DTA measure 1Fazis1 Date: 20251014:1544 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.05 s Mass = 1333.900 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2195 0.2069 252.0024 251.7955 276.6552 2.0063 0.2106 252.1669 251.9563 276.5704 2.8130 0.2154 252.2829 252.0675 276.4357 3.5990 0.2229 252.4178 252.1949 276.2743 4.4268 0.2277 252.6135 252.3859 276.1362 5.1925 0.2301 252.7944 252.5643 275.9889 6.0505 0.2360 252.9578 252.7218 275.8161 6.8165 0.2380 253.1158 252.8778 275.6478 7.6335 0.2444 253.3044 253.0600 275.4498 8.4403 0.2490 253.4768 253.2277 275.2593 9.2268 0.2504 253.6257 253.3753 275.0919 10.0540 0.2548 253.7896 253.5348 274.9007 10.8198 0.2550 253.9194 253.6644 274.7096 11.6880 0.2639 254.1067 253.8427 274.4861 12.4438 0.2714 254.2652 253.9938 274.3560 13.2710 0.2732 254.4578 254.1846 274.2528 14.0678 0.2764 254.6430 254.3667 274.1670 14.8643 0.2829 254.8307 254.5478 274.1257 15.6915 0.2914 255.0287 254.7373 274.1274 16.4473 0.2966 255.1615 254.8649 274.1671 17.3155 0.2984 255.3090 255.0105 274.2560 18.0405 0.3001 255.4510 255.1508 274.3585 18.9193 0.3063 255.6470 255.3407 274.5146 19.6848 0.3091 255.7857 255.4766 274.6931 20.5123 0.3138 255.9318 255.6180 274.9486 21.3090 0.3176 256.0661 255.7486 275.2304 22.1053 0.3196 256.2328 255.9132 275.5485 22.9328 0.3219 256.3799 256.0581 275.9198 23.6885 0.3269 256.5311 256.2042 276.2987 24.5158 0.3328 256.6932 256.3604 276.7350 25.2818 0.3376 256.8487 256.5111 277.1398 26.1295 0.3387 257.0170 256.6783 277.5639 26.8953 0.3379 257.1712 256.8334 278.0175 27.7228 0.3392 257.3558 257.0167 278.5203 28.4885 0.3426 257.4768 257.1342 278.9643 29.3160 0.3467 257.6523 257.3056 279.4069 30.1128 0.3496 257.8180 257.4684 279.8550 30.9090 0.3500 257.9709 257.6209 280.2465 31.7263 0.3522 258.1289 257.7768 280.6503 32.4923 0.3544 258.2856 257.9312 280.9823 33.3500 0.3524 258.4644 258.1121 281.3173 34.1058 0.3534 258.6053 258.2519 281.6009 34.9333 0.3530 258.7510 258.3980 281.8780 35.6988 0.3521 258.9094 258.5573 282.0816 36.5163 0.3503 259.0578 258.7075 282.2909 37.3128 0.3518 259.2107 258.8589 282.4726 38.1095 0.3493 259.3696 259.0203 282.5896 38.9268 0.3512 259.5538 259.2026 282.6651 39.7230 0.3521 259.7485 259.3964 282.7310 40.5403 0.3504 259.9040 259.5535 282.7568 41.3165 0.3535 260.0566 259.7031 282.7460 42.1640 0.3521 260.2388 259.8867 282.7200 42.9303 0.3523 260.3795 260.0272 282.6702 43.7575 0.3512 260.5549 260.2037 282.5674 44.5540 0.3472 260.7263 260.3790 282.4818 45.3508 0.3446 260.8806 260.5359 282.3808 46.1678 0.3500 261.0638 260.7137 282.2490 46.9438 0.3493 261.2190 260.8697 282.1347 47.7920 0.3453 261.4014 261.0561 282.0011 48.5370 0.3440 261.5306 261.1866 281.8648 49.3748 0.3482 261.7168 261.3687 281.7387 50.1305 0.3485 261.8659 261.5174 281.6043 50.9985 0.3487 262.0129 261.6643 281.4508 51.7543 0.3501 262.1498 261.7997 281.3463 52.5815 0.3517 262.3365 261.9849 281.2725 53.3780 0.3583 262.4832 262.1250 281.2187 54.1850 0.3608 262.6373 262.2765 281.1372 55.0023 0.3628 262.7858 262.4231 281.1076 55.7678 0.3626 262.9053 262.5427 281.1313 56.6260 0.3676 263.0784 262.7107 281.1510 57.3920 0.3683 263.2312 262.8629 281.1853 58.2190 0.3644 263.4157 263.0513 281.2619 59.0055 0.3667 263.5912 263.2245 281.4026 59.8125 0.3706 263.7456 263.3750 281.5813 60.6293 0.3743 263.9040 263.5298 281.8117 61.3953 0.3742 264.0682 263.6940 282.0614 62.2535 0.3754 264.2227 263.8473 282.3608 63.0193 0.3767 264.3387 263.9620 282.6538 63.8468 0.3768 264.5130 264.1363 283.0172 64.6330 0.3768 264.6734 264.2966 283.3718 65.4398 0.3760 264.8145 264.4384 283.7541 66.2573 0.3771 264.9537 264.5766 284.1643 67.0330 0.3752 265.0825 264.7073 284.5329 67.8808 0.3779 265.2558 264.8779 284.9779 68.6570 0.3808 265.4101 265.0293 285.4040 69.4843 0.3811 265.5704 265.1894 285.8439 70.2603 0.3791 265.7125 265.3333 286.2310 71.0878 0.3815 265.8702 265.4887 286.6315 71.8740 0.3791 266.0422 265.6631 286.9726 72.6808 0.3771 266.2107 265.8336 287.2831 73.4980 0.3726 266.3647 265.9921 287.5808 74.2638 0.3710 266.5280 266.1570 287.8565 75.1218 0.3668 266.6931 266.3264 288.1288 75.8983 0.3610 266.8133 266.4523 288.3501 76.7150 0.3602 266.9509 266.5907 288.5330 77.5118 0.3563 267.0705 266.7143 288.6798 78.3085 0.3543 267.2294 266.8751 288.8238 79.1355 0.3529 267.3933 267.0404 288.9099 79.9218 0.3526 267.5420 267.1894 288.9573 80.7185 0.3513 267.6919 267.3406 288.9883 81.5150 0.3505 267.8889 267.5384 288.9973 82.3320 0.3469 268.0427 267.6958 288.9402 83.1083 0.3446 268.1631 267.8185 288.9009 83.9560 0.3430 268.3469 268.0039 288.7921 84.7218 0.3395 268.5318 268.1923 288.7303 85.5493 0.3358 268.7164 268.3807 288.6477 86.3458 0.3373 268.8926 268.5553 288.5883 87.1423 0.3389 269.0440 268.7051 288.4812 87.9903 0.3396 269.1867 268.8472 288.3585 88.7253 0.3395 269.3191 268.9796 288.2600 89.5833 0.3330 269.4807 269.1476 288.1620 90.3390 0.3330 269.6108 269.2778 288.0863 91.1663 0.3335 269.7835 269.4500 288.0116 91.9525 0.3300 269.9525 269.6225 287.9373 92.7493 0.3294 270.0995 269.7701 287.8928 93.5765 0.3334 270.2438 269.9104 287.9103 94.3423 0.3354 270.4071 270.0717 287.9475 95.1903 0.3341 270.5742 270.2402 287.9524 95.9663 0.3331 270.7278 270.3947 287.9838 96.7833 0.3320 270.8638 270.5318 288.0818 97.5698 0.3332 271.0136 270.6804 288.2207 98.3765 0.3297 271.1525 270.8228 288.3852 99.1935 0.3267 271.2928 270.9661 288.5425 99.9493 0.3275 271.3875 271.0600 288.7149 100.8175 0.3277 271.5682 271.2405 288.9733 101.5733 0.3310 271.7023 271.3713 289.1912 102.3905 0.3317 271.8969 271.5653 289.4664 103.1970 0.3322 272.0449 271.7127 289.7749 103.9835 0.3319 272.1677 271.8358 290.1255 104.8110 0.3325 272.3156 271.9830 290.4876 105.5765 0.3291 272.4688 272.1396 290.8242 106.4245 0.3267 272.6381 272.3114 291.2471 107.1903 0.3283 272.7373 272.4090 291.5719 108.0175 0.3294 272.8894 272.5600 291.9463 108.8143 0.3244 273.0398 272.7153 292.3161 109.6110 0.3200 273.2178 272.8978 292.6283 110.4278 0.3195 273.3754 273.0559 292.9877 111.2040 0.3180 273.5419 273.2239 293.2933 112.0520 0.3148 273.6937 273.3789 293.5738 112.8175 0.3150 273.8411 273.5261 293.8145 113.6448 0.3166 274.0008 273.6842 294.0966 114.4415 0.3183 274.1424 273.8241 294.2914 115.2380 0.3113 274.3000 273.9887 294.5124 116.0550 0.3070 274.4758 274.1688 294.6952 116.8313 0.3051 274.6308 274.3256 294.8344 117.6585 0.2982 274.7945 274.4963 294.9673 118.4243 0.2927 274.9585 274.6658 295.0484 119.2723 0.2851 275.1245 274.8394 295.1136 120.0483 0.2829 275.2887 275.0058 295.1277 120.8653 0.2785 275.4302 275.1516 295.1175 121.6620 0.2757 275.6052 275.3295 295.0931 122.4585 0.2713 275.7278 275.4565 295.0908 123.2858 0.2674 275.8553 275.5879 295.0404 124.0518 0.2644 275.9927 275.7283 294.9935 124.8995 0.2604 276.1638 275.9034 294.9306 125.6755 0.2595 276.3380 276.0784 294.8786 126.4928 0.2615 276.5007 276.2392 294.8327 127.2893 0.2628 276.6181 276.3553 294.7273 128.0860 0.2630 276.7837 276.5206 294.7013 128.9238 0.2603 276.9439 276.6836 294.6276 129.6790 0.2559 277.0896 276.8337 294.5687 130.5475 0.2503 277.2541 277.0038 294.5197 131.2930 0.2493 277.4283 277.1790 294.4759 132.1508 0.2454 277.5851 277.3397 294.4266 132.9168 0.2421 277.7737 277.5316 294.4554 133.7443 0.2417 277.9260 277.6843 294.4886 134.5405 0.2367 278.0559 277.8193 294.5183 135.3273 0.2369 278.1773 277.9404 294.5839 136.1648 0.2394 278.3323 278.0929 294.6882 136.9303 0.2405 278.4849 278.2445 294.8196 137.7885 0.2401 278.6579 278.4178 295.0068 138.5443 0.2455 278.7752 278.5297 295.2007 139.3818 0.2437 278.9307 278.6870 295.4389 140.1680 0.2420 279.0730 278.8310 295.6585 140.9853 0.2392 279.2257 278.9865 295.9173 141.7815 0.2349 279.3570 279.1221 296.2119 142.5785 0.2302 279.5144 279.2842 296.5592 143.4058 0.2305 279.6918 279.4613 296.9013 144.1715 0.2286 279.8340 279.6054 297.2045 145.0298 0.2242 280.0152 279.7910 297.6000 145.7853 0.2215 280.1621 279.9406 297.9273 146.6228 0.2184 280.3382 280.1198 298.3228 147.4195 0.2169 280.4768 280.2599 298.6497 148.2160 0.2140 280.5754 280.3614 298.9984 149.0330 0.2156 280.7282 280.5125 299.3203 149.8093 0.2136 280.8340 280.6204 299.6126 150.6570 0.2095 280.9620 280.7525 299.9181 151.4228 0.2086 281.0816 280.8729 300.2025 152.2503 0.2080 281.2627 281.0546 300.4137 153.0365 0.2029 281.4268 281.2240 300.5715 153.8333 0.2014 281.6043 281.4030 300.7583 154.6300 0.1997 281.7624 281.5627 300.9125 155.4160 0.1934 281.9096 281.7162 301.0661 156.2435 0.1923 282.0898 281.8975 301.1976 157.0095 0.1941 282.2382 282.0442 301.3013 157.8570 0.1908 282.3717 282.1809 301.3305 158.6230 0.1908 282.5315 282.3408 301.3813 159.4505 0.1878 282.6971 282.5093 301.4254 160.2468 0.1817 282.8543 282.6725 301.4399 161.0438 0.1751 282.9784 282.8033 301.4337 161.8608 0.1741 283.1286 282.9544 301.4179 162.6265 0.1700 283.2860 283.1159 301.3911 163.4850 0.1688 283.4712 283.3024 301.2621 164.2403 0.1669 283.6124 283.4455 301.2082 165.0678 0.1659 283.7562 283.5903 301.1681 165.8645 0.1627 283.9152 283.7525 301.1162 166.6505 0.1627 284.0122 283.8495 301.0912 167.4780 0.1608 284.1661 284.0053 301.0489 168.2440 0.1579 284.2867 284.1289 300.9973 169.0918 0.1564 284.4528 284.2964 300.9537 169.8373 0.1552 284.5934 284.4382 300.9113 170.6850 0.1514 284.7698 284.6184 300.8782 171.4510 0.1509 284.9357 284.7847 300.8514 172.2785 0.1530 285.1071 284.9541 300.8808 173.0748 0.1516 285.2577 285.1062 300.9450 173.8718 0.1510 285.4288 285.2778 301.0058 174.6888 0.1492 285.5897 285.4405 301.1132 175.4648 0.1500 285.7329 285.5829 301.2972 176.3128 0.1454 285.9246 285.7792 301.4728 177.0785 0.1429 286.0852 285.9423 301.6461 177.9058 0.1424 286.2247 286.0823 301.8850 178.7025 0.1400 286.3535 286.2135 302.1160 179.4990 0.1384 286.4791 286.3406 302.3732 180.3160 0.1403 286.6238 286.4835 302.6921 181.0923 0.1409 286.7399 286.5991 302.9849 181.9400 0.1429 286.8978 286.7549 303.3212 182.7058 0.1431 287.0392 286.8960 303.6522 183.5335 0.1395 287.1775 287.0380 304.0025 184.3298 0.1377 287.3545 287.2169 304.3269 185.1265 0.1360 287.4702 287.3342 304.6604 185.9538 0.1344 287.6220 287.4876 305.0103 186.7195 0.1327 287.7840 287.6512 305.3271 187.5775 0.1324 287.9724 287.8400 305.6752 188.3435 0.1297 288.1500 288.0203 305.9276 189.1605 0.1274 288.3106 288.1832 306.2168 189.9673 0.1249 288.4521 288.3272 306.4899 190.7538 0.1242 288.5822 288.4581 306.7236 191.5810 0.1265 288.7317 288.6052 306.9438 192.3468 0.1238 288.8515 288.7277 307.1299 193.2053 0.1193 289.0172 288.8980 307.3093 193.9708 0.1138 289.1663 289.0525 307.4257 194.7880 0.1111 289.3196 289.2085 307.5204 195.5948 0.1109 289.4850 289.3741 307.5844 196.3913 0.1108 289.6383 289.5275 307.6532 197.2185 0.1092 289.7842 289.6750 307.6878 197.9743 0.1035 289.9441 289.8406 307.7128 198.8425 0.0962 290.1087 290.0126 307.7279 199.6083 0.0937 290.2756 290.1819 307.7277 200.4358 0.0863 290.4512 290.3649 307.7099 201.2220 0.0829 290.5662 290.4833 307.6641 202.0290 0.0840 290.6863 290.6023 307.5985 202.8155 0.0835 290.8294 290.7459 307.5369 203.6425 0.0855 290.9935 290.9080 307.4721 204.4393 0.0866 291.1366 291.0500 307.4090 205.2360 0.0856 291.2956 291.2100 307.3713 206.0528 0.0833 291.4828 291.3995 307.3269 206.8290 0.0794 291.6372 291.5578 307.3211 207.6770 0.0788 291.7646 291.6859 307.2839 208.4425 0.0765 291.9281 291.8516 307.2505 209.2700 0.0739 292.0919 292.0180 307.2341 210.0975 0.0742 292.2298 292.1556 307.2720 210.8630 0.0742 292.3798 292.3055 307.3380 211.7110 0.0750 292.5550 292.4801 307.3653 212.4873 0.0792 292.6948 292.6156 307.4263 213.3040 0.0807 292.8281 292.7474 307.5679 214.1110 0.0794 292.9963 292.9168 307.7384 214.8975 0.0786 293.1517 293.0730 307.9146 215.7348 0.0780 293.3402 293.2622 308.1286 216.4905 0.0762 293.4722 293.3960 308.3285 217.3488 0.0756 293.6267 293.5511 308.6091 218.0835 0.0757 293.7865 293.7108 308.8518 218.9315 0.0748 293.9434 293.8686 309.1620 219.6975 0.0704 294.0758 294.0054 309.4735 220.5248 0.0674 294.1959 294.1285 309.8109 221.3113 0.0652 294.3018 294.2365 310.1252 222.1078 0.0617 294.4240 294.3623 310.4580 222.9350 0.0545 294.6187 294.5642 310.8316 223.7008 0.0514 294.7757 294.7243 311.1710 224.5488 0.0499 294.9206 294.8707 311.5152 225.3143 0.0505 295.1031 295.0525 311.8235 226.1420 0.0515 295.2819 295.2304 312.1354 226.9283 0.0522 295.4194 295.3672 312.4112 227.7245 0.0474 295.5491 295.5016 312.6654 228.5520 0.0493 295.6953 295.6459 312.9037 229.3180 0.0484 295.8450 295.7966 313.0742 230.1655 0.0429 295.9951 295.9522 313.2811 230.9315 0.0396 296.1393 296.0998 313.4372 231.7590 0.0351 296.2698 296.2347 313.5733 232.5143 0.0325 296.4034 296.3709 313.6636 233.3520 0.0301 296.5776 296.5475 313.7685 234.1385 0.0280 296.7839 296.7559 313.8500 234.9348 0.0253 296.9515 296.9262 313.8923 235.7620 0.0178 297.1037 297.0859 313.9341 236.5280 0.0165 297.2324 297.2159 313.9502 237.3860 0.0140 297.3719 297.3580 313.9490 238.1415 0.0112 297.4925 297.4813 313.9800 238.9793 0.0101 297.6161 297.6060 313.9447 239.7655 0.0043 297.7564 297.7520 313.9064 240.5518 0.0002 297.9126 297.9124 313.8645 241.3895 -0.0017 298.0888 298.0905 313.7772 242.1450 -0.0054 298.2440 298.2494 313.7341 243.0030 -0.0073 298.3892 298.3966 313.6633 243.8305 -0.0083 298.5647 298.5730 313.6384 244.5963 -0.0109 298.7032 298.7141 313.5817 245.4543 -0.0106 298.8505 298.8611 313.5637 246.2100 -0.0144 298.9648 298.9792 313.5370 247.0475 -0.0155 299.0907 299.1061 313.5176 247.8340 -0.0174 299.2413 299.2586 313.5324 248.6308 -0.0173 299.3970 299.4143 313.5601 249.4578 -0.0192 299.5563 299.5755 313.5865 250.2238 -0.0227 299.7060 299.7287 313.6851 251.0820 -0.0261 299.8423 299.8684 313.8262 251.8373 -0.0291 299.9842 300.0134 313.9660 252.6750 -0.0324 300.1508 300.1832 314.1380 253.5025 -0.0279 300.3072 300.3350 314.3659 254.4730 -0.0283 300.4980 300.5263 314.6472 255.2595 -0.0315 300.6447 300.6762 314.9139 256.0973 -0.0318 300.7819 300.8137 315.2211 256.8525 -0.0339 300.9378 300.9716 315.4820 257.7213 -0.0367 301.1441 301.1809 315.8084 258.4768 -0.0369 301.2889 301.3257 316.0699 259.3040 -0.0391 301.4357 301.4749 316.3831 260.1010 -0.0458 301.5991 301.6448 316.7198 260.8973 -0.0467 301.7494 301.7962 317.0345 261.7250 -0.0497 301.9099 301.9597 317.3893 262.4805 -0.0466 302.0308 302.0775 317.7230 263.3488 -0.0464 302.1564 302.2028 318.0666 264.1045 -0.0487 302.2912 302.3400 318.3167 264.9420 -0.0505 302.4679 302.5185 318.6409 265.7283 -0.0522 302.6307 302.6829 318.8961 266.5355 -0.0503 302.7657 302.8160 319.1397 267.3523 -0.0505 302.9094 302.9599 319.3517 268.1185 -0.0555 303.0541 303.1095 319.5608 268.9765 -0.0568 303.1925 303.2492 319.7528 269.7525 -0.0615 303.3259 303.3873 319.9141 270.5698 -0.0643 303.4495 303.5138 320.0224 271.3663 -0.0676 303.6076 303.6752 320.1056 272.1628 -0.0662 303.7336 303.7997 320.1742 272.9903 -0.0692 303.8530 303.9223 320.2217 273.7560 -0.0728 304.0101 304.0829 320.2330 274.6243 -0.0777 304.1913 304.2691 320.2656 275.3493 -0.0797 304.3180 304.3977 320.2246 276.2175 -0.0826 304.5077 304.5903 320.2168 276.9730 -0.0813 304.6656 304.7469 320.1693 277.8005 -0.0826 304.8303 304.9128 320.1271 278.5970 -0.0876 304.9690 305.0565 320.0551 279.3938 -0.0934 305.0976 305.1910 319.9680 280.2213 -0.0981 305.2661 305.3641 319.9189 280.9765 -0.0983 305.4215 305.5198 319.8772 281.8348 -0.1027 305.6027 305.7054 319.7940 282.5905 -0.1029 305.7598 305.8627 319.7994 283.4178 -0.1044 305.8813 305.9857 319.8008 284.2450 -0.1011 306.0416 306.1427 319.8279 285.2160 -0.1058 306.2010 306.3067 319.8474 286.0020 -0.1047 306.3455 306.4502 319.8681 286.8193 -0.1077 306.4811 306.5888 319.9269 287.5955 -0.1071 306.6296 306.7367 320.0164 288.4123 -0.1119 306.8013 306.9131 320.0790 289.1785 -0.1159 306.9164 307.0323 320.2069 290.0365 -0.1177 307.0828 307.2005 320.3661 290.7920 -0.1167 307.2514 307.3680 320.5345 291.6195 -0.1130 307.4249 307.5379 320.7382 292.4160 -0.1092 307.5500 307.6592 320.9687 293.2125 -0.1097 307.6492 307.7589 321.2521 293.9990 -0.1141 307.7828 307.8970 321.5276 294.7955 -0.1182 307.9135 308.0317 321.8269 295.6538 -0.1177 308.1082 308.2259 322.1647 296.3890 -0.1178 308.2548 308.3726 322.4518 297.2365 -0.1185 308.3880 308.5065 322.7834 298.0128 -0.1221 308.5293 308.6514 323.1278 298.8300 -0.1270 308.6896 308.8166 323.4329 299.6263 -0.1309 308.8361 308.9670 323.7441 300.4230 -0.1321 308.9474 309.0795 324.0804 301.2300 -0.1315 309.0997 309.2312 324.3817 302.0160 -0.1311 309.2516 309.3827 324.6641 302.8333 -0.1322 309.4279 309.5601 324.9500 303.6095 -0.1345 309.5973 309.7318 325.1736 304.4570 -0.1350 309.7726 309.9075 325.3881 305.2540 -0.1373 309.9427 310.0800 325.5882 306.0505 -0.1406 310.0484 310.1890 325.7805 306.8470 -0.1459 310.2254 310.3713 325.9388 307.6438 -0.1480 310.3817 310.5298 326.0452 308.4608 -0.1503 310.5308 310.6811 326.1989 309.2365 -0.1537 310.6744 310.8281 326.2821 310.0848 -0.1566 310.8166 310.9732 326.3510 310.8505 -0.1616 310.9496 311.1112 326.4239 311.6778 -0.1654 311.1053 311.2707 326.4583 312.4745 -0.1714 311.2543 311.4257 326.4456 313.2710 -0.1751 311.4077 311.5828 326.4509 314.0880 -0.1758 311.5635 311.7393 326.4305 314.8643 -0.1796 311.7059 311.8855 326.3779 315.7325 -0.1830 311.8726 312.0556 326.3072 316.4880 -0.1820 311.9999 312.1819 326.2831 317.3155 -0.1828 312.1527 312.3355 326.2100 318.1120 -0.1837 312.2912 312.4750 326.1587 318.9085 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