DTA measure 1Pb_1-ud3.dat Date: 2026827:156 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 932.17 s Mass = 100.000 mg data_number = 1160 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2933 0.2717 195.9876 195.7158 248.0511 2.0495 0.2734 196.2548 195.9814 248.0749 2.9178 0.2739 196.5480 196.2742 248.0810 3.6738 0.2723 196.8074 196.5352 248.1084 4.4915 0.2703 197.1045 196.8342 248.1309 5.2988 0.2686 197.3657 197.0970 248.1439 6.0850 0.2702 197.6315 197.3612 248.1550 6.9130 0.2713 197.9249 197.6536 248.1730 7.6795 0.2713 198.1944 197.9231 248.1928 8.5270 0.2741 198.4562 198.1820 248.2263 9.2935 0.2741 198.7064 198.4323 248.2492 10.1215 0.2748 198.9877 198.7129 248.2624 10.8870 0.2755 199.2400 198.9645 248.2644 11.7150 0.2758 199.4987 199.2230 248.2956 12.5328 0.2730 199.7904 199.5174 248.3109 13.3090 0.2732 200.0451 199.7719 248.3469 14.1263 0.2752 200.3152 200.0400 248.3960 14.9133 0.2751 200.5813 200.3062 248.4510 15.7513 0.2758 200.8688 200.5930 248.5044 16.5068 0.2760 201.1233 200.8473 248.5364 17.3245 0.2771 201.3846 201.1075 248.5860 18.1320 0.2771 201.6442 201.3671 248.6408 18.9183 0.2778 201.8978 201.6200 248.6995 19.7460 0.2762 202.1453 201.8691 248.7640 20.5125 0.2777 202.3757 202.0980 248.8373 21.3810 0.2784 202.6968 202.4185 248.9177 22.1060 0.2788 202.9438 202.6651 248.9940 22.9648 0.2785 203.2138 202.9353 249.0865 23.7305 0.2774 203.4541 203.1767 249.1576 24.5480 0.2791 203.7397 203.4607 249.2483 25.3453 0.2829 203.9851 203.7021 249.3476 26.1425 0.2827 204.2481 203.9654 249.4431 26.9695 0.2811 204.5091 204.2280 249.5467 27.7360 0.2782 204.7488 204.4706 249.6519 28.5845 0.2753 205.0039 204.7287 249.7869 29.3603 0.2763 205.2288 204.9525 249.9085 30.1780 0.2753 205.4849 205.2097 250.0307 30.9753 0.2774 205.7318 205.4544 250.1458 31.7718 0.2780 205.9615 205.6835 250.2831 32.5893 0.2783 206.1981 205.9198 250.4213 33.3558 0.2749 206.4338 206.1589 250.5463 34.2140 0.2751 206.6944 206.4193 250.6966 34.9493 0.2716 206.9395 206.6679 250.8376 35.7978 0.2662 207.2029 206.9367 250.9655 36.5638 0.2670 207.4262 207.1592 251.0993 37.3913 0.2700 207.6662 207.3963 251.2319 38.1885 0.2685 207.9177 207.6491 251.3735 38.9753 0.2657 208.1654 207.8997 251.5036 39.8025 0.2629 208.4296 208.1667 251.6506 40.5690 0.2607 208.6517 208.3910 251.7846 41.4175 0.2612 208.9117 208.6504 251.9340 42.1935 0.2600 209.1511 208.8911 252.0517 43.0110 0.2561 209.4065 209.1504 252.2039 43.8083 0.2536 209.6424 209.3888 252.3473 44.6048 0.2543 209.8680 209.6137 252.4766 45.4325 0.2537 210.1026 209.8489 252.6336 46.1990 0.2533 210.3378 210.0845 252.7740 47.0473 0.2507 210.5959 210.3453 252.9348 47.8130 0.2476 210.8286 210.5810 253.0640 48.6410 0.2458 211.0711 210.8253 253.2047 49.4280 0.2445 211.2958 211.0513 253.3386 50.2243 0.2406 211.5413 211.3006 253.4894 51.0523 0.2377 211.7931 211.5553 253.6504 51.8085 0.2345 211.9937 211.7592 253.7836 52.6768 0.2339 212.2512 212.0172 253.9359 53.4328 0.2322 212.4688 212.2366 254.0656 54.2608 0.2291 212.7136 212.4844 254.1959 55.0573 0.2281 212.9402 212.7121 254.3215 55.8543 0.2270 213.1716 212.9447 254.4741 56.6720 0.2262 213.4095 213.1833 254.6234 57.4380 0.2251 213.6339 213.4088 254.7656 58.2963 0.2210 213.8861 213.6650 254.9422 59.0628 0.2199 214.1161 213.8961 255.0952 59.8800 0.2159 214.3381 214.1222 255.2340 60.6870 0.2114 214.5565 214.3451 255.3738 61.4740 0.2090 214.7845 214.5756 255.5174 62.2918 0.2050 215.0252 214.8202 255.6591 63.0678 0.1989 215.2368 215.0379 255.7942 63.9160 0.1954 215.5033 215.3079 255.9672 64.6825 0.1957 215.7303 215.5347 256.0976 65.5100 0.1929 215.9622 215.7693 256.2305 66.3068 0.1901 216.1801 215.9899 256.3661 67.1040 0.1863 216.4019 216.2156 256.5015 67.9213 0.1828 216.6377 216.4548 256.6499 68.6873 0.1799 216.8725 216.6926 256.7722 69.5460 0.1769 217.1068 216.9299 256.9080 70.3023 0.1756 217.3098 217.1342 257.0496 71.1395 0.1718 217.5311 217.3594 257.1966 71.9265 0.1671 217.7648 217.5977 257.3332 72.7133 0.1632 217.9854 217.8223 257.4618 73.5508 0.1607 218.2215 218.0607 257.6334 74.3070 0.1569 218.4353 218.2784 257.7771 75.1658 0.1518 218.6868 218.5349 257.9111 75.9315 0.1500 218.9023 218.7523 258.0523 76.7593 0.1491 219.1325 218.9835 258.1987 77.5565 0.1446 219.3408 219.1962 258.3379 78.3428 0.1405 219.5577 219.4172 258.4925 79.1705 0.1393 219.7723 219.6330 258.6540 79.9370 0.1354 219.9824 219.8470 258.8022 80.7853 0.1316 220.2200 220.0884 258.9667 81.5613 0.1272 220.4412 220.3140 259.0974 82.3790 0.1225 220.6532 220.5307 259.2278 83.1763 0.1184 220.8588 220.7404 259.3717 83.9725 0.1151 221.0667 220.9516 259.5207 84.8005 0.1091 221.2935 221.1843 259.6568 85.5670 0.1038 221.5017 221.3979 259.8011 86.4153 0.1026 221.7719 221.6693 259.9496 87.1810 0.0999 221.9639 221.8640 260.0706 88.0090 0.0953 222.1819 222.0865 260.2015 88.7960 0.0922 222.3893 222.2971 260.3340 89.6025 0.0871 222.6255 222.5383 260.4688 90.4203 0.0848 222.8503 222.7655 260.6191 91.1765 0.0818 223.0617 222.9799 260.7676 92.0450 0.0772 223.2925 223.2154 260.9292 92.8008 0.0732 223.4992 223.4260 261.0856 93.6185 0.0673 223.7218 223.6545 261.2241 94.4258 0.0629 223.9427 223.8798 261.3522 95.2120 0.0581 224.1471 224.0890 261.4857 96.0400 0.0526 224.3706 224.3180 261.6247 96.8065 0.0498 224.5647 224.5149 261.7628 97.6643 0.0460 224.8004 224.7544 261.9151 98.4308 0.0453 225.0241 224.9788 262.0516 99.2485 0.0448 225.2223 225.1774 262.1718 100.0448 0.0417 225.4170 225.3753 262.2970 100.8420 0.0373 225.6065 225.5692 262.4113 101.6598 0.0319 225.8251 225.7932 262.5460 102.4358 0.0258 226.0244 225.9985 262.6547 103.2840 0.0194 226.2475 226.2281 262.7886 104.0300 0.0163 226.4402 226.4239 262.9053 104.8783 0.0112 226.6569 226.6456 263.0212 105.6440 0.0088 226.8736 226.8648 263.1416 106.4720 0.0052 227.0868 227.0816 263.2761 107.2590 0.0000 227.2817 227.2817 263.4060 108.0658 -0.0041 227.4834 227.4875 263.5274 108.8833 -0.0094 227.6882 227.6975 263.6611 109.6395 -0.0134 227.8604 227.8737 263.7679 110.5080 -0.0153 228.0817 228.0970 263.8917 111.2638 -0.0187 228.2905 228.3092 264.0021 112.0918 -0.0225 228.5086 228.5311 264.1187 112.8890 -0.0272 228.7077 228.7348 264.2317 113.6750 -0.0320 228.9034 228.9354 264.3470 114.5030 -0.0391 229.0996 229.1386 264.4680 115.2695 -0.0460 229.2927 229.3387 264.5727 116.1275 -0.0524 229.5264 229.5788 264.7144 116.8630 -0.0574 229.7265 229.7839 264.8116 117.7115 -0.0607 229.9756 230.0364 264.9213 118.4875 -0.0643 230.1767 230.2410 265.0319 119.3050 -0.0686 230.3762 230.4448 265.1403 120.1023 -0.0713 230.5846 230.6559 265.2734 120.8990 -0.0759 230.7894 230.8653 265.4142 121.7163 -0.0807 230.9826 231.0634 265.5265 122.4828 -0.0863 231.1683 231.2546 265.6390 123.3413 -0.0895 231.3943 231.4838 265.7772 124.0763 -0.0953 231.5873 231.6826 265.8988 124.9453 -0.0984 231.8113 231.9097 266.0446 125.7118 -0.1048 232.0148 232.1195 266.1822 126.5288 -0.1111 232.2268 232.3380 266.3234 127.3360 -0.1164 232.4108 232.5272 266.4500 128.1230 -0.1197 232.6030 232.7227 266.5736 128.9400 -0.1213 232.8001 232.9214 266.6941 129.7165 -0.1254 232.9972 233.1227 266.8345 130.5650 -0.1325 233.2005 233.3330 266.9729 131.3310 -0.1381 233.3945 233.5326 267.0918 132.1585 -0.1421 233.6018 233.7439 267.2363 132.9558 -0.1467 233.7993 233.9460 267.3811 133.7528 -0.1530 233.9889 234.1419 267.5199 134.5698 -0.1555 234.1931 234.3486 267.6456 135.3465 -0.1582 234.3966 234.5548 267.7661 136.1950 -0.1611 234.6096 234.7707 267.9171 136.9608 -0.1631 234.7868 234.9499 268.0382 137.7885 -0.1715 234.9879 235.1595 268.1620 138.5858 -0.1752 235.1799 235.3551 268.2958 139.3720 -0.1791 235.3573 235.5365 268.4336 140.1998 -0.1832 235.5495 235.7327 268.5862 140.9663 -0.1878 235.7334 235.9213 268.7362 141.8145 -0.1922 235.9453 236.1375 268.9016 142.5803 -0.1950 236.1300 236.3250 269.0444 143.4083 -0.1997 236.3239 236.5236 269.1974 144.2055 -0.2057 236.5177 236.7234 269.3407 144.9915 -0.2083 236.6993 236.9077 269.4776 145.8298 -0.2136 236.9073 237.1208 269.6191 146.5858 -0.2186 237.0902 237.3088 269.7499 147.4335 -0.2241 237.2979 237.5220 269.8715 148.2103 -0.2297 237.4898 237.7195 269.9982 149.0280 -0.2355 237.7061 237.9416 270.1367 149.8243 -0.2413 237.8989 238.1402 270.2614 150.6215 -0.2448 238.0967 238.3414 270.4059 151.4495 -0.2507 238.2908 238.5415 270.5554 152.2153 -0.2572 238.4746 238.7318 270.6912 153.0635 -0.2633 238.6626 238.9259 270.8226 153.8403 -0.2685 238.8591 239.1276 270.9689 154.6573 -0.2735 239.0651 239.3386 271.1231 155.4543 -0.2782 239.2593 239.5374 271.2601 156.2515 -0.2841 239.4627 239.7468 271.3967 157.0788 -0.2899 239.6708 239.9606 271.5271 157.8348 -0.2946 239.8493 240.1439 271.6616 158.6935 -0.2986 240.0415 240.3401 271.8279 159.4595 -0.3052 240.2337 240.5389 271.9594 160.2768 -0.3114 240.4160 240.7274 272.1035 161.0740 -0.3153 240.6052 240.9204 272.2505 161.8713 -0.3203 240.8015 241.1218 272.3967 162.6983 -0.3223 241.0033 241.3255 272.5770 163.4545 -0.3251 241.1967 241.5217 272.7155 164.3133 -0.3318 241.4034 241.7352 272.8513 165.0585 -0.3351 241.5722 241.9073 272.9704 165.9273 -0.3374 241.7615 242.0989 273.1251 166.6938 -0.3408 241.9346 242.2754 273.2518 167.5108 -0.3467 242.1179 242.4646 273.4001 168.3180 -0.3515 242.3082 242.6597 273.5510 169.1050 -0.3541 242.5078 242.8619 273.6853 169.9225 -0.3602 242.7028 243.0630 273.8096 170.6985 -0.3650 242.8691 243.2341 273.9269 171.5470 -0.3698 243.0668 243.4366 274.0753 172.3135 -0.3748 243.2428 243.6177 274.2165 173.1405 -0.3791 243.4295 243.8086 274.3479 173.9378 -0.3832 243.6213 244.0045 274.4675 174.7350 -0.3889 243.8093 244.1983 274.6023 175.5520 -0.3921 243.9776 244.3697 274.7335 176.3183 -0.3929 244.1500 244.5429 274.8709 177.1770 -0.3990 244.3539 244.7529 275.0378 177.9325 -0.4030 244.5258 244.9288 275.1734 178.7705 -0.4086 244.7339 245.1425 275.3324 179.5575 -0.4111 244.9295 245.3406 275.4685 180.3443 -0.4129 245.1221 245.5351 275.6138 181.1818 -0.4182 245.3035 245.7217 275.7554 181.9380 -0.4239 245.4710 245.8949 275.8713 182.7965 -0.4308 245.6700 246.1008 276.0088 183.5623 -0.4358 245.8380 246.2738 276.1276 184.3800 -0.4407 246.0188 246.4595 276.2689 185.1773 -0.4445 246.2058 246.6503 276.3989 185.9738 -0.4486 246.3897 246.8383 276.5212 186.8015 -0.4533 246.5973 247.0506 276.6656 187.5680 -0.4583 246.7826 247.2409 276.7884 188.3853 -0.4613 246.9699 247.4311 276.9262 189.1615 -0.4655 247.1461 247.6116 277.0447 190.0100 -0.4699 247.3570 247.8269 277.1936 190.7760 -0.4746 247.5314 248.0060 277.3209 191.6035 -0.4785 247.7200 248.1984 277.4821 192.3905 -0.4825 247.8953 248.3778 277.6217 193.1873 -0.4852 248.0743 248.5595 277.7528 194.0148 -0.4885 248.2396 248.7282 277.8892 194.7813 -0.4939 248.4056 248.8995 278.0072 195.6400 -0.4998 248.6044 249.1043 278.1411 196.3850 -0.5024 248.7746 249.2770 278.2491 197.2335 -0.5026 248.9792 249.4818 278.3840 198.0000 -0.5072 249.1331 249.6403 278.5046 198.8275 -0.5145 249.3159 249.8304 278.6400 199.6140 -0.5201 249.4798 249.9999 278.7725 200.4215 -0.5253 249.6483 250.1735 278.9022 201.2078 -0.5302 249.8101 250.3404 279.0256 201.9945 -0.5353 249.9825 250.5178 279.1457 202.8328 -0.5364 250.1908 250.7273 279.2932 203.5883 -0.5393 250.3678 250.9071 279.4096 204.4468 -0.5419 250.5658 251.1077 279.5365 205.2133 -0.5471 250.7226 251.2698 279.6623 206.0408 -0.5514 250.9037 251.4551 279.7863 206.8170 -0.5557 251.0843 251.6401 279.9050 207.6348 -0.5634 251.2720 251.8354 280.0291 208.4313 -0.5673 251.4571 252.0244 280.1439 209.2283 -0.5703 251.6343 252.2046 280.2697 210.0460 -0.5772 251.8130 252.3903 280.4007 210.8120 -0.5825 251.9736 252.5561 280.5213 211.6703 -0.5856 252.1624 252.7480 280.6475 212.4368 -0.5856 252.3167 252.9022 280.7836 213.2545 -0.5878 252.5016 253.0893 280.9335 214.0610 -0.5927 252.6911 253.2838 281.0684 214.8480 -0.5962 252.8491 253.4453 281.1850 215.6658 -0.6011 253.0384 253.6395 281.3239 216.4420 -0.6056 253.2029 253.8085 281.4508 217.2900 -0.6142 253.3983 254.0125 281.5754 218.0565 -0.6208 253.5911 254.2119 281.6874 218.8843 -0.6237 253.7706 254.3942 281.8082 219.6500 -0.6276 253.9534 254.5810 281.9598 220.4780 -0.6317 254.1414 254.7731 282.0808 221.2650 -0.6372 254.3071 254.9443 282.2084 222.0615 -0.6405 254.4785 255.1190 282.3258 222.8893 -0.6424 254.6519 255.2942 282.4488 223.6455 -0.6465 254.8178 255.4642 282.5608 224.5145 -0.6519 255.0163 255.6681 282.6954 225.2698 -0.6572 255.1814 255.8385 282.8016 226.0875 -0.6628 255.3482 256.0110 282.9318 226.8950 -0.6689 255.5219 256.1908 283.0500 227.6810 -0.6745 255.7077 256.3821 283.1585 228.5090 -0.6781 255.8767 256.5548 283.2899 229.2755 -0.6817 256.0426 256.7244 283.4031 230.1230 -0.6840 256.2148 256.8988 283.5375 230.8895 -0.6877 256.3812 257.0688 283.6544 231.7175 -0.6901 256.5523 257.2425 283.7738 232.5143 -0.6941 256.7292 257.4233 283.8919 233.3110 -0.6983 256.8903 257.5886 284.0222 234.1288 -0.7027 257.0726 257.7753 284.1470 234.9055 -0.7068 257.2332 257.9400 284.2584 235.7530 -0.7114 257.4157 258.1270 284.3979 236.5195 -0.7134 257.5645 258.2779 284.5015 237.3475 -0.7163 257.7297 258.4460 284.6178 238.1438 -0.7196 257.9073 258.6269 284.7270 238.9410 -0.7230 258.0938 258.8168 284.8437 239.7588 -0.7280 258.2758 259.0038 284.9638 240.5245 -0.7323 258.4331 259.1654 285.0662 241.3830 -0.7371 258.6264 259.3635 285.1917 242.1393 -0.7415 258.7952 259.5367 285.2953 242.9775 -0.7452 258.9635 259.7087 285.4192 243.7635 -0.7497 259.1569 259.9066 285.5188 244.5505 -0.7545 259.3232 260.0777 285.6342 245.3888 -0.7606 259.5079 260.2685 285.7799 246.1440 -0.7617 259.6647 260.4264 285.8890 246.9925 -0.7631 259.8493 260.6124 286.0144 247.7693 -0.7685 260.0243 260.7928 286.1255 248.5860 -0.7722 260.1895 260.9617 286.2462 249.3833 -0.7753 260.3551 261.1304 286.3690 250.1805 -0.7778 260.5168 261.2946 286.4949 251.0080 -0.7814 260.6849 261.4663 286.6182 251.7740 -0.7829 260.8433 261.6262 286.7317 252.6225 -0.7881 261.0002 261.7883 286.8618 253.3985 -0.7933 261.1569 261.9501 286.9769 254.2160 -0.7961 261.3300 262.1261 287.1130 255.0030 -0.7995 261.4891 262.2887 287.2372 255.8100 -0.8037 261.6648 262.4685 287.3806 256.6273 -0.8101 261.8325 262.6426 287.5249 257.3835 -0.8135 261.9799 262.7934 287.6241 258.2523 -0.8174 262.1544 262.9718 287.7718 259.0078 -0.8224 262.3152 263.1376 287.9144 259.8358 -0.8250 262.4996 263.3245 288.0376 260.6330 -0.8277 262.6661 263.4938 288.1400 261.4295 -0.8316 262.8128 263.6443 288.2582 262.2470 -0.8338 262.9793 263.8131 288.3849 263.0135 -0.8383 263.1531 263.9914 288.5020 263.8715 -0.8422 263.3438 264.1860 288.6424 264.6378 -0.8475 263.5007 264.3482 288.7847 265.4555 -0.8527 263.6660 264.5187 288.9241 266.2520 -0.8578 263.8292 264.6870 289.0526 267.0490 -0.8598 263.9896 264.8494 289.1882 267.8668 -0.8598 264.1661 265.0258 289.3252 268.6430 -0.8635 264.3148 265.1783 289.4773 269.4910 -0.8695 264.4887 265.3582 289.6293 270.2575 -0.8741 264.6463 265.5204 289.7642 271.0850 -0.8790 264.8171 265.6961 289.8939 271.8818 -0.8842 264.9874 265.8716 290.0305 272.6790 -0.8863 265.1644 266.0507 290.1724 273.4963 -0.8898 265.3544 266.2443 290.3081 274.2725 -0.8932 265.5255 266.4186 290.4400 275.1210 -0.8983 265.6994 266.5976 290.6041 275.8773 -0.9026 265.8583 266.7610 290.7297 276.7145 -0.9027 266.0231 266.9258 290.8722 277.5015 -0.9095 266.1731 267.0826 291.0096 278.2988 -0.9164 266.3246 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