336.5661 -0.2406 252.3547 252.5953 258.3187 338.1648 -0.2337 252.5130 252.7467 258.4502 339.7695 -0.2304 252.6795 252.9098 258.6068 341.3743 -0.2281 252.8387 253.0668 258.7602 342.9631 -0.2319 252.9866 253.2185 258.9373 344.5725 -0.2325 253.1436 253.3761 259.1368 346.1773 -0.2309 253.3124 253.5433 259.3955 347.7923 -0.2284 253.5003 253.7287 259.6036 349.4016 -0.2303 253.6812 253.9116 259.9059 351.0059 -0.2259 253.8547 254.0807 260.1955 352.6209 -0.2226 254.0329 254.2556 260.4650 354.2256 -0.2237 254.1970 254.4207 260.7187 355.8346 -0.2228 254.3591 254.5818 260.9901 357.4444 -0.2218 254.5369 254.7587 261.3028 359.0696 -0.2243 254.7242 254.9485 261.5747 360.6744 -0.2178 254.9205 255.1383 261.8266 362.2843 -0.2150 255.1019 255.3169 262.0773 363.8880 -0.2156 255.3015 255.5171 262.2729 365.4928 -0.2133 255.4967 255.7100 262.4575 367.1078 -0.2077 255.6985 255.9062 262.5995 368.7074 -0.2080 255.8452 256.0532 262.7432 370.2961 -0.2139 256.0132 256.2270 262.8940 371.9159 -0.2146 256.1690 256.3836 263.0640 373.5155 -0.2166 256.3491 256.5657 263.2309 375.1253 -0.2152 256.5641 256.7793 263.3993 376.7244 -0.2173 256.7490 256.9663 263.5641 378.3288 -0.2191 256.9114 257.1305 263.7041 379.9386 -0.2179 257.1026 257.3205 263.8664 381.5430 -0.2122 257.2738 257.4860 264.0830 383.1676 -0.2105 257.4790 257.6895 264.2836 384.7724 -0.2103 257.6652 257.8754 264.4296 386.3823 -0.2098 257.8644 258.0741 264.6701 387.9866 -0.2121 258.0594 258.2715 264.9517 389.5908 -0.2140 258.2373 258.4513 265.2303 391.1853 -0.2130 258.4084 258.6214 265.5066 392.7900 -0.2098 258.5921 258.8019 265.7744 394.3996 -0.2119 258.7871 258.9990 266.0600 396.0190 -0.2138 258.9361 259.1499 266.3338 397.6289 -0.2100 259.1207 259.3307 266.5967 399.2336 -0.2120 259.3168 259.5288 266.8406 400.8381 -0.2116 259.5291 259.7407 267.0717 402.4268 -0.2064 259.7141 259.9205 267.2910 404.0315 -0.2095 259.8921 260.1017 267.5087 405.6311 -0.2154 260.0967 260.3121 267.7274 407.2409 -0.2150 260.2738 260.4888 267.9511 408.8550 -0.2162 260.4830 260.6992 268.1437 410.4649 -0.2191 260.6646 260.8837 268.3025 412.0696 -0.2182 260.8803 261.0985 268.4360 413.6744 -0.2138 261.0698 261.2836 268.5859 415.2839 -0.2108 261.2613 261.4721 268.6854 416.8880 -0.2083 261.4754 261.6837 268.8699 418.4979 -0.2097 261.6750 261.8848 269.0168 420.1180 -0.2092 261.8854 262.0946 269.1707 421.7279 -0.2097 262.0564 262.2662 269.3680 423.3318 -0.2152 262.2301 262.4452 269.5941 424.9364 -0.2209 262.4318 262.6528 269.8381 426.5463 -0.2259 262.6278 262.8537 270.0605 428.1506 -0.2228 262.8502 263.0730 270.2578 429.7650 -0.2234 263.0695 263.2929 270.5064 431.3851 -0.2166 263.3018 263.5184 270.7936 432.9899 -0.2170 263.5017 263.7187 271.0150 434.5736 -0.2145 263.6848 263.8993 271.2983 436.1779 -0.2171 263.8733 264.0904 271.6012 437.7878 -0.2170 264.0600 264.2770 271.8652 439.3918 -0.2237 264.2568 264.4804 272.1242 441.0014 -0.2259 264.4464 264.6723 272.3567 442.6010 -0.2294 264.6347 264.8641 272.5713 444.2211 -0.2296 264.8209 265.0506 272.8164 445.8301 -0.2324 265.0264 265.2587 272.9762 447.4348 -0.2322 265.2618 265.4940 273.1864 449.0498 -0.2340 265.4998 265.7338 273.3994 450.6545 -0.2350 265.6776 265.9126 273.5710 452.2489 -0.2385 265.9050 266.1435 273.7404 453.8528 -0.2403 266.1036 266.3439 273.8884 455.4626 -0.2424 266.3487 266.5911 274.0103 457.0879 -0.2458 266.5781 266.8239 274.1985 458.6920 -0.2471 266.7882 267.0353 274.3627 460.3015 -0.2467 266.9966 267.2432 274.4951 461.9114 -0.2487 267.2069 267.4555 274.6623 463.5213 -0.2487 267.4220 267.6707 274.8520 465.1260 -0.2460 267.6159 267.8619 275.0386 466.7308 -0.2466 267.7948 268.0413 275.2680 468.3509 -0.2488 267.9801 268.2289 275.5469 469.9343 -0.2486 268.1954 268.4440 275.8222 471.5440 -0.2502 268.4098 268.6600 276.0761 473.1436 -0.2541 268.5935 268.8476 276.3163 474.7483 -0.2522 268.8123 269.0644 276.5420 476.3573 -0.2485 269.0157 269.2643 276.8653 477.9620 -0.2512 269.2387 269.4899 277.1708 479.5718 -0.2548 269.4234 269.6781 277.4613 481.1910 -0.2569 269.6391 269.8961 277.7127 482.8009 -0.2622 269.8664 270.1285 277.9784 484.4056 -0.2626 270.0924 270.3550 278.2376 486.0100 -0.2648 270.3140 270.5788 278.4553 487.6193 -0.2647 270.5142 270.7789 278.6403 489.2240 -0.2624 270.7146 270.9770 278.8119 490.8339 -0.2672 270.9083 271.1756 278.9522 492.4540 -0.2692 271.1447 271.4139 279.0974 494.0639 -0.2773 271.3442 271.6215 279.2324 495.6728 -0.2823 271.5374 271.8197 279.3534 497.2775 -0.2819 271.7675 272.0494 279.4450 498.8771 -0.2872 272.0019 272.2890 279.5606 500.4816 -0.2892 272.2161 272.5053 279.7349 502.0908 -0.2939 272.4422 272.7362 279.9093 503.7058 -0.2967 272.6682 272.9648 280.1325 505.3105 -0.2968 272.8944 273.1912 280.3800 506.9204 -0.3002 273.1132 273.4135 280.6285 508.5243 -0.2993 273.3156 273.6149 280.8614 510.1340 -0.2990 273.5139 273.8129 281.1140 511.7388 -0.3035 273.6955 273.9990 281.3732 513.3425 -0.3074 273.9179 274.2253 281.6614 514.9678 -0.3105 274.1453 274.4558 281.9859 516.5725 -0.3136 274.3397 274.6533 282.3096 518.1820 -0.3122 274.5459 274.8580 282.5670 519.7861 -0.3178 274.7996 275.1174 282.8454 521.3960 -0.3241 275.0105 275.3346 283.1160 523.0008 -0.3252 275.2379 275.5631 283.3565 524.6050 -0.3285 275.4518 275.7803 283.5582 526.2349 -0.3344 275.6562 275.9906 283.7486 527.8396 -0.3396 275.8928 276.2324 283.9142 529.4495 -0.3420 276.1099 276.4519 284.0278 531.0485 -0.3433 276.3234 276.6667 284.1792 532.6324 -0.3463 276.5740 276.9203 284.3043 534.2371 -0.3455 276.7952 277.1406 284.4198 535.8470 -0.3503 277.0088 277.3591 284.5434 537.4460 -0.3501 277.2478 277.5979 284.6543 539.0504 -0.3514 277.4687 277.8202 284.8418 540.6705 -0.3559 277.6961 278.0520 285.0184 542.2753 -0.3572 277.8636 278.2208 285.1961 543.8791 -0.3627 278.0697 278.4324 285.4130 545.4889 -0.3685 278.2863 278.6548 285.6844 547.0936 -0.3691 278.4973 278.8665 285.9341 548.7035 -0.3710 278.7245 279.0955 286.2120 550.3083 -0.3728 278.9300 279.3027 286.4915 551.9328 -0.3750 279.1696 279.5446 286.7290 553.5373 -0.3790 279.3480 279.7270 287.0071 555.1420 -0.3846 279.6042 279.9888 287.3106 556.7570 -0.3801 279.8387 280.2188 287.5921 558.3610 -0.3804 280.0814 280.4618 287.8674 559.9706 -0.3852 280.3429 280.7281 288.1095 561.5600 -0.3959 280.5714 280.9673 288.3514 563.1646 -0.4006 280.7749 281.1755 288.6017 564.7788 -0.4027 280.9586 281.3613 288.8221 566.3835 -0.4071 281.1623 281.5694 289.0147 567.9883 -0.4089 281.3894 281.7983 289.1753 569.5879 -0.4101 281.6120 282.0221 289.3349 571.1919 -0.4138 281.8176 282.2314 289.5294 572.8015 -0.4188 282.0614 282.4802 289.6598 574.4063 -0.4219 282.2835 282.7055 289.7711 576.0311 -0.4217 282.5072 282.9289 289.9119 577.6353 -0.4227 282.7343 283.1570 290.0721 579.2400 -0.4275 282.9846 283.4121 290.2454 580.8499 -0.4304 283.2265 283.6569 290.4348 582.4544 -0.4334 283.4553 283.8887 290.6158 584.0686 -0.4341 283.6505 284.0846 290.7742 585.6580 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