DTA measure 2gyors Date: 20251021:1057 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.59 s Mass = 100.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2913 1.2850 229.5487 228.2637 272.3454 2.1185 1.2886 229.8338 228.5452 272.4111 2.9155 1.2927 230.0706 228.7779 272.4914 3.7015 1.2946 230.2991 229.0045 272.6357 4.5395 1.2981 230.6151 229.3170 272.8406 5.2950 1.3020 230.8518 229.5498 273.0395 6.1633 1.3060 231.1299 229.8239 273.2935 6.9193 1.3048 231.3367 230.0319 273.5111 7.7565 1.3062 231.6506 230.3444 273.7936 8.5430 1.3066 231.9431 230.6365 274.0732 9.3398 1.3113 232.1853 230.8741 274.3696 10.1360 1.3131 232.4710 231.1579 274.7176 10.9430 1.3124 232.7445 231.4321 275.0793 11.7603 1.3153 233.0326 231.7173 275.4598 12.5260 1.3158 233.3081 231.9924 275.8437 13.3740 1.3202 233.6018 232.2816 276.1946 14.1295 1.3186 233.8514 232.5328 276.4989 14.9978 1.3197 234.1089 232.7892 276.8349 15.7535 1.3164 234.3829 233.0664 277.1487 16.5808 1.3167 234.6924 233.3756 277.4326 17.3773 1.3159 234.9377 233.6217 277.7178 18.1638 1.3128 235.1834 233.8706 277.9975 18.9808 1.3130 235.4416 234.1286 278.2213 19.7568 1.3112 235.6806 234.3693 278.3966 20.6048 1.3122 235.9376 234.6254 278.5748 21.3705 1.3079 236.1792 234.8713 278.7174 22.1978 1.2959 236.4470 235.1511 278.8021 22.9640 1.2899 236.6924 235.4026 278.8628 23.7910 1.2912 236.9537 235.6625 278.8939 24.6080 1.2919 237.2326 235.9407 278.8975 25.3843 1.2894 237.4950 236.2056 278.8753 26.2013 1.2880 237.7412 236.4533 278.8609 26.9673 1.2832 237.9626 236.6794 278.7976 27.8255 1.2826 238.2462 236.9636 278.6947 28.5910 1.2840 238.4834 237.1994 278.6369 29.4185 1.2850 238.7464 237.4614 278.5571 30.2153 1.2819 239.0126 237.7307 278.4455 31.0115 1.2825 239.2568 237.9743 278.3650 31.8390 1.2851 239.5186 238.2335 278.2645 32.6050 1.2837 239.7771 238.4934 278.2065 33.4525 1.2814 240.0635 238.7821 278.1025 34.2288 1.2783 240.3396 239.0613 278.0663 35.0460 1.2794 240.6184 239.3390 278.0612 35.8525 1.2798 240.8677 239.5879 278.0783 36.6390 1.2797 241.0622 239.7825 278.1089 37.4768 1.2775 241.2999 240.0224 278.1818 38.2320 1.2757 241.5322 240.2566 278.2856 39.0903 1.2717 241.8161 240.5444 278.3949 39.8563 1.2648 242.0188 240.7540 278.5381 40.6935 1.2646 242.2414 240.9768 278.7469 41.4800 1.2663 242.4820 241.2157 278.9570 42.2768 1.2637 242.7340 241.4703 279.2241 43.1040 1.2668 242.9970 241.7302 279.5170 43.8700 1.2661 243.2463 241.9802 279.8024 44.7280 1.2671 243.5011 242.2339 280.1811 45.4938 1.2649 243.7405 242.4757 280.5130 46.3213 1.2588 243.9980 242.7391 280.8838 47.1178 1.2576 244.2225 242.9649 281.2395 47.9143 1.2508 244.4546 243.2038 281.6111 48.7315 1.2489 244.6863 243.4374 282.0098 49.5075 1.2485 244.9285 243.6800 282.3549 50.3245 1.2447 245.1570 243.9123 282.7179 51.0908 1.2407 245.3692 244.1285 283.0266 51.9485 1.2343 245.6016 244.3673 283.3594 52.7145 1.2342 245.8281 244.5938 283.6713 53.5420 1.2348 246.0829 244.8481 283.9641 54.3280 1.2314 246.3378 245.1064 284.2269 55.1353 1.2272 246.5981 245.3709 284.4379 55.9523 1.2263 246.8130 245.5867 284.6070 56.7180 1.2221 247.0574 245.8353 284.7730 57.5765 1.2156 247.2877 246.0721 284.9162 58.3420 1.2130 247.4867 246.2738 285.0068 59.1695 1.2073 247.7305 246.5232 285.0531 59.9560 1.2019 247.9727 246.7708 285.0689 60.7625 1.1981 248.2215 247.0234 285.0800 61.5800 1.1884 248.4779 247.2895 285.0495 62.3458 1.1805 248.7238 247.5432 285.0126 63.2040 1.1765 248.9770 247.8005 284.9367 63.9393 1.1741 249.2240 248.0499 284.8807 64.7970 1.1758 249.4793 248.3035 284.7854 65.5630 1.1751 249.7082 248.5330 284.7068 66.3905 1.1753 249.9428 248.7675 284.6402 67.1868 1.1712 250.1699 248.9988 284.5340 67.9835 1.1679 250.4099 249.2420 284.4160 68.8008 1.1634 250.6452 249.4819 284.3193 69.5768 1.1548 250.8693 249.7144 284.2095 70.4248 1.1544 251.1229 249.9685 284.1465 71.2008 1.1535 251.3548 250.2014 284.0941 72.0178 1.1508 251.5827 250.4319 284.0804 72.8248 1.1486 251.7931 250.6445 284.1012 73.6213 1.1442 252.0219 250.8778 284.1567 74.4485 1.1404 252.2520 251.1115 284.2182 75.2043 1.1415 252.4468 251.3053 284.3064 76.0725 1.1354 252.6990 251.5636 284.4595 76.8280 1.1340 252.8984 251.7644 284.6408 77.6660 1.1307 253.1132 251.9824 284.8586 78.4520 1.1266 253.3250 252.1984 285.1303 79.2590 1.1208 253.5276 252.4068 285.3824 80.0763 1.1150 253.7307 252.6157 285.6847 80.8418 1.1103 253.9349 252.8246 286.0001 81.6693 1.1086 254.1884 253.0799 286.3526 82.4250 1.1091 254.4156 253.3064 286.7062 83.2725 1.1068 254.6630 253.5561 287.1204 84.0490 1.1027 254.8703 253.7675 287.5194 84.8660 1.0954 255.0971 254.0017 287.9259 85.6625 1.0900 255.3400 254.2500 288.3308 86.4593 1.0833 255.5871 254.5037 288.7314 87.2865 1.0791 255.8139 254.7347 289.1367 88.0520 1.0744 255.9989 254.9244 289.4859 88.8693 1.0662 256.1931 255.1269 289.7849 89.6455 1.0626 256.3914 255.3288 290.0713 90.4930 1.0611 256.6468 255.5856 290.2930 91.2590 1.0574 256.8786 255.8211 290.5006 92.0865 1.0530 257.0857 256.0327 290.7239 92.8828 1.0459 257.3179 256.2721 290.8957 93.6795 1.0429 257.5355 256.4926 291.0371 94.4968 1.0384 257.7382 256.6998 291.1120 95.2725 1.0341 257.9698 256.9356 291.1699 96.0898 1.0354 258.1753 257.1399 291.2178 96.8558 1.0339 258.4202 257.3863 291.2543 97.7135 1.0258 258.6337 257.6080 291.2490 98.4793 1.0202 258.8547 257.8345 291.2052 99.3070 1.0181 259.0959 258.0778 291.1386 100.0930 1.0148 259.3061 258.2914 291.0716 100.9003 1.0088 259.5073 258.4985 290.9597 101.7275 1.0053 259.7313 258.7260 290.8367 102.4933 1.0031 259.9557 258.9526 290.7263 103.3413 0.9967 260.1607 259.1639 290.5895 104.1173 0.9915 260.4006 259.4091 290.4782 104.9345 0.9866 260.6046 259.6181 290.3735 105.7313 0.9827 260.8005 259.8178 290.2931 106.5275 0.9772 260.9848 260.0076 290.2098 107.3553 0.9714 261.2055 260.2341 290.1460 108.1210 0.9678 261.4373 260.4696 290.1070 108.9793 0.9641 261.6630 260.6989 290.1075 109.7453 0.9603 261.8507 260.8904 290.1199 110.5725 0.9605 262.0718 261.1113 290.1595 111.3693 0.9610 262.2937 261.3327 290.2433 112.1555 0.9566 262.4853 261.5287 290.3589 112.9930 0.9523 262.6388 261.6865 290.5106 113.7490 0.9483 262.8406 261.8924 290.7258 114.5965 0.9445 263.0361 262.0916 290.9666 115.3730 0.9397 263.2348 262.2951 291.2451 116.1900 0.9359 263.4183 262.4824 291.5478 116.9763 0.9322 263.6106 262.6783 291.8929 117.7830 0.9262 263.8402 262.9139 292.2459 118.5695 0.9220 264.0729 263.1509 292.6331 119.3660 0.9164 264.2632 263.3468 293.0315 120.1935 0.9116 264.4908 263.5793 293.4639 120.9490 0.9076 264.6901 263.7824 293.8747 121.8068 0.9016 264.9152 264.0136 294.3191 122.5728 0.8968 265.1508 264.2540 294.6893 123.4003 0.8933 265.3675 264.4742 295.0981 124.1968 0.8843 265.5578 264.6735 295.4754 124.9833 0.8782 265.7590 264.8808 295.8031 125.8003 0.8754 265.9375 265.0621 296.1170 126.6173 0.8763 266.1330 265.2567 296.3854 127.4140 0.8694 266.3518 265.4824 296.6126 128.2105 0.8640 266.5650 265.7010 296.8593 129.0378 0.8621 266.7923 265.9302 297.0438 129.8040 0.8593 266.9878 266.1285 297.1459 130.6515 0.8559 267.1961 266.3402 297.2376 131.4278 0.8536 267.3893 266.5357 297.2971 132.2450 0.8477 267.6167 266.7690 297.3238 133.0515 0.8400 267.8439 267.0039 297.2920 133.8380 0.8342 268.0298 267.1956 297.2791 134.6450 0.8270 268.2339 267.4069 297.2339 135.4413 0.8252 268.4447 267.6195 297.1534 136.2585 0.8225 268.6327 267.8102 297.0699 137.0655 0.8205 268.8090 267.9885 296.9598 137.8518 0.8185 269.0119 268.1934 296.8667 138.6485 0.8113 269.2208 268.4095 296.7931 139.5065 0.8047 269.4578 268.6531 296.6808 140.2520 0.7980 269.6435 268.8455 296.5677 141.1000 0.7964 269.8501 269.0537 296.4915 141.8655 0.7940 270.0330 269.2390 296.4071 142.6933 0.7866 270.2622 269.4756 296.3519 143.4898 0.7831 270.4659 269.6828 296.2671 144.2863 0.7788 270.6770 269.8981 296.1694 145.1035 0.7718 270.8810 270.1092 296.1142 145.8795 0.7652 271.0743 270.3090 296.1141 146.7275 0.7637 271.2672 270.5035 296.1439 147.4935 0.7588 271.4599 270.7011 296.2306 148.3205 0.7589 271.6751 270.9163 296.3415 149.1070 0.7603 271.8704 271.1101 296.4841 149.9038 0.7534 272.0530 271.2996 296.7204 150.7310 0.7446 272.2407 271.4960 296.9303 151.4970 0.7459 272.4307 271.6848 297.1580 152.3550 0.7438 272.6319 271.8881 297.4525 153.1105 0.7403 272.8139 272.0737 297.7743 153.9380 0.7369 272.9939 272.2570 298.1535 154.7345 0.7359 273.1791 272.4432 298.5283 155.5210 0.7325 273.3894 272.6569 298.9396 156.3588 0.7306 273.6175 272.8869 299.3732 157.1243 0.7267 273.7773 273.0506 299.7656 157.9823 0.7210 273.9811 273.2602 300.2003 158.7380 0.7146 274.1616 273.4470 300.5956 159.5755 0.7133 274.3844 273.6711 301.0407 160.3620 0.7088 274.5716 273.8628 301.4029 161.1588 0.7030 274.7252 274.0222 301.7527 161.9858 0.6950 274.9317 274.2367 302.0908 162.7623 0.6887 275.1105 274.4218 302.3603 163.6100 0.6844 275.3124 274.6280 302.6289 164.3758 0.6784 275.4759 274.7976 302.8112 165.2033 0.6722 275.6499 274.9777 302.9999 165.9998 0.6676 275.8360 275.1684 303.1719 166.7965 0.6626 276.0245 275.3619 303.3146 167.6138 0.6581 276.2630 275.6048 303.3956 168.3895 0.6570 276.4713 275.8144 303.4555 169.2375 0.6494 276.6546 276.0053 303.4640 170.0138 0.6394 276.8286 276.1892 303.4672 170.8305 0.6372 277.0319 276.3947 303.4516 171.6375 0.6334 277.2431 276.6098 303.3952 172.4240 0.6313 277.4203 276.7890 303.3359 173.2615 0.6236 277.5988 276.9752 303.2433 174.0173 0.6208 277.7621 277.1414 303.1242 174.8855 0.6136 277.9844 277.3709 302.9860 175.6410 0.6086 278.1662 277.5576 302.8746 176.4788 0.6067 278.3675 277.7609 302.7510 177.2343 0.6010 278.5485 277.9475 302.6277 178.0615 0.6006 278.7460 278.1454 302.5032 178.8583 0.6001 278.9293 278.3292 302.3903 179.6445 0.5947 279.0958 278.5011 302.3143 180.4720 0.5907 279.3089 278.7182 302.2626 181.2380 0.5873 279.4841 278.8968 302.2025 182.0858 0.5849 279.6814 279.0966 302.1536 182.8313 0.5840 279.8633 279.2792 302.1606 183.6790 0.5808 280.0684 279.4876 302.2369 184.4448 0.5800 280.2362 279.6562 302.3278 185.2723 0.5780 280.4228 279.8448 302.4680 186.0688 0.5775 280.6066 280.0291 302.6497 186.8653 0.5730 280.8152 280.2422 302.8397 187.6825 0.5730 281.0246 280.4516 303.0931 188.4585 0.5717 281.2004 280.6287 303.4195 189.2758 0.5658 281.3722 280.8064 303.6894 190.0418 0.5634 281.5411 280.9777 303.9736 190.8995 0.5582 281.6793 281.1211 304.3955 191.6655 0.5554 281.8468 281.2914 304.7820 192.4930 0.5518 282.0793 281.5275 305.2148 193.2793 0.5495 282.2474 281.6979 305.6671 194.0863 0.5463 282.4442 281.8978 306.1253 194.9135 0.5376 282.6304 282.0928 306.5362 195.6790 0.5375 282.7780 282.2405 306.9020 196.4963 0.5356 282.9689 282.4333 307.3225 197.2930 0.5303 283.1432 282.6129 307.6883 198.0998 0.5228 283.3486 282.8257 308.0246 198.8965 0.5163 283.5399 283.0236 308.2972 199.7238 0.5085 283.7289 283.2204 308.5644 200.4895 0.5033 283.9030 283.3997 308.7748 201.3478 0.4945 284.1159 283.6214 308.9926 202.1135 0.4919 284.3238 283.8320 309.1329 202.9408 0.4882 284.5208 284.0326 309.2749 203.7068 0.4837 284.7043 284.2206 309.3598 204.5340 0.4779 284.8419 284.3641 309.3859 205.3305 0.4752 285.0014 284.5261 309.4383 206.1273 0.4737 285.2100 284.7364 309.4557 206.9545 0.4733 285.4306 284.9573 309.4368 207.7203 0.4714 285.5939 285.1225 309.3857 208.5683 0.4705 285.7738 285.3033 309.2958 209.3443 0.4646 285.9571 285.4926 309.2405 210.1613 0.4573 286.0945 285.6372 309.1639 210.9580 0.4506 286.2252 285.7746 309.0738 211.7545 0.4454 286.4038 285.9584 308.9762 212.5408 0.4464 286.6239 286.1775 308.8640 213.3375 0.4448 286.8220 286.3773 308.7464 214.1648 0.4399 286.9948 286.5549 308.6237 214.9308 0.4356 287.1470 286.7114 308.5157 215.7890 0.4305 287.3279 286.8974 308.4060 216.5443 0.4293 287.5127 287.0834 308.2943 217.3718 0.4251 287.6852 287.2602 308.2188 218.1480 0.4237 287.8458 287.4221 308.1657 218.9753 0.4216 288.0298 287.6082 308.1573 219.7618 0.4210 288.1979 287.7770 308.1868 220.5685 0.4151 288.4087 287.9936 308.2490 221.3858 0.4093 288.5833 288.1739 308.3866 222.1518 0.4062 288.7582 288.3520 308.5511 223.0098 0.4033 288.9514 288.5482 308.7761 223.7760 0.4015 289.1103 288.7088 309.0200 224.6030 0.4001 289.2946 288.8946 309.3354 225.3895 0.3970 289.4712 289.0743 309.6469 226.1965 0.3891 289.6471 289.2580 309.9476 227.0133 0.3796 289.8365 289.4569 310.3424 227.8000 0.3808 290.0439 289.6631 310.7323 228.6068 0.3748 290.2208 289.8459 311.1499 229.4033 0.3673 290.3599 289.9926 311.6066 230.2205 0.3668 290.5350 290.1681 312.0305 230.9965 0.3631 290.7080 290.3449 312.4141 231.8443 0.3583 290.8809 290.5226 312.8448 232.6205 0.3547 291.0479 290.6932 313.2418 233.4375 0.3532 291.2349 290.8817 313.6296 234.2443 0.3496 291.4128 291.0633 313.9402 235.0308 0.3469 291.5580 291.2111 314.2292 235.8683 0.3419 291.7377 291.3958 314.5381 236.6238 0.3349 291.9302 291.5954 314.7832 237.4923 0.3302 292.1344 291.8042 315.0562 238.2273 0.3304 292.2765 291.9461 315.2236 239.1060 0.3266 292.4922 292.1656 315.3878 239.8618 0.3236 292.6516 292.3280 315.4504 240.6990 0.3210 292.8118 292.4909 315.5131 241.4550 0.3183 292.9964 292.6781 315.5455 242.2925 0.3130 293.1791 292.8661 315.5799 243.0788 0.3091 293.3464 293.0372 315.5655 243.8653 0.3047 293.5367 293.2319 315.4850 244.6925 0.2980 293.7591 293.4612 315.4327 245.4583 0.2930 293.9204 293.6274 315.3768 246.3063 0.2857 294.0881 293.8024 315.2867 247.0720 0.2828 294.2625 293.9797 315.1821 247.8993 0.2810 294.4522 294.1712 315.0572 248.6858 0.2770 294.6170 294.3400 314.9232 249.4925 0.2727 294.7978 294.5250 314.7689 250.3095 0.2730 294.9895 294.7165 314.6107 251.0755 0.2685 295.1443 294.8758 314.4845 251.9335 0.2633 295.3218 295.0585 314.3921 252.6993 0.2629 295.4575 295.1946 314.3248 253.5268 0.2620 295.6426 295.3807 314.2340 254.3130 0.2599 295.8093 295.5494 314.1742 255.1198 0.2582 295.9933 295.7351 314.1858 255.9370 0.2556 296.1554 295.8998 314.2105 256.7028 0.2518 296.3229 296.0711 314.2715 257.5610 0.2521 296.4718 296.2197 314.3933 258.3270 0.2499 296.6360 296.3861 314.5130 259.1540 0.2463 296.7990 296.5528 314.7126 259.9408 0.2425 296.9745 296.7320 314.9804 260.7475 0.2429 297.1572 296.9143 315.2540 261.5648 0.2449 297.3237 297.0788 315.5863 262.3410 0.2436 297.5295 297.2858 315.9371 263.1885 0.2388 297.7054 297.4665 316.3279 263.9650 0.2325 297.8620 297.6294 316.7052 264.7820 0.2314 298.0376 297.8063 317.1150 265.5478 0.2251 298.2193 297.9941 317.5238 266.3755 0.2205 298.3995 298.1791 317.9629 267.1820 0.2169 298.5711 298.3542 318.3759 267.9685 0.2138 298.7220 298.5083 318.7416 268.7960 0.2092 298.8770 298.6679 319.1716 269.5615 0.2096 299.0243 298.8148 319.5482 270.4198 0.2056 299.2359 299.0303 319.9280 271.1858 0.2057 299.4277 299.2219 320.2429 272.0025 0.2006 299.6038 299.4032 320.5758 272.8098 0.1926 299.7646 299.5719 320.8271 273.5960 0.1878 299.9247 299.7369 321.0557 274.4233 0.1844 300.0737 299.8893 321.2177 275.1895 0.1786 300.2424 300.0638 321.3685 276.0473 0.1746 300.4111 300.2366 321.4669 276.8028 0.1656 300.5611 300.3955 321.5087 277.6303 0.1608 300.7396 300.5788 321.5707 278.4268 0.1598 300.9051 300.7452 321.5440 279.2233 0.1553 301.0592 300.9039 321.5373 280.0405 0.1490 301.2204 301.0714 321.5015 280.8165 0.1505 301.3917 301.2412 321.4551 281.6643 0.1446 301.5594 301.4148 321.4051 282.3995 0.1427 301.7108 301.5680 321.3164 283.2575 0.1429 301.9149 301.7720 321.1684 284.0233 0.1387 302.1074 301.9687 321.0432 284.8508 0.1377 302.2692 302.1316 320.9069 285.6370 0.1319 302.4344 302.3025 320.7976 286.4438 0.1316 302.6092 302.4775 320.6687 287.2610 0.1307 302.7978 302.6671 320.5272 288.0268 0.1291 302.9743 302.8452 320.4178 288.8848 0.1277 303.1589 303.0312 320.3198 289.6510 0.1280 303.3088 303.1808 320.2698 290.4780 0.1232 303.4860 303.3627 320.2477 291.2645 0.1184 303.6285 303.5101 320.2614 292.0715 0.1174 303.8048 303.6874 320.2940 292.8985 0.1185 303.9823 303.8638 320.3655 293.6648 0.1164 304.1369 304.0205 320.4453 294.5125 0.1098 304.2855 304.1757 320.5944 295.2885 0.1016 304.4722 304.3706 320.7826 296.1058 0.0981 304.6383 304.5402 321.0068 296.8715 0.0978 304.7747 304.6769 321.2773 297.6988 0.0978 304.9330 304.8352 321.6008 298.5058 0.0940 305.1258 305.0318 321.9185 299.2920 0.0918 305.2867 305.1949 322.2430 300.1193 0.0886 305.4628 305.3743 322.6645 300.8855 0.0867 305.6442 305.5575 323.0411 301.7433 0.0836 305.8091 305.7254 323.5024 302.5093 0.0833 305.9639 305.8806 323.9051 303.3265 0.0834 306.1562 306.0728 324.3520 304.1333 0.0791 306.3371 306.2579 324.7705 304.9198 0.0746 306.5070 306.4324 325.1553 305.7573 0.0724 306.6644 306.5920 325.5285 306.5128 0.0725 306.8197 306.7473 325.8435 307.3713 0.0684 306.9887 306.9203 326.1575 308.1265 0.0643 307.1207 307.0564 326.4252 308.9540 0.0587 307.2562 307.1976 326.6878 309.7200 0.0520 307.4417 307.3897 326.8615 310.5473 0.0502 307.6389 307.5887 327.0353 311.3338 0.0473 307.8149 307.7676 327.1921 312.1303 0.0416 307.9857 307.9441 327.3314 312.9575 0.0325 308.1402 308.1077 327.4249 313.7133 0.0304 308.2930 308.2627 327.4864 314.5815 0.0248 308.4721 308.4473 327.5143 315.3373 0.0190 308.6359 308.6170 327.5263 316.1648 0.0165 308.7982 308.7817 327.4805 316.9610 0.0137 308.9832 308.9695 327.3734 317.7578 0.0109 309.1680 309.1571 327.3081 318.5545 0.0102 309.3234 309.3132 327.2243 319.3405 0.0087 309.4673 309.4586 327.1336 320.2090 0.0075 309.6283 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