DTA measure 3gyors Date: 2026324:1131 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1648.47 s Mass = 959.400 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5140 -14.7833 453.4137 468.1970 432.5714 4.1326 -14.7905 453.3708 468.1613 432.8395 5.7310 -14.7981 453.3293 468.1273 433.1057 7.3243 -14.7950 453.2826 468.0776 433.2802 8.9274 -14.7986 453.2689 468.0674 433.4232 10.5360 -14.8033 453.2458 468.0491 433.5155 12.1394 -14.8052 453.1969 468.0021 433.5107 13.7479 -14.8055 453.1006 467.9061 433.4293 15.3565 -14.8060 453.0821 467.8881 433.2062 16.9650 -14.8063 453.0636 467.8699 432.9053 18.5735 -14.8008 453.0193 467.8201 432.5657 20.1769 -14.7992 452.9898 467.7890 432.1824 21.7853 -14.8088 452.9333 467.7421 431.7081 23.3939 -14.8082 452.8873 467.6954 431.2639 25.0025 -14.8075 452.8182 467.6257 430.7759 26.6110 -14.8076 452.7503 467.5579 430.2776 28.2041 -14.8090 452.6884 467.4974 429.7830 29.8076 -14.8086 452.6415 467.4502 429.3116 31.4314 -14.8153 452.5923 467.4076 428.8738 33.0400 -14.8178 452.5199 467.3377 428.5101 34.6384 -14.8217 452.4569 467.2786 428.1827 36.2415 -14.8387 452.3863 467.2250 427.9107 37.8553 -14.8495 452.2810 467.1305 427.6951 39.4584 -14.8609 452.1597 467.0207 427.5704 41.0670 -14.8684 452.0939 466.9623 427.5234 42.6704 -14.8744 452.0294 466.9038 427.4516 44.2994 -14.8811 451.9168 466.7979 427.4594 45.9028 -14.8872 451.8059 466.6932 427.4617 47.5111 -14.8941 451.7222 466.6163 427.4193 49.1196 -14.8964 451.6291 466.5255 427.3678 50.7231 -14.8992 451.5071 466.4063 427.2998 52.3214 -14.9010 451.4306 466.3315 427.2658 53.9248 -14.9055 451.3379 466.2434 427.1673 55.5078 -14.9095 451.2236 466.1331 427.0448 57.1315 -14.9123 451.1421 466.0544 426.8564 58.7300 -14.9177 451.0198 465.9374 426.6482 60.3386 -14.9204 450.9285 465.8490 426.3991 61.9416 -14.9181 450.8207 465.7389 426.1004 63.5451 -14.9240 450.7045 465.6285 425.7797 65.1384 -14.9257 450.6031 465.5287 425.4738 66.7418 -14.9227 450.5320 465.4547 425.1389 68.3503 -14.9230 450.4434 465.3665 424.8160 69.9741 -14.9246 450.3214 465.2460 424.4780 71.5826 -14.9275 450.2242 465.1518 424.1517 73.1861 -14.9308 450.0984 465.0292 423.8425 74.7894 -14.9369 449.9758 464.9127 423.5688 76.3929 -14.9462 449.7982 464.7443 423.3200 78.0015 -14.9509 449.6669 464.6178 423.0864 79.6098 -14.9546 449.5526 464.5071 422.8228 81.2184 -14.9595 449.4614 464.4209 422.6228 82.8373 -14.9613 449.3200 464.2813 422.4694 84.4405 -14.9600 449.1979 464.1579 422.3428 86.0645 -14.9621 449.0710 464.0331 422.2255 87.6680 -14.9627 448.9197 463.8824 422.0750 89.2815 -14.9663 448.8154 463.7817 421.9382 90.8850 -14.9691 448.6537 463.6228 421.8345 92.4936 -14.9744 448.4973 463.4717 421.6833 94.1020 -14.9787 448.3658 463.3445 421.5635 95.7004 -14.9824 448.2650 463.2474 421.4383 97.3191 -14.9811 448.1513 463.1325 421.3077 98.9276 -14.9770 448.0203 462.9973 421.0871 100.5361 -14.9765 447.9401 462.9167 420.8406 102.1446 -14.9768 447.7650 462.7418 420.6376 103.7480 -14.9744 447.6132 462.5876 420.4296 105.3618 -14.9755 447.4777 462.4533 420.1951 106.9495 -14.9763 447.3390 462.3153 419.9488 108.5581 -14.9737 447.2093 462.1830 419.6772 110.1821 -14.9729 447.0508 462.0237 419.3886 111.7904 -14.9714 446.8976 461.8690 419.1472 113.3990 -14.9737 446.6990 461.6727 418.9016 114.9819 -14.9773 446.5617 461.5390 418.6346 116.5904 -14.9826 446.4354 461.4180 418.3483 118.1888 -14.9856 446.2894 461.2750 418.0973 119.7869 -14.9872 446.1392 461.1264 417.8370 121.3954 -14.9906 445.9711 460.9617 417.6091 122.9784 -14.9898 445.7955 460.7853 417.4271 124.5970 -14.9883 445.6490 460.6373 417.2402 126.2056 -14.9856 445.4951 460.4807 417.0495 127.8089 -14.9887 445.3726 460.3613 416.8453 129.4020 -14.9882 445.2314 460.2196 416.6501 131.0055 -14.9833 445.0423 460.0256 416.4651 132.6140 -14.9775 444.8909 459.8684 416.3055 134.2175 -14.9704 444.7568 459.7272 416.1374 135.8209 -14.9697 444.5382 459.5079 416.0198 137.4295 -14.9715 444.3951 459.3666 415.8607 139.0380 -14.9705 444.2289 459.1993 415.6827 140.6465 -14.9644 444.0800 459.0444 415.4381 142.2500 -14.9579 443.9257 458.8836 415.2700 143.8584 -14.9546 443.7650 458.7196 415.0669 145.4619 -14.9492 443.5668 458.5160 414.8535 147.0704 -14.9454 443.3805 458.3260 414.6369 148.6738 -14.9449 443.2182 458.1631 414.4007 150.2926 -14.9365 443.0452 457.9818 414.1627 151.9013 -14.9289 442.8732 457.8021 413.9247 153.5098 -14.9224 442.7307 457.6531 413.6743 155.1183 -14.9181 442.5716 457.4898 413.3845 156.7216 -14.9225 442.4288 457.3513 413.1730 158.3301 -14.9256 442.2682 457.1938 412.9498 159.9336 -14.9221 442.0636 456.9857 412.7510 161.5625 -14.9255 441.8749 456.8004 412.5237 163.1659 -14.9297 441.6880 456.6176 412.3131 164.7745 -14.9280 441.5064 456.4345 412.0515 166.3779 -14.9227 441.3298 456.2525 411.8466 167.9916 -14.9158 441.1601 456.0759 411.6376 169.5950 -14.9132 441.0208 455.9340 411.4183 171.1985 -14.9093 440.8445 455.7538 411.2527 172.8275 -14.9029 440.6640 455.5668 411.0229 174.4310 -14.8949 440.4818 455.3767 410.8321 176.0446 -14.8923 440.2751 455.1675 410.6408 177.6480 -14.8879 440.1223 455.0102 410.4428 179.2566 -14.8774 439.9147 454.7921 410.2820 180.8549 -14.8738 439.7309 454.6047 410.0950 182.4583 -14.8697 439.5524 454.4221 409.9621 184.0771 -14.8632 439.3678 454.2309 409.7869 185.6755 -14.8592 439.2002 454.0594 409.5970 187.2839 -14.8508 439.0180 453.8687 409.4019 188.8670 -14.8434 438.8166 453.6600 409.1761 190.4705 -14.8366 438.6683 453.5049 408.9210 192.0788 -14.8341 438.5304 453.3646 408.6866 193.6823 -14.8324 438.3622 453.1947 408.4721 195.2908 -14.8277 438.1722 452.9999 408.2184 196.8993 -14.8202 437.9643 452.7846 407.9879 198.4874 -14.8173 437.7828 452.6001 407.7785 200.1061 -14.8142 437.5605 452.3747 407.5356 201.7146 -14.8087 437.3657 452.1744 407.3018 203.3181 -14.7995 437.1878 451.9872 407.0955 204.9266 -14.7957 436.9890 451.7847 406.8485 206.5300 -14.7882 436.7957 451.5839 406.6523 208.1181 -14.7817 436.6417 451.4234 406.4159 209.7266 -14.7768 436.4866 451.2634 406.2368 211.3300 -14.7720 436.3067 451.0787 406.0092 212.9540 -14.7595 436.1166 450.8760 405.8000 214.5574 -14.7570 435.8998 450.6567 405.5854 216.1658 -14.7555 435.6776 450.4331 405.3796 217.7744 -14.7453 435.5253 450.2705 405.1523 219.3828 -14.7448 435.3840 450.1289 404.9772 220.9760 -14.7403 435.1796 449.9199 404.8038 222.5845 -14.7298 434.9596 449.6894 404.6067 224.1878 -14.7171 434.7818 449.4989 404.4069 225.8118 -14.7077 434.5738 449.2816 404.1973 227.4200 -14.7015 434.3907 449.0923 404.0059 229.0235 -14.6949 434.2356 448.9306 403.7959 230.6168 -14.6895 434.0324 448.7219 403.6019 232.2353 -14.6837 433.8679 448.5516 403.4204 233.8336 -14.6817 433.6483 448.3299 403.2059 235.4369 -14.6721 433.4519 448.1240 403.0026 237.0455 -14.6622 433.2607 447.9229 402.7825 238.6644 -14.6549 433.0519 447.7068 402.5346 240.2729 -14.6459 432.8522 447.4981 402.3021 241.8814 -14.6391 432.6677 447.3068 402.0972 243.4848 -14.6271 432.4788 447.1059 401.8803 245.0831 -14.6202 432.3032 446.9233 401.6200 246.6864 -14.6115 432.0763 446.6878 401.3902 248.3001 -14.6033 431.8884 446.4917 401.1274 249.8778 -14.5969 431.6834 446.2803 400.9435 251.4813 -14.5823 431.5089 446.0913 400.7599 253.1001 -14.5714 431.3087 445.8801 400.5452 254.7085 -14.5630 431.1140 445.6770 400.3455 256.3120 -14.5557 430.8967 445.4524 400.1453 257.8999 -14.5478 430.7074 445.2552 399.9475 259.5084 -14.5399 430.4695 445.0094 399.7419 261.1119 -14.5359 430.2899 444.8258 399.5633 262.7204 -14.5312 430.1388 444.6700 399.3330 264.3238 -14.5223 429.9431 444.4655 399.1482 265.9426 -14.5191 429.7597 444.2789 398.9553 267.5511 -14.5108 429.5614 444.0722 398.7851 269.1545 -14.5010 429.3085 443.8095 398.5978 270.7631 -14.4961 429.0934 443.5894 398.3956 272.3716 -14.4853 428.8771 443.3624 398.1727 273.9750 -14.4794 428.7069 443.1862 397.9702 275.5785 -14.4704 428.4898 442.9602 397.7421 277.1923 -14.4649 428.2952 442.7601 397.5123 278.8109 -14.4517 428.1130 442.5647 397.2350 280.4195 -14.4468 427.9049 442.3517 396.9902 282.0280 -14.4380 427.7260 442.1640 396.7614 283.6365 -14.4279 427.5489 441.9768 396.5394 285.2400 -14.4163 427.3577 441.7740 396.3204 286.8484 -14.4038 427.1631 441.5669 396.1339 288.4569 -14.3976 426.9306 441.3282 395.9020 290.0809 -14.3887 426.7345 441.1233 395.6884 291.6841 -14.3794 426.5297 440.9091 395.5003 293.2926 -14.3730 426.3069 440.6799 395.3030 294.9011 -14.3665 426.0888 440.4553 395.1189 296.5096 -14.3560 425.8808 440.2368 394.9348 298.1131 -14.3520 425.6688 440.0209 394.7475 299.7319 -14.3428 425.4502 439.7929 394.5538 301.3249 -14.3283 425.2583 439.5866 394.3542 302.9539 -14.3149 425.0609 439.3758 394.1232 304.5623 -14.3129 424.8705 439.1834 393.9243 306.1709 -14.3083 424.6501 438.9584 393.6986 307.7743 -14.2998 424.4728 438.7726 393.4869 309.3776 -14.2819 424.2680 438.5498 393.2393 310.9606 -14.2711 424.0623 438.3334 392.9799 312.5639 -14.2649 423.8945 438.1594 392.7582 314.1621 -14.2539 423.6570 437.9109 392.5540 315.7654 -14.2501 423.4380 437.6881 392.3313 317.3739 -14.2423 423.2268 437.4691 392.1286 318.9774 -14.2361 423.0248 437.2609 391.9298 320.5756 -14.2259 422.8167 437.0426 391.7019 322.1790 -14.2162 422.6051 436.8213 391.5250 323.7774 -14.2078 422.4168 436.6245 391.3181 325.3859 -14.1989 422.2363 436.4352 391.1348 326.9893 -14.1855 422.0392 436.2247 390.9331 328.5979 -14.1813 421.8062 435.9875 390.7379 330.1961 -14.1804 421.5867 435.7671 390.5273 331.7944 -14.1721 421.3740 435.5461 390.3124 333.3979 -14.1574 421.1989 435.3563 390.0894 335.0218 -14.1497 420.9825 435.1322 389.8600 336.6251 -14.1416 420.7715 434.9131 389.6741 338.2338 -14.1290 420.6160 434.7450 389.4592 339.8371 -14.1166 420.4269 434.5436 389.2442 341.4456 -14.1063 420.2382 434.3444 389.0335 343.0491 -14.0922 419.9790 434.0712 388.8315 344.6474 -14.0825 419.7513 433.8339 388.6324 346.2508 -14.0748 419.5365 433.6114 388.4355 347.8696 -14.0655 419.3375 433.4029 388.2375 349.4783 -14.0573 419.1309 433.1882 388.0277 351.0815 -14.0474 418.9390 432.9865 387.8096 352.6953 -14.0394 418.7265 432.7659 387.6011 354.3038 -14.0283 418.4901 432.5183 387.3810 355.9070 -14.0196 418.2753 432.2949 387.1567 357.5208 -14.0117 418.1068 432.1185 386.9244 359.1089 -14.0014 417.9111 431.9125 386.6909 360.7174 -13.9909 417.7040 431.6949 386.4687 362.3516 -13.9768 417.5185 431.4953 386.2916 363.9600 -13.9678 417.3290 431.2968 386.0615 365.5634 -13.9613 417.1108 431.0721 385.7986 367.1618 -13.9472 416.8581 430.8053 385.5884 368.7753 -13.9386 416.6611 430.5997 385.3275 370.3839 -13.9297 416.4479 430.3775 385.1346 371.9823 -13.9223 416.2509 430.1732 384.9260 373.5906 -13.9145 416.0440 429.9584 384.7043 375.1736 -13.9065 415.8374 429.7439 384.5132 376.7874 -13.8989 415.6622 429.5612 384.3058 378.3958 -13.8902 415.4773 429.3675 384.1179 379.9993 -13.8775 415.2547 429.1323 383.8941 381.5976 -13.8643 415.0458 428.9101 383.7055 383.2060 -13.8555 414.8130 428.6685 383.4975 384.8095 -13.8487 414.6188 428.4674 383.3134 386.4180 -13.8430 414.4064 428.2493 383.1542 388.0368 -13.8345 414.1867 428.0211 382.9539 389.6453 -13.8229 413.9860 427.8088 382.7233 391.2486 -13.8107 413.7909 427.6016 382.5229 392.8520 -13.8041 413.5863 427.3904 382.2908 394.4658 -13.7896 413.3501 427.1397 382.0880 396.0691 -13.7828 413.1145 426.8973 381.8805 397.6775 -13.7792 412.9234 426.7027 381.6815 399.2964 -13.7745 412.7332 426.5077 381.4761 400.9048 -13.7677 412.5147 426.2824 381.2587 402.5081 -13.7585 412.3447 426.1033 381.0657 404.1065 -13.7532 412.1277 425.8809 380.8746 405.7098 -13.7430 411.9404 425.6834 380.6394 407.3184 -13.7275 411.7213 425.4489 380.4073 408.9215 -13.7162 411.5301 425.2463 380.1668 410.5301 -13.7045 411.2985 425.0031 379.9582 412.1540 -13.6890 411.0724 424.7614 379.7449 413.7573 -13.6795 410.8779 424.5574 379.5222 415.3606 -13.6726 410.6838 424.3564 379.3153 416.9691 -13.6637 410.4555 424.1193 379.0735 418.5726 -13.6498 410.2086 423.8584 378.8438 420.1864 -13.6418 409.9845 423.6263 378.6190 421.7949 -13.6317 409.7665 423.3982 378.4109 423.4034 -13.6177 409.5493 423.1670 378.2058 425.0223 -13.6070 409.3388 422.9458 377.9586 426.6306 -13.5986 409.1030 422.7017 377.7104 428.2391 -13.5919 408.8972 422.4891 377.5151 429.8324 -13.5822 408.6982 422.2803 377.3298 431.4408 -13.5693 408.5090 422.0783 377.1720 433.0545 -13.5607 408.3058 421.8665 376.9734 434.6580 -13.5535 408.1045 421.6580 376.7739 436.2664 -13.5426 407.8891 421.4317 376.5484 437.8801 -13.5332 407.6946 421.2278 376.3514 439.4733 -13.5178 407.4642 420.9820 376.1515 441.0766 -13.5105 407.2664 420.7769 375.9507 442.6853 -13.5018 407.0734 420.5752 375.7331 444.2733 -13.4932 406.8892 420.3824 375.5394 445.8818 -13.4865 406.6983 420.1848 375.3285 447.4853 -13.4748 406.5145 419.9893 375.1618 449.0888 -13.4636 406.2925 419.7561 374.9328 450.7074 -13.4551 406.0788 419.5339 374.6940 452.3109 -13.4447 405.8598 419.3046 374.4684 453.9195 -13.4359 405.6300 419.0659 374.2588 455.5228 -13.4286 405.3907 418.8194 374.0515 457.1263 -13.4147 405.1574 418.5721 373.8017 458.7350 -13.4039 404.9161 418.3201 373.5921 460.3383 -13.3965 404.6768 418.0733 373.3733 461.9621 -13.3845 404.4871 417.8716 373.1873 463.5656 -13.3759 404.3163 417.6921 372.9840 465.1743 -13.3713 404.0750 417.4463 372.7464 466.7776 -13.3604 403.8805 417.2409 372.5140 468.3914 -13.3514 403.6434 416.9949 372.3265 469.9794 -13.3448 403.4495 416.7943 372.0943 471.5879 -13.3347 403.2453 416.5800 371.8770 473.2016 -13.3201 403.0600 416.3801 371.6576 474.7999 -13.3121 402.8500 416.1621 371.4255 476.4238 -13.3045 402.6046 415.9090 371.2005 478.0426 -13.2927 402.4109 415.7036 370.9925 479.6460 -13.2874 402.2108 415.4981 370.7776 481.2545 -13.2829 401.9711 415.2541 370.5737 482.8631 -13.2692 401.7719 415.0411 370.3340 484.4714 -13.2564 401.5835 414.8399 370.1386 486.0800 -13.2489 401.3732 414.6221 369.9500 487.6835 -13.2436 401.1524 414.3960 369.7461 489.3073 -13.2377 400.9454 414.1831 369.5396 490.9158 -13.2240 400.7318 413.9558 369.3549 492.5243 -13.2185 400.5038 413.7222 369.1926 494.1275 -13.2069 400.3262 413.5331 368.9908 495.7413 -13.1962 400.1181 413.3144 368.7967 497.3444 -13.1875 399.9118 413.0993 368.5563 498.9581 -13.1793 399.6990 412.8783 368.3741 500.5766 -13.1676 399.4741 412.6417 368.1910 502.1596 -13.1612 399.2863 412.4475 367.9796 503.7631 -13.1498 399.0653 412.2151 367.7456 505.3615 -13.1393 398.8415 411.9808 367.5136 506.9648 -13.1304 398.6296 411.7600 367.2502 508.5734 -13.1208 398.3900 411.5107 367.0554 510.1766 -13.1197 398.2316 411.3512 366.8476 511.7750 -13.1143 398.0303 411.1446 366.6520 513.3990 -13.1034 397.8402 410.9436 366.4165 515.0023 -13.0920 397.6360 410.7280 366.1926 516.6109 -13.0816 397.3972 410.4787 365.9607 518.2144 -13.0751 397.2050 410.2801 365.7298 519.8229 -13.0695 396.9774 410.0469 365.5637 521.4263 -13.0570 396.7308 409.7877 365.3380 523.0298 -13.0470 396.4895 409.5365 365.1058 524.6536 -13.0384 396.2516 409.2900 364.8822 526.2571 -13.0288 396.0377 409.0665 364.6749 527.8658 -13.0136 395.8581 408.8718 364.4849 529.4691 -13.0071 395.6850 408.6921 364.2572 531.0776 -13.0018 395.5004 408.5022 364.0545 532.6811 -12.9952 395.2712 408.2664 363.8174 534.2896 -12.9840 395.0516 408.0356 363.5959 535.9134 -12.9817 394.8508 407.8326 363.4110 537.5170 -12.9712 394.6311 407.6023 363.2180 539.1253 -12.9571 394.4020 407.3591 363.0005 540.7288 -12.9452 394.1903 407.1355 362.7728 542.3373 -12.9346 393.9647 406.8992 362.5768 543.9406 -12.9252 393.7679 406.6932 362.3568 545.5646 -12.9258 393.5906 406.5163 362.1633 547.1835 -12.9150 393.3965 406.3114 361.9707 548.7969 -12.9033 393.1619 406.0652 361.7433 550.4005 -12.8896 392.9361 405.8258 361.5313 551.9989 -12.8806 392.7542 405.6348 361.3276 553.6174 -12.8712 392.5597 405.4310 361.1250 555.2158 -12.8570 392.3288 405.1858 360.9089 556.8191 -12.8457 392.1240 404.9697 360.7178 558.4584 -12.8419 391.9209 404.7628 360.5255 560.0516 -12.8387 391.6943 404.5330 360.3328 561.6755 -12.8331 391.4651 404.2982 360.1700 563.2839 -12.8250 391.2455 404.0704 359.9442 564.8719 -12.8129 391.0244 403.8373 359.7283 566.4803 -12.8091 390.8523 403.6615 359.4899 568.0786 -12.8002 390.6160 403.4161 359.2572 569.6974 -12.7924 390.3593 403.1516 359.0432 571.3006 -12.7787 390.1542 402.9329 358.7811 572.9040 -12.7768 389.9581 402.7348 358.5940 574.5125 -12.7672 389.7466 402.5137 358.3426 576.1109 -12.7582 389.5456 402.3038 358.1289 577.7144 -12.7510 389.3776 402.1286 357.9568 579.3228 -12.7447 389.1578 401.9025 357.7448 580.9364 -12.7341 388.9251 401.6592 357.5032 582.5449 -12.7247 388.7061 401.4307 357.2890 584.1484 -12.7117 388.5052 401.2169 357.1254 585.7518 -12.7017 388.2942 400.9959 356.9335 587.3603 -12.6907 388.1094 400.8001 356.7460 588.9636 -12.6807 387.9058 400.5865 356.5447 590.5723 -12.6738 387.6805 400.3543 356.3177 592.1908 -12.6648 387.4595 400.1243 356.1107 593.7994 -12.6556 387.2376 399.8931 355.8974 595.4030 -12.6435 387.0204 399.6639 355.6445 597.0165 -12.6335 386.7970 399.4305 355.4775 598.6199 -12.6266 386.5799 399.2066 355.2835 600.2283 -12.6189 386.3619 398.9808 355.0387 601.8368 -12.6078 386.1446 398.7525 354.8127 603.4556 -12.6008 385.9354 398.5362 354.6341 605.0539 -12.5957 385.7131 398.3088 354.4168 606.6623 -12.5920 385.5011 398.0931 354.1783 608.2760 -12.5891 385.2964 397.8854 353.9888 609.8844 -12.5817 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1645.2475 -7.9178 248.8405 256.7582 220.1502 1646.8559 -7.9100 248.6542 256.5642 219.9532 1648.4748 -7.9005 248.4627 256.3632 219.7723