DTA measure 1gyors Date: 2025325:1054 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 911.09 s Mass = 937.500 mg data_number = 1133 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1118 -0.2577 201.3555 201.6131 260.5434 1.8735 -0.2540 201.6163 201.8702 260.5498 2.7258 -0.2485 201.8719 202.1204 260.5605 3.5178 -0.2428 202.1181 202.3609 260.5762 4.3095 -0.2367 202.3646 202.6012 260.5811 5.1318 -0.2314 202.5916 202.8230 260.5863 5.8935 -0.2271 202.8472 203.0744 260.6155 6.7455 -0.2260 203.1160 203.3420 260.6352 7.5375 -0.2192 203.3793 203.5985 260.6584 8.3295 -0.2158 203.6129 203.8287 260.7106 9.1515 -0.2116 203.8631 204.0746 260.7692 9.9135 -0.2052 204.1022 204.3074 260.8085 10.7655 -0.2000 204.3542 204.5542 260.8730 11.5575 -0.1982 204.5879 204.7860 260.9243 12.3495 -0.1940 204.8381 205.0321 261.0011 13.1715 -0.1887 205.0786 205.2673 261.0728 13.9335 -0.1885 205.3141 205.5026 261.1470 14.7855 -0.1851 205.5847 205.7697 261.2369 15.5775 -0.1844 205.8277 206.0121 261.3397 16.3703 -0.1773 206.0474 206.2248 261.4349 17.1925 -0.1768 206.3020 206.4788 261.5478 17.9543 -0.1718 206.5424 206.7143 261.6663 18.8055 -0.1687 206.7787 206.9474 261.7869 19.5935 -0.1636 207.0172 207.1808 261.9012 20.3815 -0.1587 207.2400 207.3986 262.0247 21.2000 -0.1566 207.4812 207.6378 262.1891 21.9880 -0.1517 207.7194 207.8711 262.3123 22.8070 -0.1543 207.9725 208.1269 262.4626 23.5950 -0.1526 208.2242 208.3768 262.6206 24.3840 -0.1511 208.4449 208.5960 262.7956 25.2325 -0.1469 208.7041 208.8510 262.9486 25.9920 -0.1444 208.8918 209.0362 263.0964 26.8125 -0.1456 209.1647 209.3102 263.2525 27.6043 -0.1402 209.3961 209.5363 263.4306 28.3955 -0.1396 209.6273 209.7668 263.6209 29.2475 -0.1386 209.8603 209.9989 263.8074 30.0095 -0.1414 210.0713 210.2127 263.9885 30.8315 -0.1386 210.3221 210.4607 264.1816 31.6235 -0.1389 210.5372 210.6761 264.3653 32.4155 -0.1419 210.7712 210.9131 264.5289 33.2675 -0.1364 211.0170 211.1534 264.7166 34.0295 -0.1374 211.2326 211.3701 264.8927 34.8515 -0.1333 211.4819 211.6152 265.0986 35.6435 -0.1294 211.7453 211.8747 265.3026 36.4355 -0.1298 211.9661 212.0959 265.4883 37.2875 -0.1278 212.1721 212.2999 265.6591 38.0495 -0.1323 212.3747 212.5070 265.8462 38.8715 -0.1357 212.6238 212.7596 266.0364 39.6635 -0.1322 212.8679 213.0001 266.2221 40.4555 -0.1286 213.0918 213.2204 266.4088 41.3075 -0.1213 213.3247 213.4460 266.5918 42.0695 -0.1216 213.5615 213.6831 266.7460 42.8915 -0.1196 213.7815 213.9011 266.9419 43.7135 -0.1213 214.0006 214.1218 267.1164 44.4755 -0.1203 214.2140 214.3342 267.2757 45.3270 -0.1171 214.4485 214.5655 267.4782 46.1190 -0.1229 214.6815 214.8043 267.6360 46.9123 -0.1260 214.8988 215.0249 267.7771 47.7350 -0.1218 215.1289 215.2508 267.9424 48.4965 -0.1236 215.3476 215.4712 268.1003 49.3490 -0.1235 215.5752 215.6988 268.2717 50.1108 -0.1194 215.7883 215.9077 268.4379 50.9313 -0.1222 216.0048 216.1270 268.5944 51.7493 -0.1164 216.2355 216.3520 268.7545 52.5070 -0.1133 216.4536 216.5668 268.8534 53.3540 -0.1164 216.6800 216.7963 269.0314 54.1140 -0.1181 216.9062 217.0242 269.1763 54.9325 -0.1201 217.1162 217.2364 269.3383 55.7510 -0.1226 217.3571 217.4797 269.4400 56.5095 -0.1290 217.5648 217.6938 269.5772 57.3585 -0.1308 217.7962 217.9271 269.7391 58.1173 -0.1296 218.0201 218.1497 269.8692 58.9385 -0.1297 218.2343 218.3640 269.9979 59.7305 -0.1253 218.4448 218.5700 270.1197 60.5220 -0.1181 218.6669 218.7850 270.2360 61.3735 -0.1153 218.8867 219.0020 270.3833 62.1355 -0.1193 219.1036 219.2229 270.5114 62.9575 -0.1146 219.3336 219.4482 270.6315 63.7495 -0.1176 219.5579 219.6754 270.7549 64.5415 -0.1191 219.7683 219.8874 270.8667 65.3635 -0.1177 219.9759 220.0935 271.0200 66.1553 -0.1189 220.1769 220.2958 271.1477 66.9773 -0.1200 220.3981 220.5180 271.2532 67.7693 -0.1216 220.6209 220.7425 271.3809 68.5608 -0.1227 220.8410 220.9637 271.5151 69.3833 -0.1215 221.0610 221.1825 271.6283 70.1453 -0.1206 221.2695 221.3901 271.7337 70.9973 -0.1224 221.4793 221.6017 271.8581 71.7890 -0.1209 221.7013 221.8222 271.9702 72.5805 -0.1217 221.9147 222.0364 272.0874 73.4030 -0.1238 222.1435 222.2673 272.2075 74.1645 -0.1195 222.3500 222.4695 272.3136 75.0170 -0.1179 222.5630 222.6808 272.4488 75.8690 -0.1200 222.7921 222.9121 272.5832 76.7210 -0.1226 223.0114 223.1340 272.6862 77.5130 -0.1192 223.2110 223.3301 272.7985 78.3045 -0.1151 223.4133 223.5285 272.9453 79.1273 -0.1176 223.6272 223.7449 273.0591 79.8895 -0.1239 223.8507 223.9745 273.1657 80.7418 -0.1246 224.0720 224.1967 273.2824 81.5638 -0.1262 224.2968 224.4230 273.4004 82.3255 -0.1303 224.4959 224.6262 273.5045 83.1783 -0.1389 224.7196 224.8585 273.6191 83.9390 -0.1381 224.8985 225.0365 273.7206 84.7570 -0.1382 225.1003 225.2385 273.8711 85.5750 -0.1261 225.3207 225.4467 273.9667 86.3330 -0.1218 225.5128 225.6346 274.0647 87.1800 -0.1172 225.7323 225.8496 274.2117 87.9390 -0.1136 225.9348 226.0485 274.3117 88.7570 -0.1135 226.1375 226.2509 274.4156 89.5753 -0.1139 226.3515 226.4654 274.5564 90.3330 -0.1204 226.5543 226.6747 274.6926 91.1818 -0.1179 226.7548 226.8726 274.7976 91.9708 -0.1147 226.9686 227.0834 274.9160 92.7610 -0.1152 227.1754 227.2905 275.0378 93.5830 -0.1165 227.3810 227.4975 275.1691 94.3445 -0.1206 227.5691 227.6897 275.2757 95.2273 -0.1238 227.7858 227.9096 275.4406 96.0488 -0.1301 228.0040 228.1341 275.5635 96.8710 -0.1362 228.2096 228.3458 275.7115 97.6325 -0.1417 228.4125 228.5541 275.8308 98.4850 -0.1340 228.6119 228.7459 275.9588 99.2468 -0.1394 228.8067 228.9461 276.0808 100.0688 -0.1444 229.0085 229.1528 276.2074 100.8910 -0.1486 229.2146 229.3632 276.3352 101.6525 -0.1508 229.4254 229.5761 276.4398 102.5050 -0.1524 229.6482 229.8006 276.6012 103.2668 -0.1508 229.8381 229.9889 276.7569 104.0888 -0.1465 230.0302 230.1767 276.8948 104.9108 -0.1356 230.2377 230.3733 277.0106 105.6725 -0.1285 230.4414 230.5700 277.1533 106.5248 -0.1302 230.6369 230.7671 277.2830 107.3168 -0.1286 230.8439 230.9726 277.4205 108.1085 -0.1315 231.0213 231.1528 277.5665 108.9308 -0.1356 231.2418 231.3775 277.7040 109.7225 -0.1434 231.4287 231.5721 277.8173 110.5455 -0.1479 231.6269 231.7748 277.9492 111.3378 -0.1502 231.8147 231.9648 278.1102 112.1295 -0.1520 232.0323 232.1844 278.2452 112.9518 -0.1576 232.2525 232.4101 278.3825 113.7435 -0.1596 232.4245 232.5842 278.5072 114.5655 -0.1588 232.6240 232.7828 278.6529 115.3575 -0.1558 232.8304 232.9862 278.7980 116.1470 -0.1592 233.0258 233.1850 278.9340 116.9950 -0.1578 233.2287 233.3865 279.0637 117.7530 -0.1563 233.4047 233.5609 279.1937 118.5710 -0.1592 233.6005 233.7597 279.3403 119.3590 -0.1652 233.7806 233.9459 279.4662 120.1480 -0.1665 233.9720 234.1385 279.6096 120.9665 -0.1593 234.1768 234.3361 279.7616 121.7550 -0.1639 234.3635 234.5274 279.8995 122.5738 -0.1609 234.5515 234.7124 280.0339 123.3625 -0.1626 234.7442 234.9068 280.1616 124.1535 -0.1647 234.9395 235.1042 280.3032 124.9758 -0.1700 235.1533 235.3233 280.4569 125.7375 -0.1728 235.3263 235.4991 280.5771 126.5898 -0.1712 235.5240 235.6952 280.7061 127.3818 -0.1704 235.6958 235.8662 280.8218 128.1735 -0.1728 235.9141 236.0870 280.9730 128.9955 -0.1759 236.1065 236.2824 281.1087 129.7575 -0.1777 236.2921 236.4698 281.2435 130.6098 -0.1762 236.4874 236.6637 281.4022 131.3715 -0.1812 236.6888 236.8700 281.5521 132.1938 -0.1782 236.8639 237.0421 281.6755 132.9860 -0.1797 237.0487 237.2284 281.8133 133.7775 -0.1810 237.2473 237.4284 281.9489 134.6300 -0.1837 237.4573 237.6410 282.0785 135.3915 -0.1879 237.6307 237.8186 282.2038 136.2138 -0.1897 237.8309 238.0206 282.3359 137.0055 -0.1895 238.0150 238.2045 282.4685 137.7975 -0.1865 238.2092 238.3957 282.6141 138.6495 -0.1899 238.4172 238.6071 282.7795 139.4115 -0.1977 238.5803 238.7780 282.9046 140.2335 -0.1967 238.7635 238.9602 283.0566 141.0255 -0.1966 238.9486 239.1453 283.1931 141.8175 -0.2008 239.1333 239.3340 283.3147 142.6700 -0.2020 239.3433 239.5453 283.4437 143.4325 -0.2031 239.5176 239.7208 283.5999 144.2545 -0.2023 239.7258 239.9281 283.7306 145.0465 -0.2075 239.8927 240.1002 283.8532 145.8393 -0.2123 240.0749 240.2872 283.9827 146.6615 -0.2214 240.2614 240.4828 284.1220 147.4530 -0.2284 240.4428 240.6713 284.2392 148.2718 -0.2244 240.6417 240.8661 284.3821 149.0600 -0.2191 240.8102 241.0293 284.5219 149.8480 -0.2197 241.0204 241.2401 284.6547 150.6660 -0.2249 241.2149 241.4398 284.8062 151.4540 -0.2319 241.3928 241.6246 284.9321 152.2728 -0.2300 241.5512 241.7812 285.0768 153.0610 -0.2264 241.7443 241.9707 285.1855 153.8500 -0.2288 241.9430 242.1718 285.3158 154.6988 -0.2310 242.1339 242.3649 285.4631 155.4585 -0.2320 242.2996 242.5316 285.5812 156.2793 -0.2329 242.5060 242.7389 285.7054 157.0988 -0.2422 242.6944 242.9367 285.8366 157.8605 -0.2534 242.8676 243.1210 285.9826 158.7125 -0.2589 243.0859 243.3448 286.1065 159.4745 -0.2611 243.2503 243.5115 286.2246 160.2965 -0.2630 243.4004 243.6634 286.3644 161.0908 -0.2662 243.5882 243.8544 286.5246 161.8845 -0.2703 243.7739 244.0442 286.6648 162.7365 -0.2685 243.9679 244.2364 286.7999 163.4985 -0.2706 244.1495 244.4201 286.9236 164.3205 -0.2711 244.3500 244.6211 287.0697 165.1125 -0.2750 244.5070 244.7820 287.1851 165.9045 -0.2782 244.6747 244.9528 287.3046 166.7565 -0.2794 244.8761 245.1555 287.4535 167.5185 -0.2813 245.0430 245.3243 287.5762 168.3405 -0.2850 245.2530 245.5380 287.7011 169.1325 -0.2863 245.4360 245.7223 287.8283 169.9245 -0.2837 245.6003 245.8841 287.9723 170.7765 -0.2853 245.7882 246.0735 288.0907 171.5385 -0.2862 245.9451 246.2313 288.2126 172.3605 -0.2832 246.1163 246.3994 288.3519 173.1825 -0.2859 246.3202 246.6061 288.4757 173.9443 -0.2890 246.4775 246.7665 288.5992 174.7965 -0.2907 246.6732 246.9640 288.7462 175.5883 -0.2911 246.8480 247.1391 288.8734 176.3795 -0.2954 247.0410 247.3364 289.0165 177.2023 -0.2990 247.2244 247.5233 289.1472 177.9645 -0.2982 247.3691 247.6673 289.2754 178.8170 -0.3017 247.5944 247.8961 289.4201 179.6088 -0.3042 247.7604 248.0645 289.5384 180.3983 -0.3057 247.9417 248.2474 289.6634 181.2165 -0.3061 248.1126 248.4187 289.7945 181.9740 -0.3052 248.2772 248.5824 289.9149 182.8228 -0.3070 248.4767 248.7837 290.0504 183.6105 -0.3098 248.6671 248.9768 290.1735 184.3988 -0.3118 248.8203 249.1321 290.2760 185.2173 -0.3111 249.0086 249.3197 290.4138 186.0060 -0.3191 249.1872 249.5064 290.5494 186.8265 -0.3186 249.3546 249.6733 290.6881 187.6165 -0.3186 249.5371 249.8557 290.8254 188.4068 -0.3209 249.7134 250.0343 290.9446 189.2265 -0.3233 249.8665 250.1899 291.0686 190.0185 -0.3236 250.0459 250.3695 291.1838 190.8405 -0.3286 250.2431 250.5716 291.3431 191.6325 -0.3298 250.4296 250.7594 291.4780 192.4245 -0.3370 250.5969 250.9339 291.5841 193.2465 -0.3376 250.7831 251.1207 291.6969 194.0085 -0.3377 250.9246 251.2623 291.8175 194.8605 -0.3399 251.1122 251.4521 291.9535 195.6525 -0.3410 251.2816 251.6226 292.0897 196.4443 -0.3418 251.4511 251.7929 292.2087 197.2665 -0.3485 251.6399 251.9884 292.3349 198.0280 -0.3545 251.8210 252.1755 292.4644 198.8803 -0.3510 251.9880 252.3390 292.6046 199.6720 -0.3535 252.1611 252.5146 292.7389 200.4635 -0.3543 252.3398 252.6942 292.8624 201.2863 -0.3569 252.5147 252.8716 292.9766 202.0478 -0.3562 252.6662 253.0225 293.1054 202.9000 -0.3606 252.8569 253.2175 293.2476 203.6618 -0.3619 253.0366 253.3985 293.3710 204.4838 -0.3657 253.2106 253.5763 293.4930 205.3060 -0.3634 253.3888 253.7522 293.6243 206.0675 -0.3649 253.5526 253.9175 293.7445 206.9200 -0.3692 253.7222 254.0915 293.8733 207.6818 -0.3704 253.8893 254.2597 293.9819 208.5038 -0.3702 254.0704 254.4406 294.1235 209.2960 -0.3675 254.2333 254.6008 294.2679 210.0875 -0.3703 254.4082 254.7785 294.3869 210.9403 -0.3691 254.5870 254.9561 294.5134 211.7025 -0.3697 254.7503 255.1200 294.6584 212.5245 -0.3679 254.9108 255.2787 294.8094 213.3133 -0.3690 255.0832 255.4522 294.9297 214.1010 -0.3759 255.2591 255.6350 295.0595 214.9490 -0.3807 255.4444 255.8252 295.1965 215.7070 -0.3816 255.6110 255.9926 295.3342 216.5250 -0.3814 255.7836 256.1650 295.4960 217.3138 -0.3824 255.9294 256.3118 295.6029 218.1030 -0.3889 256.1058 256.4947 295.7583 218.9520 -0.3939 256.2678 256.6617 295.8957 219.7105 -0.3956 256.4239 256.8196 296.0320 220.5310 -0.4009 256.6142 257.0151 296.1916 221.3210 -0.3996 256.8109 257.2106 296.3307 222.1125 -0.4037 256.9580 257.3617 296.4557 222.9640 -0.4014 257.1308 257.5322 296.6037 223.7258 -0.4074 257.2929 257.7004 296.7666 224.5478 -0.4092 257.4743 257.8835 296.9130 225.3400 -0.4128 257.6667 258.0795 297.0621 226.1315 -0.4174 257.8053 258.2227 297.2246 226.9540 -0.4184 257.9954 258.4138 297.3686 227.7458 -0.4176 258.1498 258.5675 297.5246 228.5678 -0.4181 258.3114 258.7295 297.6572 229.3600 -0.4176 258.4814 258.8991 297.8299 230.1515 -0.4216 258.6428 259.0644 297.9507 230.9740 -0.4217 258.8278 259.2495 298.0790 231.7658 -0.4232 258.9784 259.4016 298.2281 232.5878 -0.4233 259.1473 259.5707 298.3932 233.3800 -0.4340 259.3202 259.7542 298.5260 234.1725 -0.4439 259.4960 259.9399 298.6693 234.9950 -0.4464 259.6796 260.1261 298.7765 235.7865 -0.4460 259.8223 260.2683 298.9213 236.6088 -0.4495 260.0046 260.4541 299.0790 237.4008 -0.4526 260.1712 260.6238 299.2159 238.1925 -0.4571 260.3320 260.7891 299.3425 239.0448 -0.4554 260.5001 260.9554 299.4941 239.8065 -0.4556 260.6633 261.1189 299.6108 240.6288 -0.4651 260.8558 261.3210 299.7676 241.4208 -0.4686 261.0023 261.4709 299.8764 242.2125 -0.4728 261.1659 261.6387 299.9976 243.0645 -0.4701 261.3525 261.8226 300.1492 243.8265 -0.4742 261.5057 261.9799 300.2902 244.6488 -0.4771 261.6695 262.1466 300.4226 245.4670 -0.4799 261.8473 262.3272 300.5576 246.2250 -0.4827 262.0094 262.4921 300.6537 247.0730 -0.4809 262.1731 262.6540 300.8001 247.8310 -0.4807 262.3305 262.8112 300.9405 248.6490 -0.4809 262.4954 262.9763 301.0658 249.4675 -0.4864 262.6654 263.1519 301.1961 250.2260 -0.4856 262.8241 263.3098 301.3223 251.0748 -0.4834 262.9816 263.4650 301.4527 251.8635 -0.4853 263.1391 263.6244 301.5808 252.6538 -0.4868 263.3213 263.8081 301.6738 253.4740 -0.4874 263.4931 263.9805 301.8033 254.2648 -0.4956 263.6532 264.1488 301.9409 255.0868 -0.5049 263.8035 264.3084 302.0776 255.8788 -0.5099 263.9771 264.4869 302.1918 256.6705 -0.5129 264.1175 264.6305 302.3177 257.4928 -0.5167 264.2844 264.8010 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