DTA measure 2meres6_pb4 Date: 2026218:1046 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1722.82 s Mass = 967.900 mg data_number = 1070 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5404 0.0315 230.7347 230.7031 215.4437 4.1451 0.0340 230.7538 230.7198 215.2081 5.7443 0.0416 230.7021 230.6605 214.9568 7.3383 0.0529 230.6804 230.6276 214.7863 8.9481 0.0602 230.7309 230.6707 214.6419 10.5476 0.0653 230.7385 230.6732 214.5651 12.1464 0.0748 230.7504 230.6756 214.5623 13.7665 0.0834 230.7746 230.6913 214.6269 15.3713 0.0860 230.7848 230.6988 214.8170 16.9759 0.0866 230.7983 230.7117 215.0702 18.5695 0.0883 230.8097 230.7215 215.4234 20.1743 0.0901 230.8102 230.7200 215.8477 21.7841 0.0906 230.7993 230.7087 216.3358 23.3886 0.0922 230.8297 230.7375 216.8499 24.9978 0.0909 230.8633 230.7724 217.3891 26.6179 0.0874 230.8604 230.7730 217.9098 28.2226 0.0852 230.8488 230.7636 218.4279 29.8324 0.0810 230.8975 230.8165 218.9101 31.4363 0.0783 230.9178 230.8395 219.3279 33.0461 0.0754 230.9036 230.8282 219.7524 34.6509 0.0751 230.9264 230.8513 220.0999 36.2495 0.0736 230.9270 230.8533 220.3937 37.8748 0.0674 230.9544 230.8870 220.5867 39.4744 0.0673 230.9604 230.8930 220.7363 41.0838 0.0645 230.9416 230.8771 220.8689 42.6880 0.0601 230.9640 230.9039 220.9381 44.2928 0.0567 230.9709 230.9143 221.0029 45.8916 0.0501 230.9871 230.9370 221.0364 47.4961 0.0447 231.0033 230.9585 221.0386 49.1060 0.0425 231.0153 230.9728 221.0496 50.7308 0.0434 231.0364 230.9930 221.0409 52.3401 0.0355 231.0844 231.0489 221.0193 53.9346 0.0286 231.1025 231.0740 221.0214 55.5445 0.0217 231.0978 231.0760 221.0534 57.1483 0.0204 231.1226 231.1022 221.1216 58.7581 0.0216 231.1146 231.0930 221.2451 60.3629 0.0149 231.0985 231.0836 221.4235 61.9718 0.0138 231.1429 231.1291 221.6249 63.5868 0.0126 231.1869 231.1743 221.8369 65.2069 0.0034 231.1959 231.1925 222.0860 66.8106 -0.0068 231.2087 231.2155 222.4275 68.4205 -0.0105 231.2121 231.2226 222.7789 70.0253 -0.0118 231.2246 231.2364 223.1642 71.6341 -0.0094 231.3130 231.3224 223.5500 73.2543 -0.0133 231.3552 231.3685 223.9296 74.8538 -0.0186 231.3752 231.3938 224.2727 76.4629 -0.0271 231.3993 231.4264 224.5731 78.0829 -0.0310 231.4014 231.4324 224.8976 79.7491 -0.0351 231.3671 231.4022 225.2228 81.4558 -0.0358 231.3974 231.4332 225.5566 83.0704 -0.0436 231.4378 231.4814 225.8168 84.7161 -0.0511 231.4530 231.5041 226.0145 86.3253 -0.0566 231.4866 231.5432 226.1763 87.9298 -0.0597 231.5483 231.6080 226.3157 89.5345 -0.0627 231.5705 231.6332 226.4398 91.1386 -0.0684 231.6170 231.6855 226.5565 92.7481 -0.0735 231.6953 231.7688 226.6443 94.3529 -0.0789 231.7417 231.8207 226.7421 95.9569 -0.0853 231.7853 231.8707 226.8270 97.5716 -0.0939 231.8497 231.9435 226.9205 99.1661 -0.0969 231.9231 232.0200 227.0318 100.7705 -0.0956 231.9935 232.0891 227.1442 102.3695 -0.0995 232.0326 232.1320 227.2675 103.9640 -0.0956 232.0675 232.1631 227.4031 105.5635 -0.1011 232.1033 232.2044 227.5604 107.1725 -0.1046 232.1572 232.2618 227.7582 108.7721 -0.1040 232.2277 232.3316 227.9846 110.3923 -0.1046 232.2735 232.3781 228.2526 111.9858 -0.1069 232.3373 232.4442 228.5212 113.5905 -0.1081 232.3996 232.5077 228.7760 115.1953 -0.1144 232.4588 232.5732 229.0814 116.7941 -0.1132 232.4854 232.5986 229.3938 118.4038 -0.1165 232.5423 232.6587 229.6779 120.0085 -0.1190 232.6103 232.7293 229.9937 121.6181 -0.1199 232.6396 232.7594 230.3062 123.2221 -0.1231 232.7010 232.8241 230.6313 124.8474 -0.1296 232.7911 232.9207 230.8976 126.4419 -0.1307 232.8634 232.9941 231.1263 128.0508 -0.1342 232.9248 233.0590 231.3825 129.6555 -0.1391 232.9825 233.1216 231.6149 131.2654 -0.1434 233.0235 233.1669 231.8463 132.8694 -0.1443 233.0974 233.2417 232.0617 134.4893 -0.1484 233.1747 233.3231 232.2158 136.0991 -0.1580 233.2687 233.4266 232.3406 137.7038 -0.1610 233.3403 233.5013 232.4717 139.3128 -0.1592 233.4533 233.6125 232.5837 140.9175 -0.1604 233.5375 233.6979 232.6876 142.5223 -0.1628 233.6043 233.7671 232.7958 144.1311 -0.1633 233.6837 233.8470 232.9048 145.7461 -0.1637 233.7711 233.9348 233.0417 147.3509 -0.1640 233.8585 234.0225 233.1768 148.9601 -0.1559 233.9296 234.0855 233.3329 150.5645 -0.1523 233.9936 234.1459 233.5099 152.3948 -0.1479 234.0926 234.2405 233.7556 154.1071 -0.1476 234.1743 234.3219 233.9897 155.7160 -0.1462 234.2831 234.4293 234.2406 157.3208 -0.1454 234.3608 234.5062 234.5126 158.9255 -0.1474 234.4475 234.5949 234.7983 160.5503 -0.1510 234.5295 234.6806 235.0833 162.1443 -0.1544 234.6018 234.7563 235.3732 163.7490 -0.1542 234.7149 234.8692 235.6632 165.3435 -0.1577 234.8306 234.9884 235.9624 166.9474 -0.1572 234.9234 235.0806 236.2048 168.5418 -0.1536 235.0088 235.1624 236.4953 170.1363 -0.1530 235.1140 235.2670 236.7679 171.7401 -0.1536 235.2192 235.3728 236.9995 173.3499 -0.1521 235.3053 235.4573 237.2065 174.9649 -0.1532 235.4317 235.5849 237.4057 176.5693 -0.1502 235.5662 235.7164 237.6155 178.1734 -0.1505 235.6475 235.7980 237.7910 179.7628 -0.1502 235.7634 235.9136 237.9635 181.3726 -0.1486 235.8803 236.0289 238.1417 182.9818 -0.1469 236.0002 236.1471 238.2962 184.5811 -0.1509 236.1210 236.2720 238.4384 186.1910 -0.1520 236.2078 236.3598 238.5716 187.7796 -0.1507 236.3364 236.4871 238.6635 189.4046 -0.1471 236.4718 236.6189 238.7923 191.0094 -0.1442 236.5506 236.6948 238.9415 192.6188 -0.1480 236.6618 236.8098 239.1261 194.2076 -0.1516 236.8040 236.9555 239.3266 195.8124 -0.1520 236.9325 237.0845 239.5155 197.4223 -0.1514 237.0596 237.2110 239.7146 199.0313 -0.1447 237.1838 237.3285 239.9355 200.6410 -0.1429 237.2755 237.4183 240.1895 202.2611 -0.1433 237.4111 237.5544 240.4712 203.8710 -0.1409 237.5455 237.6864 240.7109 205.4645 -0.1378 237.6687 237.8065 241.0072 207.0693 -0.1366 237.7983 237.9350 241.2725 208.6791 -0.1361 237.9311 238.0672 241.5403 210.2829 -0.1366 238.0580 238.1945 241.8149 211.8928 -0.1312 238.1655 238.2967 242.0979 213.4975 -0.1302 238.3091 238.4393 242.3459 215.1065 -0.1262 238.4435 238.5697 242.5843 216.7316 -0.1267 238.5802 238.7069 242.8002 218.3210 -0.1315 238.6863 238.8178 242.9971 219.9611 -0.1305 238.8000 238.9304 243.1925 221.5859 -0.1256 238.9142 239.0398 243.3851 223.2111 -0.1248 239.0589 239.1837 243.5618 224.8204 -0.1238 239.1811 239.3049 243.7492 226.4248 -0.1216 239.3494 239.4710 243.9571 228.0190 -0.1233 239.4961 239.6193 244.1137 229.6281 -0.1249 239.6348 239.7597 244.2879 231.2175 -0.1215 239.7707 239.8921 244.4802 232.8171 -0.1247 239.9144 240.0391 244.6227 234.4215 -0.1199 240.0245 240.1444 244.7935 236.0205 -0.1137 240.1765 240.2901 244.9309 237.6304 -0.1086 240.3257 240.4343 245.0910 239.2198 -0.1107 240.4951 240.6058 245.2708 240.8240 -0.1088 240.6186 240.7273 245.4774 242.4283 -0.1035 240.7727 240.8762 245.7287 244.0330 -0.1044 240.8853 240.9897 245.9633 245.6480 -0.1045 241.0591 241.1635 246.2135 247.2574 -0.1027 241.2094 241.3121 246.4830 248.8565 -0.1039 241.3849 241.4888 246.7255 250.4613 -0.1064 241.5564 241.6627 246.9904 252.0711 -0.1055 241.6955 241.8010 247.2584 253.6749 -0.1015 241.8435 241.9450 247.4876 255.2745 -0.0986 242.0114 242.1100 247.7237 256.8793 -0.0991 242.1746 242.2737 247.9731 258.5041 -0.0973 242.3387 242.4361 248.2259 260.1083 -0.0962 242.5138 242.6100 248.4755 261.7028 -0.0970 242.6403 242.7373 248.7046 263.3121 -0.0926 242.7660 242.8586 248.9209 264.9318 -0.0881 242.9277 243.0159 249.1204 266.5365 -0.0893 243.1262 243.2155 249.2902 268.1463 -0.0932 243.3109 243.4040 249.4693 269.7501 -0.0958 243.4714 243.5672 249.6531 271.3703 -0.0934 243.6054 243.6988 249.8289 272.9699 -0.0903 243.7392 243.8296 249.9864 274.5741 -0.0886 243.9277 244.0162 250.1230 276.1835 -0.0872 244.0857 244.1729 250.2752 277.7934 -0.0857 244.2576 244.3433 250.4621 279.4031 -0.0817 244.4417 244.5233 250.6341 281.0070 -0.0808 244.5996 244.6804 250.7992 282.6169 -0.0824 244.7681 244.8505 250.9981 284.2370 -0.0811 244.9587 245.0398 251.1910 285.8313 -0.0791 245.1077 245.1868 251.4245 287.4404 -0.0762 245.2662 245.3424 251.6657 289.0451 -0.0739 245.4392 245.5131 251.9374 290.6490 -0.0685 245.6293 245.6978 252.1695 292.2485 -0.0640 245.8209 245.8849 252.3973 293.8430 -0.0680 245.9982 246.0661 252.6369 295.4525 -0.0703 246.1512 246.2215 252.9149 297.0361 -0.0715 246.3216 246.3931 253.2148 298.6460 -0.0731 246.5053 246.5784 253.4889 300.2504 -0.0691 246.6727 246.7417 253.7517 301.8494 -0.0660 246.8661 246.9321 253.9939 303.4593 -0.0675 247.0527 247.1202 254.2170 305.0691 -0.0695 247.2320 247.3015 254.4182 306.6578 -0.0679 247.4194 247.4873 254.6129 308.2725 -0.0666 247.5947 247.6613 254.8045 309.8721 -0.0650 247.7659 247.8309 254.9853 311.4769 -0.0672 247.9555 248.0227 255.1384 313.0858 -0.0648 248.1237 248.1884 255.2938 314.7059 -0.0620 248.3376 248.3996 255.4707 316.3106 -0.0622 248.5219 248.5841 255.6415 317.9203 -0.0611 248.6742 248.7353 255.8135 319.5191 -0.0610 248.8628 248.9239 255.9739 321.1239 -0.0609 249.0139 249.0748 256.1542 322.7338 -0.0628 249.2066 249.2694 256.3292 324.3376 -0.0672 249.4011 249.4683 256.5494 325.9474 -0.0645 249.5910 249.6555 256.7787 327.5521 -0.0607 249.7682 249.8289 256.9541 329.1768 -0.0588 249.9746 250.0334 257.2228 330.7965 -0.0575 250.1425 250.2000 257.4732 332.4013 -0.0580 250.3425 250.4005 257.7009 334.0104 -0.0554 250.5390 250.5944 257.9200 335.6149 -0.0506 250.6919 250.7425 258.1771 337.2196 -0.0464 250.9215 250.9678 258.4162 338.8388 -0.0507 251.1209 251.1716 258.7137 340.4333 -0.0507 251.2990 251.3497 258.9564 342.0380 -0.0484 251.5069 251.5553 259.1880 343.6476 -0.0494 251.6987 251.7480 259.4479 345.2670 -0.0489 251.8857 251.9347 259.6907 346.8769 -0.0539 252.0469 252.1007 259.9111 348.4816 -0.0529 252.2156 252.2685 260.1444 350.0910 -0.0506 252.4636 252.5142 260.3321 351.7055 -0.0520 252.6926 252.7446 260.5226 353.3103 -0.0474 252.9069 252.9543 260.6817 354.9090 -0.0475 253.0822 253.1297 260.8752 356.5085 -0.0489 253.2361 253.2850 261.0301 358.1286 -0.0437 253.4463 253.4900 261.1719 359.7071 -0.0469 253.6135 253.6604 261.3096 361.3269 -0.0469 253.8027 253.8496 261.4347 362.9316 -0.0443 253.9987 254.0430 261.6222 364.5364 -0.0392 254.2258 254.2650 261.8284 366.1350 -0.0384 254.4625 254.5009 262.0453 367.7346 -0.0383 254.6500 254.6882 262.2304 369.3445 -0.0407 254.8219 254.8626 262.4187 370.9534 -0.0435 255.0151 255.0586 262.6332 372.5530 -0.0435 255.2384 255.2819 262.8959 374.1731 -0.0449 255.4783 255.5232 263.1446 375.7821 -0.0481 255.6499 255.6980 263.4105 377.3816 -0.0507 255.8222 255.8730 263.6226 378.9864 -0.0471 256.0232 256.0703 263.9400 380.5959 -0.0424 256.2349 256.2773 264.2215 382.2000 -0.0411 256.4414 256.4825 264.4893 383.8099 -0.0427 256.6775 256.7202 264.7455 385.4300 -0.0422 256.9184 256.9606 265.0022 387.0443 -0.0445 257.1486 257.1932 265.2365 388.6436 -0.0480 257.3346 257.3826 265.4557 390.2586 -0.0522 257.5113 257.5635 265.6577 391.8628 -0.0576 257.7197 257.7773 265.8333 393.4671 -0.0588 257.9503 258.0091 266.0358 395.0770 -0.0619 258.1578 258.2197 266.2365 396.6971 -0.0583 258.3558 258.4141 266.4608 398.3060 -0.0562 258.5532 258.6095 266.6139 399.9108 -0.0591 258.7650 258.8241 266.7645 401.5360 -0.0559 258.9759 259.0318 266.9190 403.1405 -0.0580 259.1473 259.2053 267.0534 404.7445 -0.0604 259.3323 259.3927 267.1869 406.3698 -0.0674 259.5568 259.6243 267.3309 407.9745 -0.0729 259.7917 259.8645 267.4627 409.5841 -0.0672 260.0298 260.0970 267.6788 411.1881 -0.0642 260.2391 260.3034 267.9374 412.7826 -0.0659 260.4461 260.5120 268.1335 414.3874 -0.0646 260.6326 260.6972 268.3561 415.9921 -0.0677 260.7889 260.8565 268.6304 417.5959 -0.0707 260.9934 261.0641 268.8978 419.2006 -0.0720 261.2439 261.3159 269.1781 420.7951 -0.0705 261.4262 261.4968 269.4524 422.4043 -0.0670 261.6520 261.7191 269.6903 423.9831 -0.0697 261.8851 261.9549 269.9587 425.5879 -0.0737 262.1064 262.1801 270.2299 427.1971 -0.0727 262.3460 262.4187 270.4972 428.7861 -0.0738 262.5512 262.6250 270.7701 430.3858 -0.0725 262.7262 262.7987 271.0070 431.9949 -0.0818 262.9623 263.0441 271.1959 433.5943 -0.0857 263.2068 263.2924 271.4288 435.1888 -0.0843 263.4305 263.5148 271.6415 436.8089 -0.0848 263.6545 263.7393 271.8256 438.4128 -0.0879 263.8759 263.9637 272.0174 440.0071 -0.0872 264.0819 264.1691 272.1945 441.6119 -0.0908 264.2902 264.3810 272.3602 443.2211 -0.0973 264.4944 264.5917 272.5032 444.8255 -0.0978 264.7039 264.8017 272.6112 446.4354 -0.0990 264.8849 264.9839 272.7829 448.0396 -0.1038 265.1254 265.2292 272.9220 449.6439 -0.1055 265.3490 265.4545 273.1075 451.2589 -0.1034 265.6037 265.7071 273.2483 452.8636 -0.1004 265.8463 265.9467 273.4459 454.4571 -0.1017 266.0616 266.1633 273.6477 456.0619 -0.1050 266.2744 266.3794 273.8607 457.6718 -0.1040 266.4546 266.5586 274.0982 459.2763 -0.1066 266.6568 266.7634 274.3423 460.8854 -0.1123 266.8513 266.9635 274.5804 462.4901 -0.1124 267.0685 267.1809 274.8418 464.1000 -0.1153 267.2878 267.4031 275.1330 465.7095 -0.1146 267.5147 267.6293 275.4499 467.3136 -0.1206 267.7557 267.8764 275.7394 468.9235 -0.1253 268.0324 268.1577 275.9961 470.5283 -0.1270 268.2672 268.3942 276.2618 472.1330 -0.1244 268.4776 268.6020 276.5208 473.7371 -0.1244 268.6697 268.7941 276.7836 475.3415 -0.1310 268.8304 268.9614 277.0155 476.9514 -0.1328 269.0359 269.1687 277.2274 478.5561 -0.1371 269.2384 269.3755 277.4254 480.1703 -0.1425 269.4612 269.6037 277.5608 481.7749 -0.1467 269.7141 269.8608 277.7054 483.3745 -0.1490 269.9539 270.1029 277.8640 484.9735 -0.1494 270.1863 270.3357 278.0405 486.5728 -0.1485 270.4214 270.5699 278.1900 488.1775 -0.1438 270.6355 270.7793 278.2927 489.7616 -0.1467 270.8319 270.9786 278.4003 491.3706 -0.1517 271.0669 271.2185 278.5834 492.9856 -0.1529 271.2725 271.4254 278.7625 494.5694 -0.1523 271.5018 271.6540 278.9287 496.2300 -0.1525 271.7327 271.8851 279.1231 497.8706 -0.1621 271.9518 272.1140 279.3384 499.4751 -0.1674 272.2279 272.3953 279.5761 501.0791 -0.1737 272.4135 272.5873 279.8314 502.7044 -0.1794 272.6307 272.8100 280.1098 504.3194 -0.1860 272.8844 273.0704 280.3945 505.9231 -0.1900 273.0950 273.2850 280.6812 507.5279 -0.1927 273.3296 273.5223 280.9764 509.1326 -0.2011 273.5731 273.7743 281.2696 510.7366 -0.2003 273.7886 273.9889 281.5303 512.3411 -0.1967 273.9881 274.1848 281.7995 513.9715 -0.2027 274.2109 274.4136 282.0760 515.5551 -0.2029 274.4324 274.6353 282.3151 517.1749 -0.2080 274.6625 274.8704 282.5316 518.7899 -0.2118 274.8946 275.1064 282.7202 520.3946 -0.2116 275.1072 275.3188 282.8852 521.9833 -0.2151 275.3083 275.5234 283.0731 523.6031 -0.2209 275.5375 275.7583 283.2262 525.2130 -0.2240 275.7545 275.9785 283.3466 526.8173 -0.2253 275.9795 276.2048 283.4552 528.4266 -0.2257 276.2346 276.4603 283.5811 530.0314 -0.2350 276.4677 276.7027 283.6971 531.6565 -0.2398 276.6844 276.9241 283.8369 533.2655 -0.2413 276.9121 277.1534 284.0166 534.8805 -0.2446 277.1409 277.3855 284.2014 536.4750 -0.2394 277.3336 277.5730 284.4116 538.0791 -0.2442 277.5662 277.8104 284.6680 539.6886 -0.2525 277.7879 278.0403 284.9183 541.2934 -0.2521 278.0188 278.2709 285.1767 542.9084 -0.2539 278.2206 278.4744 285.4654 544.5275 -0.2606 278.4896 278.7502 285.7635 546.1220 -0.2652 278.7389 279.0041 286.0276 547.7370 -0.2708 278.9652 279.2361 286.3343 549.3159 -0.2728 279.1996 279.4724 286.6239 550.9148 -0.2802 279.4340 279.7142 286.8954 552.5195 -0.2813 279.6185 279.8998 287.1639 554.1749 -0.2845 279.8679 280.1524 287.4249 555.9279 -0.2880 280.1382 280.4263 287.6932 557.5275 -0.2915 280.3673 280.6589 287.9505 559.1169 -0.2923 280.5823 280.8747 288.1353 560.7206 -0.3031 280.8010 281.1041 288.2713 562.3254 -0.3097 281.0257 281.3354 288.4087 563.9353 -0.3059 281.2539 281.5597 288.5427 565.5349 -0.3040 281.4669 281.7709 288.6735 567.1438 -0.3089 281.7132 282.0220 288.7877 568.7485 -0.3163 281.9607 282.2771 288.9152 570.3533 -0.3205 282.2176 282.5381 289.0308 571.9628 -0.3214 282.4865 282.8079 289.1823 573.5669 -0.3269 282.7034 283.0303 289.3494 575.1768 -0.3329 282.9455 283.2784 289.5519 576.7814 -0.3356 283.1573 283.4929 289.7686 578.3904 -0.3351 283.3823 283.7174 289.9916 579.9951 -0.3387 283.6050 283.9437 290.2234 581.5999 -0.3445 283.7907 284.1353 290.4852 583.2090 -0.3489 283.9880 284.3370 290.7620 584.8238 -0.3526 284.2138 284.5664 291.0281 586.4336 -0.3560 284.4195 284.7755 291.3109 588.0376 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