DTA measure 1meres Date: 2025916:1533 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.26 s Mass = 967.7 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2198 -0.8997 250.2131 251.1128 272.7398 2.0373 -0.8957 250.3807 251.2763 272.6330 2.8130 -0.8930 250.5939 251.4869 272.5431 3.6610 -0.8893 250.8404 251.7297 272.4356 4.4373 -0.8814 251.0261 251.9075 272.3428 5.2540 -0.8766 251.2586 252.1352 272.2888 6.0510 -0.8724 251.4385 252.3109 272.2554 6.8475 -0.8682 251.6251 252.4934 272.2202 7.6748 -0.8653 251.7939 252.6592 272.2326 8.4408 -0.8614 251.9499 252.8114 272.2973 9.2885 -0.8557 252.1234 252.9791 272.3710 10.0645 -0.8496 252.2871 253.1366 272.4702 10.8820 -0.8455 252.4982 253.3438 272.6039 11.6885 -0.8432 252.6648 253.5080 272.7661 12.4750 -0.8414 252.8324 253.6737 272.9627 13.2820 -0.8374 253.0030 253.8404 273.2162 14.0680 -0.8338 253.1661 253.9999 273.4546 14.9058 -0.8283 253.3681 254.1964 273.7758 15.6615 -0.8301 253.5349 254.3650 274.0871 16.5295 -0.8329 253.6945 254.5274 274.4869 17.2853 -0.8297 253.8310 254.6608 274.8302 18.1128 -0.8286 254.0070 254.8357 275.2066 18.9093 -0.8266 254.1784 255.0050 275.5938 19.7060 -0.8261 254.3541 255.1803 275.9858 20.5640 -0.8303 254.5547 255.3850 276.4013 21.2888 -0.8289 254.7222 255.5511 276.7548 22.1575 -0.8284 254.8928 255.7213 277.1843 22.9438 -0.8267 255.0626 255.8893 277.5705 23.7405 -0.8302 255.2216 256.0518 277.9078 24.5678 -0.8327 255.3952 256.2279 278.2339 25.3440 -0.8349 255.5585 256.3934 278.5172 26.1613 -0.8334 255.7270 256.5604 278.7863 26.9270 -0.8318 255.8871 256.7189 279.0011 27.7855 -0.8353 256.0552 256.8906 279.2323 28.5818 -0.8378 256.2500 257.0878 279.4350 29.3785 -0.8376 256.4329 257.2705 279.5785 30.1753 -0.8396 256.5977 257.4373 279.7125 30.9718 -0.8455 256.7574 257.6028 279.8172 31.7993 -0.8455 256.9664 257.8119 279.8797 32.5650 -0.8514 257.1463 257.9977 279.8904 33.4128 -0.8528 257.3752 258.2280 279.9071 34.1890 -0.8564 257.5418 258.3982 279.8696 35.0060 -0.8553 257.7163 258.5716 279.8608 35.8435 -0.8538 257.8837 258.7375 279.8075 36.5993 -0.8573 258.0278 258.8851 279.7370 37.4368 -0.8594 258.2104 259.0698 279.6865 38.1925 -0.8576 258.3472 259.2048 279.6219 39.0608 -0.8567 258.5544 259.4111 279.5418 39.8163 -0.8590 258.7137 259.5726 279.4601 40.6540 -0.8595 258.9158 259.7753 279.3523 41.4508 -0.8574 259.1017 259.9590 279.2302 42.2470 -0.8514 259.2653 260.1167 279.1370 43.0643 -0.8505 259.4369 260.2874 279.0610 43.8200 -0.8536 259.6019 260.4555 279.0483 44.6675 -0.8554 259.7920 260.6474 279.0073 45.4028 -0.8524 259.9419 260.7942 278.9735 46.2405 -0.8509 260.0955 260.9464 278.9429 47.0063 -0.8507 260.2561 261.1068 278.9621 47.8238 -0.8488 260.4508 261.2996 278.9873 48.6200 -0.8498 260.6372 261.4869 279.0385 49.4065 -0.8492 260.8120 261.6611 279.1303 50.2033 -0.8472 260.9425 261.7897 279.2876 50.9995 -0.8440 261.0986 261.9425 279.4503 51.8170 -0.8422 261.2977 262.1399 279.6414 52.5725 -0.8453 261.4621 262.3074 279.8813 53.4408 -0.8472 261.6293 262.4765 280.1610 54.1965 -0.8479 261.8072 262.6551 280.4207 55.0135 -0.8476 261.9973 262.8449 280.6970 55.8205 -0.8519 262.1383 262.9902 281.0357 56.6068 -0.8564 262.2907 263.1471 281.3904 57.4238 -0.8595 262.4840 263.3436 281.7509 58.1998 -0.8624 262.6457 263.5081 282.1021 59.0478 -0.8677 262.8333 263.7010 282.4529 59.8135 -0.8665 263.0024 263.8689 282.8040 60.6410 -0.8666 263.1522 264.0188 283.1354 61.4378 -0.8697 263.3118 264.1815 283.5025 62.2340 -0.8741 263.4709 264.3450 283.8426 63.0513 -0.8799 263.6319 264.5117 284.1716 63.8275 -0.8833 263.7680 264.6513 284.4336 64.6750 -0.8855 263.8737 264.7592 284.7261 65.4413 -0.8908 264.0396 264.9304 284.9637 66.2685 -0.8929 264.2222 265.1151 285.1704 67.0445 -0.8950 264.3879 265.2830 285.3789 67.8615 -0.8980 264.5599 265.4580 285.5756 68.6583 -0.8995 264.7253 265.6248 285.7437 69.4545 -0.9050 264.8779 265.7829 285.8927 70.2820 -0.9078 265.0539 265.9616 285.9789 71.0480 -0.9094 265.1863 266.0957 286.0677 71.9058 -0.9146 265.3993 266.3138 286.1362 72.6718 -0.9182 265.5995 266.5177 286.1770 73.4993 -0.9220 265.7590 266.6810 286.1597 74.2958 -0.9244 265.9349 266.8593 286.1513 75.0825 -0.9269 266.1200 267.0468 286.1293 75.9198 -0.9284 266.3063 267.2347 286.0713 76.6755 -0.9325 266.4402 267.3727 286.0529 77.5440 -0.9351 266.6098 267.5449 286.0048 78.2993 -0.9364 266.7592 267.6956 285.9529 79.1370 -0.9431 266.9433 267.8864 285.8673 79.9133 -0.9447 267.0893 268.0340 285.8032 80.7303 -0.9481 267.2498 268.1978 285.7140 81.5273 -0.9516 267.4362 268.3877 285.6457 82.3235 -0.9537 267.5954 268.5491 285.6337 83.1510 -0.9550 267.7237 268.6788 285.5939 83.9170 -0.9555 267.8564 268.8119 285.5915 84.7750 -0.9530 268.0146 268.9676 285.5867 85.5410 -0.9557 268.1291 269.0848 285.5673 86.3683 -0.9562 268.2776 269.2337 285.5986 87.1648 -0.9562 268.4043 269.3605 285.6626 87.9515 -0.9588 268.5769 269.5357 285.7460 88.7580 -0.9625 268.7523 269.7148 285.8532 89.5445 -0.9630 268.9481 269.9112 285.9879 90.3823 -0.9606 269.1466 270.1071 286.1989 91.1378 -0.9614 269.3097 270.2711 286.3945 92.0060 -0.9636 269.4789 270.4425 286.6182 92.7618 -0.9654 269.6254 270.5908 286.8268 93.5993 -0.9705 269.7938 270.7643 287.1101 94.3858 -0.9753 269.9431 270.9183 287.3974 95.1925 -0.9793 270.0776 271.0569 287.6978 96.0095 -0.9783 270.2413 271.2196 288.0473 96.7755 -0.9818 270.3765 271.3583 288.3892 97.6335 -0.9850 270.5211 271.5062 288.7645 98.4095 -0.9866 270.6708 271.6573 289.0804 99.2268 -0.9943 270.8372 271.8314 289.4092 100.0233 -0.9989 271.0043 272.0033 289.7451 100.8198 -1.0040 271.1577 272.1617 290.0439 101.6473 -1.0118 271.3088 272.3206 290.3707 102.4130 -1.0182 271.4143 272.4324 290.6359 103.2710 -1.0249 271.5909 272.6158 290.9230 104.0063 -1.0302 271.7382 272.7684 291.1490 104.8643 -1.0336 271.9018 272.9354 291.4089 105.6303 -1.0391 272.0716 273.1108 291.5997 106.4578 -1.0456 272.2597 273.3052 291.7882 107.2540 -1.0560 272.4081 273.4641 291.9432 108.0508 -1.0594 272.5749 273.6344 292.0731 108.8578 -1.0638 272.7612 273.8249 292.1835 109.6233 -1.0677 272.8911 273.9587 292.2803 110.4713 -1.0675 273.0536 274.1211 292.3512 111.2373 -1.0698 273.2006 274.2703 292.4009 112.0543 -1.0731 273.3660 274.4392 292.4361 112.8513 -1.0741 273.5053 274.5794 292.4461 113.6475 -1.0784 273.6634 274.7418 292.4166 114.4340 -1.0803 273.8204 274.9008 292.3912 115.2205 -1.0819 273.9719 275.0538 292.3333 116.0580 -1.0855 274.1430 275.2286 292.2998 116.8138 -1.0864 274.3062 275.3926 292.2891 117.6615 -1.0903 274.4664 275.5567 292.2401 118.4378 -1.0938 274.6222 275.7160 292.2155 119.2550 -1.0976 274.7715 275.8691 292.1651 120.0513 -1.1013 274.9199 276.0212 292.1180 120.8480 -1.1035 275.0683 276.1719 292.0761 121.6755 -1.1065 275.2083 276.3148 292.0413 122.4410 -1.1092 275.3473 276.4565 292.0472 123.2890 -1.1093 275.5129 276.6221 292.0608 124.0653 -1.1076 275.6489 276.7565 292.1047 124.8820 -1.1063 275.8437 276.9501 292.1596 125.6788 -1.1073 276.0170 277.1243 292.2471 126.4755 -1.1123 276.1497 277.2621 292.3329 127.3025 -1.1154 276.3043 277.4197 292.4429 128.0685 -1.1173 276.4696 277.5869 292.5876 128.9165 -1.1197 276.6405 277.7602 292.7316 129.6923 -1.1233 276.7746 277.8979 292.8737 130.5095 -1.1279 276.9176 278.0455 293.0756 131.3063 -1.1318 277.0829 278.2147 293.2995 132.1028 -1.1333 277.2438 278.3771 293.5104 132.9403 -1.1381 277.4185 278.5566 293.8046 133.6960 -1.1417 277.5771 278.7188 294.0570 134.5540 -1.1464 277.7717 278.9181 294.3792 135.3200 -1.1492 277.8718 279.0210 294.7221 136.1473 -1.1537 277.9993 279.1530 295.0595 136.9438 -1.1577 278.1589 279.3166 295.3730 137.7303 -1.1590 278.3276 279.4866 295.6739 138.5678 -1.1634 278.4623 279.6257 296.0207 139.3335 -1.1684 278.5834 279.7518 296.3105 140.1918 -1.1707 278.7495 279.9203 296.5778 140.9473 -1.1730 278.8770 280.0499 296.8292 141.7745 -1.1785 279.0328 280.2113 297.0961 142.5713 -1.1832 279.1799 280.3631 297.3648 143.3575 -1.1869 279.3727 280.5596 297.6030 144.1850 -1.1881 279.5356 280.7237 297.8387 144.9510 -1.1898 279.6919 280.8817 297.9998 145.7985 -1.1962 279.8610 281.0572 298.1409 146.5440 -1.2009 280.0091 281.2100 298.3090 147.3918 -1.2095 280.1963 281.4057 298.4403 148.1575 -1.2142 280.3324 281.5465 298.5501 148.9850 -1.2178 280.5057 281.7235 298.6401 149.7815 -1.2231 280.6733 281.8964 298.7133 150.5780 -1.2295 280.8105 282.0400 298.7299 151.3950 -1.2316 280.9457 282.1774 298.7461 152.1713 -1.2362 281.1048 282.3411 298.7650 153.0190 -1.2439 281.2674 282.5112 298.7358 153.7848 -1.2478 281.4065 282.6544 298.7154 154.6123 -1.2510 281.5731 282.8241 298.6862 155.4088 -1.2547 281.7274 282.9821 298.6864 156.2053 -1.2566 281.8734 283.1299 298.6336 157.0223 -1.2591 282.0258 283.2849 298.5892 157.7985 -1.2603 282.1407 283.4010 298.5358 158.6463 -1.2670 282.3052 283.5723 298.4528 159.4228 -1.2718 282.4779 283.7497 298.4523 160.2395 -1.2710 282.6391 283.9101 298.4461 161.0465 -1.2759 282.8155 284.0914 298.4596 161.8330 -1.2757 282.9554 284.2311 298.5001 162.6600 -1.2772 283.1042 284.3814 298.5708 163.4260 -1.2793 283.2212 284.5005 298.6369 164.2945 -1.2787 283.3817 284.6604 298.7228 165.0500 -1.2809 283.5330 284.8138 298.7983 165.8775 -1.2802 283.6841 284.9643 298.9358 166.6740 -1.2834 283.8417 285.1251 299.0986 167.4705 -1.2868 283.9965 285.2833 299.2617 168.2980 -1.2846 284.1670 285.4516 299.4518 169.0638 -1.2845 284.3120 285.5965 299.6297 169.9220 -1.2880 284.4731 285.7611 299.8620 170.6983 -1.2924 284.6173 285.9097 300.1318 171.5153 -1.2979 284.7583 286.0562 300.3821 172.3120 -1.3006 284.8880 286.1885 300.6354 173.1085 -1.3021 285.0353 286.3374 300.8793 173.9258 -1.3076 285.1821 286.4896 301.1762 174.6918 -1.3081 285.3134 286.6216 301.4298 175.5495 -1.3090 285.4725 286.7815 301.6792 176.3053 -1.3150 285.6357 286.9506 301.9772 177.1328 -1.3211 285.8339 287.1549 302.2665 177.8983 -1.3235 285.9977 287.3212 302.5400 178.7155 -1.3279 286.1789 287.5068 302.8200 179.5123 -1.3335 286.3418 287.6753 303.0961 180.3085 -1.3402 286.4966 287.8368 303.3613 181.1360 -1.3447 286.6804 288.0251 303.6164 181.9020 -1.3469 286.8269 288.1738 303.8015 182.7498 -1.3543 286.9656 288.3199 303.9769 183.5260 -1.3597 287.0920 288.4517 304.1629 184.3430 -1.3628 287.2116 288.5744 304.3213 185.1395 -1.3688 287.3483 288.7171 304.4766 185.9363 -1.3715 287.5065 288.8780 304.5891 186.7635 -1.3746 287.6405 289.0151 304.7072 187.5293 -1.3791 287.8026 289.1817 304.8131 188.3465 -1.3872 287.9752 289.3623 304.8749 189.1225 -1.3873 288.0992 289.4865 304.9454 189.9808 -1.3937 288.2492 289.6429 305.0045 190.7468 -1.3993 288.3914 289.7907 305.0235 191.5635 -1.3985 288.5194 289.9180 305.0266 192.3705 -1.4033 288.6675 290.0708 305.0431 193.1673 -1.4051 288.8214 290.2265 305.0416 193.9635 -1.4077 288.9198 290.3275 305.0036 194.7500 -1.4094 289.0703 290.4797 304.9929 195.5878 -1.4100 289.2390 290.6490 304.9692 196.3533 -1.4122 289.3843 290.7964 304.9473 197.2115 -1.4149 289.5436 290.9585 304.9225 197.9673 -1.4174 289.6975 291.1149 304.9399 198.8045 -1.4236 289.8659 291.2894 304.9677 199.5913 -1.4262 290.0240 291.4501 304.9679 200.3980 -1.4324 290.2180 291.6505 304.9661 201.2153 -1.4343 290.3701 291.8043 304.9964 202.0015 -1.4332 290.4941 291.9273 305.0398 202.7980 -1.4349 290.6407 292.0756 305.1262 203.6050 -1.4327 290.7747 292.2074 305.2429 204.4325 -1.4292 290.9372 292.3663 305.3845 205.1880 -1.4308 291.0580 292.4888 305.5163 206.0463 -1.4310 291.2158 292.6468 305.6756 206.8018 -1.4319 291.3493 292.7811 305.7976 207.6293 -1.4353 291.5392 292.9744 305.9969 208.4260 -1.4348 291.7028 293.1376 306.2238 209.2223 -1.4364 291.8740 293.3104 306.4831 210.0090 -1.4395 292.0098 293.4492 306.7317 210.8055 -1.4411 292.1494 293.5905 307.0093 211.6328 -1.4482 292.2752 293.7233 307.2916 212.3988 -1.4496 292.4073 293.8569 307.5221 213.2465 -1.4541 292.5365 293.9906 307.8433 214.0225 -1.4566 292.6504 294.1070 308.1551 214.8398 -1.4621 292.8346 294.2968 308.4447 215.6363 -1.4679 293.0128 294.4807 308.7576 216.4328 -1.4712 293.1170 294.5883 309.0378 217.2600 -1.4765 293.2396 294.7161 309.3063 218.0260 -1.4765 293.3889 294.8655 309.5510 218.8735 -1.4825 293.5374 295.0199 309.8484 219.6498 -1.4870 293.6774 295.1644 310.0270 220.4670 -1.4921 293.8496 295.3417 310.2447 221.2635 -1.4978 294.0448 295.5426 310.4607 222.0603 -1.5035 294.2040 295.7075 310.6168 222.8568 -1.5069 294.3757 295.8826 310.7466 223.6840 -1.5094 294.5480 296.0573 310.8939 224.4808 -1.5116 294.6834 296.1950 311.0118 225.2875 -1.5207 294.8423 296.3629 311.1185 226.1045 -1.5266 294.9710 296.4976 311.1937 226.8705 -1.5263 295.1097 296.6361 311.2699 227.7285 -1.5298 295.2664 296.7962 311.3438 228.4945 -1.5322 295.4090 296.9412 311.3779 229.3220 -1.5294 295.5667 297.0961 311.3945 230.0773 -1.5360 295.7210 297.2569 311.3880 230.9150 -1.5426 295.8531 297.3957 311.3301 231.7118 -1.5467 296.0062 297.5529 311.3119 232.5080 -1.5465 296.1583 297.7048 311.2956 233.3355 -1.5511 296.3417 297.8928 311.2891 234.1220 -1.5543 296.4880 298.0423 311.2959 234.9490 -1.5572 296.6349 298.1921 311.2924 235.7153 -1.5608 296.7532 298.3140 311.2827 236.5733 -1.5648 296.8922 298.4570 311.2392 237.3288 -1.5668 296.9946 298.5613 311.2674 238.1563 -1.5664 297.1446 298.7110 311.3032 238.9528 -1.5690 297.3240 298.8929 311.3084 239.7495 -1.5676 297.5001 299.0676 311.3733 240.5665 -1.5678 297.6769 299.2447 311.4365 241.3425 -1.5736 297.8342 299.4078 311.5286 242.1903 -1.5828 297.9442 299.5270 311.6498 242.9155 -1.5831 298.1012 299.6843 311.7509 243.7835 -1.5848 298.2824 299.8672 311.8972 244.5493 -1.5868 298.4064 299.9932 312.0425 245.3668 -1.5904 298.5515 300.1418 312.2425 246.1630 -1.5920 298.6981 300.2901 312.4358 246.9598 -1.5894 298.8330 300.4224 312.7012 247.7873 -1.5864 298.9922 300.5785 312.9419 248.5428 -1.5915 299.1169 300.7084 313.1696 249.4113 -1.5933 299.2909 300.8843 313.4658 250.1668 -1.5923 299.4384 301.0307 313.7533 250.9940 -1.5945 299.5871 301.1816 314.0199 251.7908 -1.5993 299.7082 301.3074 314.2606 252.5873 -1.6003 299.8336 301.4340 314.5589 253.4145 -1.6003 299.9961 301.5964 314.8555 254.1805 -1.6026 300.1234 301.7260 315.1106 255.0385 -1.6055 300.2479 301.8533 315.4272 255.8045 -1.6089 300.3849 301.9938 315.7048 256.6320 -1.6180 300.5282 302.1463 315.9486 257.4183 -1.6223 300.6854 302.3078 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