DTA measure 1Sn_test.dat Test Date: 20231025:1212 Lower limit = 100.0 C Upper limit = 340.0 C Rate = 10.00 C/min Mtime = 1439.54 s Mass = 909.500 mg data_number = 1786 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2848 -1.0939 166.6291 167.7230 153.6248 2.1063 -1.0868 166.5936 167.6804 153.5763 2.8975 -1.0805 166.5570 167.6375 153.5325 3.6888 -1.0763 166.5088 167.5851 153.4704 4.5395 -1.0700 166.4595 167.5295 153.4210 5.3010 -1.0639 166.4228 167.4867 153.3768 6.1225 -1.0612 166.3973 167.4585 153.3112 6.9135 -1.0519 166.3690 167.4208 153.2604 7.7050 -1.0457 166.3254 167.3710 153.2017 8.5565 -1.0398 166.2768 167.3166 153.1499 9.3180 -1.0335 166.2394 167.2729 153.1010 10.1393 -1.0258 166.2009 167.2267 153.0642 10.9295 -1.0202 166.1492 167.1694 153.0036 11.7205 -1.0153 166.1038 167.1191 152.9524 12.5425 -1.0120 166.0647 167.0767 152.8977 13.3340 -1.0063 166.0218 167.0280 152.8632 14.1555 -0.9980 165.9934 166.9914 152.7936 14.9475 -0.9910 165.9498 166.9409 152.7405 15.7378 -0.9849 165.9042 166.8891 152.6801 16.5583 -0.9795 165.8670 166.8465 152.6319 17.3193 -0.9757 165.8289 166.8046 152.5929 18.1710 -0.9692 165.7717 166.7409 152.5328 18.9630 -0.9627 165.7324 166.6951 152.4817 19.7538 -0.9561 165.6936 166.6497 152.4253 20.5753 -0.9506 165.6664 166.6170 152.3745 21.3343 -0.9458 165.6227 166.5685 152.3171 22.1858 -0.9424 165.5649 166.5073 152.2546 22.9475 -0.9367 165.5408 166.4774 152.2091 23.7698 -0.9324 165.4965 166.4290 152.1637 24.5908 -0.9269 165.4577 166.3846 152.1240 25.3518 -0.9191 165.4121 166.3311 152.0688 26.2083 -0.9123 165.3565 166.2689 151.9955 26.9695 -0.9077 165.3153 166.2230 151.9558 27.7915 -0.9024 165.2755 166.1779 151.8960 28.5825 -0.8952 165.2266 166.1218 151.8554 29.3745 -0.8904 165.1949 166.0853 151.8127 30.2265 -0.8862 165.1564 166.0426 151.7445 30.9878 -0.8803 165.1025 165.9827 151.6954 31.8095 -0.8702 165.0642 165.9345 151.6394 32.6008 -0.8657 165.0242 165.8900 151.5841 33.3915 -0.8608 164.9876 165.8484 151.5288 34.2125 -0.8560 164.9507 165.8067 151.4891 35.0023 -0.8499 164.9103 165.7602 151.4367 35.8235 -0.8465 164.8591 165.7056 151.3813 36.6148 -0.8429 164.8109 165.6538 151.3496 37.4055 -0.8384 164.7731 165.6115 151.3040 38.2265 -0.8323 164.7176 165.5499 151.2477 39.0185 -0.8266 164.6880 165.5146 151.1757 39.8405 -0.8207 164.6546 165.4753 151.1251 40.6308 -0.8159 164.6051 165.4210 151.0724 41.4215 -0.8112 164.5496 165.3608 151.0224 42.2423 -0.8073 164.5183 165.3255 150.9775 43.0335 -0.8034 164.4727 165.2761 150.9221 43.8545 -0.7997 164.4296 165.2292 150.8804 44.6460 -0.7954 164.3725 165.1679 150.8336 45.4375 -0.7915 164.3263 165.1178 150.7672 46.2600 -0.7867 164.2902 165.0769 150.7191 47.0515 -0.7822 164.2490 165.0312 150.6608 48.0273 -0.7785 164.1946 164.9731 150.5982 48.8693 -0.7739 164.1487 164.9226 150.5611 49.6603 -0.7680 164.1045 164.8725 150.5210 50.4815 -0.7624 164.0600 164.8225 150.4667 51.2713 -0.7578 164.0195 164.7773 150.4094 52.0928 -0.7539 163.9770 164.7309 150.3629 52.8835 -0.7480 163.9318 164.6799 150.3019 53.6750 -0.7438 163.8994 164.6433 150.2576 54.4965 -0.7412 163.8486 164.5898 150.2134 55.2880 -0.7377 163.8122 164.5498 150.1514 56.1095 -0.7338 163.7617 164.4955 150.1077 56.9008 -0.7293 163.6998 164.4291 150.0631 57.6923 -0.7251 163.6572 164.3823 149.9948 58.5130 -0.7226 163.6178 164.3404 149.9526 59.3040 -0.7195 163.5829 164.3024 149.8883 60.1255 -0.7125 163.5337 164.2463 149.8402 60.9168 -0.7104 163.4822 164.1926 149.7774 61.7095 -0.7062 163.4376 164.1438 149.7358 62.5305 -0.7026 163.3894 164.0920 149.6973 63.3210 -0.6969 163.3705 164.0674 149.6597 64.1425 -0.6921 163.3047 163.9968 149.6082 64.9328 -0.6903 163.2653 163.9557 149.5479 65.7243 -0.6863 163.2190 163.9053 149.4882 66.5445 -0.6823 163.1824 163.8647 149.4382 67.3358 -0.6787 163.1447 163.8234 149.3892 68.1570 -0.6758 163.0855 163.7613 149.3399 68.9480 -0.6717 163.0606 163.7323 149.2982 69.7385 -0.6674 163.0037 163.6711 149.2444 70.5900 -0.6667 162.9460 163.6127 149.1890 71.3508 -0.6618 162.8974 163.5592 149.1369 72.1725 -0.6577 162.8586 163.5163 149.0838 72.9620 -0.6513 162.8152 163.4666 149.0371 73.7520 -0.6473 162.7749 163.4223 148.9759 74.6018 -0.6442 162.7292 163.3734 148.9260 75.3618 -0.6412 162.6822 163.3235 148.8786 76.1838 -0.6395 162.6407 163.2802 148.8312 77.0048 -0.6338 162.5998 163.2336 148.8013 77.7658 -0.6309 162.5636 163.1945 148.7387 78.7538 -0.6263 162.4831 163.1094 148.6802 79.5885 -0.6243 162.4333 163.0575 148.6091 80.3798 -0.6221 162.3986 163.0207 148.5682 81.2315 -0.6169 162.3530 162.9699 148.5166 81.9935 -0.6132 162.3101 162.9233 148.4726 82.8150 -0.6085 162.2536 162.8621 148.4108 83.6055 -0.6059 162.2016 162.8075 148.3584 84.3973 -0.6038 162.1622 162.7659 148.3222 85.2485 -0.5985 162.1189 162.7174 148.2628 86.0095 -0.5970 162.0806 162.6776 148.2224 86.8300 -0.5930 162.0368 162.6298 148.1614 87.6205 -0.5881 161.9949 162.5830 148.1087 88.4118 -0.5858 161.9547 162.5405 148.0584 89.2633 -0.5806 161.8892 162.4697 148.0109 90.0245 -0.5782 161.8387 162.4169 147.9685 90.8465 -0.5747 161.7964 162.3711 147.9242 91.6385 -0.5732 161.7550 162.3282 147.8798 92.4298 -0.5707 161.7105 162.2812 147.8274 93.2815 -0.5660 161.6493 162.2154 147.7762 94.0425 -0.5633 161.6181 162.1814 147.7355 94.8640 -0.5585 161.5717 162.1302 147.6705 95.6558 -0.5588 161.5345 162.0933 147.6160 96.4468 -0.5555 161.4719 162.0274 147.5731 97.2990 -0.5502 161.4076 161.9578 147.5367 98.0593 -0.5470 161.3763 161.9233 147.4771 98.8805 -0.5465 161.3301 161.8766 147.4255 99.6718 -0.5416 161.2889 161.8305 147.3708 100.4628 -0.5360 161.2414 161.7774 147.3217 101.3148 -0.5350 161.2021 161.7371 147.2768 102.0748 -0.5327 161.1549 161.6876 147.2347 102.8965 -0.5289 161.1023 161.6312 147.1889 103.6870 -0.5247 161.0527 161.5774 147.1235 104.4770 -0.5217 161.0237 161.5455 147.0804 105.2978 -0.5191 160.9761 161.4952 147.0263 106.0873 -0.5168 160.9296 161.4464 146.9836 106.9085 -0.5152 160.8913 161.4065 146.9149 107.6988 -0.5129 160.8307 161.3436 146.8678 108.4898 -0.5078 160.7862 161.2939 146.8372 109.4723 -0.5030 160.7224 161.2254 146.7874 110.3075 -0.5019 160.6769 161.1788 146.7325 111.0985 -0.4981 160.6537 161.1517 146.6776 111.9195 -0.4967 160.5946 161.0913 146.6241 112.7100 -0.4913 160.5376 161.0289 146.5816 113.5313 -0.4876 160.5003 160.9879 146.5339 114.3225 -0.4870 160.4526 160.9396 146.4809 115.1143 -0.4843 160.4107 160.8949 146.4372 115.9355 -0.4804 160.3480 160.8283 146.3864 116.7270 -0.4760 160.2925 160.7685 146.3196 117.5483 -0.4725 160.2572 160.7297 146.2735 118.3388 -0.4723 160.2123 160.6846 146.2202 119.1298 -0.4709 160.1643 160.6352 146.1920 119.9490 -0.4679 160.1055 160.5734 146.1426 120.7388 -0.4666 160.0747 160.5413 146.0896 121.5593 -0.4630 160.0153 160.4782 146.0352 122.3493 -0.4615 159.9758 160.4374 145.9875 123.1405 -0.4581 159.9235 160.3816 145.9319 123.9633 -0.4561 159.8660 160.3221 145.8941 124.7240 -0.4545 159.8265 160.2810 145.8481 125.5760 -0.4512 159.8057 160.2569 145.8002 126.3670 -0.4471 159.7534 160.2006 145.7594 127.1575 -0.4471 159.6992 160.1463 145.6934 127.9788 -0.4442 159.6505 160.0947 145.6410 128.7398 -0.4422 159.6051 160.0473 145.5900 129.5898 -0.4374 159.5376 159.9750 145.5523 130.3808 -0.4355 159.5081 159.9436 145.5000 131.1725 -0.4341 159.4589 159.8930 145.4458 131.9938 -0.4317 159.4115 159.8432 145.3984 132.7545 -0.4293 159.3773 159.8065 145.3541 133.6053 -0.4271 159.3267 159.7538 145.2935 134.3948 -0.4227 159.2709 159.6936 145.2459 135.1858 -0.4207 159.2243 159.6451 145.2105 136.0065 -0.4177 159.1847 159.6024 145.1669 136.7680 -0.4177 159.1355 159.5531 145.1201 137.6195 -0.4146 159.0791 159.4936 145.0771 138.3808 -0.4125 159.0311 159.4437 145.0269 139.2025 -0.4107 158.9898 159.4005 144.9662 140.0235 -0.4075 158.9387 159.3462 144.9194 140.7845 -0.4039 158.8997 159.3036 144.8708 141.6365 -0.4013 158.8478 159.2491 144.8324 142.3978 -0.3992 158.8086 159.2078 144.7834 143.2193 -0.3980 158.7385 159.1365 144.7225 144.0395 -0.3934 158.6845 159.0779 144.6653 144.7993 -0.3907 158.6650 159.0557 144.6251 145.6503 -0.3938 158.6134 159.0072 144.5767 146.4108 -0.3900 158.5766 158.9666 144.5355 147.2315 -0.3863 158.5206 158.9069 144.4907 148.0513 -0.3861 158.4620 158.8481 144.4480 148.8130 -0.3839 158.4208 158.8047 144.3940 149.6638 -0.3805 158.3739 158.7545 144.3397 150.4528 -0.3804 158.3298 158.7102 144.2885 151.2425 -0.3766 158.2820 158.6586 144.2428 152.0623 -0.3744 158.2241 158.5985 144.1933 152.8513 -0.3701 158.1757 158.5458 144.1397 153.6723 -0.3689 158.1324 158.5013 144.0896 154.4638 -0.3673 158.0783 158.4456 144.0424 155.2540 -0.3669 158.0357 158.4026 144.0022 156.1043 -0.3649 157.9852 158.3501 143.9611 156.8650 -0.3631 157.9510 158.3142 143.9172 157.6860 -0.3615 157.8864 158.2479 143.8569 158.4765 -0.3600 157.8347 158.1947 143.8148 159.2673 -0.3595 157.8008 158.1604 143.7823 160.1185 -0.3540 157.7592 158.1132 143.7076 160.8798 -0.3524 157.7119 158.0642 143.6720 161.6998 -0.3495 157.6725 158.0220 143.6148 162.4895 -0.3469 157.6197 157.9666 143.5621 163.2805 -0.3449 157.5512 157.8962 143.5219 164.1313 -0.3435 157.5094 157.8529 143.4585 164.8908 -0.3414 157.4606 157.8020 143.4292 165.7098 -0.3398 157.4245 157.7642 143.3957 166.5295 -0.3376 157.3807 157.7184 143.3255 167.2895 -0.3357 157.3275 157.6632 143.2808 168.1398 -0.3335 157.2751 157.6087 143.2330 168.9010 -0.3330 157.2321 157.5651 143.1966 169.7208 -0.3296 157.1895 157.5191 143.1300 170.6403 -0.3276 157.1303 157.4580 143.0866 171.5018 -0.3251 157.0738 157.3989 143.0284 172.3533 -0.3245 157.0165 157.3411 142.9815 173.1128 -0.3249 156.9896 157.3145 142.9468 173.9345 -0.3227 156.9298 157.2525 142.8988 174.7253 -0.3175 156.8915 157.2090 142.8529 175.5140 -0.3181 156.8532 157.1713 142.8126 176.3633 -0.3165 156.7925 157.1090 142.7652 177.1230 -0.3144 156.7544 157.0688 142.7083 177.9440 -0.3136 156.7097 157.0233 142.6481 178.7640 -0.3119 156.6525 156.9644 142.6115 179.5243 -0.3111 156.6033 156.9143 142.5687 180.3755 -0.3091 156.5541 156.8632 142.5124 181.1353 -0.3067 156.5155 156.8222 142.4663 181.9560 -0.3052 156.4602 156.7653 142.3984 182.7758 -0.3034 156.3987 156.7021 142.3469 183.5355 -0.3015 156.3683 156.6698 142.3053 184.3858 -0.2990 156.3191 156.6180 142.2733 185.1470 -0.2966 156.2773 156.5739 142.2255 185.9700 -0.2934 156.2149 156.5083 142.1818 186.7905 -0.2914 156.1593 156.4507 142.1327 187.5515 -0.2914 156.1122 156.4036 142.0847 188.4023 -0.2893 156.0631 156.3524 142.0449 189.1628 -0.2874 156.0285 156.3159 142.0005 189.9833 -0.2854 155.9608 156.2462 141.9434 190.7735 -0.2842 155.9403 156.2245 141.9085 191.5640 -0.2832 155.8946 156.1778 141.8616 192.4145 -0.2811 155.8365 156.1176 141.8039 193.1760 -0.2806 155.7964 156.0770 141.7632 193.9968 -0.2783 155.7356 156.0139 141.7134 194.7865 -0.2788 155.6937 155.9725 141.6801 195.5778 -0.2738 155.6442 155.9180 141.6167 196.4283 -0.2754 155.5851 155.8604 141.5608 197.1890 -0.2733 155.5512 155.8245 141.5308 198.0105 -0.2715 155.5104 155.7819 141.4837 198.8018 -0.2690 155.4461 155.7151 141.4349 199.5923 -0.2675 155.3953 155.6628 141.3874 200.4125 -0.2666 155.3501 155.6167 141.3531 201.1843 -0.2664 155.3079 155.5743 141.3175 202.0168 -0.2634 155.2514 155.5148 141.2614 202.8055 -0.2611 155.2057 155.4668 141.2057 203.6263 -0.2575 155.1716 155.4292 141.1594 204.4170 -0.2586 155.1309 155.3896 141.0985 205.2083 -0.2581 155.0746 155.3327 141.0555 206.0325 -0.2561 155.0362 155.2923 141.0114 206.7945 -0.2543 154.9840 155.2383 140.9757 207.6465 -0.2518 154.9263 155.1781 140.9166 208.4373 -0.2532 154.8842 155.1374 140.8768 209.2278 -0.2513 154.8369 155.0882 140.8232 210.0483 -0.2482 154.7912 155.0395 140.7606 210.8083 -0.2452 154.7367 154.9819 140.7219 211.6600 -0.2435 154.6818 154.9254 140.6859 212.4510 -0.2420 154.6425 154.8845 140.6336 213.2418 -0.2451 154.5988 154.8439 140.5941 214.0625 -0.2420 154.5535 154.7955 140.5305 214.8228 -0.2430 154.4946 154.7376 140.4974 215.6725 -0.2394 154.4503 154.6897 140.4413 216.4618 -0.2381 154.4178 154.6560 140.4100 217.2528 -0.2370 154.3582 154.5952 140.3707 218.0735 -0.2364 154.3083 154.5447 140.3112 218.8345 -0.2353 154.2550 154.4903 140.2684 219.6863 -0.2370 154.2034 154.4404 140.2166 220.4468 -0.2354 154.1565 154.3918 140.1695 221.2685 -0.2334 154.1282 154.3616 140.1216 222.0530 -0.2320 154.0712 154.3032 140.0870 222.8828 -0.2303 154.0162 154.2465 140.0385 223.6735 -0.2287 153.9777 154.2064 139.9871 224.4645 -0.2272 153.9186 154.1458 139.9362 225.3153 -0.2250 153.8720 154.0970 139.8924 226.0760 -0.2241 153.8290 154.0531 139.8442 226.8968 -0.2214 153.7867 154.0081 139.7955 227.6858 -0.2181 153.7391 153.9571 139.7568 228.4768 -0.2177 153.6918 153.9095 139.7031 229.3280 -0.2195 153.6324 153.8519 139.6640 230.0888 -0.2186 153.5921 153.8107 139.6101 230.9090 -0.2170 153.5293 153.7463 139.5617 231.6990 -0.2157 153.4853 153.7010 139.5282 232.4890 -0.2142 153.4487 153.6628 139.4867 233.3398 -0.2110 153.4036 153.6146 139.4330 234.1008 -0.2117 153.3588 153.5705 139.3916 234.9215 -0.2102 153.2924 153.5025 139.3475 235.7118 -0.2080 153.2493 153.4573 139.2997 236.5015 -0.2076 153.2180 153.4256 139.2573 237.3528 -0.2044 153.1632 153.3676 139.2059 238.1138 -0.2033 153.1229 153.3262 139.1589 238.9355 -0.2028 153.0800 153.2828 139.1046 239.7258 -0.2034 153.0248 153.2282 139.0609 240.5163 -0.2022 152.9680 153.1702 139.0053 241.3655 -0.1998 152.9193 153.1191 138.9557 242.1073 -0.2004 152.8723 153.0727 138.9253 242.9365 -0.1990 152.8198 153.0188 138.8917 243.7275 -0.1968 152.7832 152.9799 138.8773 244.5785 -0.1968 152.7338 152.9305 138.7900 245.3395 -0.1962 152.6870 152.8832 138.7553 246.1608 -0.1961 152.6317 152.8278 138.7016 246.9805 -0.1935 152.5909 152.7843 138.6495 247.7408 -0.1939 152.5315 152.7253 138.6148 248.5923 -0.1929 152.4854 152.6783 138.5652 249.3818 -0.1879 152.4398 152.6277 138.5279 250.1730 -0.1911 152.4149 152.6060 138.4768 250.9935 -0.1910 152.3619 152.5530 138.4186 251.7538 -0.1897 152.3210 152.5107 138.3809 252.6053 -0.1871 152.2658 152.4529 138.3283 253.3965 -0.1850 152.2099 152.3950 138.2982 254.1880 -0.1849 152.1545 152.3394 138.2531 255.0095 -0.1844 152.0957 152.2801 138.2000 255.7703 -0.1826 152.0444 152.2270 138.1571 256.6223 -0.1811 152.0201 152.2012 138.1093 257.4133 -0.1799 151.9743 152.1542 138.0654 258.2048 -0.1815 151.9214 152.1029 138.0053 259.0260 -0.1801 151.8640 152.0441 137.9553 259.7875 -0.1801 151.8188 151.9989 137.8986 260.6395 -0.1802 151.7865 151.9667 137.8617 261.4288 -0.1767 151.7292 151.9059 137.8072 262.2190 -0.1752 151.6889 151.8641 137.7727 263.0098 -0.1750 151.6229 151.7979 137.7274 263.8413 -0.1746 151.5773 151.7519 137.6722 264.6328 -0.1722 151.5269 151.6992 137.6215 265.4230 -0.1726 151.4765 151.6491 137.6100 266.2725 -0.1709 151.4229 151.5938 137.5524 267.0318 -0.1685 151.3991 151.5676 137.5013 267.8528 -0.1673 151.3534 151.5207 137.4571 268.6735 -0.1713 151.2898 151.4612 137.4389 269.4338 -0.1687 151.2442 151.4129 137.3815 270.2853 -0.1686 151.2130 151.3815 137.3372 271.0458 -0.1681 151.1506 151.3187 137.2914 271.8668 -0.1679 151.1044 151.2723 137.2579 272.6865 -0.1652 151.0506 151.2158 137.2150 273.4463 -0.1617 151.0059 151.1676 137.1619 274.2973 -0.1637 150.9481 151.1118 137.1313 275.0868 -0.1628 150.9039 151.0667 137.0914 275.8778 -0.1629 150.8611 151.0240 137.0546 276.6985 -0.1615 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