DTA measure 1240326-1_Pb3.dat Date: 2024326:1258 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.50 s Mass = 1410.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3145 -1.0145 264.1705 265.1850 264.3246 2.1058 -1.0136 264.1724 265.1860 264.3447 2.9265 -1.0122 264.1920 265.2041 264.3358 3.6863 -1.0134 264.1782 265.1915 264.3172 4.5373 -1.0160 264.1823 265.1983 264.3274 5.3275 -1.0128 264.1747 265.1876 264.3412 6.1193 -1.0110 264.1841 265.1951 264.3452 6.9405 -1.0121 264.1687 265.1808 264.3268 7.7025 -1.0139 264.1834 265.1973 264.3336 8.5543 -1.0121 264.1690 265.1811 264.3901 9.3445 -1.0097 264.1717 265.1814 264.3816 10.1360 -1.0097 264.1812 265.1909 264.3848 10.9575 -1.0089 264.1876 265.1965 264.3865 11.7185 -1.0115 264.1765 265.1880 264.4047 12.5703 -1.0085 264.1856 265.1941 264.4511 13.3615 -1.0091 264.1848 265.1939 264.4689 14.1525 -1.0101 264.1772 265.1874 264.5067 14.9743 -1.0101 264.1826 265.1928 264.5191 15.7355 -1.0094 264.1688 265.1783 264.5518 16.5868 -1.0075 264.1788 265.1863 264.6099 17.3780 -1.0082 264.1852 265.1934 264.6516 18.1680 -1.0095 264.1817 265.1912 264.7001 18.9878 -1.0073 264.1923 265.1995 264.7601 19.7778 -1.0075 264.2028 265.2103 264.8103 20.5998 -1.0109 264.1900 265.2009 264.8871 21.3920 -1.0087 264.1877 265.1964 264.9473 22.1828 -1.0107 264.1888 265.1995 265.0242 23.0050 -1.0125 264.1888 265.2014 265.1030 23.7658 -1.0164 264.1788 265.1952 265.1546 24.6178 -1.0131 264.1839 265.1969 265.2419 25.4098 -1.0165 264.1911 265.2076 265.3480 26.2005 -1.0175 264.1940 265.2115 265.4344 27.0215 -1.0184 264.2010 265.2195 265.5268 27.7818 -1.0201 264.2059 265.2260 265.6207 28.6333 -1.0223 264.2089 265.2312 265.7404 29.4245 -1.0212 264.2034 265.2247 265.8611 30.2165 -1.0234 264.1861 265.2095 265.9655 31.0385 -1.0253 264.2075 265.2327 266.0921 31.7995 -1.0254 264.2127 265.2381 266.1957 32.6513 -1.0277 264.2248 265.2524 266.3362 33.4125 -1.0301 264.2264 265.2565 266.4552 34.2345 -1.0315 264.2338 265.2653 266.5912 35.0565 -1.0341 264.2309 265.2650 266.7227 35.8185 -1.0353 264.2306 265.2659 266.8563 36.6470 -1.0365 264.2391 265.2755 267.0108 37.4368 -1.0385 264.2278 265.2663 267.1431 38.2578 -1.0424 264.2370 265.2794 267.2880 39.0475 -1.0445 264.2546 265.2991 267.4263 39.8385 -1.0482 264.2622 265.3103 267.5675 40.6603 -1.0488 264.2619 265.3107 267.7278 41.4515 -1.0489 264.2509 265.2998 267.8765 42.2745 -1.0513 264.2570 265.3083 268.0343 43.0650 -1.0529 264.2686 265.3215 268.1752 43.8553 -1.0551 264.2657 265.3209 268.3364 44.6770 -1.0609 264.2749 265.3359 268.4981 45.4378 -1.0651 264.2716 265.3367 268.6589 46.2898 -1.0654 264.2803 265.3457 268.8105 47.0800 -1.0679 264.2894 265.3573 268.9456 47.8708 -1.0702 264.2938 265.3641 269.1002 48.6920 -1.0732 264.3056 265.3789 269.2777 49.4518 -1.0756 264.3496 265.4252 269.4488 50.3033 -1.0818 264.3485 265.4302 269.6161 51.0945 -1.0839 264.3558 265.4397 269.7744 51.8860 -1.0874 264.3626 265.4501 269.9254 52.7075 -1.0925 264.3445 265.4370 270.0884 53.4685 -1.0949 264.3768 265.4717 270.2377 54.3203 -1.0984 264.4016 265.5000 270.4043 55.0805 -1.1009 264.4134 265.5143 270.5489 55.9018 -1.1019 264.4098 265.5117 270.7304 56.7225 -1.1025 264.4267 265.5292 270.8760 57.4838 -1.1059 264.4308 265.5367 271.0050 58.3355 -1.1090 264.4373 265.5463 271.1647 59.0958 -1.1143 264.4611 265.5754 271.2983 59.9170 -1.1168 264.4767 265.5935 271.4460 60.7085 -1.1197 264.4969 265.6166 271.5920 61.4998 -1.1247 264.5251 265.6498 271.7295 62.3515 -1.1281 264.5315 265.6595 271.8853 63.1135 -1.1325 264.5505 265.6830 272.0285 63.9355 -1.1347 264.5743 265.7091 272.1735 64.7288 -1.1364 264.5891 265.7254 272.3221 65.5185 -1.1405 264.5977 265.7382 272.4519 66.3400 -1.1456 264.6208 265.7664 272.5856 67.1308 -1.1462 264.6396 265.7858 272.7195 67.9518 -1.1489 264.6431 265.7920 272.8792 68.7465 -1.1530 264.6676 265.8206 273.0002 69.5383 -1.1561 264.7010 265.8571 273.1234 70.3600 -1.1578 264.6970 265.8548 273.2642 71.1210 -1.1602 264.7175 265.8776 273.4005 71.9730 -1.1658 264.7472 265.9129 273.5311 72.7333 -1.1679 264.7668 265.9347 273.6417 73.5555 -1.1726 264.7957 265.9683 273.7742 74.3770 -1.1740 264.8146 265.9886 273.9206 75.1380 -1.1783 264.8429 266.0212 274.0306 75.9898 -1.1826 264.8570 266.0396 274.1685 76.7515 -1.1848 264.8686 266.0534 274.2817 77.5735 -1.1858 264.8890 266.0748 274.4164 78.3655 -1.1889 264.9094 266.0982 274.5509 79.1570 -1.1914 264.9326 266.1240 274.6631 80.0075 -1.1953 264.9828 266.1782 274.7842 80.7695 -1.1986 265.0031 266.2017 274.9026 81.5915 -1.2010 265.0249 266.2260 275.0354 82.3835 -1.2038 265.0504 266.2543 275.1669 83.1748 -1.2069 265.0779 266.2848 275.2760 83.9953 -1.2094 265.1060 266.3154 275.3764 84.7840 -1.2116 265.1203 266.3319 275.5063 85.6040 -1.2139 265.1366 266.3505 275.6361 86.3955 -1.2177 265.1781 266.3958 275.7373 87.2000 -1.2194 265.2043 266.4236 275.8501 88.0065 -1.2204 265.2343 266.4547 275.9678 88.7983 -1.2275 265.2466 266.4742 276.0793 89.6205 -1.2305 265.2794 266.5099 276.1921 90.4123 -1.2336 265.3098 266.5434 276.3068 91.2335 -1.2362 265.3410 266.5772 276.4311 92.0240 -1.2391 265.3739 266.6130 276.5312 92.8145 -1.2417 265.3937 266.6354 276.6602 93.6360 -1.2421 265.4191 266.6612 276.7777 94.4268 -1.2434 265.4524 266.6958 276.8835 95.2485 -1.2462 265.4936 266.7398 276.9935 96.0400 -1.2488 265.5098 266.7586 277.0909 96.8315 -1.2530 265.5406 266.7936 277.2088 97.6540 -1.2525 265.5716 266.8242 277.3248 98.4148 -1.2574 265.6127 266.8701 277.4271 99.2670 -1.2601 265.6537 266.9137 277.5337 100.0590 -1.2618 265.6755 266.9373 277.6459 100.8505 -1.2644 265.7044 266.9688 277.7571 101.6728 -1.2674 265.7446 267.0120 277.8601 102.4345 -1.2722 265.7678 267.0399 277.9849 103.2863 -1.2696 265.8093 267.0789 278.0976 104.0765 -1.2709 265.8499 267.1208 278.2273 104.8673 -1.2740 265.9102 267.1842 278.3543 105.6885 -1.2759 265.9401 267.2160 278.4737 106.4495 -1.2810 265.9402 267.2213 278.5732 107.3013 -1.2795 265.9850 267.2645 278.7125 108.0775 -1.2811 265.9994 267.2805 278.8007 108.9010 -1.2866 266.0547 267.3413 278.9168 109.6923 -1.2885 266.1047 267.3932 279.0480 110.4835 -1.2880 266.1371 267.4251 279.1651 111.3055 -1.2910 266.1888 267.4798 279.2853 112.0958 -1.2946 266.2149 267.5095 279.4115 112.9173 -1.2977 266.2501 267.5478 279.5356 113.7083 -1.2986 266.2880 267.5866 279.6473 114.4988 -1.3000 266.3201 267.6201 279.7627 115.3195 -1.3031 266.3710 267.6741 279.8800 116.1115 -1.3037 266.4123 267.7160 280.0080 116.9320 -1.3062 266.4347 267.7409 280.1402 117.7228 -1.3089 266.4723 267.7812 280.2636 118.5135 -1.3143 266.5210 267.8353 280.3793 119.3350 -1.3167 266.5558 267.8725 280.5085 120.1258 -1.3201 266.5987 267.9188 280.6475 120.9478 -1.3222 266.6380 267.9603 280.7749 121.7400 -1.3268 266.6889 268.0157 280.8937 122.5315 -1.3300 266.7174 268.0474 281.0277 123.3540 -1.3306 266.7625 268.0931 281.1501 124.1458 -1.3295 266.8002 268.1297 281.2826 124.9678 -1.3323 266.8428 268.1751 281.4142 125.7598 -1.3374 266.8963 268.2337 281.5418 126.5515 -1.3380 266.9488 268.2868 281.6765 127.3735 -1.3382 267.0061 268.3444 281.8272 128.1418 -1.3427 267.0323 268.3750 281.9389 128.9843 -1.3456 267.0786 268.4243 282.0664 129.7450 -1.3460 267.1300 268.4760 282.2014 130.5965 -1.3462 267.1591 268.5053 282.3468 131.3575 -1.3485 267.1952 268.5437 282.4561 132.1793 -1.3507 267.2528 268.6034 282.5793 133.0005 -1.3526 267.2997 268.6522 282.7117 133.7625 -1.3559 267.3535 268.7093 282.8403 134.6145 -1.3595 267.3973 268.7568 282.9752 135.3765 -1.3616 267.4442 268.8058 283.0981 136.1980 -1.3636 267.4856 268.8492 283.2386 137.0195 -1.3675 267.5353 268.9028 283.3756 137.7793 -1.3685 267.5785 268.9471 283.4989 138.6303 -1.3710 267.6249 268.9959 283.6467 139.3905 -1.3715 267.6932 269.0647 283.7649 140.2118 -1.3768 267.7526 269.1294 283.8834 141.0628 -1.3766 267.7940 269.1706 284.0444 141.8233 -1.3789 267.8361 269.2149 284.1550 142.6448 -1.3813 267.8880 269.2693 284.2753 143.4375 -1.3834 267.9398 269.3232 284.4014 144.2278 -1.3879 267.9901 269.3780 284.5410 145.0800 -1.3871 268.0279 269.4151 284.6763 145.8418 -1.3899 268.0893 269.4792 284.7966 146.6640 -1.3960 268.1466 269.5426 284.9209 147.4550 -1.3918 268.2017 269.5935 285.0362 148.2463 -1.3980 268.2650 269.6629 285.1508 149.0618 -1.3997 268.3122 269.7119 285.2766 149.8595 -1.4016 268.3546 269.7562 285.4088 150.6815 -1.4049 268.4150 269.8199 285.5410 151.4425 -1.4090 268.4494 269.8584 285.6615 152.2945 -1.4095 268.5108 269.9203 285.8044 153.0845 -1.4100 268.5650 269.9751 285.9187 153.8750 -1.4133 268.6124 270.0257 286.0421 154.6955 -1.4143 268.6895 270.1038 286.1632 155.4558 -1.4143 268.7387 270.1530 286.2495 156.3073 -1.4192 268.8148 270.2340 286.4160 157.0985 -1.4213 268.8694 270.2906 286.5349 157.8895 -1.4226 268.9095 270.3322 286.6651 158.7105 -1.4265 268.9933 270.4198 286.7763 159.4713 -1.4282 269.0432 270.4714 286.8877 160.3225 -1.4303 269.0801 270.5104 286.9985 161.1135 -1.4301 269.1418 270.5720 287.1504 161.9040 -1.4341 269.2061 270.6402 287.2698 162.7240 -1.4382 269.2762 270.7143 287.4131 163.4848 -1.4392 269.3229 270.7621 287.5347 164.3355 -1.4402 269.3865 270.8267 287.6691 165.1265 -1.4412 269.4468 270.8880 287.7915 165.9180 -1.4429 269.5056 270.9484 287.9173 166.7393 -1.4447 269.5515 270.9963 288.0647 167.4983 -1.4467 269.6304 271.0772 288.1782 168.3488 -1.4507 269.6808 271.1315 288.3282 169.1385 -1.4540 269.7510 271.2050 288.4599 169.9285 -1.4537 269.8128 271.2665 288.5885 170.7505 -1.4579 269.8626 271.3205 288.7240 171.5125 -1.4616 269.9375 271.3991 288.8276 172.3650 -1.4617 269.9987 271.4603 288.9971 173.1268 -1.4656 270.0527 271.5183 289.1319 173.9483 -1.4695 270.1127 271.5822 289.2581 174.7395 -1.4707 270.1776 271.6483 289.3864 175.5305 -1.4727 270.2469 271.7196 289.5266 176.3528 -1.4749 270.3128 271.7877 289.6516 177.1438 -1.4776 270.3678 271.8454 289.7832 177.9655 -1.4819 270.4515 271.9334 289.9201 178.7573 -1.4832 270.5330 272.0162 290.0680 179.5480 -1.4853 270.5858 272.0710 290.1949 180.3695 -1.4885 270.6450 272.1335 290.3392 181.1305 -1.4910 270.7235 272.2144 290.4792 181.9825 -1.4916 270.7819 272.2735 290.6153 182.7735 -1.4958 270.8507 272.3465 290.7340 183.5653 -1.4950 270.9147 272.4097 290.8508 184.3865 -1.4992 270.9652 272.4644 290.9932 185.1468 -1.5009 271.0252 272.5261 291.1198 185.9985 -1.5069 271.1214 272.6283 291.2579 186.7595 -1.5077 271.1709 272.6787 291.3914 187.5813 -1.5097 271.2405 272.7502 291.5236 188.4025 -1.5108 271.3383 272.8491 291.6715 189.1628 -1.5136 271.3815 272.8952 291.7846 190.0143 -1.5218 271.4386 272.9605 291.9238 190.7755 -1.5223 271.5041 273.0264 292.0414 191.5975 -1.5228 271.5870 273.1098 292.1760 192.3893 -1.5262 271.6664 273.1925 292.3067 193.1800 -1.5283 271.7340 273.2623 292.4158 194.0313 -1.5311 271.7954 273.3265 292.5733 194.7910 -1.5334 271.8619 273.3953 292.6902 195.6115 -1.5344 271.9409 273.4754 292.8174 196.4030 -1.5363 272.0112 273.5475 292.9237 197.1948 -1.5385 272.0826 273.6211 293.0727 198.0470 -1.5410 272.1454 273.6864 293.1991 198.8073 -1.5453 272.2084 273.7537 293.3121 199.6278 -1.5496 272.2909 273.8406 293.4287 200.3908 -1.5548 272.3618 273.9166 293.5449 201.2430 -1.5527 272.4296 273.9823 293.6961 202.0048 -1.5561 272.5272 274.0833 293.8085 202.8263 -1.5572 272.5959 274.1531 293.9437 203.6475 -1.5602 272.6581 274.2183 294.0707 204.4085 -1.5624 272.7358 274.2982 294.1931 205.2598 -1.5661 272.7998 274.3659 294.2981 206.0215 -1.5690 272.8592 274.4282 294.4055 206.8443 -1.5713 272.9389 274.5102 294.5436 207.6355 -1.5707 273.0124 274.5831 294.6679 208.4263 -1.5743 273.1092 274.6835 294.7832 209.2773 -1.5774 273.1795 274.7569 294.9188 210.0260 -1.5798 273.2458 274.8256 295.0317 210.8425 -1.5818 273.3330 274.9147 295.1608 211.6645 -1.5838 273.4267 275.0105 295.2760 212.4565 -1.5852 273.5006 275.0858 295.3889 213.2478 -1.5876 273.5714 275.1590 295.4814 214.0988 -1.5921 273.6554 275.2475 295.6397 214.8598 -1.5931 273.7295 275.3227 295.7420 215.6810 -1.5937 273.8057 275.3994 295.8679 216.4725 -1.5959 273.8884 275.4843 295.9967 217.2638 -1.6000 273.9589 275.5589 296.1385 218.0853 -1.6022 274.0226 275.6248 296.2772 218.8765 -1.6041 274.1001 275.7042 296.4181 219.6973 -1.6061 274.1974 275.8035 296.5505 220.4665 -1.6123 274.2608 275.8730 296.6559 221.2950 -1.6119 274.3416 275.9535 296.8033 222.0858 -1.6139 274.4210 276.0349 296.9349 222.9070 -1.6172 274.5166 276.1338 297.0698 223.6680 -1.6215 274.5803 276.2018 297.1883 224.5198 -1.6233 274.6812 276.3046 297.3261 225.3100 -1.6239 274.7662 276.3900 297.4639 226.1010 -1.6259 274.8449 276.4708 297.6174 226.9230 -1.6262 274.9145 276.5407 297.7423 227.6845 -1.6289 275.0129 276.6419 297.8653 228.5365 -1.6327 275.0938 276.7265 298.0254 229.3268 -1.6366 275.1618 276.7984 298.1582 230.1185 -1.6400 275.2359 276.8759 298.2873 230.9075 -1.6418 275.3258 276.9677 298.4102 231.7490 -1.6426 275.4064 277.0490 298.5640 232.5110 -1.6472 275.5000 277.1472 298.7102 233.3625 -1.6480 275.5820 277.2300 298.8609 234.1235 -1.6500 275.6557 277.3057 298.9933 234.9455 -1.6522 275.7535 277.4057 299.1227 235.7675 -1.6538 275.8351 277.4889 299.2607 236.5273 -1.6577 275.9145 277.5722 299.3835 237.3785 -1.6627 275.9894 277.6521 299.5291 238.1388 -1.6631 276.0967 277.7598 299.6539 238.9605 -1.6640 276.1861 277.8501 299.7834 239.7825 -1.6670 276.2551 277.9221 299.9272 240.5435 -1.6696 276.3275 277.9972 300.0700 241.3478 -1.6716 276.4234 278.0950 300.1916 242.2003 -1.6762 276.4871 278.1633 300.3591 242.9625 -1.6806 276.5923 278.2728 300.4833 243.7843 -1.6815 276.7081 278.3896 300.6310 244.5765 -1.6847 276.7708 278.4555 300.7349 245.3668 -1.6861 276.8739 278.5599 300.8664 246.2190 -1.6874 276.9573 278.6448 301.0387 246.9800 -1.6892 277.0318 278.7210 301.1586 247.8018 -1.6931 277.1156 278.8087 301.2998 248.5940 -1.6930 277.2116 278.9047 301.4233 249.3848 -1.6952 277.3122 279.0074 301.5496 250.2390 -1.6994 277.3899 279.0893 301.6895 250.9960 -1.7022 277.4698 279.1720 301.8166 251.8020 -1.7060 277.5640 279.2700 301.9515 252.6233 -1.7076 277.6488 279.3564 302.0924 253.4148 -1.7102 277.7360 279.4462 302.2156 254.2058 -1.7129 277.8194 279.5324 302.3492 255.0573 -1.7135 277.9305 279.6440 302.4923 255.8178 -1.7163 278.0060 279.7223 302.6251 256.6390 -1.7204 278.1172 279.8376 302.7503 257.4295 -1.7229 278.2118 279.9347 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