DTA measure 1_test_1 Date: 2025212:1527 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.21 s Mass = 955.900 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2580 -0.5875 239.6596 240.2471 268.8445 2.0565 -0.5830 239.8614 240.4444 268.8002 2.8448 -0.5785 240.0587 240.6372 268.7610 3.6843 -0.5742 240.2710 240.8453 268.7037 4.4410 -0.5715 240.4588 241.0302 268.6531 5.3013 -0.5667 240.6684 241.2350 268.5972 6.0690 -0.5631 240.8566 241.4197 268.5436 6.8983 -0.5591 241.0618 241.6209 268.4869 7.6863 -0.5548 241.2535 241.8083 268.4245 8.4950 -0.5508 241.4466 241.9974 268.3602 9.3138 -0.5472 241.6459 242.1932 268.2939 10.0810 -0.5435 241.8301 242.3736 268.2300 10.9413 -0.5399 242.0393 242.5791 268.1545 11.6980 -0.5355 242.2180 242.7535 268.0927 12.5380 -0.5316 242.4112 242.9428 268.0196 13.3260 -0.5276 242.5991 243.1267 267.9525 14.1348 -0.5237 242.7908 243.3145 267.8865 14.9433 -0.5194 242.9788 243.4982 267.8224 15.7315 -0.5155 243.1651 243.6806 267.7583 16.5508 -0.5110 243.3610 243.8720 267.6940 17.3180 -0.5069 243.5364 244.0434 267.6357 18.1683 -0.5022 243.7376 244.2398 267.5700 18.9250 -0.4988 243.9149 244.4137 267.5219 19.7648 -0.4938 244.1062 244.6000 267.4620 20.5528 -0.4905 244.2858 244.7763 267.4056 21.3510 -0.4867 244.4702 244.9569 267.3551 22.1390 -0.4833 244.6539 245.1373 267.3057 22.9375 -0.4794 244.8378 245.3173 267.2575 23.7668 -0.4758 245.0263 245.5020 267.2152 24.5238 -0.4729 245.1961 245.6690 267.1810 25.3840 -0.4693 245.3872 245.8565 267.1494 26.1410 -0.4661 245.5523 246.0185 267.1263 26.9705 -0.4616 245.7344 246.1960 267.1020 27.7688 -0.4583 245.9124 246.3707 267.0825 28.5568 -0.4549 246.0846 246.5395 267.0703 29.3860 -0.4522 246.2625 246.7147 267.0584 30.1535 -0.4496 246.4256 246.8752 267.0549 31.0138 -0.4459 246.6167 247.0625 267.0606 31.7708 -0.4429 246.7804 247.2233 267.0690 32.6000 -0.4401 246.9551 247.3953 267.0854 33.3983 -0.4380 247.1243 247.5623 267.1069 34.1863 -0.4354 247.2921 247.7275 267.1308 35.0158 -0.4330 247.4732 247.9062 267.1646 35.7830 -0.4303 247.6362 248.0665 267.2016 36.6433 -0.4274 247.8159 248.2433 267.2572 37.4003 -0.4264 247.9755 248.4019 267.3114 38.2295 -0.4254 248.1511 248.5765 267.3821 39.0283 -0.4239 248.3145 248.7384 267.4545 39.8265 -0.4224 248.4772 248.8996 267.5383 40.6248 -0.4206 248.6390 249.0597 267.6348 41.4128 -0.4183 248.8016 249.2199 267.7338 42.2420 -0.4164 248.9678 249.3841 267.8416 43.0090 -0.4157 249.1235 249.5392 267.9466 43.8693 -0.4150 249.3016 249.7166 268.0784 44.6578 -0.4143 249.4634 249.8777 268.2045 45.4560 -0.4138 249.6266 250.0404 268.3433 46.2853 -0.4142 249.7976 250.2118 268.4920 47.0530 -0.4147 249.9525 250.3672 268.6348 47.8823 -0.4148 250.1198 250.5347 268.8008 48.6390 -0.4154 250.2639 250.6793 268.9634 49.4993 -0.4151 250.4344 250.8495 269.1506 50.2563 -0.4154 250.5855 251.0009 269.3236 51.0755 -0.4158 250.7440 251.1598 269.5132 51.8740 -0.4162 250.8967 251.3128 269.7155 52.6618 -0.4164 251.0560 251.4724 269.9172 53.4708 -0.4172 251.2170 251.6342 270.1337 54.2588 -0.4185 251.3700 251.7885 270.3478 55.0778 -0.4200 251.5285 251.9485 270.5706 55.8453 -0.4205 251.6791 252.0996 270.7888 56.6953 -0.4224 251.8440 252.2663 271.0375 57.4730 -0.4234 251.9893 252.4127 271.2765 58.2918 -0.4255 252.1502 252.5757 271.5289 59.0800 -0.4270 252.3055 252.7325 271.7762 59.8888 -0.4292 252.4664 252.8956 272.0355 60.6768 -0.4322 252.6186 253.0508 272.2985 61.4753 -0.4354 252.7730 253.2084 272.5682 62.2943 -0.4384 252.9275 253.3659 272.8464 63.0723 -0.4411 253.0763 253.5174 273.1115 63.9223 -0.4446 253.2366 253.6812 273.4085 64.6790 -0.4477 253.3759 253.8236 273.6787 65.5190 -0.4518 253.5362 253.9881 273.9771 66.3070 -0.4551 253.6928 254.1479 274.2670 67.1053 -0.4589 253.8460 254.3049 274.5586 67.9243 -0.4623 254.0085 254.4708 274.8565 68.7020 -0.4660 254.1586 254.6246 275.1409 69.5518 -0.4702 254.3235 254.7937 275.4514 70.3193 -0.4741 254.4760 254.9501 275.7318 71.1488 -0.4779 254.6446 255.1225 276.0378 71.9058 -0.4825 254.7960 255.2785 276.3176 72.7453 -0.4876 254.9571 255.4447 276.6268 73.5338 -0.4928 255.1005 255.5933 276.9155 74.3320 -0.4986 255.2552 255.7537 277.2088 75.1610 -0.5043 255.4197 255.9240 277.5060 75.9283 -0.5095 255.5705 256.0800 277.7791 76.7783 -0.5141 255.7390 256.2531 278.0862 77.5563 -0.5189 255.8985 256.4174 278.3626 78.3753 -0.5235 256.0639 256.5874 278.6477 79.1735 -0.5297 256.2198 256.7494 278.9322 79.9718 -0.5353 256.3779 256.9132 279.2063 80.7908 -0.5404 256.5413 257.0817 279.4863 81.5580 -0.5450 256.6875 257.2325 279.7419 82.4080 -0.5509 256.8546 257.4055 280.0213 83.1650 -0.5560 257.0014 257.5574 280.2659 84.0048 -0.5621 257.1625 257.7246 280.5353 84.7618 -0.5672 257.3108 257.8780 280.7709 85.5910 -0.5719 257.4753 258.0472 281.0315 86.3793 -0.5774 257.6362 258.2136 281.2682 87.1775 -0.5826 257.7982 258.3807 281.5044 88.0070 -0.5878 257.9653 258.5532 281.7412 88.7640 -0.5931 258.1168 258.7099 281.9530 89.6243 -0.6001 258.2830 258.8830 282.1870 90.3813 -0.6059 258.4341 259.0399 282.3897 91.2110 -0.6121 258.6043 259.2165 282.6090 92.0093 -0.6184 258.7657 259.3841 282.8132 92.7970 -0.6245 258.9251 259.5495 283.0105 93.6263 -0.6303 259.0918 259.7221 283.2079 94.3938 -0.6365 259.2507 259.8872 283.3832 95.2540 -0.6427 259.4227 260.0654 283.5792 95.9903 -0.6476 259.5730 260.2207 283.7359 96.8508 -0.6537 259.7414 260.3950 283.9176 97.6180 -0.6589 259.8930 260.5519 284.0727 98.4473 -0.6642 260.0624 260.7266 284.2339 99.2353 -0.6691 260.2197 260.8888 284.3757 100.0335 -0.6747 260.3760 261.0507 284.5202 100.8633 -0.6798 260.5494 261.2293 284.6644 101.6200 -0.6849 260.7028 261.3877 284.7866 102.4803 -0.6906 260.8806 261.5712 284.9202 103.2478 -0.6959 261.0352 261.7311 285.0371 104.0773 -0.7010 261.2070 261.9081 285.1540 104.8653 -0.7050 261.3691 262.0742 285.2633 105.6635 -0.7099 261.5318 262.2416 285.3689 106.4620 -0.7149 261.6944 262.4093 285.4676 107.2708 -0.7187 261.8596 262.5783 285.5638 108.0895 -0.7238 262.0249 262.7487 285.6554 108.8673 -0.7283 262.1864 262.9147 285.7374 109.7173 -0.7329 262.3644 263.0973 285.8224 110.4740 -0.7372 262.5191 263.2562 285.8947 111.3138 -0.7419 262.6887 263.4306 285.9689 112.1020 -0.7458 262.8507 263.5965 286.0376 112.9108 -0.7500 263.0130 263.7630 286.1023 113.7298 -0.7545 263.1812 263.9356 286.1571 114.4970 -0.7583 263.3403 264.0986 286.2054 115.3470 -0.7627 263.5167 264.2794 286.2583 116.1040 -0.7661 263.6718 264.4379 286.3029 116.9333 -0.7690 263.8432 264.6122 286.3514 117.7318 -0.7733 264.0068 264.7801 286.3909 118.5300 -0.7775 264.1692 264.9467 286.4242 119.3183 -0.7809 264.3277 265.1086 286.4583 120.1060 -0.7839 264.4848 265.2687 286.4980 120.9353 -0.7877 264.6547 265.4423 286.5331 121.7028 -0.7906 264.8114 265.6020 286.5562 122.5630 -0.7936 264.9827 265.7763 286.5890 123.3203 -0.7969 265.1385 265.9354 286.6094 124.1495 -0.8001 265.3075 266.1076 286.6266 124.9480 -0.8027 265.4712 266.2739 286.6386 125.7360 -0.8052 265.6317 266.4369 286.6551 126.5653 -0.8086 265.8003 266.6089 286.6694 127.3330 -0.8117 265.9558 266.7675 286.6853 128.1933 -0.8144 266.1260 266.9403 286.6969 128.9508 -0.8166 266.2793 267.0958 286.7074 129.7800 -0.8190 266.4430 267.2620 286.7223 130.5785 -0.8208 266.6042 267.4250 286.7336 131.3668 -0.8232 266.7617 267.5849 286.7485 132.1960 -0.8255 266.9256 267.7511 286.7591 132.9638 -0.8284 267.0788 267.9072 286.7708 133.8240 -0.8314 267.2518 268.0832 286.7802 134.5808 -0.8335 267.4029 268.2364 286.7897 135.4105 -0.8361 267.5648 268.4010 286.8006 136.2085 -0.8381 267.7246 268.5628 286.8122 137.0068 -0.8405 267.8838 268.7243 286.8307 137.8363 -0.8430 268.0494 268.8924 286.8485 138.5930 -0.8453 268.2013 269.0467 286.8614 139.4533 -0.8474 268.3712 269.2186 286.8840 140.2210 -0.8492 268.5282 269.3774 286.9002 141.0503 -0.8511 268.6897 269.5407 286.9253 141.8383 -0.8528 268.8452 269.6981 286.9536 142.6370 -0.8545 269.0070 269.8615 286.9760 143.4663 -0.8563 269.1706 270.0269 287.0090 144.2233 -0.8586 269.3173 270.1759 287.0381 145.0840 -0.8602 269.4837 270.3439 287.0815 145.8510 -0.8616 269.6308 270.4923 287.1164 146.6805 -0.8633 269.7862 270.6495 287.1596 147.4688 -0.8649 269.9423 270.8072 287.2040 148.2568 -0.8671 270.0944 270.9615 287.2525 149.0860 -0.8697 270.2467 271.1165 287.3083 149.8430 -0.8714 270.3871 271.2585 287.3631 150.6825 -0.8730 270.5483 271.4213 287.4306 151.4398 -0.8753 270.6921 271.5673 287.4935 152.2898 -0.8771 270.8546 271.7317 287.5728 153.0570 -0.8790 270.9942 271.8731 287.6394 153.8763 -0.8814 271.1474 272.0288 287.7156 154.6850 -0.8837 271.2970 272.1807 287.7985 155.4728 -0.8857 271.4388 272.3245 287.8833 156.2918 -0.8877 271.5911 272.4788 287.9819 157.0693 -0.8899 271.7385 272.6284 288.0755 157.8883 -0.8924 271.8876 272.7800 288.1815 158.6660 -0.8948 272.0291 272.9238 288.2862 159.5160 -0.8975 272.1842 273.0817 288.4041 160.2833 -0.8995 272.3286 273.2281 288.5179 161.1023 -0.9021 272.4775 273.3795 288.6477 161.9110 -0.9044 272.6208 273.5252 288.7800 162.6988 -0.9067 272.7608 273.6676 288.9098 163.5180 -0.9088 272.9064 273.8152 289.0564 164.2958 -0.9113 273.0438 273.9551 289.2029 165.1458 -0.9148 273.1954 274.1103 289.3616 165.9233 -0.9177 273.3370 274.2547 289.5113 166.7420 -0.9209 273.4877 274.4086 289.6794 167.5403 -0.9241 273.6363 274.5604 289.8464 168.3388 -0.9269 273.7812 274.7081 290.0114 169.1683 -0.9299 273.9327 274.8627 290.1879 169.9253 -0.9329 274.0685 275.0014 290.3555 170.7855 -0.9355 274.2206 275.1561 290.5560 171.5528 -0.9388 274.3579 275.2968 290.7329 172.3718 -0.9420 274.5011 275.4431 290.9291 173.1493 -0.9455 274.6444 275.5899 291.1178 173.9688 -0.9488 274.7917 275.7405 291.3178 174.7668 -0.9530 274.9367 275.8897 291.5240 175.5548 -0.9572 275.0767 276.0339 291.7291 176.3943 -0.9611 275.2271 276.1882 291.9478 177.1513 -0.9641 275.3612 276.3254 292.1484 178.0010 -0.9686 275.5115 276.4800 292.3817 178.7683 -0.9726 275.6491 276.6217 292.5911 179.5873 -0.9762 275.7955 276.7717 292.8187 180.3753 -0.9808 275.9319 276.9127 293.0399 181.1735 -0.9863 276.0766 277.0630 293.2628 181.9923 -0.9912 276.2246 277.2158 293.4925 182.7700 -0.9950 276.3615 277.3565 293.7151 183.6203 -0.9999 276.5113 277.5113 293.9611 184.3460 -1.0040 276.6408 277.6448 294.1747 185.2063 -1.0095 276.7946 277.8040 294.4197 185.9740 -1.0133 276.9317 277.9450 294.6465 186.8033 -1.0175 277.0807 278.0981 294.8920 187.5913 -1.0218 277.2267 278.2485 295.1203 188.3895 -1.0267 277.3717 278.3985 295.3558 189.2188 -1.0315 277.5262 278.5577 295.6007 189.9758 -1.0349 277.6598 278.6947 295.8227 190.8360 -1.0403 277.8123 278.8526 296.0705 191.6033 -1.0456 277.9514 278.9970 296.2921 192.4328 -1.0517 278.0990 279.1508 296.5313 193.1898 -1.0567 278.2363 279.2930 296.7507 194.0190 -1.0621 278.3899 279.4520 296.9879 194.8175 -1.0672 278.5335 279.6007 297.2212 195.6058 -1.0725 278.6772 279.7497 297.4436 196.4350 -1.0782 278.8280 279.9062 297.6703 197.2023 -1.0834 278.9683 280.0517 297.8785 198.0623 -1.0886 279.1234 280.2120 298.1111 198.8198 -1.0937 279.2618 280.3555 298.3134 199.6490 -1.0991 279.4137 280.5128 298.5389 200.4473 -1.1041 279.5608 280.6650 298.7558 201.2350 -1.1098 279.7078 280.8176 298.9613 202.0648 -1.1144 279.8597 280.9741 299.1763 202.8320 -1.1193 280.0004 281.1197 299.3704 203.6923 -1.1250 280.1518 281.2768 299.5854 204.4493 -1.1297 280.2877 281.4174 299.7705 205.2890 -1.1348 280.4438 281.5787 299.9740 206.0768 -1.1404 280.5900 281.7304 300.1634 206.8753 -1.1450 280.7341 281.8791 300.3492 207.7045 -1.1500 280.8868 282.0368 300.5483 208.4720 -1.1545 281.0333 282.1878 300.7199 209.3323 -1.1602 281.1976 282.3578 300.9118 210.0890 -1.1647 281.3405 282.5052 301.0715 210.9183 -1.1704 281.4914 282.6618 301.2437 211.7168 -1.1759 281.6452 282.8211 301.4044 212.5153 -1.1811 281.7978 282.9789 301.5587 213.3343 -1.1866 281.9534 283.1400 301.7187 214.1015 -1.1913 282.0934 283.2847 301.8643 214.9308 -1.1970 282.2535 283.4505 302.0233 215.6880 -1.2017 282.3974 283.5991 302.1665 216.5483 -1.2061 282.5568 283.7628 302.3219 217.3158 -1.2105 282.6999 283.9104 302.4558 218.1450 -1.2152 282.8597 284.0749 302.5969 218.9330 -1.2194 283.0104 284.2298 302.7245 219.7315 -1.2234 283.1631 284.3865 302.8543 220.5608 -1.2285 283.3228 284.5514 302.9814 221.3178 -1.2333 283.4676 284.7009 303.0951 222.1780 -1.2381 283.6262 284.8642 303.2211 222.9450 -1.2421 283.7698 285.0119 303.3299 223.7743 -1.2462 283.9269 285.1732 303.4375 224.5623 -1.2503 284.0766 285.3270 303.5433 225.3610 -1.2541 284.2329 285.4870 303.6498 226.1903 -1.2582 284.3977 285.6559 303.7535 226.9470 -1.2626 284.5414 285.8040 303.8435 227.8073 -1.2672 284.7081 285.9753 303.9393 228.5748 -1.2712 284.8520 286.1231 304.0238 229.4043 -1.2745 285.0046 286.2791 304.1179 230.1923 -1.2778 285.1566 286.4344 304.2039 230.9905 -1.2811 285.3112 286.5923 304.2877 231.8200 -1.2851 285.4703 286.7554 304.3742 232.5770 -1.2886 285.6129 286.9014 304.4440 233.4373 -1.2926 285.7759 287.0684 304.5215 234.2048 -1.2957 285.9211 287.2168 304.5847 235.0340 -1.2992 286.0831 287.3823 304.6523 235.8220 -1.3024 286.2321 287.5344 304.7205 236.6205 -1.3055 286.3843 287.6898 304.7857 237.4498 -1.3098 286.5397 287.8495 304.8517 238.2068 -1.3129 286.6791 287.9919 304.9077 239.0670 -1.3164 286.8423 288.1587 304.9730 239.8348 -1.3188 286.9907 288.3095 305.0289 240.6640 -1.3221 287.1506 288.4727 305.0851 241.4520 -1.3248 287.2997 288.6245 305.1396 242.2505 -1.3270 287.4517 288.7787 305.1937 243.0798 -1.3311 287.6141 288.9452 305.2483 243.8368 -1.3338 287.7642 289.0980 305.3018 244.6973 -1.3369 287.9305 289.2675 305.3598 245.4648 -1.3396 288.0729 289.4125 305.4049 246.2940 -1.3424 288.2279 289.5704 305.4597 247.0920 -1.3446 288.3748 289.7194 305.5111 247.8903 -1.3478 288.5234 289.8713 305.5588 248.7093 -1.3506 288.6778 290.0283 305.6078 249.4870 -1.3525 288.8239 290.1764 305.6567 250.3368 -1.3552 288.9823 290.3375 305.7133 251.0938 -1.3575 289.1225 290.4800 305.7618 251.9333 -1.3601 289.2830 290.6431 305.8101 252.7215 -1.3628 289.4288 290.7916 305.8605 253.5200 -1.3650 289.5762 290.9412 305.9128 254.3390 -1.3670 289.7255 291.0926 305.9700 255.1170 -1.3693 289.8699 291.2393 306.0282 255.9668 -1.3724 290.0277 291.4000 306.0908 256.7345 -1.3741 290.1720 291.5461 306.1473 257.5638 -1.3756 290.3319 291.7075 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