DTA measure 1dta_gorbe Date: 2024101:159 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.16 s Mass = 950.500 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2865 -2.0001 198.8186 200.8187 253.5615 2.1088 -1.9886 199.1298 201.1184 253.5028 2.9008 -1.9873 199.3150 201.3023 253.4930 3.6925 -1.9819 199.5341 201.5160 253.5724 4.5145 -1.9906 199.7088 201.6994 253.6099 5.3065 -1.9805 199.9652 201.9457 253.5785 6.1285 -1.9851 200.2014 202.1865 253.5630 6.9205 -1.9771 200.3826 202.3598 253.5691 7.7125 -1.9558 200.5900 202.5458 253.6261 8.5645 -1.9360 200.7873 202.7233 253.5876 9.3265 -1.9201 201.0658 202.9859 253.6332 10.1485 -1.9334 201.3130 203.2464 253.7201 10.9665 -1.9313 201.4879 203.4192 253.7488 11.7260 -1.9286 201.6872 203.6158 253.8436 12.5740 -1.9223 201.8624 203.7847 253.8226 13.3323 -1.9277 202.0625 203.9903 253.9020 14.1510 -1.9120 202.3952 204.3072 253.9311 14.9410 -1.9238 202.6376 204.5615 254.0928 15.7313 -1.9330 202.7870 204.7200 254.2394 16.5808 -1.9370 202.9247 204.8617 254.2868 17.3400 -1.9235 203.1380 205.0615 254.3888 18.1590 -1.9221 203.3421 205.2641 254.6310 18.9790 -1.9242 203.5377 205.4619 254.6882 19.7405 -1.9185 203.7431 205.6616 254.7314 20.5918 -1.9073 204.0134 205.9207 254.8919 21.3363 -1.8899 204.2876 206.1775 254.9018 22.1938 -1.9026 204.4904 206.3930 255.0591 22.9858 -1.8953 204.6714 206.5668 255.3515 23.7775 -1.8875 204.8297 206.7173 255.4977 24.5998 -1.8939 205.0504 206.9444 255.6087 25.3615 -1.8797 205.2344 207.1141 255.7537 26.2140 -1.8868 205.5183 207.4051 256.0100 26.9758 -1.8908 205.7080 207.5988 256.1071 27.7978 -1.8731 205.9288 207.8019 256.2866 28.6195 -1.8821 206.1632 208.0453 256.4342 29.3815 -1.8754 206.3178 208.1931 256.6100 30.2343 -1.8688 206.5257 208.3945 256.7843 30.9965 -1.8669 206.6270 208.4939 256.9626 31.8185 -1.8706 206.8140 208.6845 257.1919 32.6405 -1.8685 207.0376 208.9061 257.3282 33.4025 -1.8604 207.2809 209.1412 257.4847 34.2545 -1.8594 207.5073 209.3667 257.6971 35.0165 -1.8646 207.6812 209.5458 257.9408 35.8385 -1.8525 207.9146 209.7671 258.0540 36.6305 -1.8467 208.0832 209.9299 258.3421 37.4225 -1.8543 208.3485 210.2029 258.5421 38.2745 -1.8629 208.4925 210.3554 258.8035 39.0365 -1.8499 208.6681 210.5180 258.8589 39.8585 -1.8322 208.8446 210.6767 259.0230 40.6505 -1.8435 209.0405 210.8840 259.2694 41.4423 -1.8459 209.2076 211.0535 259.4789 42.2928 -1.8371 209.4153 211.2525 259.7148 43.0525 -1.8336 209.6353 211.4689 259.8238 43.8705 -1.8311 209.9138 211.7448 260.0019 44.6593 -1.8472 210.1440 211.9912 260.1396 45.4480 -1.8464 210.3879 212.2342 260.2856 46.2960 -1.8389 210.6464 212.4854 260.5003 47.0540 -1.8298 210.8914 212.7212 260.7612 47.8718 -1.8234 211.0604 212.8839 260.9187 48.6603 -1.8288 211.2636 213.0924 260.9583 49.4508 -1.8348 211.5047 213.3395 261.0152 50.2995 -1.8143 211.7867 213.6009 261.1726 51.0605 -1.8275 212.0002 213.8277 261.3124 51.8825 -1.8497 212.1415 213.9913 261.4976 52.6735 -1.8233 212.3445 214.1678 261.6231 53.4655 -1.8122 212.4934 214.3056 261.7211 54.2875 -1.8122 212.6300 214.4423 261.9373 55.0795 -1.8311 212.7140 214.5451 262.1290 55.9015 -1.8345 212.9205 214.7550 262.2815 56.6935 -1.8462 213.1246 214.9708 262.4889 57.4855 -1.8454 213.3928 215.2382 262.6471 58.3075 -1.8314 213.5678 215.3991 262.7341 59.0995 -1.8247 213.7555 215.5801 262.8283 59.9215 -1.8249 213.9371 215.7620 262.9171 60.7135 -1.8256 214.1195 215.9451 263.0654 61.5055 -1.8148 214.1658 215.9806 263.2437 62.3275 -1.8168 214.4266 216.2434 263.3521 63.1195 -1.8174 214.6424 216.4598 263.4701 63.9415 -1.8242 214.8110 216.6352 263.6432 64.7335 -1.8135 215.0274 216.8409 263.7804 65.5255 -1.8165 215.2998 217.1163 263.8667 66.3475 -1.8239 215.4177 217.2416 264.0080 67.1395 -1.8097 215.6297 217.4394 264.1400 67.9608 -1.8073 215.7410 217.5482 264.1903 68.7533 -1.8024 215.9291 217.7315 264.2963 69.5445 -1.8086 216.2006 218.0092 264.3581 70.3670 -1.8155 216.4134 218.2290 264.5728 71.1588 -1.8099 216.5441 218.3540 264.6097 71.9808 -1.8076 216.6634 218.4710 264.7384 72.7730 -1.8141 216.9338 218.7478 264.8510 73.5645 -1.8111 217.1745 218.9855 264.9418 74.4175 -1.8164 217.3804 219.1968 265.0401 75.1798 -1.8008 217.5522 219.3531 265.1883 75.9990 -1.8059 217.7508 219.5567 265.2335 76.7860 -1.8074 218.0087 219.8161 265.3757 77.5750 -1.8212 218.1312 219.9524 265.5656 78.3930 -1.8160 218.3046 220.1206 265.7097 79.1815 -1.8360 218.4320 220.2680 265.7507 79.9990 -1.8405 218.6169 220.4574 265.7768 80.7875 -1.8413 218.8053 220.6466 266.0612 81.5760 -1.8577 219.0451 220.9027 266.1892 82.4245 -1.8542 219.2290 221.0832 266.3209 83.1840 -1.8228 219.4055 221.2282 266.3745 84.0038 -1.8045 219.5353 221.3398 266.5295 84.7943 -1.7843 219.7132 221.4976 266.5957 85.5855 -1.7915 219.9822 221.7737 266.6559 86.4373 -1.8158 220.1869 222.0027 266.8310 87.1990 -1.8045 220.3903 222.1948 266.9424 88.0208 -1.8009 220.5696 222.3705 267.0712 88.8133 -1.8029 220.7314 222.5344 267.1809 89.6045 -1.8031 220.9367 222.7398 267.3078 90.4273 -1.7869 221.0918 222.8787 267.3467 91.2188 -1.7860 221.2622 223.0483 267.5094 92.0408 -1.7944 221.4547 223.2491 267.6832 92.8330 -1.7942 221.6232 223.4173 267.8958 93.6245 -1.8007 221.7967 223.5974 267.9129 94.4470 -1.7906 222.0258 223.8164 268.1427 95.2390 -1.7804 222.2908 224.0711 268.2426 96.0608 -1.7885 222.4044 224.1928 268.3863 96.8530 -1.7912 222.5246 224.3159 268.5088 97.6445 -1.8045 222.7718 224.5763 268.6850 98.4670 -1.8097 223.0169 224.8265 268.8134 99.2285 -1.8205 223.1390 224.9596 269.0582 100.0810 -1.8266 223.3562 225.1828 269.1166 100.8730 -1.8292 223.5453 225.3745 269.1969 101.6645 -1.8164 223.5965 225.4129 269.3577 102.4870 -1.7942 223.8213 225.6155 269.5411 103.2485 -1.7934 224.0781 225.8715 269.5723 104.1008 -1.8016 224.1409 225.9425 269.7391 104.8933 -1.7778 224.3200 226.0978 269.9937 105.6865 -1.7783 224.5212 226.2995 270.0128 106.5088 -1.7591 224.8128 226.5720 270.1593 107.2705 -1.7757 224.9367 226.7123 270.3103 108.1200 -1.7951 225.0585 226.8536 270.5390 108.8780 -1.8430 225.2291 227.0721 270.7067 109.6990 -1.8622 225.3955 227.2577 270.8814 110.5173 -1.8635 225.4886 227.3521 270.9283 111.2760 -1.8514 225.6216 227.4730 271.0199 112.1250 -1.8342 225.8204 227.6546 271.1865 112.8833 -1.8265 226.0098 227.8362 271.3485 113.7010 -1.8003 226.2383 228.0386 271.4935 114.5195 -1.7742 226.4837 228.2580 271.6471 115.2780 -1.7783 226.6228 228.4010 271.8517 116.1278 -1.7875 226.7963 228.5838 271.9347 116.9175 -1.7845 226.9745 228.7590 272.1063 117.7073 -1.8003 227.1911 228.9913 272.1553 118.5290 -1.8139 227.4062 229.2202 272.3061 119.2905 -1.8280 227.5204 229.3484 272.4544 120.1430 -1.8483 227.6895 229.5378 272.6607 120.9048 -1.8425 227.8737 229.7162 272.7738 121.8470 -1.8300 228.0458 229.8758 273.0097 122.6088 -1.8053 228.2320 230.0373 273.0203 123.4320 -1.7920 228.4611 230.2531 273.1917 124.2278 -1.7981 228.7450 230.5431 273.2864 125.0195 -1.7882 228.9421 230.7303 273.4125 125.8420 -1.7931 229.0189 230.8120 273.5347 126.6338 -1.8160 229.2232 231.0392 273.7385 127.4558 -1.8063 229.3859 231.1922 273.8515 128.2478 -1.8061 229.5146 231.3208 273.9322 129.0395 -1.8220 229.6786 231.5006 274.1393 129.8618 -1.8196 229.9384 231.7580 274.2142 130.6535 -1.8164 230.1643 231.9807 274.3270 131.4758 -1.8222 230.3478 232.1699 274.5061 132.2675 -1.8152 230.5591 232.3743 274.5684 133.0595 -1.8144 230.6481 232.4625 274.7045 133.8815 -1.8073 230.8223 232.6295 274.8896 134.6460 -1.8170 231.0143 232.8313 275.0584 135.5005 -1.8223 231.1856 233.0079 275.0982 136.2925 -1.8197 231.2424 233.0620 275.1754 137.0855 -1.8304 231.4742 233.3046 275.3734 137.9075 -1.8244 231.6968 233.5213 275.4729 138.6695 -1.8301 231.8840 233.7141 275.5867 139.5208 -1.8414 232.0595 233.9010 275.7872 140.3060 -1.8245 232.2511 234.0756 275.8978 141.0950 -1.8446 232.3453 234.1899 276.0536 141.9140 -1.8341 232.5573 234.3914 276.1173 142.6718 -1.8313 232.7269 234.5581 276.2403 143.5200 -1.8261 232.9174 234.7435 276.3617 144.3080 -1.8240 233.1041 234.9280 276.5330 145.0960 -1.8204 233.2626 235.0830 276.6272 145.9140 -1.8266 233.4630 235.2896 276.7826 146.6720 -1.8232 233.5015 235.3246 276.9453 147.5205 -1.8138 233.7495 235.5634 277.0523 148.3105 -1.8280 233.9143 235.7423 277.1865 149.1015 -1.8425 234.1040 235.9465 277.2945 149.9235 -1.8403 234.1923 236.0326 277.4904 150.6855 -1.8362 234.3473 236.1835 277.6466 151.5375 -1.8371 234.6231 236.4601 277.7453 152.2995 -1.8335 234.8267 236.6602 277.8902 153.1215 -1.8536 234.9826 236.8362 278.1163 153.9158 -1.8622 235.2083 237.0705 278.1756 154.7095 -1.8575 235.2846 237.1422 278.2840 155.5615 -1.8698 235.4879 237.3577 278.4729 156.3235 -1.8612 235.6276 237.4888 278.5571 157.1455 -1.8548 235.7846 237.6393 278.6492 157.9375 -1.8594 235.9669 237.8263 278.7129 158.7295 -1.8597 236.2143 238.0740 278.9047 159.5515 -1.8811 236.3314 238.2125 279.1166 160.3435 -1.8879 236.5123 238.4002 279.2869 161.1655 -1.8660 236.7783 238.6443 279.3106 161.9575 -1.8772 236.7958 238.6730 279.4878 162.7495 -1.8843 236.9371 238.8214 279.5506 163.5715 -1.8796 237.1922 239.0717 279.7652 164.3635 -1.8857 237.3493 239.2349 279.8648 165.1855 -1.8802 237.4138 239.2940 280.0381 165.9775 -1.8696 237.6377 239.5073 280.1256 166.7705 -1.8673 237.8221 239.6894 280.3240 167.5925 -1.8661 238.0085 239.8746 280.4232 168.3853 -1.8678 238.0918 239.9596 280.5682 169.2075 -1.8687 238.2969 240.1656 280.7950 169.9990 -1.8665 238.4605 240.3270 280.9974 170.7905 -1.8616 238.6935 240.5551 280.9803 171.6125 -1.8573 238.9001 240.7574 281.1097 172.4003 -1.8500 239.1037 240.9538 281.1386 173.2185 -1.8692 239.2896 241.1587 281.3135 174.0068 -1.8960 239.4439 241.3399 281.4385 174.7958 -1.8919 239.5530 241.4448 281.5777 175.6138 -1.8927 239.6790 241.5717 281.8281 176.4013 -1.8853 239.8174 241.7027 281.9845 177.2208 -1.8813 240.0067 241.8880 282.0630 178.0090 -1.8904 240.1839 242.0743 282.2279 178.7970 -1.8858 240.4104 242.2962 282.3716 179.6153 -1.8948 240.5593 242.4541 282.5421 180.4045 -1.8949 240.7120 242.6069 282.6514 181.2255 -1.9292 240.9078 242.8370 282.7388 182.0175 -1.9479 240.9842 242.9321 282.8230 182.8390 -1.9315 241.1669 243.0984 282.8900 183.6605 -1.9156 241.3629 243.2785 283.0954 184.4525 -1.9124 241.5638 243.4762 283.3081 185.2445 -1.8962 241.7813 243.6775 283.3791 186.0665 -1.9012 241.8681 243.7693 283.5782 186.8285 -1.8962 241.9816 243.8778 283.7242 187.6805 -1.8938 242.3313 244.2251 283.8223 188.4725 -1.8992 242.4075 244.3067 283.9476 189.2645 -1.8859 242.4539 244.3398 284.1157 190.0865 -1.8839 242.6726 244.5565 284.2724 190.8785 -1.8851 242.8699 244.7551 284.3742 191.7005 -1.8701 242.9419 244.8120 284.4846 192.4925 -1.8749 243.1566 245.0315 284.6621 193.2843 -1.8765 243.4022 245.2787 284.6898 194.1063 -1.8780 243.5516 245.4297 284.8494 194.8980 -1.8978 243.7110 245.6089 284.9779 195.7205 -1.8883 243.8821 245.7704 285.1187 196.5133 -1.8945 244.0399 245.9344 285.2510 197.3045 -1.9087 244.2809 246.1897 285.3558 198.1270 -1.9068 244.3913 246.2980 285.4546 198.9188 -1.8979 244.5218 246.4197 285.5559 199.7408 -1.8938 244.6977 246.5915 285.6874 200.5330 -1.9005 244.8309 246.7313 285.7726 201.3245 -1.9232 245.0584 246.9817 285.9123 202.1470 -1.9299 245.1540 247.0840 286.0850 202.9388 -1.9134 245.3369 247.2503 286.2154 203.7608 -1.9279 245.4961 247.4240 286.3637 204.5523 -1.9302 245.6152 247.5454 286.5181 205.3410 -1.9362 245.8130 247.7492 286.5889 206.1890 -1.9301 245.8980 247.8281 286.8045 206.9473 -1.9220 246.1317 248.0537 286.9184 207.7660 -1.9314 246.3580 248.2894 286.9280 208.5545 -1.9314 246.5741 248.5056 287.0569 209.3430 -1.9371 246.7057 248.6428 287.2089 210.1680 -1.9234 246.7944 248.7178 287.3243 210.9573 -1.9326 246.9633 248.8959 287.5125 211.7780 -1.9283 247.1060 249.0343 287.6441 212.5688 -1.9247 247.2812 249.2058 287.7482 213.3595 -1.9295 247.4407 249.3703 287.8693 214.1820 -1.9389 247.6082 249.5471 288.0304 214.9435 -1.9367 247.7254 249.6622 288.1606 215.7963 -1.9197 247.9615 249.8811 288.3719 216.5880 -1.9373 248.1404 250.0777 288.4262 217.3795 -1.9477 248.2843 250.2320 288.5258 218.2020 -1.9514 248.4014 250.3528 288.7377 218.9635 -1.9464 248.4933 250.4396 288.8349 219.8160 -1.9483 248.7655 250.7139 288.9134 220.6080 -1.9567 248.8878 250.8445 289.0898 221.3995 -1.9629 249.0547 251.0175 289.0904 222.2220 -1.9727 249.1972 251.1699 289.2643 222.9835 -1.9728 249.3161 251.2889 289.3900 223.8360 -1.9501 249.4822 251.4323 289.6917 224.5978 -1.9568 249.7586 251.7154 289.6695 225.4198 -1.9597 249.8752 251.8350 289.8054 226.2420 -1.9682 249.9861 251.9544 289.9276 227.0035 -1.9738 250.1347 252.1085 290.0384 227.8565 -1.9665 250.2932 252.2597 290.2421 228.6188 -1.9597 250.4130 252.3727 290.4021 229.4408 -1.9614 250.6100 252.5714 290.5034 230.2628 -1.9624 250.6866 252.6490 290.7046 231.0245 -1.9682 250.9063 252.8745 290.7326 231.8768 -1.9668 251.1303 253.0972 290.8921 232.6385 -1.9805 251.3122 253.2926 290.9314 233.4608 -1.9761 251.5025 253.4786 291.0808 234.2828 -1.9681 251.6810 253.6491 291.2742 235.0445 -1.9605 251.7536 253.7140 291.3947 235.8973 -1.9704 251.8848 253.8552 291.4922 236.6580 -1.9695 252.0315 254.0010 291.5867 237.4760 -1.9696 252.1641 254.1337 291.8243 238.2645 -1.9767 252.4351 254.4119 291.8527 239.0530 -1.9757 252.5442 254.5198 292.0135 239.9010 -1.9803 252.7154 254.6957 292.1441 240.6593 -1.9770 252.8439 254.8209 292.2918 241.4790 -1.9677 253.0039 254.9716 292.3465 242.2978 -1.9707 253.1633 255.1339 292.5564 243.0578 -1.9970 253.3473 255.3443 292.7088 243.9090 -1.9935 253.4706 255.4641 292.8898 244.6685 -1.9824 253.6485 255.6309 292.9701 245.4898 -1.9877 253.8038 255.7914 293.1313 246.3120 -1.9938 253.9908 255.9846 293.2884 247.0735 -1.9974 254.1269 256.1243 293.3811 247.9258 -1.9953 254.2695 256.2648 293.5150 248.6875 -2.0045 254.3903 256.3948 293.6678 249.5098 -1.9981 254.6601 256.6582 293.8370 250.3020 -1.9957 254.7554 256.7510 294.0020 251.0935 -1.9995 254.8960 256.8954 294.1578 251.9460 -2.0104 255.0586 257.0690 294.3005 252.7078 -2.0153 255.2331 257.2485 294.4050 253.5298 -2.0087 255.4134 257.4222 294.4362 254.3520 -2.0057 255.5924 257.5981 294.5593 255.1135 -2.0066 255.7038 257.7104 294.6805 255.9660 -2.0200 255.8609 257.8809 294.8636 256.7275 -2.0085 255.9629 257.9714 295.0173 257.5498 -2.0151 256.1750 258.1901 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