DTA measure 2240205dz1g1.dat Test Date: 202425:1625 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1649.09 s Mass = 1.000 mg data_number = 1021 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.2734 -5.0857 409.9011 414.9868 420.8267 3.8674 -5.0619 410.0942 415.1561 420.3648 5.5943 -5.0378 410.2918 415.3295 419.9091 7.2895 -5.0139 410.4827 415.4966 419.5168 8.8986 -4.9903 410.6668 415.6571 419.1912 10.4946 -4.9668 410.8210 415.7878 418.8875 12.0949 -4.9490 410.9652 415.9141 418.6273 13.6940 -4.9260 411.1313 416.0573 418.3891 15.3205 -4.9073 411.2977 416.2051 418.1763 16.9169 -4.8917 411.4362 416.3279 418.0096 18.5289 -4.8726 411.5937 416.4664 417.8591 20.1268 -4.8550 411.7209 416.5759 417.7215 21.7240 -4.8411 411.8571 416.6981 417.5980 23.3505 -4.8245 411.9943 416.8187 417.5084 24.9476 -4.8093 412.1250 416.9343 417.4496 26.5598 -4.7958 412.2232 417.0190 417.3504 28.1546 -4.7855 412.3453 417.1308 417.2789 29.7655 -4.7726 412.4733 417.2459 417.1957 31.3763 -4.7594 412.5921 417.3515 417.1286 32.9866 -4.7457 412.7129 417.4586 417.0818 34.5835 -4.7374 412.8072 417.5446 416.9754 36.3123 -4.7237 412.9238 417.6475 416.8802 38.0088 -4.7153 413.0293 417.7446 416.7785 39.6059 -4.7085 413.1205 417.8290 416.6886 41.2163 -4.6960 413.2173 417.9133 416.5939 42.8115 -4.6882 413.3121 418.0003 416.4839 44.4226 -4.6764 413.4012 418.0776 416.3421 46.0505 -4.6653 413.4783 418.1436 416.1937 47.6478 -4.6544 413.5637 418.2182 416.0549 49.2446 -4.6435 413.6504 418.2940 415.9036 50.8546 -4.6327 413.7384 418.3710 415.7494 52.4516 -4.6232 413.8184 418.4416 415.5773 54.0785 -4.6143 413.8891 418.5034 415.4055 55.6744 -4.6026 413.9615 418.5640 415.2014 57.2701 -4.5932 414.0269 418.6202 415.0181 58.8813 -4.5825 414.0936 418.6761 414.8195 60.4769 -4.5708 414.1510 418.7219 414.6280 62.0890 -4.5600 414.2045 418.7644 414.4300 63.7025 -4.5514 414.2478 418.7992 414.2170 65.3008 -4.5409 414.3039 418.8449 413.9949 66.8976 -4.5295 414.3581 418.8876 413.8088 68.4946 -4.5184 414.4165 418.9350 413.5883 70.1220 -4.5083 414.4730 418.9812 413.3922 71.7328 -4.4974 414.5024 418.9998 413.1802 73.3291 -4.4879 414.5220 419.0099 412.9688 74.9266 -4.4761 414.5715 419.0476 412.7611 76.5241 -4.4672 414.5973 419.0645 412.5640 78.1506 -4.4556 414.6151 419.0707 412.3617 79.7490 -4.4449 414.6596 419.1046 412.1454 81.3606 -4.4335 414.6849 419.1184 411.9474 82.9595 -4.4244 414.7007 419.1251 411.7626 84.5579 -4.4131 414.7336 419.1467 411.5739 86.1700 -4.4036 414.7329 419.1365 411.3654 87.7831 -4.3923 414.7469 419.1393 411.1821 89.3799 -4.3816 414.7520 419.1335 410.9695 90.9918 -4.3727 414.7677 419.1404 410.7555 92.5886 -4.3646 414.7723 419.1370 410.5609 94.2013 -4.3554 414.7552 419.1106 410.3674 95.8135 -4.3450 414.7863 419.1313 410.1585 97.4106 -4.3352 414.7649 419.1002 409.9446 99.0228 -4.3259 414.7420 419.0678 409.7376 100.6198 -4.3155 414.7653 419.0807 409.5421 102.2185 -4.3053 414.7497 419.0550 409.3278 103.8465 -4.2974 414.7401 419.0375 409.1322 105.4436 -4.2873 414.7028 418.9901 408.9264 107.0450 -4.2789 414.6926 418.9715 408.7041 108.6563 -4.2688 414.6736 418.9424 408.5025 110.2525 -4.2604 414.6594 418.9198 408.3265 111.8798 -4.2509 414.6311 418.8820 408.1184 113.4901 -4.2394 414.6016 418.8410 407.9278 115.0876 -4.2324 414.5903 418.8227 407.7453 116.6839 -4.2227 414.5701 418.7928 407.5368 118.3088 -4.2106 414.5229 418.7336 407.3295 119.9046 -4.2048 414.4908 418.6956 407.1544 121.5160 -4.1934 414.4495 418.6429 406.9678 123.1116 -4.1859 414.4123 418.5981 406.7772 124.7096 -4.1789 414.3716 418.5505 406.5997 126.3375 -4.1687 414.3284 418.4971 406.4171 127.9479 -4.1611 414.2830 418.4441 406.2370 129.5451 -4.1545 414.2348 418.3894 406.0449 131.1428 -4.1491 414.1871 418.3362 405.8346 132.7410 -4.1408 414.1363 418.2771 405.6441 134.3528 -4.1310 414.0926 418.2236 405.4593 135.9638 -4.1244 414.0433 418.1677 405.2572 137.5605 -4.1153 413.9699 418.0852 405.0702 139.1726 -4.1097 413.9132 418.0229 404.8705 140.7699 -4.1049 413.8484 417.9533 404.6718 142.3663 -4.0975 413.8054 417.9030 404.4750 143.9924 -4.0886 413.7268 417.8154 404.2794 145.5873 -4.0809 413.6584 417.7393 404.0939 147.1860 -4.0737 413.6179 417.6916 403.8987 148.7844 -4.0649 413.5391 417.6040 403.7148 150.3968 -4.0593 413.4725 417.5318 403.5266 152.0100 -4.0529 413.4087 417.4616 403.3273 153.6056 -4.0428 413.3239 417.3667 403.1166 155.2169 -4.0336 413.2758 417.3094 402.9283 156.8126 -4.0257 413.1847 417.2104 402.7261 158.4259 -4.0191 413.1120 417.1310 402.5231 160.0275 -4.0112 413.0265 417.0377 402.3094 161.6405 -4.0056 412.9502 416.9558 402.1089 163.2395 -3.9993 412.8693 416.8686 401.9074 164.8528 -3.9916 412.7873 416.7789 401.6897 166.4500 -3.9840 412.6999 416.6840 401.4873 168.0610 -3.9751 412.6118 416.5868 401.2820 169.6720 -3.9683 412.5258 416.4941 401.0737 171.2698 -3.9630 412.4365 416.3994 400.8461 172.8680 -3.9547 412.3435 416.2982 400.6163 174.4808 -3.9499 412.2481 416.1980 400.4337 176.0930 -3.9416 412.1666 416.1082 400.2442 177.7041 -3.9345 412.0611 415.9956 400.0384 179.2961 -3.9283 411.9740 415.9022 399.8270 180.9109 -3.9197 411.8618 415.7815 399.6274 182.5219 -3.9145 411.7675 415.6820 399.4327 184.1205 -3.9061 411.6688 415.5749 399.2339 185.7326 -3.8967 411.5691 415.4658 399.0251 187.3435 -3.8889 411.4664 415.3553 398.8320 188.9408 -3.8816 411.3638 415.2454 398.6469 190.5515 -3.8738 411.2599 415.1337 398.4584 192.1479 -3.8697 411.1654 415.0351 398.2802 193.7745 -3.8595 411.0438 414.9033 398.0757 195.3714 -3.8549 410.9332 414.7881 397.8792 196.9725 -3.8503 410.8272 414.6775 397.7165 198.5746 -3.8426 410.6986 414.5412 397.5133 200.1864 -3.8353 410.6033 414.4386 397.3079 201.7840 -3.8278 410.5024 414.3302 397.1102 203.3968 -3.8227 410.3825 414.2052 396.9239 205.0076 -3.8171 410.2648 414.0818 396.7053 206.6038 -3.8080 410.1484 413.9564 396.4943 208.1994 -3.8005 410.0366 413.8371 396.2879 209.8118 -3.7935 409.9040 413.6975 396.0968 211.4231 -3.7896 409.7847 413.5743 395.8957 213.0346 -3.7829 409.6680 413.4509 395.6873 214.6299 -3.7759 409.5511 413.3269 395.4880 216.2263 -3.7689 409.4364 413.2053 395.2875 217.8234 -3.7624 409.3096 413.0720 395.0707 219.4513 -3.7516 409.1952 412.9468 394.8780 221.0478 -3.7457 409.0765 412.8222 394.6645 222.6585 -3.7399 408.9420 412.6819 394.4696 224.2546 -3.7356 408.8033 412.5389 394.2601 225.8511 -3.7271 408.6902 412.4173 394.0596 227.4769 -3.7198 408.5527 412.2725 393.8555 229.0743 -3.7142 408.4447 412.1589 393.6432 230.6653 -3.7073 408.3033 412.0106 393.4579 232.2936 -3.7036 408.1711 411.8747 393.2648 233.8905 -3.6960 408.0478 411.7439 393.0776 235.4873 -3.6919 407.8940 411.5859 392.8776 237.0988 -3.6828 407.7725 411.4553 392.6614 238.7110 -3.6780 407.6336 411.3115 392.4669 240.3229 -3.6745 407.5076 411.1821 392.2622 241.9189 -3.6674 407.3668 411.0343 392.0593 243.5163 -3.6585 407.2200 410.8786 391.8554 245.1279 -3.6540 407.0930 410.7470 391.6528 246.7400 -3.6462 406.9321 410.5783 391.4619 248.3516 -3.6408 406.8082 410.4489 391.2332 249.9489 -3.6366 406.6806 410.3172 391.0450 251.5468 -3.6304 406.5325 410.1629 390.8348 253.1690 -3.6222 406.3866 410.0087 390.6406 254.7669 -3.6176 406.2527 409.8704 390.4175 256.3799 -3.6095 406.0989 409.7084 390.2096 257.9919 -3.6017 405.9541 409.5558 390.0170 259.6031 -3.5983 405.8227 409.4210 389.7977 261.2003 -3.5891 405.6864 409.2755 389.5897 262.7981 -3.5873 405.5309 409.1182 389.3791 264.4244 -3.5773 405.3792 408.9565 389.1810 266.0203 -3.5757 405.2265 408.8022 388.9697 267.6308 -3.5694 405.0864 408.6558 388.7509 269.2261 -3.5621 404.9306 408.4927 388.5561 270.8369 -3.5596 404.7936 408.3532 388.3593 272.4463 -3.5501 404.6439 408.1941 388.1648 274.0591 -3.5440 404.4843 408.0283 387.9604 275.6710 -3.5418 404.3343 407.8761 387.7714 277.2660 -3.5346 404.1753 407.7099 387.5561 278.8759 -3.5276 404.0254 407.5530 387.3449 280.4714 -3.5223 403.8801 407.4024 387.1583 282.0820 -3.5177 403.7304 407.2482 386.9867 283.6946 -3.5115 403.5778 407.0893 386.7865 285.2918 -3.5044 403.4282 406.9327 386.6057 286.9030 -3.4994 403.2684 406.7678 386.3924 288.4980 -3.4941 403.1182 406.6123 386.2105 290.1099 -3.4910 402.9542 406.4452 386.0127 291.7069 -3.4842 402.8014 406.2856 385.8256 293.3073 -3.4818 402.6339 406.1157 385.6321 294.9194 -3.4754 402.4962 405.9715 385.4208 296.5309 -3.4702 402.3138 405.7840 385.2170 298.1279 -3.4660 402.1635 405.6295 385.0176 299.7259 -3.4592 402.0144 405.4736 384.8038 301.3386 -3.4551 401.8498 405.3049 384.6021 302.9508 -3.4462 401.6719 405.1180 384.3929 304.5470 -3.4414 401.5360 404.9774 384.1970 306.1581 -3.4359 401.3822 404.8182 383.9786 307.7519 -3.4317 401.2136 404.6453 383.7764 309.3481 -3.4272 401.0628 404.4900 383.5748 310.9759 -3.4225 400.8837 404.3063 383.3663 312.5641 -3.4173 400.7208 404.1381 383.1710 314.1820 -3.4103 400.5590 403.9693 382.9772 315.7931 -3.4074 400.4023 403.8097 382.7572 317.3899 -3.3990 400.2293 403.6284 382.5653 318.9865 -3.3939 400.0648 403.4588 382.3542 320.5984 -3.3886 399.9058 403.2944 382.1632 322.2240 -3.3840 399.7426 403.1266 381.9571 323.8209 -3.3774 399.5756 402.9530 381.7621 325.4189 -3.3706 399.4116 402.7823 381.5707 327.0304 -3.3674 399.2443 402.6117 381.3555 328.6288 -3.3659 399.0704 402.4363 381.1534 330.2559 -3.3587 398.9117 402.2704 380.9600 331.8523 -3.3511 398.7298 402.0809 380.7550 333.4511 -3.3462 398.5787 401.9249 380.5588 335.0713 -3.3403 398.4002 401.7406 380.3475 336.6683 -3.3355 398.2241 401.5596 380.1395 338.2651 -3.3300 398.0667 401.3968 379.9372 339.8935 -3.3280 397.9058 401.2338 379.7073 341.5064 -3.3219 397.7365 401.0584 379.5026 343.1046 -3.3130 397.5650 400.8780 379.3040 344.7034 -3.3113 397.3985 400.7098 379.0756 346.3145 -3.3081 397.2361 400.5442 378.8580 347.9251 -3.3012 397.0616 400.3628 378.6461 349.5378 -3.2961 396.8909 400.1871 378.4484 351.1358 -3.2925 396.7056 399.9981 378.2330 352.7325 -3.2869 396.5395 399.8264 377.9975 354.3496 -3.2807 396.3656 399.6463 377.7781 355.9468 -3.2746 396.1953 399.4699 377.5539 357.5434 -3.2707 396.0252 399.2958 377.3667 359.1695 -3.2651 395.8576 399.1226 377.1490 360.7675 -3.2602 395.6670 398.9272 376.9344 362.3654 -3.2528 395.4931 398.7459 376.7309 363.9518 -3.2492 395.3162 398.5654 376.5250 365.5795 -3.2423 395.1571 398.3994 376.3120 367.1776 -3.2366 394.9834 398.2199 376.1114 368.7896 -3.2311 394.7841 398.0152 375.8912 370.3856 -3.2240 394.6116 397.8357 375.6914 371.9836 -3.2195 394.4453 397.6648 375.4875 373.6006 -3.2156 394.2653 397.4809 375.2854 375.1986 -3.2073 394.0891 397.2964 375.0682 376.7951 -3.1989 393.9133 397.1122 374.8924 378.4223 -3.1942 393.7331 396.9273 374.6771 380.0189 -3.1888 393.5697 396.7585 374.4690 381.6151 -3.1838 393.3917 396.5755 374.2971 383.2274 -3.1795 393.2125 396.3920 374.0802 384.8354 -3.1718 393.0311 396.2029 373.8844 386.4423 -3.1664 392.8689 396.0353 373.6932 388.0395 -3.1590 392.6809 395.8399 373.4883 389.6373 -3.1530 392.5208 395.6738 373.2901 391.2491 -3.1491 392.3272 395.4763 373.1123 392.8750 -3.1436 392.1297 395.2732 372.9014 394.4649 -3.1371 391.9572 395.0942 372.7006 396.0701 -3.1327 391.7693 394.9020 372.5043 397.6871 -3.1281 391.5900 394.7180 372.3046 399.2829 -3.1229 391.4316 394.5545 372.1081 400.8944 -3.1193 391.2394 394.3587 371.9351 402.4906 -3.1136 391.0576 394.1712 371.7492 404.0963 -3.1130 390.8667 393.9797 371.5702 405.7156 -3.1086 390.6983 393.8069 371.3830 407.3135 -3.1058 390.5209 393.6267 371.1685 408.9116 -3.1008 390.3473 393.4481 370.9752 410.5236 -3.0939 390.1519 393.2458 370.7871 412.1343 -3.0918 389.9631 393.0549 370.5716 413.7315 -3.0890 389.8077 392.8968 370.3671 415.3274 -3.0833 389.6107 392.6940 370.1580 416.9434 -3.0779 389.4481 392.5260 369.9494 418.5541 -3.0742 389.2518 392.3260 369.7515 420.1505 -3.0708 389.0796 392.1504 369.5343 421.7474 -3.0672 388.8915 391.9586 369.3189 423.3600 -3.0639 388.7039 391.7678 369.1178 424.9881 -3.0579 388.5152 391.5731 368.9137 426.5739 -3.0529 388.3405 391.3933 368.6964 428.1704 -3.0466 388.1657 391.2122 368.4967 429.7975 -3.0425 387.9744 391.0170 368.2750 431.3941 -3.0353 387.7983 390.8336 368.0659 433.0049 -3.0287 387.6154 390.6441 367.8683 434.6000 -3.0284 387.4417 390.4701 367.6637 436.2223 -3.0193 387.2499 390.2693 367.4608 437.8183 -3.0155 387.0558 390.0712 367.2592 439.4158 -3.0116 386.8624 389.8740 367.0560 441.0133 -3.0093 386.6903 389.6996 366.8438 442.6226 -3.0048 386.4994 389.5042 366.6329 444.2499 -3.0018 386.3032 389.3051 366.4334 445.8534 -2.9983 386.1320 389.1304 366.2259 447.4369 -2.9916 385.9480 388.9396 366.0318 449.0633 -2.9842 385.7712 388.7554 365.8420 450.6585 -2.9819 385.5872 388.5691 365.6354 452.2698 -2.9789 385.3950 388.3739 365.4218 453.8648 -2.9714 385.2174 388.1889 365.2247 455.4970 -2.9675 385.0274 387.9950 365.0316 457.0813 -2.9630 384.8216 387.7846 364.8264 458.6889 -2.9550 384.6404 387.5954 364.6276 460.2853 -2.9532 384.4676 387.4208 364.4349 461.9118 -2.9487 384.2785 387.2272 364.2322 463.5214 -2.9423 384.0981 387.0404 364.0227 465.1176 -2.9388 383.8939 386.8328 363.8184 466.7161 -2.9313 383.7030 386.6342 363.6027 468.3273 -2.9273 383.5295 386.4568 363.3944 469.9396 -2.9233 383.3259 386.2492 363.1922 471.5513 -2.9200 383.1536 386.0736 362.9841 473.1484 -2.9133 382.9717 385.8850 362.7703 474.7463 -2.9065 382.7772 385.6837 362.5525 476.3808 -2.9041 382.5779 385.4820 362.3542 477.9719 -2.8987 382.4116 385.3103 362.1369 479.5701 -2.8944 382.2197 385.1141 361.9294 481.1956 -2.8884 382.0204 384.9088 361.7011 482.7913 -2.8834 381.8355 384.7189 361.5057 484.3870 -2.8786 381.6459 384.5245 361.2940 485.9969 -2.8712 381.4540 384.3252 361.0790 487.6098 -2.8659 381.2706 384.1364 360.8842 489.2209 -2.8619 381.0783 383.9402 360.6604 490.8186 -2.8590 380.8849 383.7439 360.4584 492.4291 -2.8498 380.6920 383.5418 360.2380 494.0243 -2.8470 380.5171 383.3641 360.0413 495.6354 -2.8442 380.3254 383.1697 359.8270 497.2463 -2.8393 380.1461 382.9853 359.6180 498.8605 -2.8318 379.9456 382.7774 359.4243 500.4575 -2.8278 379.7684 382.5962 359.2187 502.0523 -2.8231 379.5744 382.3976 359.0069 503.6630 -2.8195 379.3817 382.2012 358.8035 505.2749 -2.8148 379.1868 382.0016 358.6101 506.8909 -2.8065 379.0016 381.8081 358.4253 508.4923 -2.8019 378.7957 381.5976 358.2127 510.0885 -2.7994 378.6146 381.4140 358.0199 511.6995 -2.7920 378.4266 381.2186 357.8136 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