DTA measure 1Fazis3 Date: 20251014:174 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.14 s Mass = 1333.900 mg data_number = 1070 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4010 -0.0527 282.5086 282.5613 241.3109 3.9845 -0.0548 282.3106 282.3654 241.1241 5.5890 -0.0601 282.1397 282.1999 240.9116 7.1886 -0.0589 281.9205 281.9795 240.7056 8.7875 -0.0620 281.7138 281.7759 240.4947 10.3971 -0.0655 281.5022 281.5677 240.2886 12.0019 -0.0712 281.3431 281.4143 240.1038 13.6059 -0.0704 281.1672 281.2376 239.8798 15.2309 -0.0693 280.9430 281.0122 239.6815 16.8356 -0.0709 280.7347 280.8056 239.4914 18.4399 -0.0703 280.5060 280.5763 239.3069 20.0288 -0.0742 280.3426 280.4168 239.1357 21.6386 -0.0823 280.1823 280.2646 238.9069 23.2431 -0.0826 279.9869 280.0695 238.6521 24.9291 -0.0856 279.7670 279.8526 238.4148 26.5493 -0.0858 279.5779 279.6636 238.2310 28.1588 -0.0874 279.3346 279.4220 238.0437 29.7629 -0.0872 279.1488 279.2361 237.8428 31.3728 -0.0884 278.9510 279.0394 237.6541 32.9874 -0.0902 278.7595 278.8497 237.4616 34.5710 -0.0924 278.5837 278.6761 237.2668 36.1604 -0.0904 278.3855 278.4759 237.0789 37.7750 -0.0859 278.1752 278.2611 236.9301 39.3740 -0.0849 277.9721 278.0570 236.7622 40.9788 -0.0794 277.7661 277.8455 236.5513 42.5834 -0.0742 277.5881 277.6623 236.3187 44.1924 -0.0790 277.3766 277.4556 236.1014 45.7869 -0.0760 277.1481 277.2241 235.9277 47.4019 -0.0785 276.9161 276.9946 235.7289 48.9955 -0.0837 276.7062 276.7900 235.4947 50.6001 -0.0876 276.5253 276.6129 235.3057 52.2203 -0.0876 276.3123 276.3999 235.1174 53.8300 -0.0831 276.0643 276.1474 234.9113 55.4236 -0.0840 275.8670 275.9510 234.7082 57.0438 -0.0834 275.6597 275.7431 234.5463 58.6383 -0.0853 275.4530 275.5383 234.3839 60.2529 -0.0822 275.2859 275.3681 234.2079 61.8570 -0.0813 275.0854 275.1667 233.9883 63.4618 -0.0824 274.8799 274.9623 233.7857 65.0711 -0.0812 274.6638 274.7450 233.6230 66.6805 -0.0814 274.4594 274.5408 233.3875 68.2596 -0.0840 274.2776 274.3616 233.1831 69.8593 -0.0875 274.0457 274.1332 233.0128 71.4738 -0.0844 273.8754 273.9599 232.8446 73.0831 -0.0821 273.6796 273.7616 232.6420 74.6828 -0.0849 273.4574 273.5423 232.4504 76.2924 -0.0853 273.2317 273.3169 232.2532 77.8913 -0.0930 272.9775 273.0705 232.0795 79.4960 -0.0925 272.8028 272.8953 231.8874 81.1008 -0.0863 272.6189 272.7052 231.7009 82.7098 -0.0836 272.4270 272.5106 231.5402 84.3041 -0.0786 272.2305 272.3090 231.3238 85.9191 -0.0780 271.9916 272.0695 231.1062 87.5388 -0.0808 271.7537 271.8345 230.9340 89.1481 -0.0829 271.5319 271.6148 230.7420 90.7529 -0.0831 271.3605 271.4436 230.5669 92.3525 -0.0805 271.1847 271.2652 230.3921 93.9614 -0.0798 270.9403 271.0202 230.1730 95.5713 -0.0795 270.7766 270.8561 229.9616 97.1760 -0.0824 270.5989 270.6813 229.7017 98.7800 -0.0776 270.3593 270.4369 229.5592 100.3640 -0.0768 270.1026 270.1794 229.4163 101.9841 -0.0791 269.8206 269.8998 229.2856 103.5879 -0.0809 269.6297 269.7107 229.0943 105.1875 -0.0812 269.4588 269.5400 228.9586 106.7923 -0.0812 269.3000 269.3813 228.8662 108.3861 -0.0868 269.0707 269.1574 228.8356 109.9956 -0.0891 268.8598 268.9489 228.8508 111.6055 -0.0863 268.6734 268.7597 228.8861 113.2096 -0.0841 268.4890 268.5731 228.9952 114.8345 -0.0901 268.2260 268.3161 229.1966 116.4393 -0.0910 268.0108 268.1018 229.4285 118.0436 -0.0889 267.8367 267.9256 229.7247 119.6529 -0.0928 267.6558 267.7486 230.0637 121.2576 -0.0969 267.4829 267.5798 230.5010 122.8723 -0.0972 267.2849 267.3821 230.9506 124.4661 -0.0977 267.0317 267.1293 231.3602 126.0811 -0.1061 266.8439 266.9501 231.7677 127.7013 -0.1147 266.6372 266.7519 232.2016 129.3101 -0.1143 266.4499 266.5642 232.6354 130.8995 -0.1131 266.2576 266.3707 233.0099 132.4991 -0.1215 266.0666 266.1881 233.3677 134.1034 -0.1263 265.8829 266.0092 233.6948 135.7025 -0.1287 265.6990 265.8277 233.9765 137.3124 -0.1345 265.5132 265.6477 234.2402 138.9166 -0.1383 265.3212 265.4594 234.3998 140.5055 -0.1429 265.1576 265.3005 234.4866 142.1308 -0.1470 264.9814 265.1284 234.5871 143.7355 -0.1526 264.7909 264.9434 234.6814 145.3444 -0.1618 264.6305 264.7923 234.7078 146.9491 -0.1690 264.4759 264.6449 234.7255 148.5690 -0.1729 264.3128 264.4857 234.7533 150.1679 -0.1780 264.1524 264.3303 234.8144 151.7726 -0.1859 264.0261 264.2121 234.8651 153.3770 -0.1862 263.9001 264.0862 234.9248 155.0016 -0.1936 263.7370 263.9306 235.0245 156.6115 -0.2007 263.5821 263.7828 235.1636 158.2214 -0.1996 263.4283 263.6279 235.3066 159.8253 -0.1988 263.2535 263.4523 235.4940 161.4299 -0.1975 263.1126 263.3101 235.6666 163.0295 -0.2028 262.9623 263.1651 235.8734 164.6288 -0.2081 262.7950 263.0031 236.1601 166.2431 -0.2124 262.6161 262.8285 236.4127 167.8530 -0.2213 262.4424 262.6637 236.6992 169.4525 -0.2204 262.2972 262.5176 237.0520 171.0513 -0.2256 262.1820 262.4076 237.3914 172.6611 -0.2300 262.0560 262.2860 237.7671 174.2656 -0.2332 261.8796 262.1127 238.1156 175.8748 -0.2338 261.7827 262.0165 238.4607 177.4949 -0.2339 261.6602 261.8941 238.7372 179.0945 -0.2405 261.5270 261.7675 239.0205 180.7036 -0.2452 261.4053 261.6505 239.2674 182.3081 -0.2477 261.2548 261.5025 239.4972 183.9078 -0.2548 261.1664 261.4212 239.7124 185.5116 -0.2623 261.0790 261.3413 239.9096 187.1214 -0.2661 260.9831 261.2492 240.0746 188.7261 -0.2652 260.8504 261.1156 240.1909 190.3456 -0.2682 260.7321 261.0003 240.3101 191.9551 -0.2696 260.5848 260.8544 240.4327 193.5599 -0.2660 260.4587 260.7247 240.5555 195.1694 -0.2738 260.3570 260.6308 240.6456 196.7735 -0.2795 260.2560 260.5354 240.7508 198.3526 -0.2820 260.2030 260.4851 240.8717 199.9574 -0.2807 260.1476 260.4284 240.9828 201.5566 -0.2809 260.0676 260.3485 241.0928 203.1761 -0.2794 259.9470 260.2265 241.2147 204.7860 -0.2841 259.8072 260.0913 241.3829 206.3903 -0.2899 259.7273 260.0172 241.5845 207.9996 -0.2919 259.6602 259.9521 241.7925 209.6095 -0.2914 259.6112 259.9026 242.0097 211.2040 -0.2952 259.5515 259.8467 242.2327 212.8078 -0.3004 259.4755 259.7759 242.5067 214.4176 -0.2991 259.4471 259.7462 242.8175 216.0275 -0.2945 259.3638 259.6582 243.1506 217.6528 -0.2980 259.3121 259.6101 243.4530 219.2565 -0.2994 259.2231 259.5226 243.7653 220.8715 -0.2995 259.1600 259.4595 244.0841 222.4813 -0.2962 259.1102 259.4064 244.3855 224.0851 -0.2955 259.0244 259.3200 244.7162 225.6950 -0.2927 258.9544 259.2471 245.0032 227.2938 -0.2915 258.8992 259.1907 245.2175 228.8779 -0.2933 258.8096 259.1029 245.4097 230.4980 -0.2980 258.7612 259.0593 245.5753 232.0970 -0.2989 258.7469 259.0457 245.7207 233.6911 -0.3061 258.7268 259.0329 245.8397 235.3061 -0.3100 258.6803 258.9903 245.9781 236.9153 -0.3085 258.6635 258.9720 246.1245 238.5146 -0.3033 258.6040 258.9073 246.2503 240.1911 -0.3017 258.5184 258.8202 246.3431 241.9235 -0.3025 258.4802 258.7828 246.4534 243.5278 -0.3025 258.4735 258.7761 246.5629 245.1428 -0.3015 258.4379 258.7394 246.7096 246.7471 -0.3031 258.4045 258.7076 246.8654 248.3564 -0.2970 258.3776 258.6746 247.0761 249.9509 -0.2926 258.3793 258.6719 247.3219 251.5651 -0.2932 258.3530 258.6461 247.5145 253.1850 -0.2975 258.3025 258.5999 247.7828 254.7949 -0.2937 258.3133 258.6070 248.0730 256.3996 -0.2911 258.3020 258.5931 248.3695 258.0085 -0.2937 258.3124 258.6061 248.6258 259.5928 -0.2963 258.3338 258.6302 248.9617 261.1975 -0.2958 258.3411 258.6369 249.3001 262.7964 -0.2974 258.3643 258.6618 249.5671 264.4163 -0.2906 258.3702 258.6608 249.8555 266.0364 -0.2886 258.3278 258.6164 250.1365 267.6354 -0.2924 258.2469 258.5393 250.3872 269.2398 -0.2936 258.2219 258.5155 250.6162 270.8445 -0.2880 258.2643 258.5523 250.8325 272.4536 -0.2880 258.3091 258.5970 251.0294 274.0581 -0.2858 258.3547 258.6404 251.1746 275.6783 -0.2875 258.4321 258.7196 251.3203 277.2770 -0.2847 258.4425 258.7271 251.4734 278.8816 -0.2802 258.3952 258.6754 251.5646 280.4915 -0.2788 258.4049 258.6836 251.6855 282.0954 -0.2726 258.3800 258.6526 251.7958 283.7051 -0.2696 258.4078 258.6774 251.8265 285.3099 -0.2716 258.4401 258.7117 251.9166 286.9193 -0.2724 258.4703 258.7427 252.0844 288.5389 -0.2742 258.5208 258.7950 252.3093 290.1436 -0.2722 258.5365 258.8087 252.5263 291.7479 -0.2673 258.5565 258.8238 252.7531 293.3470 -0.2642 258.6109 258.8750 252.9675 294.9313 -0.2624 258.6335 258.8959 253.2218 296.5411 -0.2564 258.6729 258.9293 253.5402 298.1450 -0.2516 258.7098 258.9614 253.8512 299.7445 -0.2496 258.7612 259.0108 254.1491 301.3641 -0.2490 258.7980 259.0470 254.4721 302.9735 -0.2497 258.7958 259.0455 254.7958 304.5629 -0.2512 258.8753 259.1265 255.0943 306.1778 -0.2487 258.9116 259.1603 255.3716 307.7816 -0.2442 258.9356 259.1798 255.6225 309.3915 -0.2434 258.9535 259.1968 255.8459 310.9860 -0.2389 259.0202 259.2591 256.0680 312.5805 -0.2371 259.0835 259.3206 256.2670 314.1998 -0.2354 259.1551 259.3905 256.4583 315.8095 -0.2339 259.2126 259.4464 256.6068 317.4143 -0.2294 259.2816 259.5110 256.7066 319.0389 -0.2251 259.3240 259.5491 256.7385 320.6433 -0.2305 259.3980 259.6285 256.8272 322.2326 -0.2324 259.4598 259.6923 256.8991 323.8525 -0.2302 259.5423 259.7725 257.0172 325.4565 -0.2194 259.5898 259.8092 257.1789 327.0459 -0.2173 259.6885 259.9057 257.3475 328.6555 -0.2179 259.7454 259.9633 257.5245 330.2544 -0.2113 259.7898 260.0012 257.7284 331.8540 -0.2115 259.8391 260.0507 257.9517 333.4588 -0.2109 259.8868 260.0977 258.2092 335.0630 -0.2094 260.0024 260.2118 258.4877 336.6878 -0.2072 260.1203 260.3275 258.8138 338.2874 -0.2039 260.2236 260.4275 259.1384 339.8966 -0.2020 260.3465 260.5486 259.4717 341.5010 -0.1990 260.3504 260.5494 259.7991 343.0955 -0.2000 260.4003 260.6003 260.0849 344.7200 -0.1959 260.4783 260.6742 260.3576 346.3245 -0.2005 260.5474 260.7479 260.6426 347.9344 -0.1959 260.6590 260.8550 260.8854 349.5390 -0.1914 260.7995 260.9909 261.1335 351.1378 -0.1952 260.8756 261.0708 261.3826 352.7476 -0.1970 260.9323 261.1293 261.6093 354.3729 -0.1971 261.0372 261.2343 261.7365 355.9769 -0.1949 261.1180 261.3128 261.8996 357.5660 -0.1875 261.1920 261.3796 262.0142 359.1656 -0.1827 261.2900 261.4728 262.1066 360.7651 -0.1847 261.3925 261.5772 262.2109 362.3741 -0.1842 261.4767 261.6609 262.3011 363.9789 -0.1843 261.6070 261.7914 262.4050 365.5781 -0.1782 261.7426 261.9208 262.5285 367.1874 -0.1788 261.8670 262.0458 262.6498 368.7921 -0.1765 261.9246 262.1011 262.7898 370.4121 -0.1709 262.0474 262.2183 262.9382 372.0211 -0.1635 262.1463 262.3098 263.1760 373.6156 -0.1543 262.2097 262.3640 263.4194 375.2358 -0.1532 262.3033 262.4565 263.7017 376.8449 -0.1524 262.3636 262.5160 263.9661 378.4494 -0.1513 262.4828 262.6341 264.2349 380.0490 -0.1481 262.5940 262.7421 264.5484 381.6528 -0.1478 262.7047 262.8525 264.8705 383.2575 -0.1487 262.8261 262.9749 265.2321 384.8828 -0.1436 262.9343 263.0780 265.5819 386.4919 -0.1401 263.0872 263.2273 265.8974 388.0964 -0.1372 263.2420 263.3792 266.2253 389.6960 -0.1419 263.3583 263.5002 266.5068 391.2899 -0.1435 263.4712 263.6147 266.7493 392.8943 -0.1422 263.5974 263.7396 266.9747 394.4939 -0.1432 263.7277 263.8710 267.1687 396.0979 -0.1430 263.8785 264.0215 267.3172 397.7075 -0.1433 264.0288 264.1721 267.4225 399.3071 -0.1428 264.1629 264.3058 267.5301 400.9221 -0.1434 264.2622 264.4056 267.6301 402.5105 -0.1392 264.3482 264.4874 267.7846 404.1409 -0.1360 264.4877 264.6237 267.8669 405.7559 -0.1325 264.6490 264.7816 267.9216 407.3598 -0.1329 264.7583 264.8912 267.9476 408.9644 -0.1288 264.8917 265.0205 268.0488 410.5743 -0.1218 265.0030 265.1248 268.1867 412.1786 -0.1146 265.1673 265.2819 268.3770 413.7879 -0.1098 265.3440 265.4539 268.6187 415.4131 -0.1121 265.5315 265.6435 268.8956 417.0123 -0.1165 265.6710 265.7874 269.1682 418.6524 -0.1121 265.8204 265.9325 269.4916 420.2418 -0.1052 265.9616 266.0668 269.8260 421.8354 -0.1015 266.0770 266.1785 270.1725 423.4349 -0.0984 266.2143 266.3127 270.5352 425.0499 -0.0935 266.3605 266.4539 270.8526 426.6341 -0.0878 266.4954 266.5832 271.2127 428.2379 -0.0840 266.6412 266.7251 271.5328 429.8478 -0.0851 266.8325 266.9176 271.8007 431.4628 -0.0878 266.9757 267.0635 272.0823 433.0668 -0.0861 267.1283 267.2144 272.2547 434.6764 -0.0838 267.2252 267.3090 272.4818 436.2914 -0.0872 267.3522 267.4394 272.6166 437.8901 -0.0847 267.5008 267.5854 272.7551 439.4948 -0.0863 267.6127 267.6990 272.8736 441.1046 -0.0902 267.7390 267.8291 272.9584 442.7089 -0.0876 267.8724 267.9600 272.9896 444.3336 -0.0822 268.0746 268.1567 273.0699 445.9384 -0.0813 268.2547 268.3360 273.1424 447.5481 -0.0774 268.4178 268.4953 273.2437 449.1520 -0.0728 268.5900 268.6628 273.3492 450.7568 -0.0715 268.7776 268.8491 273.4801 452.3666 -0.0665 268.9265 268.9930 273.6596 453.9504 -0.0610 269.0790 269.1400 273.8638 455.5444 -0.0599 269.3148 269.3747 274.1259 457.1696 -0.0570 269.4249 269.4818 274.4413 458.7689 -0.0525 269.5839 269.6364 274.8064 460.3576 -0.0551 269.7760 269.8311 275.1807 461.9675 -0.0521 269.9492 270.0012 275.5286 463.5721 -0.0505 270.1638 270.2143 275.8438 465.1811 -0.0455 270.3259 270.3715 276.1428 466.7808 -0.0496 270.4764 270.5260 276.4467 468.3853 -0.0496 270.6422 270.6918 276.7824 470.0046 -0.0491 270.7903 270.8394 277.0562 471.6094 -0.0449 270.9372 270.9821 277.3301 473.2193 -0.0431 271.0638 271.1070 277.5846 474.8231 -0.0441 271.2642 271.3083 277.7420 476.4226 -0.0408 271.4131 271.4540 277.9420 478.0376 -0.0377 271.5686 271.6063 278.0791 479.6475 -0.0396 271.7301 271.7697 278.1612 481.2515 -0.0404 271.9294 271.9698 278.2505 482.8663 -0.0396 272.0922 272.1318 278.3372 484.4710 -0.0400 272.2901 272.3301 278.4244 486.0700 -0.0393 272.4354 272.4747 278.4569 487.6795 -0.0324 272.6103 272.6427 278.5341 489.2740 -0.0268 272.8175 272.8443 278.6506 490.8783 -0.0246 272.9662 272.9908 278.8132 492.4876 -0.0236 273.1401 273.1636 278.9821 494.0770 -0.0202 273.3203 273.3405 279.1689 495.6816 -0.0138 273.5461 273.5599 279.4175 497.3009 -0.0167 273.7257 273.7423 279.7150 498.9056 -0.0187 273.8823 273.9009 280.0329 500.5155 -0.0143 274.0186 274.0329 280.4174 502.1194 -0.0119 274.1975 274.2094 280.7632 503.7291 -0.0144 274.4231 274.4375 281.1031 505.3336 -0.0178 274.5767 274.5945 281.4546 506.9530 -0.0180 274.7716 274.7896 281.8199 508.5526 -0.0216 274.9898 275.0114 282.1713 510.1574 -0.0219 275.1582 275.1801 282.4426 511.7614 -0.0234 275.3509 275.3743 282.7017 513.3710 -0.0264 275.5779 275.6043 282.9500 514.9911 -0.0209 275.7779 275.7988 283.1317 516.6006 -0.0208 275.9442 275.9649 283.2995 518.2048 -0.0183 276.0692 276.0874 283.4268 519.8095 -0.0194 276.2382 276.2576 283.5152 521.4090 -0.0192 276.4604 276.4796 283.5909 522.9975 -0.0182 276.6913 276.7095 283.6157 524.5971 -0.0220 276.9455 276.9675 283.6544 526.2019 -0.0234 277.1563 277.1797 283.7059 527.8315 -0.0250 277.3575 277.3825 283.7890 529.4155 -0.0247 277.5388 277.5635 283.9173 531.0203 -0.0222 277.6843 277.7065 284.0939 532.6501 -0.0196 277.8523 277.8719 284.2719 534.2441 -0.0178 278.0510 278.0688 284.4795 535.8489 -0.0133 278.2688 278.2821 284.7388 537.4639 -0.0162 278.4550 278.4712 285.0535 539.1038 -0.0155 278.6433 278.6588 285.3861 540.7083 -0.0167 278.7787 278.7955 285.7446 542.3335 -0.0130 278.9723 278.9853 286.1022 543.9374 -0.0112 279.1477 279.1589 286.4799 545.5471 -0.0076 279.3820 279.3896 286.8928 547.1468 -0.0054 279.5774 279.5828 287.2345 548.7508 -0.0083 279.8020 279.8103 287.5565 550.3501 -0.0099 280.0135 280.0233 287.8630 551.9548 -0.0102 280.1966 280.2069 288.0827 553.5484 -0.0104 280.4196 280.4301 288.2292 555.1583 -0.0115 280.6186 280.6302 288.3517 556.7579 -0.0140 280.8000 280.8140 288.4432 558.3619 -0.0161 281.0270 281.0431 288.5177 559.9664 -0.0152 281.2349 281.2501 288.5832 561.6019 -0.0137 281.4319 281.4456 288.6280 563.2115 -0.0132 281.6393 281.6525 288.6899 564.8309 -0.0121 281.8315 281.8436 288.7663 566.4356 -0.0142 282.0275 282.0417 288.8951 568.0448 -0.0140 282.2482 282.2622 289.0649 569.6390 -0.0150 282.4798 282.4948 289.1493 571.2489 -0.0112 282.6493 282.6605 289.3357 572.8528 -0.0118 282.8267 282.8385 289.5733 574.4625 -0.0093 283.0307 283.0400 289.8402 576.0673 -0.0079 283.2366 283.2445 290.1532 577.6923 -0.0065 283.4565 283.4630 290.4878 579.2860 -0.0045 283.6373 283.6418 290.8156 580.8908 -0.0036 283.8736 283.8772 291.2177 582.4953 -0.0032 284.1041 284.1073 291.5547 584.0941 -0.0060 284.3077 284.3136 291.9211 585.6938 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