DTA measure 11240326-1_Pb4.dat Date: 2024326:141 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.45 s Mass = 1410.000 mg data_number = 1584 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1450 -1.0289 259.2624 260.2913 263.9143 1.9965 -1.0302 259.2891 260.3192 263.9187 2.7570 -1.0292 259.3065 260.3357 263.9211 3.5785 -1.0264 259.3384 260.3648 263.9121 4.4005 -1.0272 259.3639 260.3912 263.8994 5.1620 -1.0264 259.3877 260.4142 263.9042 6.0138 -1.0265 259.4215 260.4480 263.9211 6.7755 -1.0271 259.4425 260.4696 263.9268 7.5965 -1.0259 259.4418 260.4677 263.9382 8.3885 -1.0284 259.4819 260.5104 263.9407 9.1805 -1.0256 259.5007 260.5264 263.9474 10.0323 -1.0256 259.5243 260.5499 263.9736 10.7715 -1.0252 259.5508 260.5760 263.9956 11.6313 -1.0241 259.5995 260.6236 263.9908 12.3918 -1.0252 259.6142 260.6394 264.0180 13.2133 -1.0260 259.6295 260.6555 264.0422 14.0345 -1.0268 259.6563 260.6831 264.0674 14.7955 -1.0279 259.6623 260.6902 264.0829 15.6475 -1.0294 259.6855 260.7149 264.1127 16.4095 -1.0266 259.7033 260.7299 264.1723 17.2308 -1.0272 259.7330 260.7602 264.2094 18.0225 -1.0265 259.7764 260.8029 264.2542 18.8130 -1.0303 259.7869 260.8171 264.2892 19.6650 -1.0295 259.8207 260.8503 264.3398 20.4260 -1.0277 259.8268 260.8545 264.3917 21.2473 -1.0260 259.8568 260.8827 264.4590 22.0380 -1.0274 259.8654 260.8928 264.5243 22.8288 -1.0309 259.8928 260.9236 264.5936 23.6808 -1.0316 259.9149 260.9464 264.6692 24.4410 -1.0322 259.9384 260.9706 264.7314 25.2623 -1.0329 259.9587 260.9916 264.8113 26.0540 -1.0341 259.9814 261.0155 264.8854 26.8448 -1.0374 260.0035 261.0409 264.9541 27.6668 -1.0374 260.0295 261.0669 265.0435 28.4578 -1.0379 260.0511 261.0889 265.1457 29.2788 -1.0387 260.0765 261.1151 265.2358 30.0695 -1.0390 260.0895 261.1284 265.3358 30.8615 -1.0427 260.1132 261.1559 265.4148 31.6545 -1.0428 260.1252 261.1680 265.5040 32.4765 -1.0415 260.1617 261.2032 265.6178 33.2985 -1.0439 260.1982 261.2421 265.7260 34.0590 -1.0478 260.2273 261.2750 265.8287 34.9103 -1.0489 260.2336 261.2825 265.9457 35.6705 -1.0484 260.2595 261.3080 266.0560 36.4943 -1.0492 260.2774 261.3266 266.1523 37.2865 -1.0518 260.2977 261.3495 266.2801 38.0783 -1.0531 260.3212 261.3743 266.3868 38.8995 -1.0553 260.3307 261.3860 266.5299 39.6915 -1.0595 260.3598 261.4193 266.6347 40.5130 -1.0619 260.3868 261.4487 266.7783 41.3045 -1.0602 260.4150 261.4752 266.8800 42.0958 -1.0643 260.4267 261.4909 267.0101 42.9168 -1.0680 260.4783 261.5463 267.1464 43.6765 -1.0709 260.5001 261.5710 267.2689 44.5278 -1.0710 260.5116 261.5827 267.3937 45.3180 -1.0694 260.5497 261.6191 267.5136 46.1090 -1.0707 260.5629 261.6336 267.6298 46.9308 -1.0746 260.5892 261.6638 267.7751 47.7195 -1.0777 260.5959 261.6736 267.9078 48.5408 -1.0787 260.6262 261.7049 268.0402 49.3320 -1.0826 260.6615 261.7441 268.1502 50.1233 -1.0852 260.6915 261.7767 268.2921 50.9450 -1.0871 260.7283 261.8154 268.4363 51.7298 -1.0873 260.7486 261.8359 268.5641 52.5315 -1.0881 260.7624 261.8505 268.6762 53.3238 -1.0919 260.7797 261.8716 268.7922 54.1755 -1.0956 260.8341 261.9296 268.9608 54.9348 -1.0966 260.8503 261.9469 269.0699 55.7563 -1.1012 260.8879 261.9892 269.1822 56.5475 -1.1023 260.9027 262.0050 269.2964 57.3390 -1.1063 260.9272 262.0335 269.4263 58.1888 -1.1090 260.9488 262.0579 269.5653 58.9505 -1.1100 260.9773 262.0873 269.6899 59.7725 -1.1148 261.0103 262.1251 269.8146 60.5645 -1.1195 261.0373 262.1568 269.9256 61.3558 -1.1198 261.0603 262.1801 270.0379 62.1430 -1.1206 261.0841 262.2046 270.1454 62.9845 -1.1236 261.1139 262.2376 270.2650 63.7465 -1.1265 261.1552 262.2817 270.3690 64.5985 -1.1285 261.1822 262.3108 270.5135 65.3605 -1.1295 261.2131 262.3426 270.6154 66.1818 -1.1343 261.2529 262.3872 270.7324 67.0023 -1.1380 261.2887 262.4267 270.8301 67.7633 -1.1382 261.3138 262.4520 270.9430 68.6150 -1.1393 261.3503 262.4896 271.0583 69.3770 -1.1422 261.3665 262.5086 271.1701 70.1988 -1.1474 261.3904 262.5378 271.2890 70.9910 -1.1471 261.4316 262.5787 271.3917 71.7915 -1.1485 261.4488 262.5972 271.4900 72.5835 -1.1526 261.4849 262.6375 271.5769 73.4353 -1.1534 261.5055 262.6589 271.6959 74.1968 -1.1565 261.5403 262.6969 271.7934 75.0183 -1.1584 261.5690 262.7273 271.9052 75.8100 -1.1617 261.6273 262.7889 272.0093 76.6015 -1.1634 261.6694 262.8328 272.1128 77.4238 -1.1643 261.6984 262.8627 272.2084 78.2158 -1.1699 261.7407 262.9107 272.3089 79.0368 -1.1722 261.7628 262.9350 272.4160 79.8275 -1.1743 261.7990 262.9733 272.5229 80.6190 -1.1762 261.8117 262.9879 272.6175 81.4408 -1.1782 261.8515 263.0296 272.7283 82.2193 -1.1804 261.8983 263.0787 272.8207 83.0365 -1.1818 261.9256 263.1074 272.9197 83.8585 -1.1837 261.9453 263.1290 273.0148 84.6495 -1.1880 261.9943 263.1823 273.1192 85.4408 -1.1897 262.0401 263.2298 273.2209 86.2615 -1.1898 262.0833 263.2731 273.3238 87.0235 -1.1944 262.1102 263.3046 273.4206 87.8755 -1.1978 262.1423 263.3401 273.5231 88.6675 -1.1982 262.1668 263.3651 273.6196 89.4590 -1.2017 262.2127 263.4144 273.6912 90.2805 -1.2020 262.2475 263.4495 273.7718 91.0415 -1.2030 262.2658 263.4688 273.8751 91.8935 -1.2072 262.2981 263.5052 273.9738 92.6603 -1.2083 262.3543 263.5625 274.0523 93.4593 -1.2106 262.4008 263.6114 274.1518 94.2810 -1.2130 262.4221 263.6351 274.2375 95.1033 -1.2146 262.4601 263.6746 274.3276 95.8635 -1.2196 262.4986 263.7183 274.4047 96.7160 -1.2198 262.5434 263.7632 274.5092 97.4780 -1.2226 262.5848 263.8074 274.6023 98.2983 -1.2214 262.6295 263.8509 274.6887 99.1200 -1.2234 262.6479 263.8713 274.7823 99.8798 -1.2260 262.7011 263.9270 274.8804 100.7318 -1.2280 262.7310 263.9591 274.9693 101.5220 -1.2320 262.7680 264.0001 275.0437 102.3133 -1.2328 262.8227 264.0554 275.1209 103.1003 -1.2314 262.8485 264.0799 275.1972 103.9415 -1.2355 262.8901 264.1255 275.2900 104.7035 -1.2403 262.9456 264.1859 275.3777 105.5555 -1.2422 262.9815 264.2238 275.4532 106.3158 -1.2426 263.0230 264.2657 275.5333 107.1370 -1.2423 263.0527 264.2950 275.6414 107.9580 -1.2435 263.1148 264.3583 275.7196 108.7195 -1.2482 263.1481 264.3963 275.8100 109.5713 -1.2497 263.1824 264.4321 275.9138 110.3325 -1.2511 263.2240 264.4750 276.0006 111.1538 -1.2535 263.2702 264.5237 276.0986 111.9733 -1.2534 263.2991 264.5525 276.1782 112.7340 -1.2559 263.3440 264.6000 276.2603 113.5423 -1.2588 263.3841 264.6429 276.3618 114.3945 -1.2618 263.4519 264.7137 276.4401 115.1565 -1.2659 263.4811 264.7470 276.5306 115.9785 -1.2689 263.5207 264.7896 276.6330 116.7700 -1.2709 263.5781 264.8490 276.7311 117.5615 -1.2720 263.6231 264.8951 276.8325 118.3825 -1.2732 263.6566 264.9298 276.9294 119.1735 -1.2741 263.6860 264.9600 277.0291 119.9948 -1.2764 263.7392 265.0156 277.1259 120.7870 -1.2781 263.7954 265.0735 277.2188 121.5778 -1.2794 263.8512 265.1306 277.3090 122.4298 -1.2813 263.8808 265.1621 277.3900 123.1870 -1.2843 263.9190 265.2033 277.4738 123.9950 -1.2856 263.9732 265.2588 277.5756 124.8168 -1.2863 264.0205 265.3068 277.6739 125.6090 -1.2884 264.0494 265.3378 277.7870 126.3998 -1.2890 264.1062 265.3952 277.8827 127.2218 -1.2913 264.1639 265.4553 277.9729 128.0130 -1.2939 264.1964 265.4904 278.0872 128.8345 -1.2962 264.2488 265.5450 278.2044 129.6255 -1.2995 264.3022 265.6017 278.3043 130.4178 -1.3004 264.3509 265.6513 278.3956 131.2395 -1.3000 264.3807 265.6806 278.5048 132.0308 -1.3057 264.4353 265.7410 278.6169 132.8520 -1.3086 264.4988 265.8074 278.7034 133.6190 -1.3086 264.5336 265.8421 278.8383 134.4475 -1.3104 264.5783 265.8887 278.9375 135.2395 -1.3141 264.6156 265.9297 279.0370 136.0615 -1.3134 264.6731 265.9866 279.1504 136.8230 -1.3157 264.7323 266.0480 279.2632 137.6743 -1.3194 264.7891 266.1085 279.3871 138.4655 -1.3210 264.8249 266.1459 279.4995 139.2575 -1.3234 264.8590 266.1824 279.6061 140.0805 -1.3253 264.9382 266.2635 279.7122 140.8483 -1.3262 264.9779 266.3041 279.8189 141.7000 -1.3266 265.0206 266.3471 279.9354 142.4613 -1.3323 265.0767 266.4090 280.0385 143.2810 -1.3342 265.1123 266.4466 280.1559 144.0618 -1.3362 265.1867 266.5229 280.2488 144.9003 -1.3370 265.2416 266.5786 280.3841 145.6605 -1.3431 265.2837 266.6268 280.4927 146.5108 -1.3416 265.3373 266.6789 280.6068 147.2718 -1.3408 265.3865 266.7273 280.7068 148.0938 -1.3452 265.4402 266.7854 280.8137 148.8850 -1.3497 265.4909 266.8406 280.9294 149.6753 -1.3514 265.5456 266.8970 281.0330 150.5270 -1.3546 265.5968 266.9514 281.1665 151.2870 -1.3559 265.6559 267.0118 281.2820 152.1085 -1.3570 265.6995 267.0565 281.3946 152.8995 -1.3586 265.7521 267.1107 281.4753 153.6893 -1.3628 265.8010 267.1638 281.5864 154.5005 -1.3638 265.8609 267.2246 281.7210 155.3225 -1.3659 265.9218 267.2877 281.8099 156.1128 -1.3667 265.9694 267.3361 281.9120 156.9345 -1.3680 266.0274 267.3954 282.0456 157.7260 -1.3707 266.0868 267.4575 282.1394 158.5175 -1.3736 266.1393 267.5129 282.2505 159.3395 -1.3751 266.2006 267.5757 282.3575 160.1005 -1.3787 266.2469 267.6256 282.4484 160.9543 -1.3786 266.3175 267.6961 282.5594 161.7143 -1.3787 266.3682 267.7469 282.6691 162.5348 -1.3823 266.4042 267.7865 282.7742 163.3548 -1.3861 266.4800 267.8660 282.8896 164.1353 -1.3900 266.5265 267.9165 283.0051 164.9235 -1.3910 266.5838 267.9748 283.0963 165.7755 -1.3925 266.6407 268.0332 283.2195 166.5373 -1.3945 266.6919 268.0864 283.3252 167.3570 -1.3970 266.7586 268.1557 283.4451 168.1485 -1.3988 266.8232 268.2219 283.5426 168.9405 -1.4002 266.8625 268.2627 283.6505 169.7623 -1.4009 266.9267 268.3277 283.7571 170.5533 -1.4014 266.9952 268.3966 283.8617 171.3743 -1.4044 267.0497 268.4541 283.9602 172.1650 -1.4053 267.1095 268.5148 284.0704 172.9565 -1.4110 267.1692 268.5802 284.1704 173.7790 -1.4141 267.2260 268.6401 284.2883 174.5773 -1.4176 267.2762 268.6938 284.3828 175.3455 -1.4169 267.3327 268.7496 284.4812 176.1978 -1.4186 267.3949 268.8135 284.5686 176.9580 -1.4217 267.4399 268.8616 284.6735 177.7793 -1.4248 267.5194 268.9442 284.7793 178.6010 -1.4271 267.5828 269.0099 284.8938 179.3625 -1.4314 267.6488 269.0801 284.9904 180.2140 -1.4340 267.7176 269.1516 285.0975 180.9755 -1.4339 267.7880 269.2218 285.1800 181.7958 -1.4345 267.8331 269.2676 285.2842 182.6168 -1.4364 267.8994 269.3358 285.3887 183.3775 -1.4404 267.9444 269.3848 285.4832 184.2295 -1.4398 268.0209 269.4607 285.5895 185.0183 -1.4445 268.0834 269.5279 285.7096 185.7978 -1.4480 268.1372 269.5852 285.7931 186.6195 -1.4491 268.1905 269.6397 285.9083 187.4125 -1.4498 268.2651 269.7149 285.9964 188.2043 -1.4518 268.3365 269.7883 286.0792 189.0250 -1.4515 268.3921 269.8436 286.1931 189.7865 -1.4536 268.4456 269.8992 286.2672 190.6385 -1.4554 268.5260 269.9815 286.3605 191.4305 -1.4579 268.5722 270.0302 286.4607 192.2210 -1.4583 268.6266 270.0849 286.5638 193.0415 -1.4590 268.7079 270.1670 286.6733 193.8015 -1.4627 268.7701 270.2328 286.7565 194.6530 -1.4659 268.8148 270.2806 286.8609 195.4643 -1.4682 268.8974 270.3656 286.9678 196.2248 -1.4717 268.9573 270.4290 287.0715 197.0460 -1.4716 269.0319 270.5035 287.1548 197.8660 -1.4697 269.1000 270.5697 287.2395 198.6275 -1.4726 269.1508 270.6234 287.3404 199.4798 -1.4747 269.2154 270.6901 287.4378 200.2408 -1.4776 269.2768 270.7543 287.5368 201.0623 -1.4790 269.3651 270.8441 287.6279 201.8530 -1.4781 269.4357 270.9138 287.7214 202.6438 -1.4783 269.4764 270.9547 287.8155 203.4660 -1.4786 269.5364 271.0150 287.9108 204.2570 -1.4813 269.6193 271.1006 287.9968 205.0958 -1.4838 269.6917 271.1755 288.1083 205.8813 -1.4886 269.7550 271.2436 288.2054 206.6723 -1.4884 269.8169 271.3053 288.2855 207.4628 -1.4913 269.8928 271.3841 288.3800 208.2845 -1.4920 269.9522 271.4442 288.4570 209.0758 -1.4954 270.0178 271.5133 288.5671 209.8970 -1.4985 270.0828 271.5813 288.6569 210.6885 -1.4976 270.1647 271.6623 288.7668 211.4805 -1.4988 270.2347 271.7335 288.8567 212.3025 -1.4982 270.2900 271.7882 288.9489 213.0935 -1.5011 270.3576 271.8586 289.0726 213.9155 -1.5042 270.4251 271.9293 289.1925 214.7075 -1.5056 270.4845 271.9901 289.2669 215.5363 -1.5056 270.5857 272.0913 289.3762 216.3055 -1.5075 270.6590 272.1665 289.4843 217.1265 -1.5109 270.7235 272.2344 289.5783 217.8878 -1.5148 270.7782 272.2930 289.6797 218.7385 -1.5140 270.8507 272.3647 289.7946 219.5305 -1.5160 270.9134 272.4293 289.8960 220.3220 -1.5165 270.9790 272.4955 289.9922 221.1443 -1.5180 271.0562 272.5742 290.1130 221.9048 -1.5192 271.1329 272.6521 290.2153 222.7558 -1.5225 271.2079 272.7304 290.3108 223.5470 -1.5243 271.2713 272.7956 290.4230 224.3378 -1.5272 271.3372 272.8644 290.5369 225.1600 -1.5321 271.4067 272.9388 290.6694 225.9773 -1.5317 271.4701 273.0018 290.7558 226.7250 -1.5301 271.5411 273.0713 290.8575 227.5768 -1.5337 271.6176 273.1513 290.9645 228.3378 -1.5365 271.6655 273.2020 291.0613 229.1585 -1.5391 271.7532 273.2924 291.1784 229.9800 -1.5389 271.8269 273.3658 291.2728 230.7410 -1.5406 271.8867 273.4272 291.3717 231.5923 -1.5441 271.9714 273.5154 291.5063 232.3535 -1.5474 272.0513 273.5987 291.6197 233.1740 -1.5491 272.1358 273.6849 291.7163 233.9955 -1.5513 272.1994 273.7507 291.8303 234.7575 -1.5522 272.2605 273.8127 291.9346 235.6095 -1.5551 272.3588 273.9139 292.0326 236.4173 -1.5568 272.4129 273.9696 292.1320 237.1775 -1.5558 272.4639 274.0197 292.2388 237.9995 -1.5577 272.5525 274.1102 292.3543 238.8215 -1.5617 272.6151 274.1768 292.4543 239.5820 -1.5637 272.6888 274.2524 292.5490 240.4335 -1.5645 272.7712 274.3357 292.6452 241.1948 -1.5687 272.8393 274.4080 292.7423 242.0163 -1.5705 272.9151 274.4856 292.8583 242.8075 -1.5706 272.9916 274.5623 292.9685 243.5990 -1.5752 273.0624 274.6377 293.0867 244.4505 -1.5768 273.1336 274.7104 293.1911 245.2115 -1.5789 273.2147 274.7936 293.2959 246.0525 -1.5796 273.3225 274.9021 293.3880 246.8430 -1.5780 273.3897 274.9677 293.4845 247.6340 -1.5811 273.4456 275.0267 293.5974 248.4258 -1.5798 273.5200 275.0998 293.6969 249.2480 -1.5836 273.6013 275.1849 293.8111 250.0388 -1.5889 273.6772 275.2662 293.9010 250.8603 -1.5904 273.7488 275.3393 294.0046 251.6520 -1.5913 273.8241 275.4154 294.1155 252.4428 -1.5922 273.9016 275.4938 294.2103 253.2650 -1.5935 273.9931 275.5866 294.3162 254.0550 -1.5961 274.0608 275.6569 294.4048 254.8760 -1.5971 274.1384 275.7355 294.5128 255.6668 -1.5985 274.2262 275.8248 294.6252 256.4943 -1.5998 274.2884 275.8882 294.7111 257.2628 -1.6040 274.3485 275.9525 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