DTA measure 1_T250214.dat Date: 2025214:1329 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.22 s Mass = 100.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2063 0.2134 225.9040 225.6907 271.0281 1.9740 0.2133 226.1776 225.9642 270.9252 2.7928 0.2131 226.4695 226.2564 270.8154 3.6013 0.2131 226.7501 226.5370 270.7051 4.3893 0.2134 227.0270 226.8136 270.5875 5.2088 0.2134 227.3113 227.0979 270.4648 5.9865 0.2130 227.5834 227.3704 270.3429 6.8368 0.2133 227.8818 227.6686 270.2073 7.6040 0.2143 228.1517 227.9374 270.0818 8.4233 0.2150 228.4327 228.2176 269.9445 9.2630 0.2165 228.7203 228.5037 269.7994 10.0198 0.2175 228.9727 228.7553 269.6685 10.8800 0.2187 229.2631 229.0444 269.5152 11.6165 0.2199 229.5118 229.2919 269.3863 12.4668 0.2204 229.7988 229.5784 269.2411 13.2443 0.2219 230.0606 229.8388 269.1058 14.0635 0.2229 230.3348 230.1119 268.9621 14.8620 0.2249 230.5993 230.3744 268.8229 15.6600 0.2261 230.8668 230.6407 268.6843 16.4893 0.2272 231.1503 230.9231 268.5382 17.2465 0.2290 231.3973 231.1683 268.4011 18.0968 0.2317 231.6699 231.4382 268.2519 18.8743 0.2329 231.9259 231.6930 268.1196 19.6830 0.2350 232.1904 231.9554 267.9886 20.4920 0.2374 232.4541 232.2166 267.8541 21.2798 0.2395 232.7077 232.4682 267.7262 22.0988 0.2409 232.9727 232.7318 267.5979 22.8660 0.2432 233.2152 232.9721 267.4839 23.6850 0.2453 233.4747 233.2294 267.3602 24.4630 0.2470 233.7250 233.4780 267.2510 25.3128 0.2485 233.9918 233.7433 267.1350 26.0698 0.2501 234.2276 233.9775 267.0377 26.9093 0.2519 234.4866 234.2346 266.9324 27.6970 0.2535 234.7256 234.4721 266.8368 28.4955 0.2544 234.9691 234.7147 266.7454 29.3148 0.2554 235.2153 234.9599 266.6575 30.0820 0.2566 235.4479 235.1913 266.5807 30.9428 0.2575 235.7087 235.4512 266.5141 31.6998 0.2586 235.9381 235.6795 266.4545 32.5290 0.2593 236.1795 235.9202 266.4000 33.3275 0.2600 236.4179 236.1579 266.3536 34.1258 0.2609 236.6579 236.3970 266.3171 34.9240 0.2617 236.8989 236.6371 266.2918 35.7223 0.2625 237.1353 236.8728 266.2718 36.5413 0.2628 237.3776 237.1147 266.2647 37.3085 0.2631 237.5998 237.3367 266.2651 38.1693 0.2633 237.8479 237.5847 266.2746 38.9263 0.2634 238.0658 237.8024 266.2969 39.7658 0.2629 238.3065 238.0436 266.3296 40.5540 0.2624 238.5278 238.2654 266.3735 41.3523 0.2626 238.7459 238.4833 266.4275 42.1713 0.2615 238.9760 238.7145 266.4947 42.9490 0.2605 239.1946 238.9341 266.5657 43.7990 0.2592 239.4272 239.1679 266.6523 44.5355 0.2586 239.6281 239.3694 266.7333 45.3958 0.2573 239.8688 239.6114 266.8442 46.1528 0.2558 240.0792 239.8233 266.9533 46.9923 0.2544 240.3064 240.0520 267.0865 47.7803 0.2517 240.5182 240.2665 267.2242 48.5785 0.2489 240.7362 240.4873 267.3729 49.4080 0.2467 240.9598 240.7131 267.5374 50.1753 0.2452 241.1763 240.9311 267.6975 51.0253 0.2424 241.4086 241.1662 267.8948 51.7820 0.2399 241.6088 241.3690 268.0799 52.6113 0.2368 241.8297 241.5929 268.2842 53.3993 0.2329 242.0403 241.8074 268.4951 54.1980 0.2288 242.2515 242.0227 268.7211 55.0273 0.2251 242.4651 242.2399 268.9652 55.7845 0.2210 242.6633 242.4423 269.1934 56.6140 0.2173 242.8746 242.6573 269.4544 57.3810 0.2141 243.0720 242.8579 269.7045 58.2418 0.2093 243.2930 243.0837 269.9925 58.9988 0.2049 243.4893 243.2844 270.2538 59.8178 0.1993 243.6971 243.4978 270.5497 60.6160 0.1948 243.9056 243.7108 270.8459 61.4143 0.1890 244.1097 243.9207 271.1462 62.2440 0.1824 244.3213 244.1389 271.4617 63.0008 0.1768 244.5147 244.3379 271.7582 63.8610 0.1701 244.7280 244.5579 272.0961 64.6285 0.1641 244.9218 244.7576 272.4039 65.4475 0.1572 245.1288 244.9716 272.7395 66.2460 0.1500 245.3289 245.1789 273.0729 67.0440 0.1430 245.5275 245.3845 273.4059 67.8733 0.1361 245.7346 245.5985 273.7547 68.6308 0.1287 245.9230 245.7943 274.0835 69.5013 0.1204 246.1443 246.0239 274.4682 70.2583 0.1135 246.3366 246.2231 274.7996 71.0875 0.1059 246.5485 246.4427 275.1655 71.8550 0.0979 246.7428 246.6449 275.5059 72.6740 0.0883 246.9465 246.8582 275.8693 73.4723 0.0794 247.1428 247.0634 276.2189 74.2708 0.0708 247.3400 247.2692 276.5737 75.1000 0.0613 247.5535 247.4922 276.9446 75.8678 0.0517 247.7483 247.6965 277.2851 76.7280 0.0411 247.9664 247.9253 277.6607 77.4848 0.0317 248.1551 248.1234 277.9928 78.3143 0.0214 248.3658 248.3444 278.3542 79.1128 0.0109 248.5711 248.5602 278.6956 79.9110 0.0001 248.7734 248.7734 279.0332 80.7403 -0.0111 248.9783 248.9894 279.3783 81.4973 -0.0206 249.1682 249.1888 279.6866 82.3573 -0.0317 249.3880 249.4197 280.0382 83.1145 -0.0415 249.5761 249.6176 280.3432 83.9335 -0.0525 249.7798 249.8323 280.6683 84.7320 -0.0627 249.9853 250.0481 280.9785 85.5198 -0.0731 250.1868 250.2599 281.2786 86.3593 -0.0841 250.3991 250.4833 281.5971 87.1163 -0.0946 250.5882 250.6827 281.8808 87.9663 -0.1063 250.8037 250.9099 282.1890 88.7030 -0.1153 250.9951 251.1104 282.4495 89.5528 -0.1267 251.2080 251.3347 282.7440 90.3303 -0.1372 251.4048 251.5420 283.0067 91.1493 -0.1488 251.6105 251.7593 283.2768 91.9375 -0.1589 251.8107 251.9696 283.5267 92.7463 -0.1697 252.0178 252.1875 283.7773 93.5650 -0.1813 252.2228 252.4041 284.0195 94.3323 -0.1908 252.4169 252.6077 284.2366 95.1825 -0.2025 252.6310 252.8334 284.4699 95.9603 -0.2127 252.8296 253.0423 284.6767 96.7793 -0.2222 253.0353 253.2575 284.8884 97.5670 -0.2322 253.2362 253.4683 285.0883 98.3760 -0.2434 253.4466 253.6900 285.2883 99.1950 -0.2537 253.6563 253.9100 285.4792 99.9625 -0.2635 253.8465 254.1100 285.6472 100.8128 -0.2747 254.0603 254.3350 285.8317 101.5903 -0.2833 254.2583 254.5416 285.9932 102.4093 -0.2924 254.4644 254.7569 286.1518 103.1978 -0.3020 254.6667 254.9687 286.2925 104.0063 -0.3114 254.8700 255.1814 286.4390 104.8253 -0.3209 255.0792 255.4001 286.5800 105.5930 -0.3299 255.2717 255.6016 286.7039 106.4530 -0.3392 255.4879 255.8271 286.8278 107.2203 -0.3488 255.6784 256.0272 286.9284 108.0393 -0.3580 255.8870 256.2450 287.0319 108.8483 -0.3672 256.0914 256.4586 287.1286 109.6363 -0.3762 256.2893 256.6655 287.2207 110.4345 -0.3844 256.4943 256.8788 287.3029 111.2328 -0.3926 256.6993 257.0919 287.3799 112.0520 -0.4012 256.9045 257.3058 287.4526 112.8298 -0.4087 257.0997 257.5084 287.5154 113.6798 -0.4170 257.3195 257.7365 287.5811 114.4473 -0.4251 257.5131 257.9382 287.6319 115.2660 -0.4334 257.7192 258.1525 287.6859 116.0540 -0.4409 257.9166 258.3575 287.7282 116.8523 -0.4488 258.1152 258.5640 287.7646 117.6713 -0.4569 258.3210 258.7778 287.8004 118.4493 -0.4643 258.5189 258.9832 287.8300 119.2993 -0.4715 258.7296 259.2011 287.8541 120.0560 -0.4779 258.9156 259.3935 287.8695 120.8855 -0.4842 259.1270 259.6112 287.8814 121.6838 -0.4918 259.3288 259.8207 287.8876 122.4823 -0.4983 259.5307 260.0290 287.8918 123.3013 -0.5045 259.7333 260.2378 287.8886 124.0685 -0.5109 259.9250 260.4358 287.8841 124.9293 -0.5182 260.1429 260.6611 287.8774 125.6550 -0.5235 260.3231 260.8466 287.8701 126.5158 -0.5302 260.5369 261.0670 287.8617 127.2830 -0.5353 260.7285 261.2638 287.8424 128.1125 -0.5412 260.9339 261.4752 287.8189 128.9008 -0.5461 261.1271 261.6732 287.8016 129.6990 -0.5517 261.3231 261.8748 287.7830 130.5288 -0.5574 261.5261 262.0835 287.7598 131.2858 -0.5625 261.7125 262.2749 287.7335 132.1463 -0.5676 261.9232 262.4908 287.6911 132.9138 -0.5723 262.1099 262.6822 287.6623 133.7430 -0.5771 262.3073 262.8844 287.6406 134.5310 -0.5818 262.4939 263.0757 287.6189 135.3295 -0.5860 262.6856 263.2717 287.5930 136.1588 -0.5903 262.8797 263.4700 287.5676 136.9158 -0.5937 263.0596 263.6533 287.5374 137.7763 -0.5979 263.2707 263.8686 287.5100 138.5438 -0.6022 263.4564 264.0586 287.4859 139.3730 -0.6062 263.6568 264.2629 287.4586 140.1613 -0.6100 263.8424 264.4524 287.4333 140.9595 -0.6134 264.0322 264.6456 287.4114 141.7890 -0.6173 264.2262 264.8435 287.3917 142.5565 -0.6213 264.4042 265.0255 287.3726 143.4168 -0.6261 264.6027 265.2288 287.3515 144.1738 -0.6293 264.7765 265.4057 287.3387 145.0030 -0.6331 264.9613 265.5944 287.3315 145.8015 -0.6360 265.1442 265.7802 287.3218 146.6000 -0.6387 265.3299 265.9687 287.3119 147.4190 -0.6411 265.5216 266.1628 287.3121 148.1760 -0.6442 265.6951 266.3393 287.3171 149.0363 -0.6477 265.8912 266.5389 287.3210 149.7623 -0.6509 266.0581 266.7090 287.3328 150.6120 -0.6549 266.2487 266.9036 287.3506 151.3898 -0.6574 266.4251 267.0825 287.3750 152.2088 -0.6615 266.6122 267.2737 287.4086 153.0070 -0.6650 266.7877 267.4527 287.4411 153.7948 -0.6685 266.9632 267.6317 287.4752 154.6243 -0.6713 267.1480 267.8194 287.5214 155.3918 -0.6741 267.3145 267.9885 287.5709 156.2418 -0.6781 267.5043 268.1824 287.6352 157.0090 -0.6813 267.6745 268.3557 287.6921 157.8278 -0.6849 267.8535 268.5384 287.7576 158.6363 -0.6883 268.0349 268.7231 287.8291 159.4245 -0.6912 268.2028 268.8940 287.9093 160.2438 -0.6952 268.3776 269.0728 288.0003 161.0213 -0.6984 268.5436 269.2421 288.0879 161.8713 -0.7021 268.7284 269.4305 288.1922 162.6078 -0.7061 268.8804 269.5865 288.2878 163.4578 -0.7103 269.0613 269.7717 288.4049 164.2353 -0.7135 269.2289 269.9423 288.5180 165.0543 -0.7169 269.4085 270.1255 288.6445 165.8630 -0.7210 269.5862 270.3072 288.7820 166.6508 -0.7255 269.7510 270.4766 288.9228 167.4700 -0.7303 269.9221 270.6524 289.0734 168.2478 -0.7345 270.0797 270.8142 289.2269 169.0978 -0.7396 270.2603 270.9999 289.3961 169.8650 -0.7436 270.4187 271.1623 289.5530 170.6945 -0.7479 270.5917 271.3396 289.7269 171.4930 -0.7518 270.7576 271.5094 289.9039 172.2808 -0.7561 270.9241 271.6802 290.0828 173.1203 -0.7611 271.0993 271.8604 290.2848 173.8775 -0.7655 271.2553 272.0208 290.4649 174.7273 -0.7708 271.4248 272.1956 290.6760 175.4743 -0.7757 271.5794 272.3551 290.8607 176.3240 -0.7804 271.7511 272.5315 291.0768 177.1018 -0.7851 271.9083 272.6934 291.2944 177.9210 -0.7904 272.0698 272.8601 291.5212 178.7193 -0.7958 272.2353 273.0311 291.7481 179.5073 -0.8014 272.3944 273.1958 291.9728 180.3363 -0.8070 272.5643 273.3713 292.2151 181.1038 -0.8124 272.7220 273.5343 292.4423 181.9123 -0.8174 272.8866 273.7040 292.6893 182.7213 -0.8233 273.0502 273.8736 292.9316 183.5403 -0.8290 273.2157 274.0448 293.1837 184.2970 -0.8348 273.3709 274.2057 293.4242 185.1365 -0.8409 273.5383 274.3793 293.6930 185.9248 -0.8472 273.6992 274.5464 293.9443 186.7230 -0.8539 273.8577 274.7116 294.1985 187.5418 -0.8607 274.0255 274.8861 294.4605 188.3095 -0.8671 274.1835 275.0507 294.7117 189.1698 -0.8739 274.3594 275.2333 294.9937 189.9268 -0.8809 274.5155 275.3965 295.2417 190.7560 -0.8887 274.6929 275.5817 295.5116 191.5540 -0.8958 274.8565 275.7523 295.7732 192.3525 -0.9026 275.0178 275.9205 296.0396 193.1408 -0.9084 275.1776 276.0860 296.3051 193.9390 -0.9153 275.3413 276.2565 296.5614 194.7993 -0.9230 275.5126 276.4356 296.8410 195.5250 -0.9301 275.6570 276.5871 297.0755 196.3858 -0.9370 275.8306 276.7677 297.3507 197.1530 -0.9435 275.9863 276.9298 297.5971 197.9823 -0.9509 276.1561 277.1069 297.8659 198.7703 -0.9574 276.3157 277.2731 298.1206 199.5690 -0.9645 276.4781 277.4426 298.3746 200.4293 -0.9737 276.6528 277.6265 298.6416 201.1553 -0.9804 276.7956 277.7759 298.8634 202.0158 -0.9880 276.9749 277.9629 299.1210 202.7830 -0.9951 277.1313 278.1264 299.3539 203.6123 -1.0028 277.2976 278.3004 299.6016 204.4108 -1.0102 277.4583 278.4685 299.8353 205.2090 -1.0170 277.6200 278.6369 300.0645 206.0278 -1.0247 277.7814 278.8061 300.2989 206.7953 -1.0318 277.9414 278.9732 300.5174 207.6558 -1.0398 278.1140 279.1538 300.7470 208.4128 -1.0470 278.2684 279.3154 300.9463 209.2523 -1.0550 278.4404 279.4954 301.1632 210.0400 -1.0624 278.6040 279.6665 301.3619 210.8385 -1.0693 278.7683 279.8376 301.5622 211.6578 -1.0763 278.9342 280.0105 301.7656 212.4148 -1.0833 279.0858 280.1690 301.9491 213.2750 -1.0910 279.2621 280.3531 302.1431 214.0318 -1.0979 279.4212 280.5190 302.3141 214.8615 -1.1051 279.5931 280.6981 302.4961 215.6598 -1.1122 279.7527 280.8648 302.6664 216.4478 -1.1196 279.9168 281.0364 302.8337 217.2770 -1.1272 280.0917 281.2189 303.0023 218.0338 -1.1341 280.2490 281.3831 303.1472 218.8940 -1.1417 280.4281 281.5698 303.3128 219.6618 -1.1483 280.5880 281.7363 303.4570 220.4808 -1.1552 280.7601 281.9154 303.6015 221.2790 -1.1618 280.9289 282.0907 303.7350 222.0770 -1.1681 281.0955 282.2636 303.8635 222.8753 -1.1744 281.2669 282.4413 303.9958 223.6638 -1.1812 281.4312 282.6124 304.1173 224.5033 -1.1880 281.6112 282.7992 304.2407 225.2603 -1.1937 281.7715 282.9652 304.3494 226.1205 -1.2002 281.9495 283.1496 304.4654 226.8878 -1.2067 282.1036 283.3103 304.5655 227.7068 -1.2130 282.2710 283.4839 304.6724 228.5053 -1.2191 282.4349 283.6539 304.7692 229.3038 -1.2249 282.6023 283.8272 304.8589 230.1330 -1.2317 282.7807 284.0124 304.9513 230.8898 -1.2373 282.9441 284.1814 305.0329 231.7500 -1.2444 283.1246 284.3690 305.1217 232.5175 -1.2501 283.2798 284.5299 305.1927 233.3368 -1.2554 283.4488 284.7042 305.2711 234.1350 -1.2609 283.6174 284.8783 305.3448 234.9330 -1.2661 283.7797 285.0458 305.4096 235.7625 -1.2710 283.9518 285.2228 305.4751 236.5198 -1.2753 284.1116 285.3868 305.5309 237.3903 -1.2810 284.2946 285.5756 305.5930 238.1470 -1.2859 284.4489 285.7348 305.6429 238.9765 -1.2911 284.6218 285.9129 305.6961 239.7748 -1.2962 284.7868 286.0830 305.7445 240.5628 -1.3016 284.9507 286.2524 305.7869 241.3920 -1.3061 285.1236 286.4296 305.8278 242.1598 -1.3100 285.2806 286.5907 305.8662 243.0200 -1.3143 285.4580 286.7723 305.9062 243.7768 -1.3178 285.6157 286.9335 305.9419 244.5960 -1.3219 285.7868 287.1088 305.9834 245.3943 -1.3262 285.9533 287.2796 306.0216 246.1823 -1.3303 286.1188 287.4491 306.0535 247.0010 -1.3350 286.2823 287.6173 306.0879 247.7790 -1.3388 286.4388 287.7776 306.1196 248.6290 -1.3426 286.6153 287.9579 306.1572 249.3963 -1.3458 286.7713 288.1171 306.1889 250.2153 -1.3494 286.9368 288.2862 306.2237 251.0033 -1.3534 287.0985 288.4519 306.2548 251.8123 -1.3568 287.2621 288.6189 306.2876 252.6310 -1.3600 287.4278 288.7878 306.3184 253.3983 -1.3630 287.5845 288.9476 306.3514 254.2178 -1.3668 287.7508 289.1176 306.3854 255.0263 -1.3706 287.9210 289.2916 306.4174 255.8453 -1.3743 288.0805 289.4548 306.4521 256.6330 -1.3774 288.2423 289.6198 306.4865 257.4420 -1.3801 288.4067 289.7868 306.5234 258.2300 -1.3828 288.5659 289.9487 306.5616 259.0283 -1.3858 288.7281 290.1139 306.6005 259.8578 -1.3891 288.8916 290.2808 306.6455 260.6250 -1.3919 289.0464 290.4382 306.6899 261.4753 -1.3947 289.2130 290.6077 306.7409 262.2530 -1.3975 289.3640 290.7616 306.7888 263.0718 -1.4007 289.5253 290.9260 306.8408 263.8598 -1.4038 289.6803 291.0841 306.8937 264.6683 -1.4067 289.8418 291.2485 306.9511 265.4870 -1.4095 290.0067 291.4162 307.0131 266.2648 -1.4120 290.1626 291.5745 307.0743 267.1150 -1.4145 290.3341 291.7486 307.1427 267.8823 -1.4173 290.4838 291.9011 307.2108 268.7013 -1.4206 290.6419 292.0625 307.2833 269.5100 -1.4233 290.7939 292.2172 307.3637 270.2978 -1.4265 290.9429 292.3695 307.4417 271.1168 -1.4294 291.0970 292.5264 307.5244 271.8948 -1.4326 291.2485 292.6810 307.6046 272.7448 -1.4361 291.4154 292.8515 307.6991 273.5223 -1.4392 291.5622 293.0014 307.7882 274.3410 -1.4426 291.7173 293.1599 307.8908 275.1083 -1.4456 291.8603 293.3059 307.9889 275.9273 -1.4485 292.0176 293.4660 308.0963 276.7155 -1.4507 292.1731 293.6238 308.2054 277.5140 -1.4535 292.3257 293.7792 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