DTA measure 1fazis2 Date: 20241113:1037 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1468.35 s Mass = 1305.000 mg data_number = 1820 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1315 -0.3110 205.5379 205.8490 193.8492 1.9235 -0.3093 205.5045 205.8139 193.8092 2.7755 -0.3077 205.4849 205.7927 193.7361 3.5375 -0.3064 205.4579 205.7644 193.6766 4.3595 -0.3057 205.4136 205.7193 193.5969 5.1515 -0.3052 205.3703 205.6755 193.5514 5.9435 -0.3040 205.3266 205.6306 193.4995 6.7955 -0.3044 205.3131 205.6175 193.4430 7.5575 -0.3035 205.2891 205.5926 193.4095 8.3795 -0.3016 205.2539 205.5555 193.3471 9.2018 -0.3003 205.2300 205.5303 193.3107 9.9645 -0.3001 205.1998 205.4998 193.2664 10.8165 -0.2966 205.1747 205.4713 193.2340 11.5783 -0.2976 205.1456 205.4432 193.1880 12.4003 -0.2953 205.1013 205.3966 193.1622 13.2220 -0.2921 205.0673 205.3594 193.1345 13.9835 -0.2909 205.0420 205.3328 193.1148 14.8360 -0.2962 204.9976 205.2938 193.0795 15.6280 -0.2975 204.9602 205.2577 193.0586 16.4195 -0.2986 204.9253 205.2239 193.0464 17.2423 -0.2979 204.9002 205.1981 193.0351 18.0045 -0.2982 204.8695 205.1677 193.0426 18.8570 -0.2967 204.8354 205.1321 193.0541 19.6490 -0.2970 204.7868 205.0838 193.0454 20.4415 -0.2959 204.7617 205.0576 193.0474 21.2640 -0.2967 204.7314 205.0281 193.0615 22.0240 -0.2950 204.6838 204.9788 193.0809 22.8723 -0.2954 204.6659 204.9613 193.1077 23.6600 -0.2967 204.6412 204.9380 193.1518 24.4480 -0.2957 204.5812 204.8769 193.1820 25.2650 -0.2959 204.5541 204.8501 193.2413 26.0240 -0.2968 204.5192 204.8160 193.2795 26.8723 -0.2963 204.4813 204.7775 193.3001 27.6603 -0.2986 204.4667 204.7653 193.3415 28.4490 -0.3003 204.4298 204.7301 193.4091 29.2678 -0.3018 204.3890 204.6907 193.4769 30.0260 -0.3033 204.3561 204.6594 193.5404 30.8743 -0.3005 204.3341 204.6345 193.6102 31.6620 -0.3000 204.2879 204.5878 193.6893 32.4500 -0.3041 204.2460 204.5500 193.7578 33.2688 -0.3044 204.2229 204.5273 193.8545 34.0595 -0.3048 204.1923 204.4971 193.9423 34.8810 -0.3063 204.1600 204.4663 194.0253 35.6698 -0.3094 204.1112 204.4206 194.1196 36.4590 -0.3111 204.0769 204.3879 194.2156 37.3088 -0.3129 204.0357 204.3485 194.3416 38.0703 -0.3116 204.0107 204.3224 194.4404 38.8913 -0.3164 203.9812 204.2976 194.5643 39.6830 -0.3188 203.9527 204.2714 194.6736 40.4740 -0.3207 203.9288 204.2496 194.7862 41.2958 -0.3254 203.8764 204.2019 194.9022 42.0875 -0.3243 203.8388 204.1631 195.0389 42.9098 -0.3232 203.8142 204.1374 195.1568 43.7020 -0.3268 203.7844 204.1111 195.2903 44.4935 -0.3300 203.7499 204.0799 195.4325 45.3158 -0.3320 203.7080 204.0399 195.5664 46.1075 -0.3357 203.6959 204.0316 195.7144 46.9298 -0.3389 203.6628 204.0017 195.8581 47.7215 -0.3375 203.6201 203.9576 195.9990 48.5135 -0.3398 203.5879 203.9277 196.1547 49.3355 -0.3415 203.5810 203.9225 196.2833 50.1275 -0.3454 203.5316 203.8771 196.4357 50.9495 -0.3495 203.5016 203.8511 196.5929 51.7415 -0.3522 203.4721 203.8243 196.7365 52.5335 -0.3508 203.4399 203.7908 196.8772 53.3603 -0.3538 203.3983 203.7521 197.0438 54.1245 -0.3587 203.3841 203.7428 197.1892 54.9633 -0.3604 203.3493 203.7097 197.3453 55.7255 -0.3643 203.3331 203.6973 197.5029 56.5775 -0.3639 203.2993 203.6632 197.6643 57.3695 -0.3687 203.2566 203.6252 197.8248 58.1615 -0.3705 203.2423 203.6128 197.9780 58.9835 -0.3736 203.2125 203.5861 198.1628 59.7455 -0.3802 203.1883 203.5686 198.3145 60.5975 -0.3827 203.1588 203.5415 198.4745 61.3890 -0.3815 203.1491 203.5306 198.6136 62.1813 -0.3842 203.1159 203.5001 198.7668 63.0033 -0.3882 203.0830 203.4712 198.9249 63.7653 -0.3923 203.0617 203.4541 199.0755 64.6190 -0.3939 203.0327 203.4266 199.2462 65.4110 -0.3987 203.0123 203.4110 199.3952 66.2025 -0.4010 202.9867 203.3878 199.5553 67.0250 -0.4029 202.9743 203.3772 199.7000 67.7865 -0.4050 202.9457 203.3507 199.8345 68.6390 -0.4076 202.9219 203.3295 200.0123 69.4008 -0.4087 202.8888 203.2975 200.1470 70.2228 -0.4117 202.8817 203.2934 200.2850 71.0450 -0.4158 202.8568 203.2726 200.4512 71.8065 -0.4185 202.8378 203.2563 200.5967 72.6590 -0.4206 202.8227 203.2433 200.7412 73.4205 -0.4230 202.7959 203.2189 200.8838 74.2428 -0.4281 202.7669 203.1950 201.0166 75.0650 -0.4324 202.7395 203.1720 201.1579 75.8275 -0.4344 202.7342 203.1686 201.2935 76.6798 -0.4368 202.7088 203.1456 201.4502 77.4415 -0.4409 202.6924 203.1333 201.5733 78.2635 -0.4437 202.6629 203.1066 201.7140 79.0855 -0.4476 202.6563 203.1039 201.8435 79.8475 -0.4514 202.6417 203.0931 201.9781 80.7000 -0.4541 202.6427 203.0967 202.1074 81.4625 -0.4579 202.6123 203.0701 202.2330 82.2845 -0.4621 202.5886 203.0508 202.3693 83.1065 -0.4638 202.5688 203.0326 202.4901 83.8685 -0.4679 202.5527 203.0206 202.6100 84.7210 -0.4672 202.5603 203.0275 202.7556 85.4835 -0.4674 202.5224 202.9898 202.8701 86.3055 -0.4692 202.5078 202.9770 203.0026 87.0955 -0.4763 202.4946 202.9709 203.1289 87.8835 -0.4789 202.4962 202.9751 203.2762 88.7325 -0.4825 202.4785 202.9609 203.4018 89.4908 -0.4813 202.4871 202.9684 203.5067 90.3090 -0.4847 202.4815 202.9662 203.6204 91.0970 -0.4856 202.4641 202.9496 203.7575 91.8853 -0.4881 202.4325 202.9206 203.8761 92.7048 -0.4917 202.4193 202.9110 203.9893 93.4935 -0.4931 202.4064 202.8995 204.1033 94.3125 -0.4947 202.3839 202.8786 204.2328 95.1010 -0.5004 202.3772 202.8777 204.3210 95.8900 -0.5033 202.3766 202.8799 204.4504 96.7088 -0.5013 202.3627 202.8640 204.5660 97.4980 -0.5050 202.3592 202.8642 204.6888 98.3160 -0.5073 202.3463 202.8535 204.7955 99.1048 -0.5107 202.3385 202.8492 204.9057 99.8940 -0.5151 202.3290 202.8440 205.0107 100.7428 -0.5164 202.3207 202.8371 205.1396 101.5023 -0.5187 202.3244 202.8431 205.2415 102.3223 -0.5217 202.3127 202.8344 205.3494 103.1118 -0.5226 202.3152 202.8379 205.4545 103.9020 -0.5254 202.3100 202.8354 205.5832 104.7515 -0.5282 202.3013 202.8295 205.6902 105.5123 -0.5305 202.2983 202.8288 205.7823 106.3340 -0.5325 202.2931 202.8257 205.8840 107.1253 -0.5324 202.2854 202.8178 206.0198 107.9163 -0.5321 202.2994 202.8315 206.1161 108.7685 -0.5364 202.2899 202.8263 206.2258 109.5303 -0.5416 202.2778 202.8194 206.3257 110.3520 -0.5436 202.2802 202.8238 206.4463 111.1440 -0.5436 202.2774 202.8210 206.5498 111.9355 -0.5439 202.2650 202.8089 206.6625 112.7580 -0.5464 202.2667 202.8130 206.7770 113.5498 -0.5476 202.2625 202.8100 206.8659 114.3720 -0.5473 202.2672 202.8146 206.9798 115.1640 -0.5482 202.2758 202.8239 207.0920 115.9555 -0.5499 202.2708 202.8207 207.2019 116.7780 -0.5528 202.2707 202.8235 207.3137 117.5698 -0.5538 202.2590 202.8128 207.4175 118.3918 -0.5548 202.2558 202.8106 207.5354 119.1840 -0.5584 202.2666 202.8249 207.6346 119.9755 -0.5591 202.2795 202.8386 207.7392 120.7980 -0.5600 202.2662 202.8262 207.8611 121.5898 -0.5641 202.2735 202.8375 207.9779 122.4118 -0.5672 202.2654 202.8327 208.1013 123.2040 -0.5699 202.2809 202.8508 208.2171 123.9955 -0.5710 202.2849 202.8559 208.3340 124.8178 -0.5690 202.3086 202.8775 208.4446 125.6095 -0.5706 202.3119 202.8825 208.5534 126.4318 -0.5715 202.3227 202.8942 208.6946 127.2235 -0.5737 202.3305 202.9042 208.8223 128.0155 -0.5771 202.3194 202.8965 208.9361 128.8375 -0.5788 202.3209 202.8997 209.0365 129.6295 -0.5791 202.3345 202.9136 209.1550 130.4515 -0.5797 202.3489 202.9286 209.2833 131.2435 -0.5835 202.3567 202.9401 209.3877 132.0365 -0.5843 202.3561 202.9404 209.5197 132.8885 -0.5872 202.3560 202.9431 209.6540 133.6505 -0.5894 202.3873 202.9767 209.7778 134.4725 -0.5923 202.3778 202.9701 209.8885 135.2645 -0.5927 202.3791 202.9719 210.0047 136.0565 -0.5914 202.3895 202.9808 210.1343 136.9128 -0.5924 202.4064 202.9988 210.2842 137.6743 -0.5965 202.4252 203.0216 210.3621 138.4963 -0.5986 202.4266 203.0252 210.5023 139.2885 -0.5975 202.4397 203.0371 210.6170 140.0798 -0.5994 202.4586 203.0580 210.7442 140.9325 -0.6003 202.4766 203.0769 210.8709 141.6948 -0.6031 202.4862 203.0892 211.0005 142.5175 -0.6054 202.5104 203.1158 211.1297 143.3100 -0.6083 202.5302 203.1385 211.2670 144.1015 -0.6097 202.5350 203.1447 211.4056 144.9540 -0.6100 202.5473 203.1572 211.5242 145.7158 -0.6107 202.5690 203.1798 211.6433 146.5378 -0.6107 202.5727 203.1834 211.7834 147.3600 -0.6133 202.5889 203.2022 211.9120 148.1215 -0.6190 202.5941 203.2131 212.0421 148.9740 -0.6205 202.6046 203.2251 212.1683 149.7358 -0.6225 202.6288 203.2513 212.2987 150.5575 -0.6238 202.6418 203.2655 212.4256 151.3728 -0.6258 202.6593 203.2851 212.5716 152.1320 -0.6257 202.6667 203.2924 212.7034 152.9800 -0.6214 202.7189 203.3403 212.8464 153.7680 -0.6226 202.7323 203.3549 212.9810 154.5560 -0.6241 202.7552 203.3793 213.1084 155.3745 -0.6267 202.7890 203.4157 213.2344 156.1330 -0.6280 202.7996 203.4277 213.3640 156.9810 -0.6278 202.8165 203.4443 213.4983 157.7690 -0.6296 202.8418 203.4714 213.6502 158.5580 -0.6298 202.8565 203.4863 213.7930 159.3763 -0.6321 202.8638 203.4959 213.9207 160.1360 -0.6364 202.8799 203.5163 214.0223 160.9850 -0.6341 202.9016 203.5357 214.1591 161.7733 -0.6373 202.9329 203.5702 214.2804 162.5628 -0.6388 202.9740 203.6128 214.4222 163.3813 -0.6386 202.9973 203.6360 214.5525 164.1400 -0.6399 203.0132 203.6531 214.6794 164.9885 -0.6400 203.0432 203.6833 214.8103 165.7780 -0.6442 203.0558 203.7000 214.9429 166.5678 -0.6452 203.0926 203.7379 215.0583 167.3878 -0.6445 203.1271 203.7716 215.1766 168.1485 -0.6478 203.1623 203.8101 215.3178 169.0010 -0.6462 203.1832 203.8295 215.4665 169.7630 -0.6481 203.1953 203.8434 215.5781 170.5848 -0.6528 203.2137 203.8665 215.6809 171.4058 -0.6549 203.2385 203.8935 215.8021 172.1675 -0.6588 203.2645 203.9233 215.9429 173.0195 -0.6598 203.2935 203.9533 216.0793 173.7815 -0.6616 203.3325 203.9941 216.1966 174.6035 -0.6651 203.3518 204.0169 216.3143 175.3955 -0.6659 203.3826 204.0485 216.4216 176.1875 -0.6685 203.4195 204.0880 216.5462 177.0395 -0.6696 203.4585 204.1281 216.6774 177.8015 -0.6688 203.4887 204.1575 216.7975 178.6235 -0.6729 203.5045 204.1773 216.9228 179.4155 -0.6725 203.5371 204.2096 217.0408 180.2075 -0.6726 203.5681 204.2407 217.1707 181.0295 -0.6718 203.6128 204.2845 217.2955 181.8215 -0.6743 203.6354 204.3097 217.4142 182.6435 -0.6744 203.6634 204.3378 217.5346 183.4355 -0.6742 203.6932 204.3674 217.6564 184.2275 -0.6750 203.7462 204.4212 217.7811 185.0495 -0.6761 203.7720 204.4481 217.9186 185.8115 -0.6788 203.8018 204.4806 218.0300 186.6635 -0.6804 203.8324 204.5128 218.1545 187.4553 -0.6818 203.8781 204.5599 218.2798 188.2468 -0.6847 203.9309 204.6156 218.4022 189.0695 -0.6832 203.9633 204.6465 218.5210 189.8313 -0.6862 204.0057 204.6918 218.6476 190.6830 -0.6895 204.0197 204.7091 218.7991 191.4750 -0.6912 204.0593 204.7505 218.9192 192.2665 -0.6884 204.1008 204.7893 219.0341 193.0893 -0.6941 204.1289 204.8230 219.1624 193.8515 -0.6936 204.1755 204.8691 219.2772 194.7040 -0.6944 204.2130 204.9074 219.4140 195.4658 -0.6958 204.2482 204.9440 219.5170 196.2878 -0.6982 204.2884 204.9866 219.6367 197.1100 -0.6969 204.3351 205.0320 219.7940 197.8715 -0.6971 204.3848 205.0819 219.9350 198.7240 -0.6989 204.4282 205.1270 220.0519 199.4858 -0.7008 204.4662 205.1670 220.1790 200.3078 -0.7033 204.5058 205.2090 220.3053 201.1298 -0.7056 204.5285 205.2341 220.4212 201.8915 -0.7063 204.5580 205.2643 220.5382 202.7438 -0.7069 204.6070 205.3139 220.6670 203.5055 -0.7076 204.6673 205.3748 220.8069 204.3278 -0.7049 204.7072 205.4121 220.9230 205.1495 -0.7074 204.7413 205.4488 221.0442 205.9115 -0.7103 204.7870 205.4973 221.1780 206.7635 -0.7082 204.8401 205.5483 221.3284 207.5255 -0.7093 204.8912 205.6005 221.4405 208.3475 -0.7079 204.9153 205.6233 221.5561 209.1698 -0.7110 204.9613 205.6723 221.6746 209.9325 -0.7119 205.0086 205.7206 221.8177 210.7850 -0.7130 205.0620 205.7749 221.9350 211.5475 -0.7153 205.1006 205.8159 222.0445 212.3695 -0.7183 205.1590 205.8773 222.1761 213.1915 -0.7130 205.1889 205.9019 222.3150 213.9535 -0.7138 205.2328 205.9466 222.4355 214.8050 -0.7126 205.3192 206.0318 222.5737 215.5640 -0.7139 205.3549 206.0688 222.6885 216.3815 -0.7114 205.3837 206.0951 222.8083 217.1683 -0.7133 205.4515 206.1648 222.9286 217.9573 -0.7131 205.4961 206.2091 223.0767 218.8060 -0.7134 205.5416 206.2550 223.2034 219.5638 -0.7184 205.5918 206.3103 223.3209 220.3823 -0.7162 205.6308 206.3470 223.4441 221.1703 -0.7169 205.6784 206.3953 223.5636 221.9588 -0.7185 205.7236 206.4420 223.6943 222.8078 -0.7207 205.7787 206.4994 223.8105 223.5658 -0.7218 205.8291 206.5509 223.9291 224.3848 -0.7226 205.9039 206.6265 224.0623 225.2033 -0.7239 205.9431 206.6671 224.2014 225.9618 -0.7252 206.0006 206.7258 224.3220 226.8108 -0.7265 206.0639 206.7904 224.4844 227.5990 -0.7271 206.1010 206.8282 224.6178 228.3878 -0.7308 206.1378 206.8686 224.7552 229.2075 -0.7317 206.1932 206.9249 224.8831 229.9970 -0.7299 206.2460 206.9759 224.9973 230.8163 -0.7316 206.3102 207.0418 225.1242 231.6065 -0.7331 206.3562 207.0893 225.2594 232.3983 -0.7345 206.4069 207.1413 225.3832 233.2193 -0.7331 206.4659 207.1991 225.5439 234.0110 -0.7343 206.5314 207.2657 225.6641 234.8328 -0.7337 206.5697 207.3034 225.7914 235.6253 -0.7377 206.6181 207.3557 225.9263 236.4165 -0.7398 206.6892 207.4290 226.0516 237.2393 -0.7406 206.7491 207.4897 226.1928 238.0005 -0.7417 206.8120 207.5537 226.3207 238.8530 -0.7419 206.8635 207.6053 226.4693 239.6450 -0.7443 206.9028 207.6471 226.6050 240.4365 -0.7476 206.9822 207.7298 226.7318 241.2590 -0.7462 207.0502 207.7964 226.8926 242.0205 -0.7476 207.1006 207.8482 227.0113 242.8730 -0.7523 207.1694 207.9217 227.1420 243.6650 -0.7493 207.2408 207.9901 227.2694 244.4565 -0.7531 207.2826 208.0358 227.4139 245.2790 -0.7546 207.3402 208.0948 227.5583 246.0405 -0.7569 207.3953 208.1521 227.6729 246.8930 -0.7541 207.4578 208.2119 227.8195 247.6848 -0.7516 207.5145 208.2661 227.9444 248.4765 -0.7555 207.5752 208.3307 228.0693 249.2985 -0.7559 207.6256 208.3814 228.2017 250.0605 -0.7641 207.7007 208.4647 228.3342 250.9130 -0.7660 207.7767 208.5427 228.4648 251.7048 -0.7654 207.8279 208.5933 228.5844 252.4965 -0.7692 207.8977 208.6669 228.7063 253.3185 -0.7690 207.9500 208.7190 228.8401 254.1105 -0.7674 208.0008 208.7682 228.9804 254.9335 -0.7711 208.0860 208.8571 229.1105 255.7255 -0.7758 208.1368 208.9126 229.2254 256.5175 -0.7797 208.1875 208.9673 229.3506 257.3395 -0.7763 208.2515 209.0278 229.4770 258.1315 -0.7737 208.3360 209.1098 229.6022 258.9543 -0.7744 208.4032 209.1776 229.7400 259.7465 -0.7769 208.4718 209.2487 229.8542 260.5385 -0.7780 208.5383 209.3163 229.9891 261.3605 -0.7784 208.6003 209.3787 230.1076 262.1525 -0.7811 208.6622 209.4433 230.2311 262.9745 -0.7822 208.7148 209.4970 230.3637 263.7665 -0.7833 208.7817 209.5651 230.4868 264.5583 -0.7851 208.8526 209.6377 230.6100 265.4103 -0.7808 208.8944 209.6752 230.7327 266.1723 -0.7832 208.9751 209.7583 230.8712 266.9938 -0.7884 209.0578 209.8462 230.9956 267.7868 -0.7823 209.1317 209.9140 231.1065 268.5805 -0.7842 209.2040 209.9882 231.2289 269.4335 -0.7837 209.2780 210.0617 231.3398 270.1958 -0.7855 209.3548 210.1403 231.4485 271.0178 -0.7868 209.4126 210.1994 231.5755 271.8100 -0.7909 209.4805 210.2714 231.6929 272.6015 -0.7937 209.5543 210.3480 231.8202 273.4545 -0.7972 209.6220 210.4192 231.9384 274.2168 -0.7946 209.6994 210.4940 232.0627 275.0395 -0.7939 209.7730 210.5669 232.1916 275.8320 -0.7922 209.8416 210.6338 232.3112 276.6245 -0.7937 209.9041 210.6978 232.4258 277.4470 -0.7980 209.9822 210.7802 232.5270 278.2385 -0.8004 210.0487 210.8490 232.6618 279.0593 -0.8016 210.1136 210.9152 232.7944 279.8223 -0.8010 210.1995 211.0005 232.9024 280.6490 -0.8022 210.2657 211.0680 233.0341 281.4360 -0.8035 210.3389 211.1424 233.1692 282.2250 -0.8056 210.4181 211.2237 233.2705 283.0730 -0.8030 210.4809 211.2839 233.4405 283.8310 -0.8032 210.5667 211.3699 233.5385 284.6490 -0.8043 210.6432 211.4474 233.6617 285.4373 -0.8077 210.7114 211.5191 233.7997 286.2250 -0.8085 210.7848 211.5933 233.9176 287.0738 -0.8133 210.8667 211.6800 234.0513 287.8323 -0.8126 210.9298 211.7423 234.1737 288.6518 -0.8073 211.0090 211.8163 234.2895 289.4405 -0.8093 211.0837 211.8929 234.4247 290.2300 -0.8106 211.1497 211.9604 234.5566 291.0790 -0.8112 211.2161 212.0273 234.6851 291.8380 -0.8137 211.3109 212.1247 234.8011 292.6570 -0.8160 211.4050 212.2210 234.9491 293.4455 -0.8155 211.4764 212.2919 235.0886 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