DTA measure 2Gyors Date: 2026428:1052 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.32 s Mass = 1156.700 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2820 -3.6653 185.1215 188.7868 246.1898 2.1098 -3.6646 185.3773 189.0419 246.1531 2.8960 -3.6640 185.4068 189.0709 246.0537 3.7035 -3.6734 185.6163 189.2897 245.9897 4.5213 -3.6739 185.9955 189.6694 245.9971 5.2878 -3.6482 186.2686 189.9168 246.0271 6.1465 -3.6104 186.6625 190.2729 245.9340 6.9120 -3.6057 186.9424 190.5481 245.9097 7.7400 -3.6116 187.3426 190.9542 245.8982 8.5373 -3.6131 187.6294 191.2425 245.7943 9.3343 -3.6239 187.8663 191.4902 245.8909 10.1615 -3.6035 188.2025 191.8060 245.7853 10.9280 -3.5752 188.5392 192.1144 245.6197 11.7458 -3.5590 188.7720 192.3310 245.4576 12.5220 -3.5586 188.9760 192.5346 245.2721 13.3700 -3.5416 189.1067 192.6483 245.0167 14.1365 -3.5099 189.3018 192.8117 245.1932 14.9645 -3.5176 189.6201 193.1377 245.2942 15.7618 -3.5228 189.8919 193.4147 245.1454 16.5580 -3.5047 190.2071 193.7118 245.0477 17.3758 -3.4858 190.4465 193.9323 245.0114 18.1525 -3.4807 190.7655 194.2462 245.2247 19.0010 -3.4460 191.0348 194.4808 245.2275 19.7675 -3.4445 191.2687 194.7132 245.2540 20.5950 -3.4551 191.4256 194.8807 245.3884 21.3918 -3.4333 191.5464 194.9797 245.3974 22.1890 -3.4367 191.7778 195.2145 245.4204 23.0068 -3.4265 192.0984 195.5249 245.3038 23.7835 -3.3872 192.2962 195.6834 245.2819 24.6315 -3.3604 192.4547 195.8151 245.3852 25.3975 -3.3563 192.7637 196.1201 245.4114 26.2255 -3.3634 192.9770 196.3404 245.2315 27.0023 -3.3259 193.2646 196.5905 245.3093 27.8198 -3.3217 193.4779 196.7996 245.4140 28.6163 -3.3073 193.6543 196.9616 245.4512 29.4135 -3.3048 193.9636 197.2684 245.4347 30.2415 -3.2898 194.1670 197.4568 245.5488 31.0080 -3.2701 194.3965 197.6667 245.6338 31.8563 -3.2667 194.5825 197.8492 245.4895 32.6323 -3.2803 194.6829 197.9632 245.6943 33.4500 -3.2452 194.8036 198.0488 246.0805 34.2575 -3.2429 195.0235 198.2664 246.1716 35.0445 -3.2337 195.3732 198.6069 246.2680 35.8818 -3.2329 195.6571 198.8900 246.4848 36.6380 -3.2418 195.8460 199.0878 246.6262 37.4968 -3.2157 196.0465 199.2622 246.5084 38.2633 -3.2188 196.2658 199.4846 246.4669 39.0810 -3.2044 196.4821 199.6865 246.6205 39.8465 -3.1693 196.7089 199.8781 246.7458 40.6745 -3.1379 196.9650 200.1029 246.8754 41.4615 -3.1419 197.2205 200.3624 246.9242 42.2483 -3.1467 197.2807 200.4274 247.0637 43.0755 -3.1501 197.3739 200.5240 247.1393 43.8420 -3.1465 197.5140 200.6605 247.3255 44.6905 -3.1487 197.9463 201.0950 247.4735 45.4673 -3.1336 198.0725 201.2061 247.6095 46.2840 -3.1152 198.2002 201.3154 247.8326 47.0710 -3.1024 198.5238 201.6262 248.0070 47.8785 -3.1024 198.7675 201.8698 248.1578 48.6963 -3.0786 199.0553 202.1339 248.2530 49.4623 -3.0769 199.3322 202.4091 248.3245 50.2898 -3.0754 199.3803 202.4557 248.5913 51.0460 -3.0739 199.7121 202.7860 248.8129 51.9048 -3.0720 199.9980 203.0700 248.9993 52.6713 -3.0623 200.1727 203.2350 249.0815 53.4983 -3.0219 200.5054 203.5273 249.1619 54.2955 -3.0228 200.7894 203.8122 249.3514 55.0825 -3.0580 200.8025 203.8605 249.5335 55.9208 -3.0491 200.8956 203.9447 249.6458 56.6763 -3.0276 201.1853 204.2129 249.7464 57.5348 -3.0211 201.3311 204.3522 249.9658 58.3013 -3.0097 201.6206 204.6303 250.3762 59.1293 -2.9893 201.8402 204.8295 250.7085 59.9258 -2.9971 202.1073 205.1045 250.8458 60.7125 -2.9954 202.3146 205.3099 250.8347 61.5508 -2.9995 202.5324 205.5319 251.1189 62.3070 -2.9924 202.6612 205.6536 251.6151 63.1655 -2.9922 202.9097 205.9019 251.9159 63.9005 -2.9838 202.9788 205.9626 252.0059 64.7593 -2.9647 203.2167 206.1814 252.2856 65.5258 -2.9496 203.3561 206.3057 252.5520 66.3435 -2.9523 203.6829 206.6352 252.6112 67.1500 -2.9246 203.8521 206.7767 252.7068 67.9370 -2.9252 204.0464 206.9716 252.7731 68.7650 -2.9155 204.1734 207.0889 252.9815 69.5315 -2.8878 204.4367 207.3245 253.2338 70.3900 -2.9000 204.6602 207.5601 253.4385 71.1558 -2.8858 204.7960 207.6817 253.6972 71.9838 -2.8678 205.1207 207.9885 253.7432 72.7810 -2.8717 205.3877 208.2594 254.0123 73.5680 -2.8625 205.5401 208.4027 254.2372 74.3955 -2.8646 205.5907 208.4553 254.3900 75.1615 -2.8771 205.7512 208.6283 254.6707 76.0203 -2.8890 206.0825 208.9716 254.7156 76.8175 -2.8637 206.4251 209.2888 254.8900 77.6045 -2.8682 206.6174 209.4856 255.3148 78.4420 -2.8768 206.8719 209.7487 255.4427 79.1980 -2.8686 207.1493 210.0179 255.5365 80.0568 -2.8491 207.2711 210.1202 256.0357 80.8233 -2.8700 207.5638 210.4338 256.3256 81.6513 -2.8685 207.7997 210.6682 256.5416 82.4475 -2.8418 208.0405 210.8824 256.6397 83.2448 -2.8420 208.2327 211.0747 256.6985 84.0728 -2.8509 208.3997 211.2506 256.9517 84.8393 -2.8514 208.6856 211.5370 256.9964 85.6970 -2.8365 208.9609 211.7974 257.1867 86.4533 -2.8479 209.1799 212.0278 257.4068 87.2915 -2.8389 209.3427 212.1816 257.5505 88.0785 -2.8391 209.5694 212.4085 257.5313 88.8855 -2.8316 209.6021 212.4337 257.6682 89.7028 -2.8033 209.7554 212.5587 257.9288 90.4795 -2.7984 209.8997 212.6981 257.9505 91.2973 -2.8127 209.9860 212.7987 257.9872 92.0945 -2.8236 210.1976 213.0212 258.1359 92.9218 -2.8443 210.4565 213.3008 258.3629 93.6983 -2.8472 210.6474 213.4946 258.5715 94.5160 -2.8394 210.7862 213.6256 258.8325 95.3133 -2.8341 211.0193 213.8534 258.9163 96.1103 -2.8117 211.2268 214.0385 258.9141 96.9375 -2.8045 211.4566 214.2611 258.9316 97.7040 -2.8074 211.7514 214.5588 259.1318 98.5525 -2.7933 211.9535 214.7469 259.3474 99.3293 -2.7938 212.0919 214.8857 259.3913 100.1460 -2.7854 212.4862 215.2716 259.4358 100.9433 -2.7805 212.6185 215.3990 259.5289 101.7405 -2.7777 212.7506 215.5283 259.7951 102.5583 -2.7784 212.8562 215.6346 259.9021 103.3138 -2.7759 213.0229 215.7988 260.0177 104.1723 -2.7815 213.3799 216.1614 260.4112 104.9285 -2.7947 213.5594 216.3541 260.6578 105.7565 -2.8067 213.5629 216.3697 260.7945 106.5538 -2.7984 213.6853 216.4837 260.8542 107.3400 -2.7972 213.9578 216.7551 260.8804 108.1370 -2.8165 214.2960 217.1125 260.9995 108.9343 -2.8170 214.6124 217.4295 261.0308 109.7520 -2.8170 214.8789 217.6959 260.9759 110.5178 -2.8093 215.0756 217.8849 260.9443 111.3763 -2.8102 215.2675 218.0777 261.1850 112.1325 -2.7744 215.4922 218.2666 261.2059 112.9605 -2.7613 215.6870 218.4483 261.3407 113.7578 -2.7626 215.8896 218.6522 261.4826 114.5543 -2.7464 216.1280 218.8744 261.6814 115.3718 -2.7666 216.2711 219.0377 261.9363 116.1485 -2.7446 216.2269 218.9715 262.0598 116.9663 -2.7245 216.3582 219.0827 262.4015 117.7320 -2.7270 216.6292 219.3562 262.5036 118.5905 -2.7456 216.8864 219.6320 262.5554 119.3570 -2.7451 216.9778 219.7230 262.7504 120.1850 -2.7328 217.0623 219.7951 262.8643 120.9713 -2.7133 217.3282 220.0415 262.8661 121.7785 -2.7082 217.4913 220.1995 262.8647 122.5963 -2.7099 217.6916 220.4015 263.1216 123.3628 -2.6913 217.9140 220.6053 263.2417 124.1908 -2.6941 218.0924 220.7865 263.1138 124.9563 -2.6930 218.1987 220.8917 263.0913 125.8150 -2.7148 218.3367 221.0514 263.2824 126.5713 -2.6999 218.4500 221.1499 263.3555 127.4095 -2.6873 218.6432 221.3304 263.4393 128.1958 -2.6534 218.8608 221.5141 263.6279 129.0030 -2.6284 219.1290 221.7574 263.6813 129.8208 -2.6407 219.4441 222.0849 263.8134 130.5975 -2.6559 219.6736 222.3295 264.0519 131.4460 -2.6616 219.8371 222.4987 264.3963 132.1808 -2.6509 219.8194 222.4703 264.4469 133.0395 -2.6646 220.0310 222.6956 264.4072 133.8060 -2.6740 220.2403 222.9143 264.4915 134.6338 -2.6747 220.4066 223.0812 264.6071 135.4200 -2.6678 220.4826 223.1503 264.4858 136.2275 -2.6762 220.6578 223.3340 264.5343 137.0453 -2.6559 220.7317 223.3876 264.5863 137.8118 -2.6331 220.9379 223.5711 264.6749 138.6703 -2.6332 221.2983 223.9315 264.9018 139.4463 -2.6296 221.3543 223.9840 264.9856 140.2640 -2.6531 221.6400 224.2932 265.0383 141.0305 -2.6707 221.9045 224.5752 265.0930 141.8585 -2.6726 222.0168 224.6893 265.1365 142.6550 -2.6662 222.2434 224.9096 265.4661 143.4520 -2.6524 222.6791 225.3315 265.6460 144.2698 -2.6518 222.8598 225.5116 265.7865 145.0465 -2.6355 223.0036 225.6391 265.8113 145.8950 -2.6204 223.1253 225.7456 265.8064 146.6605 -2.6321 223.3586 225.9907 265.8207 147.4885 -2.6121 223.5979 226.2100 265.8197 148.2858 -2.5991 223.5457 226.1448 265.9400 149.0830 -2.6169 223.6494 226.2662 266.2079 149.9005 -2.6032 223.8660 226.4692 266.6250 150.6765 -2.5981 224.1587 226.7568 266.8782 151.5250 -2.6061 224.5031 227.1092 266.9952 152.2915 -2.5980 224.5999 227.1979 267.0802 153.1195 -2.5911 224.8365 227.4276 267.2565 153.9165 -2.5937 224.9799 227.5736 267.4167 154.7130 -2.5889 225.1232 227.7122 267.5870 155.5308 -2.6012 225.2437 227.8450 267.6538 156.3075 -2.5986 225.5306 228.1292 267.5727 157.1560 -2.5799 225.6121 228.1920 267.7316 157.9215 -2.5652 225.7394 228.3046 267.9321 158.7495 -2.5590 225.8963 228.4552 268.1089 159.5468 -2.5704 226.1078 228.6782 268.1112 160.3440 -2.5599 226.4117 228.9716 268.3489 161.1618 -2.5783 226.5507 229.1290 268.6529 161.9375 -2.5728 226.7606 229.3334 268.8999 162.7860 -2.5767 226.9438 229.5206 269.0503 163.5628 -2.5646 227.2082 229.7728 269.1138 164.3805 -2.5474 227.4341 229.9815 269.2113 165.1770 -2.5292 227.6249 230.1541 269.2489 165.9740 -2.5172 227.7965 230.3137 269.4165 166.7918 -2.5057 227.9738 230.4795 269.5684 167.5583 -2.5241 228.1124 230.6365 269.7545 168.4170 -2.5722 228.2704 230.8426 269.9163 169.1420 -2.5646 228.4263 230.9909 269.9283 170.0003 -2.5458 228.7297 231.2754 269.9998 170.7565 -2.5329 228.8381 231.3710 269.9878 171.5845 -2.5351 228.8336 231.3687 270.1786 172.3818 -2.5249 228.9260 231.4509 270.4167 173.1680 -2.5310 228.9544 231.4853 270.5936 173.9958 -2.5457 229.0708 231.6165 270.6470 174.7623 -2.5368 229.3419 231.8787 270.9660 175.6210 -2.5433 229.6209 232.1642 271.2844 176.3765 -2.5459 229.6640 232.2100 271.3991 177.2145 -2.5582 229.8801 232.4383 271.3971 178.0015 -2.5560 230.1640 232.7200 271.4786 178.7988 -2.5764 230.2967 232.8732 271.7073 179.6268 -2.5632 230.3766 232.9398 271.9952 180.3820 -2.5463 230.4747 233.0211 272.1470 181.2408 -2.5395 230.7474 233.2869 272.4004 182.0073 -2.5239 230.8916 233.4155 272.5603 182.8353 -2.5311 231.0084 233.5396 272.8327 183.6218 -2.5555 231.2124 233.7679 272.8852 184.4185 -2.5491 231.5434 234.0924 273.0032 185.2465 -2.5463 231.8685 234.4149 273.3009 186.0130 -2.5376 232.0757 234.6133 273.4525 186.8615 -2.5066 232.2073 234.7139 273.5956 187.6378 -2.4894 232.2677 234.7572 273.5926 188.4550 -2.4830 232.4390 234.9220 273.5620 189.2523 -2.4715 232.5737 235.0452 273.5164 190.0495 -2.4730 232.6732 235.1462 273.6345 190.8770 -2.4408 232.9235 235.3643 273.7874 191.6430 -2.4470 233.1359 235.5829 273.8872 192.4915 -2.4563 233.1029 235.5592 274.1140 193.2683 -2.4596 233.3195 235.7791 274.3390 194.0860 -2.4853 233.4925 235.9778 274.4623 194.8823 -2.4978 233.5066 236.0044 274.5865 195.6795 -2.5200 233.5871 236.1070 274.7252 196.5075 -2.5044 233.8820 236.3864 274.7366 197.2740 -2.5093 234.2017 236.7110 274.8560 198.1218 -2.4991 234.3682 236.8673 274.9154 198.8983 -2.4958 234.5461 237.0419 275.0571 199.7160 -2.4935 234.8293 237.3228 275.1474 200.5133 -2.4936 235.1081 237.6017 275.2842 201.3103 -2.5156 235.2529 237.7685 275.5414 202.1375 -2.5261 235.2810 237.8071 275.6566 202.9040 -2.4988 235.4418 237.9406 275.8160 203.7525 -2.4864 235.6738 238.1602 275.7960 204.5293 -2.4828 235.8148 238.2976 275.9463 205.3468 -2.4672 235.9719 238.4391 276.0667 206.1433 -2.4630 236.0013 238.4643 276.2226 206.9405 -2.4444 236.1098 238.5542 276.4101 207.7788 -2.4392 236.1627 238.6019 276.5454 208.5350 -2.4527 236.3678 238.8205 276.6815 209.3933 -2.4699 236.6530 239.1229 276.7474 210.1593 -2.4579 236.6049 239.0628 276.9593 210.9873 -2.4601 236.8002 239.2603 277.0536 211.7845 -2.4498 236.9595 239.4093 277.2767 212.5715 -2.4469 237.0586 239.5055 277.4492 213.4088 -2.4366 237.3755 239.8121 277.7238 214.1753 -2.4316 237.5998 240.0314 277.6798 215.0033 -2.4279 237.9117 240.3396 277.8202 215.7595 -2.4013 237.9729 240.3742 278.0937 216.6275 -2.3958 238.0932 240.4890 278.2006 217.3838 -2.3945 238.0524 240.4469 278.2048 218.2118 -2.3903 238.1325 240.5227 278.3592 219.0090 -2.3835 238.4472 240.8307 278.5674 219.8058 -2.3846 238.8516 241.2362 278.7732 220.6333 -2.3884 238.9719 241.3603 278.8240 221.3998 -2.3863 239.0336 241.4199 278.8120 222.2585 -2.4045 239.0845 241.4890 278.9503 223.0250 -2.3983 239.2567 241.6550 279.0569 223.8523 -2.3829 239.4663 241.8491 279.2243 224.6493 -2.3843 239.7253 242.1096 279.4883 225.4465 -2.3719 239.9450 242.3169 279.5808 226.2438 -2.3458 240.1793 242.5250 279.6498 227.0408 -2.3443 240.3502 242.6944 279.6496 227.8578 -2.3445 240.5912 242.9357 279.7410 228.6345 -2.3348 240.8735 243.2083 279.5963 229.4830 -2.3615 241.2332 243.5947 279.6434 230.2495 -2.3814 241.4908 243.8722 279.8181 231.0768 -2.4001 241.5680 243.9681 279.8641 231.8635 -2.4264 241.7893 244.2156 280.0498 232.6505 -2.4287 241.8921 244.3208 280.3942 233.4785 -2.4238 242.0195 244.4433 280.4903 234.2445 -2.4250 242.1162 244.5412 280.4761 235.0618 -2.4193 242.1757 244.5951 280.5374 235.8385 -2.4090 242.3255 244.7345 280.8095 236.6870 -2.4153 242.5659 244.9813 280.9508 237.4535 -2.4078 242.6633 245.0712 281.0280 238.2808 -2.4072 242.7273 245.1345 281.0841 239.0675 -2.4001 242.7637 245.1638 281.2091 239.8648 -2.3750 242.8621 245.2371 281.3652 240.6620 -2.3772 242.9630 245.3402 281.5805 241.4490 -2.3895 243.0104 245.3999 281.6683 242.2763 -2.3601 243.2956 245.6557 281.8011 243.0425 -2.3491 243.5232 245.8723 281.8230 243.8910 -2.3528 243.5904 245.9432 282.0740 244.6575 -2.3618 243.7146 246.0763 282.2004 245.4850 -2.3569 243.7333 246.0903 282.4740 246.2818 -2.3713 243.9149 246.2861 282.5106 247.0790 -2.3574 244.2573 246.6147 282.4399 247.8968 -2.3460 244.5564 246.9024 282.5377 248.6735 -2.3236 244.7464 247.0700 282.6598 249.5210 -2.3505 244.8621 247.2127 282.7692 250.2773 -2.3642 244.9245 247.2886 282.9736 251.1155 -2.3551 245.2179 247.5729 283.1244 251.9025 -2.3358 245.2167 247.5524 283.1994 252.6993 -2.3366 245.3126 247.6493 283.4136 253.5268 -2.3414 245.6424 247.9838 283.4952 254.2933 -2.3338 245.8193 248.1531 283.6814 255.1520 -2.3201 245.8972 248.2173 283.7956 255.8770 -2.3321 245.9850 248.3170 283.8816 256.7455 -2.3224 246.1872 248.5096 284.0557 257.5018 -2.3292 246.3128 248.6420 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