DTA measure 11Pb_1-ud4.dat Date: 2026827:172 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1722.85 s Mass = 100.000 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3600 -0.6479 205.3694 206.0173 196.7857 3.9604 -0.6498 205.3466 205.9963 196.8161 5.5654 -0.6492 205.3407 205.9899 196.8129 7.1906 -0.6467 205.3259 205.9727 196.8152 8.7954 -0.6476 205.3398 205.9874 196.8227 10.3950 -0.6503 205.3590 206.0092 196.8362 12.0049 -0.6522 205.3719 206.0241 196.8632 13.6055 -0.6524 205.3545 206.0069 196.8672 15.2000 -0.6519 205.3709 206.0229 196.9007 16.8150 -0.6505 205.3628 206.0133 196.9375 18.4351 -0.6526 205.3762 206.0288 196.9946 20.0399 -0.6552 205.3972 206.0524 197.0524 21.6298 -0.6543 205.3997 206.0540 197.0781 23.2299 -0.6547 205.3905 206.0452 197.1402 24.8551 -0.6600 205.3812 206.0412 197.2170 26.4599 -0.6632 205.3481 206.0113 197.3001 28.0595 -0.6662 205.3586 206.0248 197.3773 29.6695 -0.6679 205.3784 206.0464 197.4507 31.2751 -0.6658 205.4039 206.0697 197.5202 32.8799 -0.6677 205.4183 206.0860 197.6234 34.4846 -0.6658 205.4171 206.0830 197.7473 36.0843 -0.6655 205.4066 206.0721 197.8615 37.6951 -0.6642 205.4007 206.0649 197.9749 39.2999 -0.6679 205.4146 206.0825 198.0976 40.9046 -0.6693 205.4420 206.1113 198.2334 42.5248 -0.6709 205.4536 206.1246 198.3911 44.1298 -0.6745 205.4443 206.1188 198.5421 45.7353 -0.6760 205.4467 206.1227 198.6703 47.3349 -0.6760 205.4623 206.1383 198.8051 48.9396 -0.6749 205.4823 206.1572 198.9707 50.5445 -0.6782 205.4742 206.1524 199.1422 52.1501 -0.6791 205.4769 206.1560 199.2940 53.7651 -0.6806 205.4715 206.1521 199.4751 55.3750 -0.6810 205.4855 206.1665 199.6597 56.9746 -0.6822 205.4977 206.1799 199.8440 58.5798 -0.6828 205.5238 206.2066 199.9981 60.1851 -0.6842 205.5325 206.2166 200.1630 61.7899 -0.6863 205.5502 206.2365 200.3327 63.3793 -0.6869 205.5783 206.2651 200.4784 64.9994 -0.6886 205.5984 206.2869 200.6256 66.5995 -0.6939 205.6106 206.3044 200.8079 68.2099 -0.6957 205.6155 206.3112 200.9846 69.8146 -0.6991 205.6355 206.3346 201.1925 71.4143 -0.7024 205.6659 206.3682 201.3805 73.0241 -0.7016 205.6741 206.3757 201.5728 74.6289 -0.7047 205.6947 206.3993 201.7492 76.2345 -0.7078 205.6985 206.4063 201.9224 77.8240 -0.7072 205.6990 206.4061 202.0961 79.4441 -0.7084 205.7093 206.4177 202.2548 81.0489 -0.7061 205.7372 206.4432 202.4411 82.6486 -0.7109 205.7270 206.4378 202.6263 84.2543 -0.7139 205.7409 206.4548 202.8161 85.8641 -0.7161 205.7766 206.4927 203.0009 87.4535 -0.7163 205.8224 206.5386 203.1667 89.0583 -0.7190 205.8612 206.5802 203.3593 90.6630 -0.7208 205.8959 206.6167 203.5252 92.2784 -0.7209 205.9219 206.6428 203.7134 93.8838 -0.7240 205.9515 206.6755 203.9274 95.4885 -0.7230 205.9955 206.7185 204.1574 97.0933 -0.7273 206.0236 206.7508 204.3555 98.6980 -0.7274 206.0763 206.8037 204.5309 100.2983 -0.7296 206.1094 206.8390 204.7169 101.9034 -0.7303 206.1358 206.8661 204.9088 103.5286 -0.7323 206.1685 206.9008 205.1161 105.1283 -0.7322 206.2032 206.9354 205.3080 106.7279 -0.7345 206.2257 206.9602 205.4931 108.3385 -0.7399 206.2788 207.0187 205.6900 109.9435 -0.7434 206.3219 207.0654 205.8788 111.5483 -0.7442 206.3702 207.1144 206.0636 113.1530 -0.7450 206.4029 207.1479 206.2556 114.7741 -0.7499 206.4636 207.2135 206.4373 116.3789 -0.7527 206.5077 207.2604 206.6012 117.9836 -0.7550 206.5625 207.3176 206.7745 119.5833 -0.7554 206.6216 207.3770 206.9556 121.1939 -0.7544 206.6575 207.4118 207.1342 122.7989 -0.7548 206.7033 207.4581 207.3311 124.4036 -0.7528 206.7546 207.5074 207.5207 126.0238 -0.7562 206.8155 207.5717 207.7034 127.6133 -0.7583 206.8511 207.6094 207.8997 129.2343 -0.7606 206.9141 207.6746 208.0754 130.8390 -0.7614 206.9752 207.7366 208.2532 132.4233 -0.7613 207.0202 207.7815 208.4440 134.0331 -0.7587 207.0659 207.8246 208.6264 135.6379 -0.7589 207.1445 207.9034 208.8148 137.2436 -0.7627 207.2111 207.9738 209.0300 138.8638 -0.7609 207.2735 208.0344 209.2440 140.4685 -0.7616 207.3330 208.0946 209.4471 142.0784 -0.7649 207.4077 208.1727 209.6523 143.6785 -0.7665 207.4740 208.2404 209.8502 145.2838 -0.7683 207.5234 208.2917 210.0377 146.8936 -0.7663 207.5866 208.3530 210.2265 148.4779 -0.7680 207.6443 208.4122 210.4236 150.0878 -0.7670 207.7109 208.4779 210.6409 151.7080 -0.7686 207.7779 208.5465 210.8375 153.3083 -0.7720 207.8528 208.6248 210.9957 154.9184 -0.7732 207.9464 208.7195 211.1787 156.5231 -0.7732 208.0104 208.7836 211.3570 158.1125 -0.7722 208.0665 208.8387 211.5359 159.7173 -0.7739 208.1469 208.9208 211.7316 161.3226 -0.7772 208.2199 208.9971 211.9230 162.9278 -0.7764 208.3075 209.0839 212.0982 164.5479 -0.7745 208.3744 209.1489 212.2704 166.1526 -0.7755 208.4580 209.2335 212.4424 167.7471 -0.7770 208.5396 209.3165 212.6285 169.3468 -0.7765 208.6253 209.4017 212.7932 170.9566 -0.7775 208.7227 209.5002 212.9494 172.5570 -0.7764 208.7920 209.5684 213.1377 174.1620 -0.7742 208.8614 209.6356 213.3254 175.7668 -0.7758 208.9645 209.7403 213.5247 177.3869 -0.7784 209.0499 209.8283 213.7251 178.9920 -0.7776 209.1197 209.8972 213.9086 180.5974 -0.7799 209.2048 209.9847 214.0986 182.1868 -0.7811 209.2906 210.0717 214.2770 183.7864 -0.7806 209.3781 210.1587 214.4667 185.3963 -0.7730 209.4647 210.2377 214.6826 186.9964 -0.7691 209.5694 210.3385 214.8801 188.6068 -0.7698 209.6561 210.4258 215.0616 190.2269 -0.7728 209.7495 210.5223 215.2576 191.8265 -0.7743 209.8453 210.6196 215.4374 193.4364 -0.7707 209.9138 210.6846 215.6563 195.0365 -0.7720 210.0190 210.7909 215.8501 196.6366 -0.7735 210.1322 210.9057 216.0612 198.2465 -0.7737 210.2275 211.0012 216.2459 199.8513 -0.7723 210.3303 211.1026 216.4370 201.4663 -0.7722 210.4303 211.2025 216.6364 203.0771 -0.7727 210.5287 211.3014 216.8171 204.6819 -0.7715 210.6213 211.3927 217.0123 206.2918 -0.7689 210.7214 211.4903 217.2189 207.8965 -0.7665 210.8168 211.5833 217.4199 209.4969 -0.7656 210.9218 211.6874 217.5958 211.1070 -0.7625 211.0470 211.8095 217.7854 212.7271 -0.7611 211.1675 211.9286 217.9845 214.3319 -0.7606 211.2681 212.0287 218.1846 215.9321 -0.7590 211.3857 212.1447 218.3759 217.5373 -0.7593 211.4753 212.2346 218.5813 219.1471 -0.7604 211.5938 212.3542 218.7832 220.7519 -0.7594 211.7041 212.4635 219.0107 222.3566 -0.7571 211.8258 212.5829 219.2097 223.9778 -0.7570 211.9393 212.6962 219.4247 225.5825 -0.7558 212.0527 212.8085 219.6513 227.1873 -0.7562 212.1674 212.9236 219.8532 228.7869 -0.7558 212.2838 213.0396 220.0576 230.3916 -0.7514 212.4065 213.1579 220.2652 232.0023 -0.7534 212.5221 213.2756 220.4789 233.6021 -0.7558 212.6338 213.3896 220.7026 235.2223 -0.7560 212.7449 213.5009 220.9314 236.8270 -0.7560 212.8733 213.6293 221.1393 238.4320 -0.7578 213.0004 213.7581 221.3441 240.0324 -0.7560 213.1329 213.8889 221.5649 241.6371 -0.7533 213.2451 213.9984 221.7895 243.2419 -0.7542 213.3687 214.1229 222.0040 244.8466 -0.7521 213.4881 214.2402 222.2161 246.4368 -0.7504 213.6146 214.3650 222.4115 248.0571 -0.7520 213.7333 214.4852 222.6310 249.6619 -0.7526 213.8592 214.6118 222.8457 251.2615 -0.7527 213.9796 214.7323 223.0647 252.8668 -0.7505 214.1067 214.8573 223.2492 254.4771 -0.7499 214.2211 214.9710 223.4460 256.0768 -0.7514 214.3736 215.1249 223.6642 257.6610 -0.7484 214.4856 215.2340 223.8695 259.2715 -0.7473 214.6007 215.3480 224.0444 260.8920 -0.7453 214.7213 215.4667 224.2445 262.4916 -0.7434 214.8643 215.6077 224.4379 264.1015 -0.7428 215.0134 215.7561 224.6270 265.6909 -0.7417 215.1481 215.8898 224.8227 267.3013 -0.7377 215.2854 216.0231 225.0200 268.9065 -0.7389 215.4122 216.1512 225.2240 270.5113 -0.7356 215.5385 216.2741 225.4017 272.1160 -0.7341 215.6660 216.4001 225.5923 273.7054 -0.7310 215.7938 216.5248 225.7778 275.3260 -0.7259 215.9352 216.6611 225.9587 276.9261 -0.7249 216.0881 216.8130 226.1268 278.5309 -0.7244 216.2309 216.9553 226.3199 280.1408 -0.7197 216.3793 217.0989 226.5257 281.7455 -0.7220 216.5353 217.2573 226.7222 283.3503 -0.7226 216.6772 217.3997 226.8940 284.9554 -0.7210 216.8066 217.5276 227.0786 286.5710 -0.7168 216.9517 217.6685 227.2579 288.1809 -0.7157 217.0949 217.8106 227.4221 289.7805 -0.7162 217.2653 217.9815 227.5911 291.3853 -0.7172 217.4073 218.1245 227.7603 292.9951 -0.7187 217.5829 218.3016 227.9613 294.6006 -0.7186 217.7314 218.4500 228.1461 296.1851 -0.7174 217.8678 218.5853 228.3370 297.7950 -0.7204 218.0214 218.7418 228.5428 299.4100 -0.7228 218.1666 218.8894 228.7365 301.0201 -0.7225 218.3332 219.0558 228.9496 302.6205 -0.7240 218.4779 219.2019 229.1555 304.2253 -0.7228 218.6310 219.3538 229.3617 305.8351 -0.7235 218.7872 219.5107 229.5814 307.4399 -0.7240 218.9287 219.6527 229.8059 309.0395 -0.7250 219.0746 219.7996 230.0144 310.6598 -0.7241 219.2366 219.9607 230.2167 312.2654 -0.7237 219.3900 220.1137 230.4369 313.8701 -0.7232 219.5309 220.2541 230.6583 315.4749 -0.7239 219.6850 220.4089 230.8644 317.0796 -0.7244 219.8180 220.5424 231.0755 318.6844 -0.7235 219.9656 220.6890 231.3038 320.2901 -0.7228 220.1214 220.8442 231.5200 321.9103 -0.7225 220.3242 221.0467 231.7343 323.5150 -0.7236 220.4920 221.2156 231.9576 325.1201 -0.7244 220.6392 221.3636 232.1838 326.7306 -0.7229 220.7977 221.5206 232.3995 328.3303 -0.7237 220.9330 221.6567 232.6137 329.9350 -0.7250 221.0885 221.8134 232.7840 331.5398 -0.7217 221.2557 221.9774 232.9946 333.1609 -0.7173 221.4179 222.1352 233.2105 334.7503 -0.7169 221.5716 222.2885 233.4083 336.3601 -0.7172 221.7350 222.4522 233.6247 337.9598 -0.7177 221.9021 222.6198 233.8434 339.5645 -0.7213 222.0602 222.7814 234.0767 341.1700 -0.7202 222.2258 222.9460 234.2709 342.7699 -0.7153 222.3834 223.0987 234.4776 344.3798 -0.7180 222.5447 223.2627 234.7022 345.9999 -0.7171 222.7318 223.4489 234.9171 347.5944 -0.7157 222.9007 223.6165 235.1066 349.2051 -0.7143 223.0768 223.7911 235.3014 350.7946 -0.7160 223.2579 223.9740 235.4978 352.4045 -0.7187 223.4196 224.1383 235.7235 354.0093 -0.7195 223.5858 224.3053 235.9293 355.6140 -0.7208 223.7551 224.4759 236.1186 357.2195 -0.7209 223.9285 224.6494 236.3093 358.8091 -0.7184 224.0932 224.8116 236.5246 360.4139 -0.7163 224.2525 224.9689 236.7158 362.0238 -0.7162 224.4380 225.1542 236.9074 363.6388 -0.7161 224.6333 225.3494 237.0874 365.2443 -0.7180 224.8090 225.5270 237.2949 366.8493 -0.7199 224.9695 225.6894 237.5041 368.4540 -0.7196 225.1529 225.8725 237.6772 370.0383 -0.7188 225.3140 226.0328 237.8657 371.6635 -0.7178 225.4773 226.1951 238.0576 373.2534 -0.7171 225.6476 226.3647 238.2816 374.8535 -0.7179 225.8293 226.5472 238.4825 376.4736 -0.7141 226.0008 226.7149 238.6560 378.0784 -0.7142 226.1732 226.8874 238.8406 379.6886 -0.7113 226.3561 227.0675 239.0235 381.2889 -0.7114 226.5278 227.2392 239.2058 382.8936 -0.7098 226.7081 227.4179 239.3860 384.4881 -0.7097 226.8747 227.5844 239.5825 386.0929 -0.7095 227.0668 227.7763 239.7754 387.6976 -0.7112 227.2728 227.9840 239.9594 389.3188 -0.7118 227.4483 228.1600 240.1463 390.9235 -0.7103 227.6496 228.3599 240.3380 392.5283 -0.7117 227.8342 228.5459 240.5295 394.1330 -0.7137 228.0090 228.7226 240.7397 395.7326 -0.7163 228.1745 228.8908 240.9475 397.3426 -0.7170 228.3476 229.0646 241.1726 398.9483 -0.7166 228.5126 229.2292 241.3921 400.5735 -0.7135 228.7093 229.4228 241.6116 402.1731 -0.7140 228.9071 229.6211 241.8063 403.7783 -0.7145 229.0795 229.7941 242.0323 405.3888 -0.7162 229.2518 229.9680 242.2456 406.9884 -0.7199 229.4358 230.1557 242.4423 408.5880 -0.7231 229.6206 230.3437 242.6458 410.1979 -0.7210 229.8006 230.5216 242.8484 411.8139 -0.7210 229.9814 230.7024 243.0719 413.4186 -0.7200 230.1592 230.8792 243.3075 415.0285 -0.7221 230.3589 231.0810 243.5142 416.6281 -0.7210 230.5528 231.2738 243.7289 418.2336 -0.7207 230.7481 231.4687 243.9467 419.8540 -0.7224 230.9469 231.6693 244.1685 421.4690 -0.7224 231.1220 231.8445 244.4013 423.0789 -0.7233 231.3007 232.0240 244.6009 424.6836 -0.7220 231.4870 232.2089 244.7943 426.2835 -0.7209 231.6824 232.4033 244.9864 427.8941 -0.7227 231.8716 232.5943 245.1738 429.4989 -0.7272 232.0562 232.7833 245.3827 431.1036 -0.7296 232.2336 232.9633 245.5759 432.7238 -0.7300 232.4456 233.1756 245.7635 434.3236 -0.7309 232.6327 233.3636 245.9726 435.9291 -0.7331 232.8246 233.5577 246.1763 437.5339 -0.7357 233.0305 233.7662 246.3768 439.1335 -0.7388 233.2316 233.9704 246.5841 440.7435 -0.7399 233.4238 234.1636 246.8101 442.3439 -0.7382 233.6032 234.3414 247.0193 443.9641 -0.7384 233.7904 234.5288 247.2202 445.5689 -0.7421 233.9821 234.7242 247.4132 447.1736 -0.7439 234.1643 234.9082 247.6163 448.7738 -0.7436 234.3606 235.1042 247.8172 450.3688 -0.7444 234.5423 235.2866 248.0188 451.9838 -0.7490 234.7360 235.4850 248.2298 453.5885 -0.7477 234.9223 235.6699 248.4401 455.1933 -0.7487 235.1112 235.8599 248.6381 456.7936 -0.7499 235.3121 236.0620 248.8471 458.4038 -0.7488 235.4982 236.2469 249.0273 460.0239 -0.7496 235.7053 236.4549 249.2099 461.6286 -0.7504 235.8983 236.6487 249.4006 463.2334 -0.7522 236.0693 236.8215 249.6161 464.8381 -0.7546 236.2751 237.0298 249.7962 466.4384 -0.7561 236.4986 237.2547 249.9653 468.0486 -0.7577 236.7057 237.4634 250.1663 469.6483 -0.7602 236.9102 237.6704 250.3484 471.2684 -0.7612 237.1047 237.8659 250.5199 472.8581 -0.7664 237.2859 238.0524 250.6863 474.4789 -0.7681 237.4669 238.2349 250.8672 476.0836 -0.7664 237.6528 238.4192 251.0419 477.6833 -0.7666 237.8643 238.6309 251.2311 479.2880 -0.7681 238.0615 238.8296 251.4197 480.8825 -0.7702 238.2579 239.0280 251.6171 482.4881 -0.7714 238.4379 239.2093 251.8216 484.1033 -0.7713 238.6368 239.4081 252.0229 485.7131 -0.7745 238.8525 239.6270 252.2255 487.3179 -0.7765 239.0592 239.8357 252.4418 488.9226 -0.7785 239.2588 240.0373 252.6472 490.5228 -0.7814 239.4528 240.2342 252.8653 492.1280 -0.7846 239.6433 240.4279 253.0899 493.7328 -0.7847 239.8451 240.6297 253.2880 495.3529 -0.7835 240.0420 240.8256 253.5186 496.9576 -0.7855 240.2545 241.0400 253.7247 498.5624 -0.7872 240.4512 241.2383 253.9388 500.1675 -0.7872 240.6401 241.4273 254.1636 501.7729 -0.7894 240.8376 241.6270 254.3817 503.3776 -0.7911 241.0048 241.7959 254.5851 504.9824 -0.7916 241.2277 242.0193 254.7845 506.6031 -0.7957 241.4411 242.2368 254.9924 508.2031 -0.7986 241.6533 242.4519 255.2133 509.8079 -0.7978 241.8910 242.6888 255.4406 511.4178 -0.7993 242.0834 242.8827 255.6423 513.0228 -0.8026 242.2935 243.0961 255.8574 514.6231 -0.8054 242.4854 243.2908 256.0531 516.2279 -0.8090 242.6850 243.4939 256.2624 517.8480 -0.8100 242.8858 243.6958 256.4801 519.4528 -0.8124 243.0923 243.9047 256.6923 521.0579 -0.8128 243.2857 244.0985 256.8876 522.6633 -0.8135 243.4924 244.3059 257.0951 524.2578 -0.8173 243.6814 244.4987 257.3092 525.8625 -0.8182 243.8756 244.6937 257.5105 527.4621 -0.8193 244.0783 244.8976 257.7200 529.0833 -0.8196 244.2784 245.0979 257.8992 530.6880 -0.8215 244.4949 245.3163 258.0961 532.2928 -0.8226 244.6971 245.5197 258.3055 533.8975 -0.8274 244.9247 245.7521 258.5171 535.5028 -0.8307 245.1365 245.9672 258.7000 537.1080 -0.8336 245.3516 246.1852 258.8868 538.7076 -0.8329 245.5472 246.3800 259.0913 540.3124 -0.8349 245.7370 246.5720 259.2912 541.9376 -0.8383 245.9325 246.7708 259.5008 543.5373 -0.8414 246.1326 246.9740 259.7106 545.1375 -0.8457 246.3522 247.1979 259.9227 546.7478 -0.8494 246.5467 247.3961 260.1198 548.3371 -0.8493 246.7441 247.5933 260.3228 549.9470 -0.8515 246.9581 247.8096 260.5195 551.5474 -0.8545 247.1589 248.0134 260.7066 553.1524 -0.8577 247.3622 248.2199 260.8918 554.7776 -0.8619 247.5715 248.4334 261.0795 556.3773 -0.8626 247.7770 248.6396 261.2358 557.9773 -0.8614 247.9677 248.8291 261.4225 559.5878 -0.8645 248.1761 249.0406 261.6203 561.1925 -0.8679 248.3920 249.2599 261.8165 562.7973 -0.8723 248.6027 249.4750 262.0412 564.4020 -0.8736 248.8181 249.6917 262.2401 566.0178 -0.8738 249.0507 249.9245 262.4287 567.6228 -0.8758 249.2690 250.1448 262.6447 569.2275 -0.8793 249.4835 250.3628 262.8747 570.8323 -0.8824 249.6874 250.5698 263.0947 572.4269 -0.8859 249.9109 250.7968 263.3278 574.0274 -0.8890 250.1226 251.0116 263.5434 575.6321 -0.8942 250.3191 251.2134 263.7644 577.2420 -0.8977 250.5201 251.4178 264.0010 578.8570 -0.8982 250.7190 251.6172 264.2523 580.4670 -0.8995 250.9232 251.8228 264.5068 582.0675 -0.9029 251.1450 252.0479 264.7206 583.6723 -0.9041 251.3717 252.2759 264.9397 585.2821 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