DTA measure 2fazis2 Date: 20241113:117 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1647.80 s Mass = 1305.000 mg data_number = 1020 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3698 -4.2812 418.6917 422.9729 420.5640 3.9990 -4.2820 418.7303 423.0123 420.5675 5.5978 -4.2841 418.8125 423.0966 420.5597 7.2131 -4.2834 418.8603 423.1436 420.5330 8.8123 -4.2843 418.9142 423.1986 420.4961 10.4050 -4.2844 418.9879 423.2722 420.4296 12.0269 -4.2866 419.0443 423.3309 420.3430 13.6184 -4.2882 419.0769 423.3651 420.2375 15.2103 -4.2879 419.1307 423.4186 420.1185 16.8185 -4.2870 419.1872 423.4742 419.9767 18.4263 -4.2873 419.2427 423.5300 419.7982 20.0341 -4.2823 419.2840 423.5664 419.6367 21.6293 -4.2797 419.3326 423.6124 419.4526 23.2413 -4.2773 419.3729 423.6502 419.2592 24.8383 -4.2751 419.4150 423.6901 419.0586 26.4516 -4.2698 419.4494 423.7192 418.8377 28.0645 -4.2644 419.4964 423.7608 418.6272 29.6636 -4.2588 419.5227 423.7815 418.3767 31.2628 -4.2530 419.5458 423.7988 418.1281 32.8766 -4.2476 419.5860 423.8336 417.8843 34.4755 -4.2438 419.6178 423.8616 417.6252 36.1045 -4.2350 419.6481 423.8831 417.3624 37.7035 -4.2248 419.6707 423.8955 417.1182 39.3025 -4.2274 419.6944 423.9218 416.8622 40.9165 -4.2141 419.6984 423.9125 416.6070 42.5304 -4.2021 419.7292 423.9313 416.3680 44.1443 -4.1949 419.7374 423.9323 416.1175 45.7433 -4.1871 419.7584 423.9455 415.8960 47.3568 -4.1826 419.7780 423.9607 415.6547 48.9558 -4.1715 419.7913 423.9628 415.4114 50.5856 -4.1633 419.7882 423.9515 415.1775 52.1849 -4.1579 419.7828 423.9406 414.9625 53.7988 -4.1510 419.7841 423.9351 414.7464 55.3980 -4.1458 419.8050 423.9508 414.5256 57.0126 -4.1358 419.7887 423.9245 414.3119 58.6266 -4.1261 419.7645 423.8905 414.1136 60.2418 -4.1204 419.7635 423.8839 413.9049 61.8415 -4.1163 419.7515 423.8678 413.6825 63.4405 -4.1084 419.7392 423.8476 413.4965 65.0545 -4.1038 419.7168 423.8206 413.2876 66.6685 -4.0925 419.7071 423.7997 413.0855 68.2834 -4.0873 419.6782 423.7655 412.8896 69.8825 -4.0807 419.6686 423.7493 412.7059 71.4813 -4.0737 419.6462 423.7200 412.5111 73.0935 -4.0696 419.6320 423.7017 412.3343 74.7159 -4.0597 419.6075 423.6672 412.1321 76.3079 -4.0521 419.5736 423.6258 411.9522 77.9004 -4.0476 419.5367 423.5844 411.7745 79.4934 -4.0431 419.5007 423.5438 411.6073 81.1019 -4.0359 419.4554 423.4913 411.4166 82.7108 -4.0281 419.4339 423.4620 411.2410 84.3193 -4.0251 419.3930 423.4181 411.0768 85.9150 -4.0217 419.3528 423.3745 410.9195 87.5108 -4.0171 419.3065 423.3236 410.7612 89.1083 -4.0082 419.2629 423.2712 410.5829 90.7364 -3.9993 419.2162 423.2155 410.4067 92.3353 -3.9935 419.1700 423.1635 410.2485 93.9338 -3.9881 419.1391 423.1273 410.0761 95.5329 -3.9831 419.0856 423.0687 409.8939 97.1468 -3.9816 419.0362 423.0178 409.7214 98.7458 -3.9724 418.9824 422.9548 409.5591 100.3599 -3.9673 418.9162 422.8835 409.3728 101.9588 -3.9622 418.8763 422.8385 409.2054 103.5726 -3.9574 418.8363 422.7936 409.0306 105.1718 -3.9495 418.7683 422.7179 408.8321 106.7708 -3.9423 418.7046 422.6469 408.6436 108.3996 -3.9378 418.6400 422.5778 408.4612 109.9988 -3.9305 418.5887 422.5192 408.2642 111.5975 -3.9232 418.5183 422.4414 408.0550 113.2119 -3.9182 418.4597 422.3779 407.8531 114.8115 -3.9123 418.3908 422.3031 407.6531 116.4255 -3.9050 418.3207 422.2257 407.4593 118.0395 -3.8973 418.2537 422.1510 407.2525 119.6386 -3.8901 418.1729 422.0630 407.0351 121.2534 -3.8838 418.0992 421.9830 406.8527 122.8521 -3.8763 418.0260 421.9023 406.6481 124.4818 -3.8661 417.9447 421.8108 406.4376 126.0809 -3.8630 417.8733 421.7363 406.2160 127.6950 -3.8552 417.8021 421.6573 406.0358 129.2948 -3.8515 417.7197 421.5712 405.8559 130.8955 -3.8448 417.6427 421.4875 405.6562 132.5264 -3.8372 417.5517 421.3889 405.4463 134.1260 -3.8330 417.4598 421.2928 405.2601 135.7429 -3.8269 417.3672 421.1941 405.0703 137.3401 -3.8192 417.2818 421.1009 404.8562 138.9320 -3.8130 417.1908 421.0038 404.6463 140.5541 -3.8091 417.1075 420.9166 404.4467 142.1476 -3.8054 417.0179 420.8233 404.2496 143.7553 -3.7978 416.9319 420.7297 404.0309 145.3530 -3.7933 416.8389 420.6321 403.8205 146.9493 -3.7869 416.7313 420.5182 403.6313 148.5601 -3.7802 416.6347 420.4149 403.4368 150.1701 -3.7727 416.5239 420.2966 403.2164 151.7808 -3.7699 416.4297 420.1997 403.0021 153.3779 -3.7639 416.3459 420.1098 402.8091 154.9758 -3.7597 416.2354 419.9951 402.5991 156.6046 -3.7543 416.1292 419.8835 402.3806 158.2036 -3.7496 416.0351 419.7847 402.1858 159.8025 -3.7425 415.9267 419.6692 401.9897 161.4165 -3.7319 415.8171 419.5490 401.7788 163.0155 -3.7263 415.7124 419.4387 401.5865 164.6295 -3.7215 415.6062 419.3277 401.3951 166.2435 -3.7191 415.4966 419.2157 401.1962 167.8425 -3.7160 415.3887 419.1047 400.9934 169.4415 -3.7094 415.2758 418.9851 400.8161 171.0550 -3.7030 415.1631 418.8661 400.6034 172.6540 -3.6942 415.0469 418.7412 400.4194 174.2679 -3.6885 414.9260 418.6146 400.2335 175.8819 -3.6836 414.8162 418.4998 400.0437 177.4808 -3.6782 414.7117 418.3899 399.8519 179.0798 -3.6711 414.5870 418.2581 399.6660 180.6938 -3.6658 414.4598 418.1256 399.4592 182.3079 -3.6588 414.3427 418.0015 399.2682 183.9068 -3.6544 414.2194 417.8738 399.0808 185.5219 -3.6515 414.1018 417.7533 398.8620 187.1220 -3.6495 413.9775 417.6270 398.6725 188.7221 -3.6440 413.8550 417.4990 398.4758 190.3274 -3.6378 413.7351 417.3729 398.2729 191.9573 -3.6322 413.6076 417.2398 398.0697 193.5565 -3.6256 413.4839 417.1095 397.8603 195.1555 -3.6202 413.3608 416.9811 397.6462 196.7700 -3.6159 413.2257 416.8415 397.4593 198.3701 -3.6122 413.0919 416.7041 397.2599 199.9846 -3.6064 412.9720 416.5784 397.0451 201.5974 -3.5994 412.8496 416.4491 396.8468 203.1891 -3.5924 412.7122 416.3046 396.6499 204.7806 -3.5894 412.5761 416.1656 396.4419 206.3876 -3.5824 412.4518 416.0342 396.2445 207.9946 -3.5782 412.3016 415.8798 396.0541 209.6049 -3.5722 412.1721 415.7442 395.8494 211.2009 -3.5687 412.0458 415.6145 395.6472 212.7950 -3.5648 411.9046 415.4694 395.4397 214.3915 -3.5589 411.7657 415.3246 395.2662 216.0186 -3.5526 411.6268 415.1794 395.0624 217.6164 -3.5488 411.4847 415.0336 394.8801 219.2300 -3.5438 411.3497 414.8935 394.6727 220.8290 -3.5400 411.2249 414.7650 394.4903 222.4278 -3.5321 411.0888 414.6209 394.2789 224.0414 -3.5281 410.9359 414.4640 394.0740 225.6549 -3.5235 410.8081 414.3316 393.8784 227.2538 -3.5185 410.6592 414.1778 393.6626 228.8528 -3.5155 410.5103 414.0257 393.4517 230.4666 -3.5076 410.3670 413.8746 393.2559 232.0656 -3.5068 410.2055 413.7124 393.0509 233.6946 -3.5015 410.0632 413.5647 392.8604 235.2936 -3.4956 409.9212 413.4169 392.6439 236.8925 -3.4925 409.7926 413.2851 392.4321 238.5065 -3.4798 409.6422 413.1221 392.2417 240.1055 -3.4686 409.4967 412.9653 392.0227 241.7371 -3.4681 409.3500 412.8180 391.8226 243.3380 -3.4613 409.1845 412.6457 391.6173 244.9388 -3.4511 409.0264 412.4775 391.4224 246.5541 -3.4580 408.8797 412.3377 391.2129 248.1573 -3.4542 408.7401 412.1943 391.0099 249.7721 -3.4463 408.5932 412.0395 390.8082 251.3859 -3.4432 408.4393 411.8825 390.6217 252.9848 -3.4410 408.2650 411.7060 390.4288 254.5988 -3.4325 408.1219 411.5544 390.2246 256.2129 -3.4317 407.9689 411.4005 390.0352 257.8269 -3.4253 407.8103 411.2356 389.8413 259.4266 -3.4176 407.6518 411.0694 389.6440 261.0410 -3.4166 407.4905 410.9071 389.4454 262.6411 -3.4101 407.3540 410.7641 389.2525 264.2705 -3.4079 407.1971 410.6050 389.0289 265.8693 -3.4027 407.0372 410.4399 388.8473 267.4623 -3.3939 406.8857 410.2796 388.6247 269.0684 -3.3915 406.7292 410.1207 388.4349 270.6614 -3.3887 406.5518 409.9405 388.2222 272.2539 -3.3835 406.3917 409.7752 388.0208 273.8758 -3.3751 406.2420 409.6171 387.8024 275.4684 -3.3705 406.0810 409.4516 387.5792 277.0613 -3.3675 405.9191 409.2866 387.3779 278.6714 -3.3631 405.7736 409.1367 387.1662 280.2654 -3.3560 405.5901 408.9461 386.9579 281.8888 -3.3510 405.4264 408.7775 386.7441 283.4829 -3.3466 405.2788 408.6254 386.5411 285.0791 -3.3433 405.1226 408.4659 386.3223 286.6925 -3.3393 404.9609 408.3001 386.1244 288.2915 -3.3330 404.7912 408.1242 385.9271 289.8905 -3.3298 404.6126 407.9425 385.7227 291.5045 -3.3251 404.4483 407.7734 385.5099 293.1185 -3.3191 404.2829 407.6020 385.3103 294.7174 -3.3164 404.1136 407.4300 385.1056 296.3161 -3.3139 403.9420 407.2559 384.9221 297.9153 -3.3085 403.7727 407.0812 384.7010 299.5290 -3.3033 403.6115 406.9147 384.5073 301.1430 -3.2999 403.4477 406.7475 384.3082 302.7418 -3.2947 403.2922 406.5869 384.0899 304.3408 -3.2899 403.1194 406.4094 383.8934 305.9548 -3.2819 402.9544 406.2362 383.6823 307.5538 -3.2781 402.7721 406.0502 383.5005 309.1679 -3.2700 402.6057 405.8757 383.2871 310.7818 -3.2645 402.4436 405.7081 383.0937 312.3806 -3.2580 402.2798 405.5378 382.8882 313.9795 -3.2456 402.0981 405.3437 382.6951 315.5935 -3.2482 401.9249 405.1730 382.5009 317.2075 -3.2410 401.7569 404.9980 382.3204 318.8215 -3.2332 401.5818 404.8151 382.1204 320.4208 -3.2427 401.4097 404.6524 381.9260 322.0209 -3.2380 401.2424 404.4804 381.7191 323.6355 -3.2298 401.0880 404.3178 381.5156 325.2569 -3.2263 400.8851 404.1114 381.3206 326.8570 -3.2213 400.7156 403.9368 381.1058 328.4718 -3.2171 400.5428 403.7598 380.8953 330.0698 -3.2114 400.3752 403.5866 380.7038 331.6621 -3.2046 400.2096 403.4141 380.4841 333.2685 -3.1980 400.0310 403.2289 380.2690 334.8751 -3.1900 399.8539 403.0439 380.0532 336.4668 -3.1880 399.6807 402.8687 379.8362 338.0751 -3.1843 399.5013 402.6856 379.6327 339.6676 -3.1802 399.3317 402.5119 379.4436 341.2764 -3.1770 399.1474 402.3244 379.2196 342.8858 -3.1720 398.9617 402.1338 379.0062 344.4958 -3.1689 398.7924 401.9613 378.7944 346.0934 -3.1620 398.6294 401.7915 378.5848 347.6909 -3.1582 398.4532 401.6114 378.3739 349.3199 -3.1519 398.2630 401.4149 378.1628 350.9189 -3.1456 398.0857 401.2312 377.9511 352.5178 -3.1353 397.9077 401.0430 377.7576 354.1318 -3.1288 397.7417 400.8705 377.5390 355.7308 -3.1268 397.5601 400.6869 377.3299 357.3448 -3.1151 397.3887 400.5037 377.1287 358.9588 -3.1151 397.1960 400.3111 376.9421 360.5576 -3.1141 397.0127 400.1268 376.7414 362.1716 -3.1122 396.8290 399.9411 376.5427 363.7705 -3.1073 396.6546 399.7619 376.3683 365.3995 -3.1031 396.4803 399.5834 376.1485 366.9985 -3.0988 396.2971 399.3959 375.9599 368.6125 -3.0954 396.1104 399.2058 375.7701 370.2115 -3.0894 395.9351 399.0245 375.5802 371.8124 -3.0881 395.7575 398.8456 375.3780 373.4433 -3.0848 395.5703 398.6552 375.1946 375.0424 -3.0765 395.3913 398.4678 375.0039 376.6564 -3.0751 395.2050 398.2800 374.7908 378.2549 -3.0676 395.0124 398.0800 374.5951 379.8688 -3.0635 394.8447 397.9082 374.3947 381.4829 -3.0617 394.6578 397.7195 374.1674 383.0978 -3.0596 394.4816 397.5412 373.9734 384.6968 -3.0518 394.3040 397.3558 373.7699 386.2961 -3.0499 394.1150 397.1648 373.5512 387.9106 -3.0487 393.9168 396.9655 373.3555 389.5248 -3.0365 393.7426 396.7791 373.1425 391.1389 -3.0352 393.5539 396.5891 372.9442 392.7385 -3.0328 393.3831 396.4159 372.7244 394.3350 -3.0281 393.2023 396.2304 372.5149 395.9275 -3.0180 393.0092 396.0272 372.3069 397.5498 -3.0130 392.8321 395.8451 372.1073 399.1410 -3.0061 392.6410 395.6471 371.8920 400.7473 -3.0010 392.4556 395.4566 371.6961 402.3394 -3.0004 392.2817 395.2820 371.5133 403.9346 -2.9979 392.0929 395.0908 371.2988 405.5609 -2.9963 391.9153 394.9117 371.0801 407.1563 -2.9925 391.7313 394.7237 370.8840 408.7689 -2.9871 391.5451 394.5322 370.6881 410.3644 -2.9798 391.3472 394.3270 370.4899 411.9613 -2.9757 391.1701 394.1459 370.2832 413.5895 -2.9712 390.9783 393.9495 370.0833 415.1885 -2.9674 390.8106 393.7780 369.8803 416.8025 -2.9649 390.6212 393.5862 369.6721 418.4015 -2.9588 390.4328 393.3915 369.4630 420.0005 -2.9571 390.2328 393.1899 369.2769 421.6294 -2.9533 390.0320 392.9853 369.0630 423.2294 -2.9440 389.8525 392.7965 368.8650 424.8434 -2.9367 389.6721 392.6088 368.6698 426.4423 -2.9337 389.4973 392.4310 368.4699 428.0414 -2.9298 389.3038 392.2336 368.2695 429.6710 -2.9272 389.1330 392.0602 368.0660 431.2849 -2.9247 388.9245 391.8492 367.8673 432.8838 -2.9160 388.7283 391.6444 367.6547 434.4828 -2.9132 388.5550 391.4682 367.4577 436.0966 -2.9115 388.3613 391.2729 367.2439 437.7108 -2.9065 388.1629 391.0694 367.0340 439.3248 -2.8992 387.9845 390.8837 366.8147 440.9235 -2.8967 387.7907 390.6874 366.6100 442.5375 -2.8943 387.6027 390.4970 366.3949 444.1365 -2.8909 387.4024 390.2932 366.1899 445.7655 -2.8848 387.2294 390.1142 365.9801 447.3645 -2.8791 387.0368 389.9159 365.7579 448.9789 -2.8745 386.8531 389.7276 365.5604 450.5790 -2.8725 386.6566 389.5291 365.3581 452.1935 -2.8686 386.4654 389.3340 365.1397 453.8073 -2.8621 386.2692 389.1313 364.9226 455.4208 -2.8569 386.0788 388.9358 364.7229 457.0198 -2.8560 385.9063 388.7622 364.5203 458.6170 -2.8538 385.6994 388.5532 364.3111 460.2378 -2.8475 385.5186 388.3661 364.1157 461.8319 -2.8395 385.3257 388.1652 363.9041 463.4404 -2.8243 385.1501 387.9744 363.7037 465.0349 -2.8236 384.9513 387.7748 363.4935 466.6269 -2.8229 384.7643 387.5872 363.2940 468.2506 -2.8187 384.5503 387.3689 363.0656 469.8594 -2.8153 384.3618 387.1772 362.8636 471.4561 -2.8135 384.1879 387.0014 362.6626 473.0521 -2.8041 383.9909 386.7950 362.4629 474.6640 -2.8044 383.7988 386.6032 362.2702 476.2778 -2.8015 383.6075 386.4090 362.0738 477.8763 -2.7901 383.4085 386.1986 361.8722 479.4925 -2.7864 383.2278 386.0142 361.6822 481.0918 -2.7825 383.0382 385.8207 361.4782 482.6925 -2.7805 382.8511 385.6315 361.2684 484.3078 -2.7703 382.6459 385.4163 361.0806 485.9216 -2.7656 382.4599 385.2255 360.8831 487.5208 -2.7662 382.2843 385.0506 360.6888 489.1346 -2.7652 382.0825 384.8477 360.4863 490.7335 -2.7582 381.8807 384.6390 360.2904 492.3625 -2.7528 381.6809 384.4337 360.0892 493.9618 -2.7484 381.4954 384.2438 359.8972 495.5765 -2.7427 381.3163 384.0589 359.6763 497.1755 -2.7413 381.1174 383.8587 359.4954 498.7745 -2.7365 380.9172 383.6537 359.2780 500.4035 -2.7332 380.7342 383.4674 359.0764 502.0029 -2.7260 380.5199 383.2459 358.8670 503.6071 -2.7225 380.3422 383.0648 358.6586 505.2219 -2.7252 380.1484 382.8736 358.4454 506.8208 -2.7234 379.9683 382.6917 358.2457 508.4349 -2.7103 379.7832 382.4935 358.0396 510.0489 -2.7075 379.5713 382.2789 357.8250 511.6628 -2.7020 379.3811 382.0831 357.6296 513.2621 -2.7015 379.1967 381.8982 357.4299 514.8616 -2.6961 379.0051 381.7011 357.2096 516.4906 -2.6939 378.7976 381.4915 357.0131 518.0908 -2.6858 378.6081 381.2939 356.8058 519.7075 -2.6814 378.4165 381.0979 356.5937 521.3065 -2.6819 378.2400 380.9219 356.3890 522.9195 -2.6746 378.0329 380.7075 356.1835 524.5265 -2.6691 377.8210 380.4901 355.9720 526.1189 -2.6638 377.6307 380.2946 355.7816 527.7254 -2.6672 377.4416 380.1088 355.5596 529.3180 -2.6603 377.2482 379.9086 355.3548 530.9090 -2.6496 377.0632 379.7128 355.1565 532.5150 -2.6474 376.8602 379.5076 354.9369 534.1210 -2.6449 376.6784 379.3233 354.7483 535.7274 -2.6401 376.4720 379.1121 354.5577 537.3226 -2.6392 376.2840 378.9233 354.3563 538.9195 -2.6371 376.0880 378.7251 354.1462 540.5485 -2.6310 375.9096 378.5406 353.9279 542.1475 -2.6283 375.7054 378.3337 353.7460 543.7465 -2.6226 375.5155 378.1381 353.5450 545.3455 -2.6192 375.3210 377.9402 353.3448 546.9595 -2.6166 375.1276 377.7442 353.1393 548.5584 -2.6018 374.9317 377.5335 352.9454 550.1724 -2.5953 374.7227 377.3180 352.7423 551.7861 -2.5925 374.5407 377.1332 352.5141 553.3849 -2.5878 374.3387 376.9265 352.3148 554.9844 -2.5874 374.1538 376.7412 352.1043 556.5988 -2.5795 373.9674 376.5469 351.9008 558.2130 -2.5719 373.7629 376.3348 351.6905 559.8129 -2.5645 373.5704 376.1349 351.4672 561.4298 -2.5602 373.3669 375.9271 351.2574 563.0288 -2.5510 373.1784 375.7293 351.0523 564.6275 -2.5516 372.9740 375.5256 350.8519 566.2566 -2.5419 372.7717 375.3136 350.6459 567.8555 -2.5441 372.5809 375.1250 350.4321 569.4695 -2.5391 372.4006 374.9398 350.2186 571.0685 -2.5348 372.2016 374.7364 350.0059 572.6680 -2.5325 371.9966 374.5290 349.8006 574.2975 -2.5284 371.8008 374.3292 349.5943 575.8965 -2.5235 371.5988 374.1224 349.3865 577.5105 -2.5206 371.3991 373.9197 349.1799 579.1095 -2.5145 371.2018 373.7163 348.9712 580.7084 -2.5102 371.0125 373.5227 348.7589 582.3371 -2.4968 370.8225 373.3193 348.5433 583.9359 -2.4938 370.6161 373.1099 348.3501 585.5505 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