DTA measure 2240326-1_Pb3.dat Date: 2024326:1327 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.48 s Mass = 1410.000 mg data_number = 1024 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5200 -4.4198 411.8229 416.2427 420.2895 4.1368 -4.4181 411.9415 416.3596 420.3152 5.7348 -4.4197 412.0527 416.4724 420.2972 7.3348 -4.4160 412.1837 416.5997 420.2812 8.9546 -4.4135 412.2832 416.6967 420.2407 10.5506 -4.4126 412.4031 416.8157 420.1680 12.1641 -4.4083 412.5307 416.9390 420.1051 13.7623 -4.4072 412.6189 417.0261 419.9915 15.3889 -4.3991 412.7295 417.1286 419.8654 16.9844 -4.3966 412.8247 417.2213 419.7266 18.5779 -4.3944 412.9221 417.3165 419.5687 20.2044 -4.3917 413.0283 417.4200 419.3827 21.8024 -4.3823 413.1298 417.5121 419.1943 23.4001 -4.3669 413.2294 417.5963 418.9887 25.0126 -4.3508 413.3164 417.6671 418.7680 26.6124 -4.3420 413.4079 417.7499 418.5659 28.2228 -4.3375 413.4987 417.8362 418.3271 29.8348 -4.3305 413.5852 417.9157 418.0714 31.4468 -4.3230 413.6727 417.9957 417.8203 33.0451 -4.3143 413.7580 418.0723 417.5750 34.6414 -4.3162 413.8575 418.1737 417.3308 36.2541 -4.3130 413.9223 418.2353 417.0789 37.8669 -4.3069 413.9870 418.2939 416.8208 39.4704 -4.2983 414.0618 418.3601 416.5634 41.0705 -4.2851 414.1334 418.4185 416.3226 42.6844 -4.2762 414.1947 418.4709 416.0561 44.2799 -4.2669 414.2535 418.5204 415.8217 45.8759 -4.2556 414.3164 418.5721 415.5817 47.5144 -4.2382 414.3637 418.6018 415.3388 49.0945 -4.2192 414.4213 418.6406 415.1084 50.7065 -4.2096 414.4676 418.6772 414.8918 52.3196 -4.1983 414.5265 418.7248 414.6741 53.9304 -4.1891 414.5543 418.7435 414.4778 55.5275 -4.1795 414.6118 418.7913 414.2671 57.1249 -4.1697 414.6505 418.8202 414.0540 58.7444 -4.1607 414.6827 418.8434 413.8714 60.3415 -4.1490 414.7249 418.8739 413.6673 61.9395 -4.1402 414.7738 418.9140 413.4883 63.5381 -4.1309 414.7889 418.9198 413.3140 65.1496 -4.1223 414.8216 418.9440 413.1156 66.7620 -4.1226 414.8393 418.9619 412.9551 68.3736 -4.1166 414.8545 418.9711 412.7679 69.9678 -4.1084 414.8900 418.9985 412.6113 71.5795 -4.1010 414.8997 419.0007 412.4485 73.1770 -4.0933 414.9222 419.0155 412.2928 74.7900 -4.0862 414.9369 419.0232 412.1258 76.3864 -4.0798 414.9476 419.0274 411.9608 78.0038 -4.0731 414.9675 419.0407 411.7928 79.5996 -4.0691 414.9623 419.0314 411.6152 81.1980 -4.0612 414.9670 419.0282 411.4455 82.8101 -4.0531 414.9802 419.0333 411.2974 84.4076 -4.0444 414.9833 419.0277 411.1147 86.0205 -4.0372 414.9745 419.0117 410.9379 87.6190 -4.0294 414.9721 419.0015 410.7686 89.4019 -4.0208 414.9642 418.9850 410.5782 91.0230 -4.0141 414.9627 418.9767 410.3917 92.6354 -4.0060 414.9619 418.9678 410.2042 94.2453 -3.9899 414.9435 418.9333 410.0239 95.8569 -3.9783 414.9308 418.9091 409.8188 97.4549 -3.9760 414.9164 418.8925 409.6535 99.0526 -3.9657 414.8919 418.8576 409.4636 100.6494 -3.9612 414.8831 418.8444 409.2669 102.2763 -3.9564 414.8571 418.8135 409.0750 103.8708 -3.9472 414.8349 418.7821 408.8941 105.4828 -3.9399 414.8147 418.7547 408.7182 107.0813 -3.9327 414.7925 418.7252 408.5269 108.6785 -3.9217 414.7750 418.6967 408.3195 110.3060 -3.9156 414.7397 418.6553 408.1196 111.9045 -3.9120 414.7032 418.6152 407.9216 113.5031 -3.9029 414.6714 418.5743 407.7251 115.1151 -3.8938 414.6317 418.5255 407.5137 116.7123 -3.8874 414.5926 418.4800 407.3162 118.3101 -3.8770 414.5533 418.4303 407.1220 120.1073 -3.8657 414.5068 418.3725 406.8943 121.7279 -3.8584 414.4666 418.3249 406.6972 123.3268 -3.8536 414.4159 418.2695 406.4966 124.9399 -3.8449 414.3879 418.2328 406.2848 126.5519 -3.8394 414.3380 418.1774 406.0840 128.1658 -3.8312 414.2823 418.1134 405.8853 129.7623 -3.8227 414.2300 418.0527 405.6754 131.3585 -3.8144 414.1733 417.9877 405.4880 132.9725 -3.8072 414.1164 417.9236 405.2868 134.5859 -3.8016 414.0662 417.8678 405.0935 136.1834 -3.7966 414.0144 417.8110 404.8951 137.7958 -3.7877 413.9449 417.7326 404.6918 139.3936 -3.7771 413.8841 417.6612 404.4912 140.9906 -3.7572 413.8179 417.5751 404.2959 142.6189 -3.7472 413.7546 417.5018 404.1185 144.2184 -3.7398 413.6861 417.4259 403.9263 145.8170 -3.7304 413.6276 417.3580 403.7350 147.4291 -3.7233 413.5683 417.2916 403.5292 149.0276 -3.7168 413.4840 417.2007 403.3428 150.6251 -3.7120 413.4221 417.1341 403.1265 152.2388 -3.7040 413.3447 417.0487 402.9293 153.8565 -3.6978 413.2796 416.9774 402.7159 155.4543 -3.6908 413.1889 416.8797 402.5140 157.0516 -3.6860 413.1091 416.7951 402.3291 158.6526 -3.6808 413.0224 416.7033 402.1235 160.2811 -3.6726 412.9569 416.6295 401.9185 161.8773 -3.6580 412.8619 416.5200 401.7295 163.4886 -3.6548 412.7648 416.4196 401.5228 165.0868 -3.6505 412.6989 416.3494 401.3199 166.6835 -3.6438 412.6138 416.2575 401.1253 168.2964 -3.6354 412.5224 416.1577 400.9414 169.9305 -3.6291 412.4376 416.0667 400.7240 171.7130 -3.6193 412.3346 415.9539 400.5226 173.3111 -3.6130 412.2308 415.8438 400.3135 174.9090 -3.6067 412.1467 415.7534 400.1166 176.5368 -3.6024 412.0596 415.6620 399.9182 178.1349 -3.5950 411.9634 415.5584 399.7077 179.7474 -3.5861 411.8766 415.4627 399.5095 181.3439 -3.5813 411.7601 415.3414 399.3115 182.9411 -3.5750 411.6569 415.2319 399.1120 184.5680 -3.5668 411.5607 415.1275 398.8824 186.1635 -3.5628 411.4530 415.0158 398.6895 187.7625 -3.5572 411.3548 414.9121 398.4992 189.3745 -3.5489 411.2534 414.8022 398.2957 190.9705 -3.5422 411.1483 414.6906 398.0888 192.5985 -3.5377 411.0410 414.5787 397.8735 194.1974 -3.5325 410.9399 414.4724 397.6615 195.8085 -3.5349 410.8216 414.3565 397.4635 197.4044 -3.5292 410.7173 414.2464 397.2577 199.0026 -3.5233 410.6178 414.1411 397.0730 200.6134 -3.5100 410.4938 414.0039 396.8663 202.2246 -3.4962 410.3744 413.8706 396.6717 203.8366 -3.4900 410.2750 413.7650 396.4734 205.4338 -3.4861 410.1595 413.6456 396.2708 207.0316 -3.4803 410.0514 413.5317 396.0849 208.6301 -3.4721 409.9329 413.4050 395.8846 210.2581 -3.4634 409.7913 413.2547 395.6978 211.8555 -3.4566 409.6788 413.1355 395.5002 213.4524 -3.4511 409.5493 413.0004 395.3103 215.0505 -3.4457 409.4412 412.8869 395.1193 216.6493 -3.4394 409.3185 412.7579 394.9384 218.2776 -3.4335 409.2007 412.6343 394.7452 219.8770 -3.4260 409.0797 412.5057 394.5617 221.4744 -3.4219 408.9524 412.3742 394.3521 223.0868 -3.4164 408.8237 412.2401 394.1608 224.6820 -3.4081 408.7021 412.1101 393.9750 226.2794 -3.4019 408.5794 411.9813 393.7614 227.9080 -3.3975 408.4468 411.8443 393.5605 229.5055 -3.3915 408.3173 411.7088 393.3629 231.1020 -3.3843 408.1964 411.5806 393.1608 232.6989 -3.3798 408.0521 411.4319 392.9495 234.3105 -3.3729 407.9240 411.2968 392.7498 235.9219 -3.3658 407.8138 411.1796 392.5570 237.5341 -3.3577 407.6737 411.0314 392.3485 239.1313 -3.3513 407.5233 410.8747 392.1469 240.7283 -3.3455 407.3891 410.7347 391.9545 242.3263 -3.3354 407.2653 410.6007 391.7715 243.9539 -3.3328 407.1330 410.4657 391.5707 245.5518 -3.3286 406.9956 410.3242 391.3626 247.1494 -3.3214 406.8635 410.1849 391.1704 248.7619 -3.3140 406.7199 410.0339 390.9703 250.3594 -3.3112 406.5786 409.8898 390.7889 251.9586 -3.3045 406.4467 409.7513 390.5859 253.5809 -3.2974 406.2932 409.5906 390.3915 255.1791 -3.2941 406.1547 409.4488 390.1870 256.7919 -3.2891 406.0151 409.3042 389.9978 258.3905 -3.2842 405.8745 409.1588 389.8064 259.9895 -3.2777 405.7236 409.0014 389.5881 261.6030 -3.2707 405.5890 408.8597 389.3691 263.2159 -3.2656 405.4501 408.7157 389.1590 264.8145 -3.2586 405.3053 408.5639 388.9544 266.4124 -3.2542 405.1646 408.4189 388.7613 268.0250 -3.2488 405.0125 408.2613 388.5519 269.6219 -3.2426 404.8654 408.1080 388.3579 271.2489 -3.2389 404.7041 407.9429 388.1346 272.8265 -3.2326 404.5753 407.8079 387.9395 274.4569 -3.2264 404.4354 407.6618 387.7173 276.0546 -3.2217 404.2645 407.4863 387.5098 277.6526 -3.2159 404.1312 407.3470 387.3078 279.2645 -3.2106 403.9618 407.1724 387.0922 280.8893 -3.2052 403.8154 407.0207 386.8892 282.4876 -3.2016 403.6740 406.8756 386.6989 284.0845 -3.1945 403.5153 406.7098 386.4937 285.6960 -3.1881 403.3519 406.5400 386.2901 287.2930 -3.1845 403.2113 406.3958 386.0947 288.9210 -3.1802 403.0638 406.2440 385.8924 290.5180 -3.1749 402.9085 406.0834 385.6857 292.1165 -3.1685 402.7655 405.9340 385.4870 293.7295 -3.1643 402.6080 405.7723 385.2882 295.3315 -3.1591 402.4446 405.6037 385.0866 296.9465 -3.1532 402.2930 405.4462 384.8847 298.5438 -3.1478 402.1279 405.2758 384.6808 300.1560 -3.1437 401.9562 405.0999 384.4968 301.7548 -3.1404 401.8085 404.9489 384.3113 303.3533 -3.1353 401.6665 404.8018 384.1067 304.9804 -3.1301 401.4999 404.6300 383.9102 306.5788 -3.1241 401.3327 404.4568 383.7087 308.1775 -3.1187 401.1797 404.2984 383.4990 309.7903 -3.1128 401.0337 404.1465 383.2963 311.3873 -3.1076 400.8640 403.9716 383.1005 313.0001 -3.1015 400.7050 403.8065 382.8786 314.6128 -3.0989 400.5386 403.6375 382.6710 316.2106 -3.0942 400.3762 403.4704 382.4497 317.8084 -3.0889 400.2076 403.2965 382.2540 319.4214 -3.0839 400.0562 403.1401 382.0379 321.0190 -3.0800 399.8956 402.9756 381.8398 322.6318 -3.0768 399.7332 402.8100 381.6270 324.2348 -3.0682 399.5642 402.6324 381.4177 325.8380 -3.0610 399.3986 402.4597 381.2111 327.4509 -3.0584 399.2431 402.3016 381.0048 329.0489 -3.0522 399.0727 402.1249 380.8023 330.6464 -3.0463 398.8935 401.9398 380.5801 332.2740 -3.0415 398.7291 401.7706 380.3785 333.8706 -3.0342 398.5611 401.5953 380.1744 335.4806 -3.0293 398.3886 401.4179 379.9625 337.0771 -3.0252 398.2288 401.2540 379.7725 338.6751 -3.0204 398.0559 401.0763 379.5580 340.3035 -3.0160 397.9018 400.9178 379.3750 341.9016 -3.0114 397.7286 400.7400 379.1577 343.4994 -3.0011 397.5562 400.5574 378.9606 345.1030 -2.9978 397.3821 400.3799 378.7581 346.7074 -2.9920 397.2155 400.2075 378.5519 348.3049 -2.9881 397.0618 400.0499 378.3619 349.9158 -2.9814 396.8780 399.8595 378.1658 351.5274 -2.9762 396.7028 399.6790 377.9671 353.1253 -2.9725 396.5415 399.5140 377.7629 354.7035 -2.9691 396.3693 399.3384 377.5743 356.3439 -2.9630 396.1872 399.1502 377.3760 357.9423 -2.9598 396.0247 398.9845 377.1840 359.5405 -2.9542 395.8478 398.8020 377.0026 361.1385 -2.9485 395.6714 398.6199 376.8046 362.7511 -2.9429 395.5030 398.4459 376.6102 364.3479 -2.9394 395.3357 398.2751 376.3984 365.9588 -2.9341 395.1562 398.0903 376.2137 367.5561 -2.9301 394.9784 397.9085 376.0058 369.1676 -2.9262 394.8166 397.7428 375.8087 370.7804 -2.9197 394.6149 397.5347 375.5902 372.3785 -2.9174 394.4643 397.3817 375.4102 373.9766 -2.9116 394.2866 397.1982 375.2053 375.5673 -2.9052 394.1058 397.0110 375.0069 377.2034 -2.8998 393.9342 396.8340 374.7877 378.8018 -2.8967 393.7572 396.6539 374.5880 380.3989 -2.8929 393.5758 396.4687 374.3931 381.9966 -2.8868 393.4018 396.2886 374.1978 383.6105 -2.8813 393.2243 396.1056 373.9977 385.2263 -2.8751 393.0419 395.9170 373.7823 386.8193 -2.8711 392.8745 395.7457 373.5816 388.4169 -2.8669 392.6949 395.5618 373.3867 390.0439 -2.8627 392.5121 395.3748 373.1930 391.6411 -2.8588 392.3567 395.2155 373.0065 393.2388 -2.8535 392.1667 395.0202 372.8027 394.8515 -2.8484 391.9835 394.8319 372.6062 396.4561 -2.8461 391.8162 394.6623 372.4057 398.0635 -2.8398 391.6389 394.4787 372.2114 399.6603 -2.8344 391.4576 394.2920 371.9923 401.2724 -2.8288 391.2756 394.1043 371.8041 402.8696 -2.8239 391.0991 393.9230 371.5869 404.4980 -2.8165 390.9114 393.7278 371.3948 406.0876 -2.8146 390.7296 393.5442 371.1916 407.6933 -2.8099 390.5496 393.3595 370.9834 409.3068 -2.8045 390.3846 393.1891 370.7753 410.9204 -2.7964 390.1977 392.9940 370.5618 412.5175 -2.7919 390.0162 392.8081 370.3443 414.1135 -2.7887 389.8218 392.6105 370.1304 415.7239 -2.7858 389.6560 392.4418 369.9201 417.3255 -2.7821 389.4778 392.2599 369.7127 418.9389 -2.7756 389.2953 392.0709 369.4966 420.5368 -2.7684 389.1168 391.8852 369.3039 422.1496 -2.7627 388.9184 391.6811 369.0883 423.7619 -2.7581 388.7486 391.5067 368.8774 425.3588 -2.7540 388.5636 391.3176 368.6630 426.9549 -2.7499 388.3772 391.1271 368.4456 428.5729 -2.7434 388.1896 390.9329 368.2315 430.1858 -2.7393 388.0098 390.7491 368.0158 431.7813 -2.7345 387.8311 390.5656 367.8009 433.3923 -2.7289 387.6506 390.3794 367.5878 434.9881 -2.7261 387.4670 390.1932 367.3855 436.6130 -2.7218 387.2762 389.9980 367.1817 438.2003 -2.7166 387.0992 389.8158 366.9849 439.8126 -2.7091 386.9147 389.6238 366.7609 441.4250 -2.7046 386.7339 389.4385 366.5569 443.0369 -2.6992 386.5468 389.2461 366.3559 444.6316 -2.6920 386.3629 389.0548 366.1538 446.2430 -2.6918 386.1644 388.8561 365.9685 447.8458 -2.6865 385.9822 388.6687 365.7530 449.4588 -2.6833 385.8104 388.4938 365.5403 451.0560 -2.6764 385.6098 388.2862 365.3404 452.6535 -2.6731 385.4147 388.0877 365.1404 454.2803 -2.6675 385.2359 387.9034 364.9362 455.8779 -2.6642 385.0485 387.7128 364.7440 457.4810 -2.6602 384.8648 387.5250 364.5332 459.1031 -2.6515 384.6727 387.3242 364.3368 460.6995 -2.6385 384.4872 387.1258 364.1445 462.2975 -2.6318 384.3081 386.9400 363.9488 463.8999 -2.6329 384.1100 386.7428 363.7625 465.5143 -2.6336 383.9299 386.5635 363.5565 467.1289 -2.6336 383.7428 386.3763 363.3663 468.7218 -2.6266 383.5415 386.1680 363.1700 470.3340 -2.6209 383.3676 385.9886 362.9837 471.9443 -2.6181 383.1728 385.7909 362.7871 473.5559 -2.6164 383.0003 385.6167 362.5818 475.1516 -2.6091 382.8006 385.4097 362.3665 476.7636 -2.6040 382.6032 385.2072 362.1680 478.3716 -2.5994 382.4439 385.0433 361.9669 479.9786 -2.5903 382.2482 384.8385 361.7652 481.5753 -2.5781 382.0564 384.6345 361.5518 483.1884 -2.5811 381.8609 384.4420 361.3331 484.7856 -2.5795 381.6746 384.2542 361.1069 486.4119 -2.5752 381.4894 384.0647 360.8990 488.0033 -2.5669 381.3048 383.8717 360.6859 489.6090 -2.5632 381.1068 383.6700 360.4860 491.2354 -2.5604 380.9332 383.4936 360.2792 492.8313 -2.5561 380.7316 383.2877 360.0664 494.4275 -2.5510 380.5367 383.0877 359.8573 496.0405 -2.5487 380.3463 382.8950 359.6436 497.6494 -2.5428 380.1688 382.7116 359.4269 499.2559 -2.5364 379.9545 382.4910 359.2211 500.8531 -2.5352 379.7723 382.3075 359.0321 502.4650 -2.5303 379.5995 382.1298 358.8062 504.0763 -2.5273 379.4046 381.9319 358.6003 505.6891 -2.5241 379.2098 381.7340 358.3844 507.2853 -2.5200 379.0334 381.5535 358.1924 508.8829 -2.5173 378.8289 381.3462 357.9878 510.5001 -2.5129 378.6304 381.1433 357.7770 512.1126 -2.5027 378.4488 380.9515 357.5691 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