DTA measure 1meres6_pb3 Date: 2026218:922 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.04 s Mass = 967.900 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2095 1.5178 236.3899 234.8721 275.5738 2.0783 1.5168 236.6754 235.1586 275.5778 2.8438 1.5150 236.9512 235.4363 275.5668 3.6610 1.5109 237.2525 235.7416 275.5211 4.4680 1.5076 237.5386 236.0310 275.4379 5.2540 1.5070 237.8123 236.3054 275.3231 6.0815 1.5099 238.0990 236.5890 275.2062 6.8475 1.5077 238.3439 236.8362 275.0962 7.7053 1.5081 238.6503 237.1422 274.9627 8.4713 1.5060 238.9226 237.4166 274.8377 9.2885 1.5038 239.1788 237.6750 274.6877 10.0950 1.4991 239.4299 237.9308 274.5329 10.8815 1.4925 239.6908 238.1983 274.4155 11.7090 1.4913 239.9595 238.4682 274.3008 12.4748 1.4889 240.1765 238.6876 274.1967 13.3330 1.4910 240.4166 238.9255 274.0895 14.0988 1.4898 240.6628 239.1730 274.0162 14.9158 1.4926 240.9408 239.4482 273.9899 15.7228 1.4959 241.2141 239.7182 273.9631 16.5090 1.4968 241.4813 239.9844 273.9613 17.3363 1.4917 241.7584 240.2667 274.0306 18.1023 1.4914 242.0096 240.5182 274.0832 18.9705 1.4893 242.3157 240.8264 274.1885 19.7260 1.4848 242.5694 241.0846 274.3077 20.5535 1.4852 242.8337 241.3486 274.4591 21.3500 1.4838 243.0790 241.5951 274.6790 22.1363 1.4839 243.3350 241.8511 274.9326 22.9330 1.4825 243.5848 242.1023 275.2103 23.7295 1.4754 243.8315 242.3561 275.4834 24.5465 1.4725 244.0716 242.5991 275.8208 25.3125 1.4678 244.3033 242.8355 276.1780 26.1705 1.4625 244.5705 243.1080 276.5995 26.9260 1.4567 244.7888 243.3321 276.9724 27.7433 1.4490 245.0461 243.5971 277.3751 28.5500 1.4420 245.2940 243.8519 277.7733 29.3363 1.4354 245.5261 244.0907 278.1548 30.1640 1.4321 245.7856 244.3535 278.5877 30.9295 1.4272 246.0313 244.6042 278.9471 31.7878 1.4242 246.3119 244.8877 279.3239 32.5538 1.4185 246.5362 245.1177 279.6679 33.3705 1.4136 246.7845 245.3709 280.0267 34.1775 1.4093 247.0488 245.6395 280.3452 34.9640 1.4063 247.2928 245.8865 280.6024 35.7913 1.4015 247.5507 246.1492 280.8408 36.5570 1.3950 247.7890 246.3940 281.0360 37.4153 1.3874 248.0557 246.6683 281.2209 38.1810 1.3785 248.2732 246.8947 281.3546 38.9983 1.3698 248.4977 247.1278 281.5107 39.8050 1.3654 248.7287 247.3632 281.6412 40.5913 1.3580 248.9726 247.6146 281.7139 41.4188 1.3522 249.2317 247.8795 281.7646 42.1845 1.3476 249.4463 248.0987 281.7948 43.0223 1.3420 249.7130 248.3710 281.7888 43.7780 1.3369 249.9269 248.5900 281.7703 44.6463 1.3315 250.1964 248.8650 281.7306 45.4020 1.3284 250.4324 249.1039 281.6787 46.2395 1.3208 250.6802 249.3594 281.5968 47.0258 1.3161 250.9187 249.6025 281.5079 47.8225 1.3097 251.1376 249.8279 281.4087 48.6498 1.2995 251.3844 250.0849 281.3207 49.4155 1.2953 251.6231 250.3278 281.2238 50.2740 1.2880 251.8787 250.5907 281.0963 51.0293 1.2827 252.1092 250.8265 281.0166 51.8670 1.2772 252.3537 251.0766 280.9533 52.6535 1.2740 252.6023 251.3283 280.9192 53.4498 1.2702 252.8429 251.5727 280.8898 54.2773 1.2654 253.0745 251.8091 280.8408 55.0330 1.2625 253.2858 252.0233 280.7991 55.8910 1.2550 253.5134 252.2584 280.8153 56.6570 1.2486 253.7257 252.4770 280.8400 57.4843 1.2469 253.9696 252.7227 280.9293 58.2398 1.2419 254.1719 252.9300 281.0417 59.0673 1.2369 254.4007 253.1637 281.1779 59.8638 1.2292 254.6324 253.4032 281.3178 60.6603 1.2233 254.8496 253.6263 281.4997 61.4775 1.2145 255.1025 253.8880 281.7030 62.2433 1.2076 255.3228 254.1151 281.9321 63.1015 1.2018 255.5576 254.3558 282.2336 63.8573 1.1968 255.7419 254.5451 282.4886 64.6945 1.1867 255.9715 254.7848 282.8071 65.4808 1.1810 256.1783 254.9973 283.1422 66.2778 1.1736 256.3698 255.1962 283.4830 67.1048 1.1686 256.6425 255.4740 283.8421 67.8708 1.1674 256.8667 255.6992 284.1871 68.7290 1.1590 257.1186 255.9597 284.5685 69.4843 1.1516 257.3153 256.1637 284.8881 70.3220 1.1452 257.5310 256.3857 285.2338 71.1085 1.1341 257.7533 256.6192 285.5711 71.9048 1.1236 258.0045 256.8809 285.8750 72.7323 1.1172 258.2435 257.1263 286.1898 73.5085 1.1103 258.4603 257.3500 286.4913 74.3355 1.0994 258.6525 257.5531 286.7891 75.1015 1.0916 258.8436 257.7520 287.0099 75.9495 1.0815 259.0641 257.9825 287.2104 76.7253 1.0743 259.2901 258.2158 287.3970 77.5630 1.0682 259.5194 258.4512 287.5900 78.3905 1.0639 259.7444 258.6805 287.7283 79.2175 1.0573 259.9520 258.8946 287.8354 80.1575 1.0451 260.2279 259.1828 287.9500 80.9953 1.0407 260.4487 259.4080 287.9982 81.8430 1.0312 260.6885 259.6573 288.0137 82.6190 1.0233 260.8813 259.8581 288.0510 83.4465 1.0124 261.1155 260.1031 288.0525 84.2430 1.0056 261.3250 260.3194 288.0137 85.0500 0.9971 261.5437 260.5465 287.9815 85.8365 0.9875 261.7503 260.7628 287.9195 86.6225 0.9793 261.9553 260.9760 287.8674 87.4505 0.9692 262.1988 261.2296 287.8172 88.2160 0.9637 262.3943 261.4305 287.7789 89.0640 0.9555 262.6368 261.6813 287.7318 89.8608 0.9480 262.8536 261.9056 287.7198 90.6570 0.9399 263.0751 262.1352 287.6785 91.4745 0.9298 263.3223 262.3924 287.6009 92.2505 0.9248 263.5079 262.5830 287.5703 93.0983 0.9238 263.7331 262.8092 287.5655 93.8643 0.9189 263.9327 263.0138 287.5633 94.7120 0.9148 264.1273 263.2125 287.5908 95.4778 0.9119 264.3080 263.3961 287.6312 96.3055 0.9066 264.5357 263.6291 287.6390 97.1018 0.9018 264.7212 263.8195 287.7240 97.8985 0.8975 264.9183 264.0207 287.8626 98.6953 0.8922 265.1185 264.2264 288.0318 99.4915 0.8845 265.3081 264.4235 288.1821 100.3293 0.8753 265.5235 264.6482 288.3647 101.0953 0.8733 265.7282 264.8549 288.5774 101.9530 0.8700 265.9558 265.0857 288.8216 102.7090 0.8638 266.1300 265.2662 289.0718 103.5568 0.8577 266.3361 265.4784 289.3755 104.3020 0.8485 266.5287 265.6802 289.6185 105.1603 0.8396 266.7719 265.9322 289.9215 105.9260 0.8278 266.9499 266.1221 290.2019 106.7533 0.8219 267.1610 266.3392 290.5186 107.5500 0.8168 267.3396 266.5228 290.8286 108.3465 0.8073 267.5468 266.7395 291.1542 109.1740 0.7991 267.7315 266.9325 291.4742 110.0323 0.7887 267.9520 267.1632 291.8038 111.0438 0.7797 268.2431 267.4635 292.2030 111.9020 0.7706 268.4630 267.6923 292.5086 112.6783 0.7639 268.6490 267.8851 292.7347 113.4950 0.7551 268.8505 268.0954 292.9891 114.2815 0.7484 269.0274 268.2790 293.1857 115.1090 0.7412 269.2206 268.4794 293.3591 115.8950 0.7315 269.4185 268.6869 293.5244 116.7020 0.7229 269.6440 268.9212 293.6930 117.5295 0.7142 269.8386 269.1244 293.8753 118.2848 0.7067 270.0423 269.3356 294.0174 119.1430 0.6986 270.2686 269.5700 294.1284 119.8988 0.6889 270.4428 269.7539 294.2101 120.7258 0.6823 270.6279 269.9456 294.2759 121.5225 0.6778 270.8150 270.1371 294.3126 122.3190 0.6695 270.9982 270.3287 294.3374 123.1155 0.6603 271.1959 270.5357 294.3594 123.9120 0.6524 271.3945 270.7420 294.3793 124.7295 0.6455 271.6214 270.9758 294.3963 125.5155 0.6373 271.8315 271.1943 294.3913 126.3533 0.6288 272.0490 271.4202 294.3679 127.1090 0.6239 272.2677 271.6438 294.3281 127.9360 0.6166 272.4635 271.8469 294.3281 128.7020 0.6129 272.6528 272.0399 294.3269 129.5603 0.6127 272.8375 272.2248 294.2704 130.3258 0.6087 273.0016 272.3930 294.2275 131.1428 0.6038 273.2238 272.6201 294.1940 131.9500 0.5938 273.4137 272.8199 294.1805 132.7360 0.5839 273.6284 273.0445 294.1920 133.5635 0.5787 273.8358 273.2572 294.2099 134.3398 0.5744 274.0207 273.4463 294.2395 135.1975 0.5674 274.2267 273.6593 294.2925 135.9738 0.5602 274.4263 273.8660 294.3805 136.7910 0.5566 274.6201 274.0635 294.4663 137.5873 0.5526 274.7990 274.2464 294.6081 138.3840 0.5467 274.9919 274.4452 294.7453 139.2115 0.5431 275.1875 274.6444 294.9232 139.9770 0.5364 275.3907 274.8543 295.1315 140.8250 0.5260 275.6046 275.0786 295.3525 141.6013 0.5219 275.7973 275.2754 295.5496 142.4180 0.5183 275.9821 275.4638 295.7878 143.2148 0.5104 276.1688 275.6584 296.0549 144.0115 0.5048 276.3335 275.8287 296.3291 144.8385 0.4978 276.5215 276.0236 296.6183 145.6045 0.4923 276.7321 276.2398 296.8866 146.4525 0.4838 276.9445 276.4607 297.1553 147.2285 0.4808 277.1224 276.6416 297.4251 148.0458 0.4722 277.3035 276.8313 297.7267 148.8423 0.4668 277.4928 277.0259 298.0127 149.6388 0.4578 277.6691 277.2113 298.2975 150.4663 0.4514 277.8709 277.4195 298.5542 151.2218 0.4429 278.0746 277.6318 298.7861 152.0800 0.4325 278.2733 277.8407 299.0568 152.8358 0.4279 278.4489 278.0210 299.3020 153.6628 0.4195 278.6349 278.2154 299.5428 154.4595 0.4146 278.7863 278.3717 299.7433 155.2460 0.4025 278.9535 278.5510 299.9160 156.0730 0.3944 279.1463 278.7520 300.0817 156.8393 0.3912 279.3509 278.9597 300.2190 157.6665 0.3812 279.5528 279.1715 300.3565 158.4323 0.3781 279.7074 279.3294 300.4519 159.2803 0.3721 279.8921 279.5200 300.5684 160.0563 0.3652 280.0802 279.7150 300.6409 160.8735 0.3590 280.2867 279.9278 300.6948 161.6703 0.3508 280.4764 280.1256 300.7481 162.4665 0.3425 280.6721 280.3296 300.7605 163.2940 0.3330 280.8772 280.5442 300.7840 164.0600 0.3235 281.0533 280.7298 300.8173 164.9078 0.3156 281.2752 280.9596 300.7984 165.7148 0.3114 281.4497 281.1382 300.7822 166.5010 0.3008 281.6295 281.3288 300.7767 167.3283 0.2929 281.8121 281.5192 300.7490 168.0945 0.2849 281.9868 281.7019 300.7336 168.9523 0.2807 282.2107 281.9300 300.7360 169.7183 0.2761 282.3656 282.0895 300.7367 170.5355 0.2719 282.5478 282.2758 300.7575 171.3420 0.2605 282.7316 282.4711 300.7781 172.1288 0.2533 282.8781 282.6248 300.8205 172.9560 0.2487 283.0623 282.8137 300.8648 173.7525 0.2452 283.2591 283.0139 300.9288 174.5800 0.2407 283.4549 283.2142 300.9971 175.3560 0.2335 283.6299 283.3964 301.0644 176.1833 0.2273 283.8349 283.6076 301.1859 176.9800 0.2219 284.0057 283.7838 301.3179 177.7765 0.2177 284.1961 283.9784 301.4721 178.6038 0.2107 284.3636 284.1529 301.6452 179.3700 0.2038 284.5269 284.3230 301.8104 180.2175 0.1944 284.7135 284.5191 302.0143 180.9938 0.1845 284.8978 284.7133 302.2088 181.8213 0.1805 285.0799 284.8994 302.4289 182.6175 0.1754 285.2839 285.1085 302.6665 183.4043 0.1717 285.4639 285.2922 302.9369 184.2315 0.1697 285.6518 285.4821 303.1892 184.9868 0.1648 285.8276 285.6629 303.4147 185.9578 0.1610 286.0747 285.9137 303.7632 186.8365 0.1622 286.2560 286.0938 304.0827 187.5818 0.1589 286.4340 286.2750 304.3258 188.4298 0.1550 286.6019 286.4469 304.5971 189.1955 0.1494 286.7420 286.5926 304.8436 190.0230 0.1461 286.9141 286.7680 305.0907 190.8198 0.1395 287.0761 286.9366 305.3345 191.6160 0.1327 287.2690 287.1363 305.5763 192.4333 0.1287 287.4470 287.3183 305.7930 193.1993 0.1220 287.6036 287.4816 305.9790 194.0573 0.1146 287.7753 287.6607 306.1841 194.8130 0.1095 287.9315 287.8220 306.3285 195.6505 0.1023 288.1613 288.0590 306.4994 196.4368 0.0976 288.3180 288.2204 306.6569 197.2335 0.0879 288.5017 288.4138 306.7861 198.0608 0.0812 288.6512 288.5701 306.8728 198.8265 0.0778 288.8408 288.7631 306.9640 199.6848 0.0725 289.0480 288.9755 307.0601 200.4710 0.0632 289.2072 289.1441 307.1516 201.2778 0.0607 289.3841 289.3234 307.2096 202.0953 0.0586 289.5536 289.4950 307.2514 202.8608 0.0527 289.7099 289.6571 307.2854 203.7190 0.0448 289.8982 289.8535 307.3045 204.4850 0.0372 290.0710 290.0339 307.3228 205.3120 0.0305 290.2513 290.2208 307.3366 206.0985 0.0257 290.4104 290.3846 307.3293 206.9055 0.0077 290.5610 290.5533 307.3189 207.7225 0.0008 290.7466 290.7457 307.3133 208.4885 0.0009 290.9370 290.9362 307.3220 209.3465 -0.0038 291.1393 291.1431 307.3585 210.1123 -0.0072 291.3102 291.3173 307.3937 210.9398 -0.0124 291.5080 291.5204 307.4104 211.7363 -0.0169 291.7030 291.7199 307.4363 212.5328 -0.0224 291.8633 291.8857 307.4858 213.3603 -0.0278 292.0511 292.0788 307.5576 214.1260 -0.0365 292.2094 292.2459 307.6262 214.9738 -0.0425 292.3843 292.4269 307.7212 215.7503 -0.0523 292.5368 292.5892 307.8487 216.5773 -0.0552 292.7475 292.8026 307.9963 217.3330 -0.0565 292.9166 292.9731 308.1395 218.1810 -0.0580 293.0849 293.1429 308.2833 218.9363 -0.0588 293.2268 293.2856 308.4479 219.7743 -0.0663 293.3805 293.4468 308.6746 220.5605 -0.0726 293.5525 293.6252 308.8989 221.3468 -0.0779 293.7223 293.8002 309.1348 222.1848 -0.0839 293.9144 293.9983 309.3631 222.9400 -0.0898 294.0685 294.1583 309.5756 223.7983 -0.0970 294.2649 294.3618 309.8505 224.5643 -0.1028 294.4380 294.5408 310.0989 225.3810 -0.1091 294.6197 294.7287 310.3385 226.1780 -0.1157 294.7920 294.9077 310.5789 226.9950 -0.1270 294.9651 295.0921 310.8485 227.7608 -0.1341 295.1211 295.2551 311.0721 228.5885 -0.1392 295.2878 295.4270 311.3243 229.4155 -0.1431 295.4631 295.6062 311.5807 230.1815 -0.1483 295.6489 295.7972 311.8053 231.0295 -0.1523 295.8318 295.9841 312.0531 231.8055 -0.1570 295.9792 296.1362 312.2662 232.6228 -0.1606 296.1385 296.2991 312.4605 233.4193 -0.1695 296.3323 296.5018 312.6272 234.2160 -0.1747 296.5044 296.6791 312.7959 235.0435 -0.1812 296.6583 296.8395 312.9634 235.8090 -0.1853 296.8045 296.9898 313.0912 236.6670 -0.1884 297.0238 297.2123 313.2186 237.4228 -0.1939 297.1768 297.3707 313.2966 238.2500 -0.2017 297.3320 297.5337 313.3806 239.0160 -0.2083 297.4763 297.6846 313.4451 239.8743 -0.2154 297.6821 297.8975 313.4901 240.6398 -0.2213 297.8423 298.0636 313.5572 241.4570 -0.2297 298.0020 298.2317 313.6162 242.2640 -0.2331 298.1744 298.4075 313.6705 243.0500 -0.2397 298.3275 298.5672 313.7280 243.8878 -0.2453 298.4935 298.7387 313.7633 244.6435 -0.2523 298.6509 298.9032 313.7498 245.5115 -0.2576 298.8479 299.1054 313.7668 246.2670 -0.2652 298.9970 299.2622 313.7743 247.1153 -0.2702 299.1636 299.4338 313.7751 247.8808 -0.2734 299.3362 299.6097 313.8146 248.6980 -0.2760 299.5117 299.7877 313.8327 249.4743 -0.2797 299.6859 299.9656 313.8522 250.2910 -0.2878 299.8622 300.1500 313.8857 251.0878 -0.2911 300.0215 300.3126 313.9544 251.8845 -0.2933 300.1922 300.4855 314.0297 252.7115 -0.2962 300.3512 300.6474 314.0959 253.4670 -0.2974 300.5070 300.8044 314.1673 254.3255 -0.3041 300.6942 300.9983 314.2990 255.0910 -0.3079 300.8710 301.1789 314.4393 255.9185 -0.3152 301.0446 301.3598 314.6021 256.6740 -0.3192 301.2059 301.5252 314.7447 257.5320 -0.3246 301.3745 301.6991 314.8991 258.2875 -0.3304 301.5286 301.8590 315.0830 259.1253 -0.3379 301.6913 302.0291 315.3054 259.9115 -0.3482 301.8614 302.2095 315.5064 260.7080 -0.3484 302.0065 302.3550 315.7379 261.5048 -0.3516 302.1473 302.4989 315.9626 262.3013 -0.3548 302.3207 302.6755 316.2015 263.1285 -0.3565 302.5055 302.8620 316.4442 263.8843 -0.3627 302.6674 303.0301 316.6572 264.7525 -0.3686 302.8570 303.2256 316.8997 265.5080 -0.3726 302.9998 303.3724 317.1457 266.3355 -0.3838 303.1764 303.5603 317.4071 267.1320 -0.3890 303.3450 303.7340 317.6578 267.9388 -0.3905 303.5035 303.8940 317.9095 268.7458 -0.3950 303.6687 304.0637 318.1229 269.5320 -0.4029 303.7859 304.1888 318.3369 270.3593 -0.4107 303.9436 304.3543 318.5550 271.1255 -0.4176 304.1069 304.5245 318.7592 271.9525 -0.4272 304.2914 304.7185 318.9458 272.7185 -0.4350 304.4528 304.8878 319.1074 273.5665 -0.4435 304.6285 305.0720 319.2768 274.3423 -0.4467 304.7851 305.2318 319.4336 275.1595 -0.4518 304.9549 305.4067 319.5371 275.9563 -0.4570 305.1387 305.5956 319.6032 276.7525 -0.4645 305.2947 305.7592 319.6944 277.5800 -0.4684 305.4689 305.9374 319.7937 278.3460 -0.4704 305.6420 306.1124 319.8619 279.1935 -0.4787 305.8381 306.3168 319.9284 279.9698 -0.4798 306.0110 306.4908 319.9501 280.7870 -0.4816 306.1694 306.6510 319.9671 281.5730 -0.4883 306.3506 306.8388 320.0089 282.3800 -0.4934 306.5236 307.0170 320.0354 283.1973 -0.5006 306.6700 307.1706 320.0926 283.9525 -0.5044 306.8113 307.3157 320.1103 284.8210 -0.5125 306.9436 307.4561 320.1503 285.5460 -0.5130 307.0910 307.6039 320.1586 286.4038 -0.5174 307.2859 307.8033 320.1814 287.1698 -0.5256 307.4510 307.9766 320.2225 287.9973 -0.5312 307.6185 308.1497 320.2770 288.7935 -0.5346 307.7707 308.3053 320.3281 289.5803 -0.5375 307.9364 308.4739 320.3831 290.4178 -0.5405 308.1164 308.6569 320.4460 291.1733 -0.5463 308.2495 308.7958 320.5346 292.0315 -0.5531 308.4054 308.9585 320.6510 292.7973 -0.5615 308.5768 309.1383 320.7598 293.6248 -0.5690 308.7748 309.3438 320.8814 294.4215 -0.5687 308.9298 309.4985 321.0142 295.2078 -0.5730 309.0921 309.6650 321.1751 296.0148 -0.5705 309.2441 309.8146 321.3366 296.8010 -0.5721 309.3875 309.9596 321.5077 297.6285 -0.5747 309.5407 310.1153 321.7040 298.4253 -0.5783 309.6596 310.2380 321.8983 299.2525 -0.5836 309.8321 310.4156 322.1134 300.0493 -0.5887 310.0170 310.6056 322.3416 300.8355 -0.5953 310.1812 310.7765 322.5815 301.6730 -0.6047 310.3757 310.9803 322.8327 302.4288 -0.6109 310.5242 311.1351 323.1056 303.2970 -0.6178 310.7030 311.3208 323.3970 304.0528 -0.6202 310.8478 311.4679 323.6308 304.8903 -0.6237 311.0550 311.6787 323.8595 305.6765 -0.6266 311.2110 311.8377 324.0786 306.4733 -0.6325 311.3661 311.9986 324.2996 307.3005 -0.6391 311.5481 312.1872 324.5323 308.0663 -0.6458 311.6988 312.3446 324.7348 308.9143 -0.6508 311.8804 312.5312 324.9938 309.6803 -0.6554 312.0225 312.6779 325.1799 310.5380 -0.6623 312.2126 312.8749 325.3485 311.2940 -0.6654 312.3570 313.0224 325.4701 312.1315 -0.6704 312.5285 313.1989 325.6223 312.8868 -0.6753 312.6667 313.3420 325.7520 313.7043 -0.6802 312.8012 313.4814 325.8657 314.5008 -0.6845 312.9558 313.6403 325.9448 315.2973 -0.6910 313.1310 313.8220 326.0000 316.1145 -0.6947 313.2864 313.9811 326.0621 316.8803 -0.6969 313.4417 314.1386 326.1317 317.7385 -0.7033 313.6079 314.3112 326.1918 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