DTA measure 1fázis_1 Date: 2026318:96 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.18 s Mass = 934.200 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2195 -4.0014 182.8625 186.8639 246.4439 1.9758 -3.9887 183.1682 187.1569 246.3739 2.8035 -3.9791 183.4480 187.4271 246.2714 3.6000 -3.9672 183.7271 187.6943 246.2090 4.3973 -3.9541 183.9989 187.9530 246.1787 5.2253 -3.9437 184.2746 188.2183 246.1206 5.9808 -3.9405 184.5301 188.4706 246.0626 6.8188 -3.9267 184.7914 188.7182 246.0197 7.6058 -3.9190 185.0036 188.9227 245.9567 8.4333 -3.9090 185.2625 189.1715 245.8941 9.1993 -3.8949 185.5338 189.4287 245.8315 10.0375 -3.8795 185.7746 189.6541 245.7935 10.8245 -3.8687 186.0092 189.8779 245.7379 11.6208 -3.8571 186.2269 190.0840 245.6627 12.4488 -3.8490 186.4924 190.3414 245.5919 13.2153 -3.8380 186.7492 190.5873 245.5163 14.0738 -3.8275 187.0204 190.8479 245.4649 14.8293 -3.8166 187.2473 191.0639 245.4491 15.6675 -3.8022 187.5183 191.3205 245.3989 16.4543 -3.7896 187.7897 191.5792 245.3746 17.2610 -3.7762 188.0635 191.8397 245.3771 18.0788 -3.7671 188.3123 192.0794 245.3568 18.8553 -3.7569 188.5516 192.3085 245.3161 19.7030 -3.7488 188.8165 192.5654 245.2729 20.4695 -3.7339 189.0424 192.7763 245.2796 21.2973 -3.7205 189.2813 193.0018 245.3120 22.0835 -3.7078 189.5238 193.2316 245.3348 22.8705 -3.6994 189.7611 193.4605 245.3563 23.6985 -3.6914 190.0113 193.7027 245.3825 24.4640 -3.6843 190.2511 193.9354 245.4188 25.3125 -3.6656 190.5234 194.1890 245.4406 26.0583 -3.6489 190.7307 194.3796 245.4688 26.9060 -3.6347 190.9735 194.6081 245.4879 27.6623 -3.6212 191.2177 194.8389 245.5356 28.5003 -3.6060 191.4483 195.0543 245.5676 29.2865 -3.5962 191.6657 195.2619 245.6398 30.0838 -3.5860 191.9018 195.4878 245.7199 30.9113 -3.5766 192.1397 195.7163 245.8087 31.6773 -3.5629 192.3743 195.9372 245.9033 32.5360 -3.5514 192.6399 196.1913 246.0124 33.2918 -3.5414 192.8825 196.4239 246.1191 34.1295 -3.5230 193.1081 196.6311 246.2347 34.9165 -3.5061 193.3501 196.8563 246.2997 35.7133 -3.4930 193.5825 197.0755 246.3325 36.5408 -3.4813 193.7935 197.2748 246.4104 37.3073 -3.4662 194.0286 197.4948 246.5097 38.1658 -3.4515 194.2991 197.7507 246.6646 38.9213 -3.4393 194.5281 197.9675 246.7748 39.7595 -3.4279 194.7695 198.1974 246.8965 40.5465 -3.4190 194.9915 198.4105 247.0167 41.3430 -3.4054 195.2020 198.6074 247.1695 42.1708 -3.3920 195.4442 198.8362 247.3258 42.9373 -3.3802 195.6685 199.0487 247.4666 43.7950 -3.3688 195.9132 199.2820 247.6321 44.5513 -3.3588 196.1165 199.4753 247.8030 45.3895 -3.3529 196.3622 199.7151 247.9659 46.1860 -3.3412 196.5682 199.9094 248.1462 46.9830 -3.3293 196.7627 200.0921 248.2699 47.8008 -3.3170 196.9859 200.3029 248.4284 48.5765 -3.3084 197.2093 200.5177 248.5563 49.4250 -3.3025 197.4248 200.7273 248.7262 50.1913 -3.2921 197.6441 200.9362 248.8758 51.0185 -3.2842 197.8958 201.1800 249.0766 51.8158 -3.2699 198.1533 201.4232 249.2790 52.6130 -3.2596 198.3598 201.6194 249.4584 53.4298 -3.2481 198.5406 201.7887 249.6534 54.1963 -3.2378 198.7608 201.9986 249.8219 55.0448 -3.2288 199.0147 202.2435 250.0004 55.8105 -3.2186 199.2042 202.4228 250.2120 56.6280 -3.2123 199.4405 202.6528 250.3963 57.4253 -3.2059 199.6656 202.8714 250.5970 58.2220 -3.1967 199.8555 203.0522 250.8014 59.0495 -3.1864 200.1019 203.2883 251.0197 59.8160 -3.1792 200.3084 203.4877 251.2151 60.6643 -3.1722 200.5501 203.7223 251.4282 61.4300 -3.1645 200.7520 203.9165 251.6212 62.2580 -3.1605 200.9412 204.1017 251.8514 63.0448 -3.1520 201.1391 204.2910 252.0702 63.8515 -3.1405 201.3582 204.4986 252.2705 64.6385 -3.1316 201.5299 204.6615 252.4526 65.4355 -3.1226 201.7739 204.8965 252.6781 66.2628 -3.1176 202.0122 205.1298 252.8805 67.0293 -3.1148 202.2143 205.3291 253.0692 67.8880 -3.1040 202.4793 205.5833 253.2573 68.6433 -3.0979 202.6784 205.7763 253.4004 69.4815 -3.0940 202.9031 205.9971 253.6106 70.2785 -3.0876 203.1182 206.2058 253.7989 71.0750 -3.0827 203.3099 206.3927 253.9935 71.8928 -3.0797 203.5074 206.5871 254.1560 72.6690 -3.0716 203.7095 206.7811 254.3012 73.5170 -3.0658 203.9211 206.9869 254.4935 74.2835 -3.0584 204.1127 207.1711 254.6523 75.1113 -3.0525 204.3175 207.3699 254.8469 75.9078 -3.0471 204.5523 207.5995 255.0270 76.7050 -3.0404 204.7503 207.7907 255.2608 77.5225 -3.0341 204.9385 207.9727 255.4342 78.2985 -3.0268 205.1636 208.1904 255.5948 79.1470 -3.0176 205.4294 208.4470 255.7668 79.9130 -3.0114 205.6347 208.6461 255.9114 80.7405 -3.0047 205.8718 208.8765 256.0639 81.5173 -3.0006 206.0501 209.0507 256.2199 82.3348 -2.9951 206.2926 209.2877 256.3894 83.1313 -2.9921 206.4687 209.4608 256.5515 83.9285 -2.9834 206.6734 209.6568 256.7027 84.7565 -2.9778 206.8620 209.8398 256.8492 85.5220 -2.9743 207.0745 210.0488 257.0130 86.3705 -2.9703 207.2636 210.2339 257.2085 87.1370 -2.9664 207.4384 210.4048 257.3467 87.9540 -2.9588 207.6616 210.6204 257.5087 88.7510 -2.9466 207.8701 210.8167 257.6461 89.5483 -2.9423 208.0713 211.0136 257.7924 90.3345 -2.9361 208.2724 211.2085 257.9352 91.1315 -2.9306 208.4814 211.4119 258.0669 91.9595 -2.9274 208.6983 211.6257 258.2292 92.7253 -2.9203 208.8976 211.8180 258.3804 93.5735 -2.9178 209.1438 212.0616 258.4749 94.3503 -2.9171 209.3563 212.2734 258.6209 95.1673 -2.9116 209.5387 212.4503 258.7453 95.9643 -2.9051 209.7154 212.6205 258.8645 96.7615 -2.8943 209.9063 212.8006 258.9918 97.5583 -2.8903 210.1200 213.0103 259.1198 98.3550 -2.8869 210.2882 213.1751 259.2448 99.1728 -2.8825 210.5193 213.4018 259.3861 99.9490 -2.8787 210.7184 213.5970 259.4995 100.7970 -2.8726 210.9352 213.8077 259.6422 101.5635 -2.8642 211.1085 213.9727 259.7944 102.3910 -2.8580 211.3492 214.2072 259.9372 103.1878 -2.8507 211.5273 214.3781 260.0361 103.9850 -2.8463 211.7198 214.5661 260.1487 104.8023 -2.8439 211.9597 214.8036 260.3026 105.5785 -2.8377 212.1710 215.0087 260.4196 106.4270 -2.8282 212.3702 215.1984 260.5660 107.1725 -2.8265 212.5735 215.4000 260.6928 108.0205 -2.8245 212.7871 215.6116 260.8098 108.7973 -2.8209 212.9779 215.7989 260.8956 109.6145 -2.8140 213.1602 215.9742 261.0106 110.4113 -2.8064 213.3511 216.1575 261.1330 111.2085 -2.8015 213.5815 216.3831 261.2481 112.0355 -2.7955 213.7977 216.5931 261.3659 112.8020 -2.7877 214.0075 216.7952 261.4551 113.6608 -2.7839 214.2442 217.0281 261.5964 114.4268 -2.7774 214.4210 217.1984 261.7229 115.2543 -2.7792 214.5871 217.3663 261.8275 116.0515 -2.7715 214.7176 217.4892 261.9360 116.8380 -2.7614 214.9137 217.6751 262.0728 117.6758 -2.7589 215.1314 217.8903 262.1921 118.4320 -2.7552 215.3198 218.0750 262.3036 119.2800 -2.7489 215.4987 218.2476 262.4152 120.0460 -2.7480 215.6943 218.4423 262.5214 120.8740 -2.7507 215.8697 218.6204 262.6460 121.6608 -2.7470 216.0371 218.7841 262.7671 122.4573 -2.7425 216.2501 218.9925 262.8664 123.2853 -2.7357 216.4375 219.1732 262.9614 124.0410 -2.7296 216.6312 219.3608 263.1042 124.8685 -2.7279 216.8309 219.5588 263.2312 125.6350 -2.7243 217.0106 219.7349 263.3369 126.4828 -2.7244 217.2246 219.9491 263.4367 127.2593 -2.7182 217.3853 220.1035 263.5219 128.0873 -2.7118 217.5819 220.2938 263.6404 128.8838 -2.7092 217.7883 220.4974 263.7449 129.6705 -2.7032 217.9902 220.6933 263.8686 130.5088 -2.6956 218.2006 220.8963 264.0153 131.2643 -2.6870 218.3837 221.0707 264.1492 132.1228 -2.6787 218.5759 221.2547 264.2832 132.8893 -2.6720 218.7361 221.4081 264.3742 133.7168 -2.6668 218.9201 221.5869 264.4814 134.5135 -2.6596 219.1273 221.7869 264.5919 135.3005 -2.6532 219.3014 221.9546 264.7376 136.1383 -2.6516 219.5152 222.1668 264.8827 136.8940 -2.6479 219.6790 222.3269 264.9869 137.7528 -2.6470 219.8523 222.4993 265.1170 138.5193 -2.6441 220.0179 222.6621 265.1826 139.3463 -2.6389 220.1202 222.7592 265.3409 140.1435 -2.6337 220.3311 222.9648 265.4525 140.9305 -2.6276 220.5503 223.1780 265.5359 141.7683 -2.6212 220.7549 223.3761 265.6253 142.5240 -2.6162 220.9485 223.5647 265.7533 143.3828 -2.6147 221.1530 223.7677 265.9076 144.1490 -2.6100 221.3266 223.9366 266.0538 144.9763 -2.6026 221.5274 224.1300 266.1787 145.7735 -2.6034 221.7036 224.3069 266.2918 146.5603 -2.6021 221.8915 224.4936 266.3814 147.3978 -2.5937 222.1076 224.7014 266.5198 148.1540 -2.5943 222.2805 224.8748 266.6203 149.0125 -2.5884 222.4713 225.0597 266.7648 149.7783 -2.5799 222.6553 225.2352 266.8731 150.5960 -2.5731 222.8154 225.3886 267.0158 151.3933 -2.5670 222.9821 225.5490 267.1663 152.1898 -2.5649 223.1915 225.7564 267.2794 153.0073 -2.5671 223.4108 225.9779 267.3916 153.7738 -2.5627 223.5976 226.1603 267.5244 154.6318 -2.5589 223.8038 226.3627 267.6460 155.3980 -2.5543 223.9472 226.5015 267.7699 156.2158 -2.5445 224.1253 226.6698 267.8788 157.0123 -2.5359 224.2894 226.8253 268.0018 157.8093 -2.5324 224.4671 226.9996 268.1532 158.6373 -2.5298 224.6380 227.1679 268.2822 159.4030 -2.5289 224.8285 227.3574 268.4221 160.2615 -2.5263 225.0492 227.5755 268.5506 161.0280 -2.5194 225.2521 227.7715 268.6707 161.8550 -2.5161 225.4226 227.9386 268.7986 162.6420 -2.5137 225.5899 228.1036 268.9479 163.4493 -2.5116 225.7846 228.2963 269.0971 164.2663 -2.5062 225.9690 228.4751 269.2363 165.0328 -2.5003 226.1574 228.6577 269.3822 165.8913 -2.4903 226.3760 228.8663 269.5466 166.6570 -2.4836 226.5226 229.0062 269.6595 167.4850 -2.4811 226.6694 229.1505 269.7699 168.2720 -2.4833 226.8195 229.3028 269.8794 169.0785 -2.4827 227.0239 229.5066 270.0145 169.9065 -2.4762 227.2357 229.7119 270.1433 170.6730 -2.4731 227.4373 229.9105 270.2548 171.5205 -2.4715 227.6406 230.1122 270.4030 172.2665 -2.4666 227.7967 230.2633 270.5312 173.1150 -2.4605 228.0077 230.4682 270.6559 173.8805 -2.4525 228.1897 230.6422 270.7502 174.7085 -2.4480 228.3469 230.7950 270.8706 175.5058 -2.4444 228.5064 230.9508 271.0397 176.3020 -2.4420 228.6863 231.1283 271.1711 177.1300 -2.4367 228.8594 231.2961 271.3307 177.8965 -2.4329 229.0215 231.4544 271.4841 178.7543 -2.4335 229.2028 231.6364 271.6419 179.5208 -2.4327 229.3374 231.7701 271.7610 180.3383 -2.4320 229.5327 231.9648 271.8677 181.1450 -2.4256 229.7234 232.1491 271.9749 181.9320 -2.4190 229.8956 232.3147 272.0749 182.7498 -2.4126 230.0928 232.5053 272.2023 183.5255 -2.4063 230.2835 232.6897 272.3142 184.3740 -2.4041 230.4433 232.8474 272.4484 185.0993 -2.4006 230.5794 232.9800 272.5567 185.9573 -2.3945 230.7890 233.1835 272.6994 186.7238 -2.3919 230.9554 233.3473 272.8290 187.5415 -2.3856 231.1295 233.5151 272.9671 188.3380 -2.3820 231.3045 233.6865 273.0703 189.1350 -2.3790 231.4906 233.8697 273.1966 189.9528 -2.3766 231.6942 234.0709 273.3891 190.7288 -2.3721 231.8448 234.2170 273.5319 191.5770 -2.3711 232.0395 234.4106 273.6733 192.3435 -2.3705 232.2061 234.5766 273.7992 193.1705 -2.3714 232.3727 234.7441 273.9294 193.9370 -2.3721 232.5434 234.9156 274.0206 194.7650 -2.3659 232.7339 235.0997 274.1355 195.5513 -2.3654 232.8729 235.2384 274.2955 196.3585 -2.3679 233.0144 235.3823 274.4180 197.1763 -2.3637 233.1796 235.5433 274.5653 197.9420 -2.3628 233.3508 235.7136 274.7182 198.8005 -2.3604 233.5611 235.9215 274.8478 199.5670 -2.3555 233.7234 236.0788 274.9797 200.3945 -2.3512 233.8926 236.2439 275.1051 201.1810 -2.3451 234.0565 236.4016 275.2393 201.9885 -2.3439 234.2214 236.5652 275.3777 202.8058 -2.3416 234.3969 236.7386 275.4953 203.5718 -2.3375 234.5320 236.8696 275.6130 204.4305 -2.3338 234.6895 237.0233 275.7504 205.1970 -2.3266 234.8727 237.1993 275.8971 206.0240 -2.3217 235.0571 237.3788 276.0522 206.8110 -2.3193 235.2092 237.5285 276.1917 207.6183 -2.3194 235.3846 237.7040 276.3503 208.4353 -2.3182 235.5523 237.8705 276.4929 209.2018 -2.3167 235.7025 238.0192 276.6165 210.0605 -2.3175 235.8907 238.2082 276.7265 210.8260 -2.3141 236.0333 238.3474 276.8626 211.6540 -2.3082 236.1586 238.4667 277.0021 212.4205 -2.3058 236.3276 238.6333 277.1423 213.2478 -2.3023 236.5231 238.8254 277.2855 214.0448 -2.3015 236.6596 238.9611 277.3939 214.8420 -2.2991 236.8259 239.1251 277.5241 215.6588 -2.2979 237.0235 239.3213 277.6645 216.4253 -2.2931 237.2041 239.4972 277.8147 217.2738 -2.2860 237.4013 239.6873 277.9741 218.0088 -2.2839 237.5563 239.8402 278.0886 218.8673 -2.2835 237.7504 240.0339 278.2165 219.6338 -2.2771 237.9294 240.2065 278.3217 220.4610 -2.2719 238.1106 240.3825 278.4718 221.2580 -2.2718 238.2652 240.5370 278.6052 222.0553 -2.2711 238.4358 240.7069 278.7346 222.8720 -2.2689 238.6028 240.8717 278.8879 223.6385 -2.2701 238.7753 241.0454 278.9826 224.4970 -2.2706 238.9451 241.2157 279.1121 225.2628 -2.2704 239.1081 241.3785 279.1929 226.0805 -2.2697 239.2712 241.5409 279.3252 226.8573 -2.2716 239.3840 241.6556 279.4584 227.6740 -2.2662 239.5765 241.8427 279.5766 228.4713 -2.2642 239.7547 242.0189 279.7101 229.2683 -2.2624 239.8687 242.1311 279.8533 230.0955 -2.2627 240.0366 242.2993 279.9548 230.8620 -2.2627 240.2068 242.4695 280.0830 231.7105 -2.2609 240.3916 242.6525 280.2492 232.4863 -2.2542 240.5458 242.7999 280.3885 233.3040 -2.2498 240.7010 242.9508 280.5365 234.1013 -2.2525 240.8804 243.1329 280.6668 234.8975 -2.2513 241.0747 243.3260 280.7975 235.7255 -2.2475 241.2550 243.5025 280.9167 236.4918 -2.2431 241.4138 243.6569 281.0851 237.3395 -2.2457 241.5634 243.8091 281.2541 238.1163 -2.2433 241.7023 243.9457 281.3697 238.9340 -2.2408 241.8755 244.1163 281.5242 239.7405 -2.2380 242.0464 244.2844 281.7015 240.5275 -2.2375 242.2301 244.4676 281.8020 241.3658 -2.2412 242.3831 244.6243 281.9369 242.1213 -2.2413 242.5241 244.7654 282.0488 242.9798 -2.2420 242.6953 244.9374 282.1853 243.7463 -2.2461 242.8286 245.0747 282.3557 244.5840 -2.2420 242.9871 245.2290 282.4896 245.3705 -2.2364 243.1802 245.4166 282.6364 246.1678 -2.2336 243.3360 245.5696 282.7746 246.9955 -2.2320 243.5053 245.7373 282.9214 247.7510 -2.2262 243.6685 245.8948 283.0621 248.5995 -2.2198 243.8415 246.0614 283.2331 249.3760 -2.2211 244.0232 246.2443 283.3806 250.2033 -2.2225 244.1873 246.4098 283.5429 250.9493 -2.2215 244.3393 246.5608 283.6933 251.8075 -2.2202 244.5031 246.7234 283.8712 252.5633 -2.2211 244.6209 246.8420 283.9928 253.3913 -2.2164 244.8078 247.0242 284.1372 254.1880 -2.2122 244.9638 247.1760 284.2704 254.9745 -2.2120 245.1215 247.3335 284.4170 255.8128 -2.2076 245.2718 247.4794 284.5857 256.5688 -2.2097 245.3980 247.6077 284.7207 257.4370 -2.2031 245.5789 247.7820 284.8880 258.1933 -2.2030 245.7267 247.9298 285.0018 259.0310 -2.2019 245.8925 248.0944 285.1610 259.8175 -2.2007 246.0350 248.2357 285.2857 260.6045 -2.1978 246.2189 248.4167 285.4257 261.4425 -2.2012 246.4103 248.6115 285.5784 262.1980 -2.2000 246.5492 248.7492 285.7191 263.0568 -2.1989 246.6865 248.8854 285.9206 263.8233 -2.1978 246.8708 249.0686 286.0746 264.6503 -2.1963 247.0884 249.2847 286.2034 265.4475 -2.1989 247.2081 249.4069 286.3117 266.2345 -2.1988 247.3558 249.5547 286.4482 267.0718 -2.1931 247.4961 249.6893 286.5671 267.8280 -2.1924 247.6246 249.8170 286.6669 268.6868 -2.1922 247.8239 250.0161 286.8272 269.4525 -2.1932 247.9875 250.1807 286.9558 270.2905 -2.1927 248.1501 250.3429 287.0806 271.0775 -2.1901 248.3375 250.5276 287.1927 271.8738 -2.1927 248.5210 250.7137 287.3334 272.7018 -2.1900 248.6930 250.8830 287.4479 273.4678 -2.1865 248.8222 251.0087 287.5620 274.3260 -2.1849 248.9754 251.1603 287.7232 275.0823 -2.1848 249.1075 251.2924 287.8272 275.9205 -2.1814 249.2902 251.4716 287.9726 276.7070 -2.1765 249.4536 251.6301 288.1073 277.5038 -2.1773 249.6060 251.7832 288.2635 278.3318 -2.1767 249.7526 251.9294 288.4097 279.0875 -2.1786 249.8754 252.0540 288.5149 279.9355 -2.1780 250.1162 252.2942 288.6465 280.7123 -2.1767 250.3203 252.4970 288.7236 281.5295 -2.1722 250.4778 252.6500 288.8143 282.2853 -2.1716 250.6095 252.7810 288.9595 283.1235 -2.1720 250.7949 252.9669 289.1249 283.9100 -2.1742 250.9330 253.1072 289.2526 284.6965 -2.1741 251.0658 253.2399 289.3750 285.5348 -2.1779 251.2183 253.3962 289.4760 286.2905 -2.1780 251.3906 253.5685 289.5452 287.1385 -2.1765 251.5827 253.7592 289.6270 287.9153 -2.1796 251.7231 253.9027 289.7384 288.7325 -2.1772 251.8517 254.0289 289.8809 289.5293 -2.1786 252.0251 254.2037 290.0250 290.3265 -2.1779 252.1970 254.3748 290.1373 291.1230 -2.1725 252.3486 254.5211 290.2505 291.9200 -2.1685 252.5060 254.6745 290.3578 292.7378 -2.1666 252.6593 254.8259 290.5060 293.5138 -2.1631 252.8069 254.9700 290.5882 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