DTA measure 1Pb_1 Date: 2025916:1124 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.10 s Mass = 100.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1375 -0.1233 237.2243 237.3476 271.7445 1.9338 -0.1215 237.4892 237.6107 271.7592 2.7613 -0.1232 237.7233 237.8466 271.7871 3.5273 -0.1216 237.9568 238.0784 271.8457 4.3850 -0.1241 238.2338 238.3580 271.9471 5.1510 -0.1241 238.4751 238.5992 272.0679 5.9785 -0.1202 238.7528 238.8730 272.2014 6.7748 -0.1190 238.9967 239.1156 272.3628 7.5715 -0.1165 239.2345 239.3510 272.5148 8.3888 -0.1136 239.4988 239.6124 272.6808 9.1645 -0.1142 239.7641 239.8783 272.8841 10.0125 -0.1088 240.0082 240.1170 273.1392 10.7785 -0.1108 240.2543 240.3650 273.4011 11.6055 -0.1152 240.5453 240.6605 273.6983 12.3920 -0.1202 240.7796 240.8998 273.9665 13.1888 -0.1237 241.0137 241.1374 274.2822 14.0158 -0.1295 241.2747 241.4042 274.6140 14.7715 -0.1340 241.5418 241.6757 274.8847 15.5990 -0.1372 241.7822 241.9194 275.2162 16.3645 -0.1344 242.0155 242.1499 275.5190 17.2230 -0.1357 242.2271 242.3628 275.8662 17.9888 -0.1325 242.4689 242.6014 276.1581 18.8058 -0.1304 242.7126 242.8430 276.4273 19.6025 -0.1380 242.9725 243.1105 276.6763 20.3990 -0.1511 243.2145 243.3656 276.9209 21.2160 -0.1555 243.4585 243.6140 277.1453 21.9925 -0.1615 243.6608 243.8223 277.3540 22.8400 -0.1678 243.9116 244.0794 277.5541 23.6060 -0.1747 244.1494 244.3241 277.7211 24.4335 -0.1770 244.4221 244.5990 277.8511 25.2095 -0.1786 244.6531 244.8317 277.9847 26.0268 -0.1786 244.8702 245.0488 278.0870 26.8233 -0.1806 245.1029 245.2835 278.1368 27.6198 -0.1831 245.3333 245.5164 278.2313 28.4575 -0.1852 245.5798 245.7649 278.2864 29.2130 -0.1887 245.8023 245.9910 278.3229 30.0713 -0.1971 246.0677 246.2648 278.3364 30.8373 -0.2041 246.2836 246.4878 278.3293 31.6643 -0.2109 246.5382 246.7490 278.2865 32.4613 -0.2153 246.7698 246.9851 278.3068 33.2475 -0.2150 247.0126 247.2276 278.2797 34.0850 -0.2171 247.2655 247.4826 278.2595 34.8513 -0.2245 247.4976 247.7221 278.2487 35.6783 -0.2292 247.7220 247.9512 278.2496 36.4340 -0.2337 247.9295 248.1632 278.2437 37.3023 -0.2319 248.1643 248.3962 278.2198 38.0578 -0.2304 248.3839 248.6144 278.2444 38.8953 -0.2333 248.6017 248.8350 278.2621 39.6820 -0.2330 248.8305 249.0636 278.2524 40.4885 -0.2338 249.0660 249.2999 278.2806 41.3058 -0.2367 249.3214 249.5581 278.3448 42.0718 -0.2417 249.5773 249.8189 278.3398 42.9298 -0.2449 249.8304 250.0753 278.4242 43.6855 -0.2492 250.0456 250.2948 278.5325 44.5025 -0.2514 250.2774 250.5288 278.6818 45.3095 -0.2522 250.4828 250.7350 278.8427 46.0958 -0.2517 250.6996 250.9513 279.0312 46.9230 -0.2566 250.8857 251.1422 279.2473 47.6888 -0.2625 251.0953 251.3578 279.4516 48.5163 -0.2688 251.2995 251.5683 279.6786 49.2820 -0.2713 251.5149 251.7861 279.9182 50.1298 -0.2744 251.7940 252.0684 280.1470 50.9060 -0.2800 251.9935 252.2735 280.3888 51.7230 -0.2873 252.2253 252.5125 280.6545 52.5195 -0.2951 252.4584 252.7535 280.9370 53.3160 -0.3009 252.6744 252.9752 281.2293 54.1435 -0.3035 252.9089 253.2124 281.5358 54.9090 -0.3070 253.1075 253.4145 281.8228 55.7573 -0.3138 253.3437 253.6575 282.1290 56.5333 -0.3199 253.5819 253.9018 282.4048 57.3503 -0.3289 253.8112 254.1401 282.6591 58.1470 -0.3372 253.9970 254.3342 282.9099 58.9435 -0.3464 254.1989 254.5453 283.1884 59.7705 -0.3546 254.4522 254.8068 283.4480 60.5365 -0.3639 254.6563 255.0202 283.6467 61.3845 -0.3684 254.8394 255.2079 283.8733 62.1605 -0.3740 255.0543 255.4283 284.0300 62.9878 -0.3787 255.2399 255.6186 284.2110 63.7845 -0.3816 255.4620 255.8436 284.3308 64.5705 -0.3884 255.6913 256.0797 284.4704 65.4085 -0.3958 255.9265 256.3223 284.5780 66.1743 -0.3998 256.1273 256.5272 284.6042 67.0323 -0.4016 256.3592 256.7607 284.6435 67.7880 -0.4080 256.5757 256.9838 284.6447 68.6255 -0.4111 256.7889 257.2000 284.6671 69.4118 -0.4163 256.9759 257.3921 284.7047 70.2085 -0.4230 257.1714 257.5944 284.7328 71.0358 -0.4267 257.4073 257.8340 284.7203 71.8120 -0.4310 257.6221 258.0532 284.6869 72.6600 -0.4364 257.8332 258.2696 284.6767 73.4255 -0.4482 258.0169 258.4651 284.6674 74.2530 -0.4530 258.2039 258.6569 284.6456 75.0395 -0.4526 258.3891 258.8417 284.6424 75.8255 -0.4579 258.6076 259.0655 284.6614 76.6635 -0.4635 258.8292 259.2927 284.6706 77.4190 -0.4690 259.0607 259.5297 284.6653 78.2770 -0.4752 259.3027 259.7779 284.6888 79.0433 -0.4786 259.4743 259.9529 284.6963 79.8600 -0.4790 259.7119 260.1910 284.7634 80.6568 -0.4831 259.9210 260.4042 284.8462 81.4535 -0.4865 260.1378 260.6243 284.9578 82.2500 -0.4930 260.3438 260.8368 285.0585 83.0468 -0.4946 260.5066 261.0012 285.1856 83.8638 -0.4967 260.7099 261.2067 285.3036 84.6398 -0.4979 260.9239 261.4218 285.4516 85.4880 -0.5032 261.1542 261.6574 285.6325 86.2535 -0.5107 261.3393 261.8500 285.8245 87.0810 -0.5136 261.5368 262.0504 286.0691 87.8778 -0.5181 261.7125 262.2306 286.3228 88.6740 -0.5268 261.8898 262.4167 286.5356 89.4913 -0.5302 262.0901 262.6204 286.8043 90.2675 -0.5363 262.2802 262.8165 287.0690 91.1150 -0.5402 262.4793 263.0195 287.3711 91.8913 -0.5445 262.6833 263.2278 287.6249 92.7085 -0.5543 262.9006 263.4548 287.9149 93.5150 -0.5603 263.0616 263.6219 288.1811 94.3018 -0.5658 263.2346 263.8004 288.4470 95.1290 -0.5719 263.4514 264.0233 288.7456 95.8948 -0.5753 263.6131 264.1884 288.9611 96.7530 -0.5850 263.8172 264.4022 289.2410 97.5188 -0.5913 263.9957 264.5871 289.4754 98.3358 -0.5951 264.1943 264.7895 289.7218 99.1428 -0.6021 264.4161 265.0182 289.9150 99.9290 -0.6100 264.5964 265.2064 290.0995 100.7565 -0.6183 264.8223 265.4405 290.2708 101.5533 -0.6300 265.0033 265.6334 290.4640 102.3805 -0.6355 265.2089 265.8445 290.6166 103.1773 -0.6420 265.3944 266.0365 290.7435 103.9635 -0.6488 265.5741 266.2229 290.8507 104.8013 -0.6539 265.7546 266.4085 290.9543 105.5570 -0.6590 265.9168 266.5758 291.0368 106.4150 -0.6680 266.1506 266.8186 291.1108 107.1503 -0.6733 266.3421 267.0155 291.1260 107.9980 -0.6819 266.5587 267.2406 291.1763 108.7640 -0.6849 266.7483 267.4331 291.1862 109.5915 -0.6847 266.9438 267.6284 291.1972 110.3878 -0.6885 267.1009 267.7894 291.1746 111.1845 -0.6914 267.2636 267.9550 291.1706 112.0018 -0.6963 267.4912 268.1875 291.1490 112.7775 -0.7049 267.6892 268.3942 291.1232 113.5948 -0.7105 267.8786 268.5890 291.1351 114.3813 -0.7148 268.0546 268.7694 291.1414 115.2188 -0.7228 268.2647 268.9875 291.1447 115.9748 -0.7283 268.4248 269.1532 291.1440 116.8018 -0.7322 268.6020 269.3341 291.1610 117.5985 -0.7356 268.8005 269.5360 291.2070 118.3953 -0.7379 268.9871 269.7250 291.2709 119.2223 -0.7410 269.1902 269.9312 291.2965 119.9780 -0.7500 269.3530 270.1030 291.3471 120.8465 -0.7566 269.5388 270.2954 291.4774 121.6120 -0.7615 269.6956 270.4570 291.5955 122.4395 -0.7692 269.8954 270.6646 291.7281 123.2260 -0.7707 270.0872 270.8579 291.8486 124.0325 -0.7728 270.2865 271.0593 292.0007 124.8498 -0.7793 270.4560 271.2353 292.1609 125.6260 -0.7847 270.6561 271.4408 292.3930 126.4428 -0.7866 270.8691 271.6557 292.6038 127.2190 -0.7852 271.0524 271.8376 292.8128 128.0670 -0.7901 271.2273 272.0174 293.0854 128.8428 -0.7970 271.3890 272.1861 293.3694 129.6600 -0.8038 271.5510 272.3548 293.6525 130.4670 -0.8083 271.7620 272.5703 293.9277 131.2530 -0.8183 271.9776 272.7959 294.2098 132.0908 -0.8231 272.1773 273.0004 294.5225 132.8465 -0.8263 272.3235 273.1498 294.8086 133.7145 -0.8344 272.5164 273.3508 295.1108 134.4703 -0.8393 272.6867 273.5259 295.3555 135.2978 -0.8434 272.8847 273.7280 295.5970 136.0943 -0.8524 273.0836 273.9360 295.8396 136.8910 -0.8611 273.2729 274.1341 296.1056 137.7183 -0.8688 273.4343 274.3031 296.3558 138.4738 -0.8770 273.6131 274.4900 296.5428 139.3013 -0.8825 273.8107 274.6933 296.7319 140.0670 -0.8903 274.0023 274.8927 296.9011 140.9150 -0.8975 274.1818 275.0793 297.0622 141.6810 -0.9002 274.3719 275.2721 297.1598 142.5083 -0.9057 274.5239 275.4296 297.2713 143.2948 -0.9118 274.6960 275.6078 297.3559 144.1015 -0.9169 274.8799 275.7968 297.4018 144.9185 -0.9253 275.0728 275.9981 297.4397 145.6845 -0.9325 275.2450 276.1776 297.4985 146.5425 -0.9405 275.4660 276.4065 297.5562 147.3085 -0.9448 275.6434 276.5882 297.5413 148.1360 -0.9459 275.8340 276.7799 297.5310 148.8915 -0.9506 275.9544 276.9049 297.5348 149.7293 -0.9597 276.1101 277.0697 297.5148 150.5155 -0.9649 276.2761 277.2410 297.5583 151.3120 -0.9651 276.4658 277.4309 297.5837 152.1398 -0.9730 276.6280 277.6010 297.5790 152.9053 -0.9828 276.7909 277.7736 297.5947 153.7638 -0.9877 276.9628 277.9505 297.6154 154.5295 -0.9911 277.1375 278.1286 297.6317 155.3565 -0.9929 277.3407 278.3336 297.6572 156.1533 -0.9937 277.5127 278.5063 297.6720 156.9500 -0.9939 277.6647 278.6586 297.7053 157.7668 -1.0022 277.8305 278.8327 297.7784 158.5430 -1.0057 278.0245 279.0302 297.8506 159.3910 -1.0168 278.1654 279.1821 297.9384 160.1565 -1.0205 278.3556 279.3761 298.0277 160.9840 -1.0263 278.5604 279.5867 298.1722 161.7910 -1.0335 278.7312 279.7647 298.2972 162.5770 -1.0404 278.9124 279.9528 298.4436 163.4048 -1.0409 279.0898 280.1307 298.6331 164.1705 -1.0424 279.2837 280.3261 298.7851 165.0285 -1.0459 279.4531 280.4990 298.9876 165.7945 -1.0497 279.6145 280.6642 299.2278 166.6115 -1.0585 279.7845 280.8430 299.5089 167.4185 -1.0656 279.9597 281.0253 299.7743 168.2050 -1.0717 280.1133 281.1850 300.0195 169.0423 -1.0846 280.3002 281.3848 300.2372 169.7980 -1.0922 280.4403 281.5325 300.5006 170.6663 -1.0962 280.6172 281.7133 300.7923 171.4218 -1.1025 280.7634 281.8660 301.0540 172.2388 -1.1030 280.9186 282.0216 301.3955 173.0458 -1.1058 281.1086 282.2144 301.6789 173.8320 -1.1083 281.2600 282.3684 301.9225 174.6490 -1.1089 281.4384 282.5474 302.1925 175.4253 -1.1166 281.6180 282.7346 302.4227 176.2423 -1.1226 281.7990 282.9216 302.6315 177.0083 -1.1291 281.9541 283.0832 302.8428 177.8665 -1.1283 282.1174 283.2457 303.0138 178.6218 -1.1329 282.2823 283.4152 303.1585 179.4495 -1.1373 282.4893 283.6265 303.3314 180.2460 -1.1444 282.6781 283.8225 303.4929 181.0428 -1.1536 282.8576 284.0112 303.6341 181.8703 -1.1574 283.0140 284.1714 303.7606 182.6255 -1.1607 283.1768 284.3374 303.8409 183.4940 -1.1619 283.3381 284.5000 303.8935 184.2498 -1.1682 283.4965 284.6647 303.9214 185.0768 -1.1736 283.6637 284.8373 303.9460 185.8738 -1.1789 283.8368 285.0157 303.9492 186.6703 -1.1817 284.0333 285.2149 303.9941 187.4975 -1.1866 284.2268 285.4134 304.0383 188.2535 -1.1949 284.3896 285.5845 304.0243 189.1215 -1.2025 284.5501 285.7526 304.0294 189.9080 -1.2046 284.7076 285.9122 304.0301 190.7048 -1.2080 284.9131 286.1211 304.0458 191.5320 -1.2111 285.0777 286.2888 304.0856 192.3083 -1.2168 285.2382 286.4550 304.1034 193.1560 -1.2195 285.4091 286.6286 304.1110 193.9218 -1.2138 285.5470 286.7609 304.0995 194.7493 -1.2176 285.7078 286.9255 304.0977 195.5253 -1.2224 285.8498 287.0722 304.1295 196.3423 -1.2263 286.0246 287.2509 304.2064 197.1390 -1.2286 286.1921 287.4207 304.2682 197.9355 -1.2336 286.3459 287.5795 304.3684 198.7628 -1.2401 286.5150 287.7552 304.4674 199.5288 -1.2442 286.6851 287.9293 304.5945 200.3765 -1.2437 286.8594 288.1031 304.7360 201.1528 -1.2479 287.0292 288.2771 304.8472 201.9700 -1.2538 287.2095 288.4632 305.0092 202.7663 -1.2608 287.3988 288.6596 305.1893 203.5630 -1.2662 287.5483 288.8145 305.3985 204.3905 -1.2711 287.7183 288.9894 305.6301 205.1458 -1.2725 287.8688 289.1413 305.8921 206.0043 -1.2794 288.0374 289.3167 306.1505 206.7700 -1.2853 288.1685 289.4538 306.3901 207.5870 -1.2925 288.3166 289.6091 306.6466 208.3840 -1.2957 288.4851 289.7809 306.9030 209.1803 -1.3006 288.6273 289.9279 307.1657 209.9770 -1.3123 288.7800 290.0923 307.4483 210.7635 -1.3182 288.9446 290.2628 307.7349 211.6010 -1.3223 289.0989 290.4212 308.0892 212.3568 -1.3278 289.2432 290.5709 308.3472 213.2148 -1.3342 289.4443 290.7785 308.6361 213.9808 -1.3397 289.6119 290.9516 308.8749 214.8083 -1.3489 289.7992 291.1481 309.1037 215.6045 -1.3552 289.9845 291.3396 309.2757 216.3910 -1.3598 290.1815 291.5413 309.4675 217.2288 -1.3607 290.3640 291.7247 309.6642 217.9843 -1.3651 290.4943 291.8595 309.8034 218.8220 -1.3674 290.6753 292.0427 309.9230 219.5775 -1.3716 290.8052 292.1768 310.0498 220.4458 -1.3765 290.9833 292.3598 310.1595 221.2015 -1.3838 291.1556 292.5394 310.2151 222.0288 -1.3890 291.3190 292.7080 310.2796 222.8253 -1.3922 291.4535 292.8457 310.3094 223.6323 -1.3955 291.5987 292.9941 310.3144 224.4493 -1.3981 291.7590 293.1572 310.3388 225.2150 -1.4026 291.9323 293.3348 310.3488 226.0733 -1.4108 292.1170 293.5278 310.3676 226.8390 -1.4127 292.2957 293.7083 310.3866 227.6665 -1.4134 292.4951 293.9086 310.3552 228.4530 -1.4172 292.6715 294.0886 310.3539 229.2595 -1.4239 292.8259 294.2497 310.3505 230.0870 -1.4291 293.0093 294.4385 310.3254 230.8530 -1.4365 293.1710 294.6075 310.3182 231.6698 -1.4387 293.2898 294.7285 310.3499 232.4460 -1.4429 293.4470 294.8899 310.3808 233.2940 -1.4484 293.6219 295.0703 310.3907 234.0598 -1.4533 293.7916 295.2449 310.4072 234.8873 -1.4602 293.9344 295.3946 310.4617 235.6838 -1.4620 294.0738 295.5357 310.5624 236.4805 -1.4649 294.2459 295.7108 310.6645 237.2978 -1.4677 294.3930 295.8607 310.7651 238.0633 -1.4695 294.5490 296.0185 310.8909 238.9218 -1.4715 294.6757 296.1472 311.0113 239.6465 -1.4715 294.7690 296.2405 311.1763 240.5148 -1.4742 294.9214 296.3956 311.4016 241.2705 -1.4737 295.0931 296.5668 311.6008 242.0978 -1.4783 295.2803 296.7586 311.8494 242.8945 -1.4806 295.4405 296.9210 312.1209 243.6913 -1.4826 295.5901 297.0727 312.3725 244.5183 -1.4887 295.7734 297.2621 312.6111 245.2743 -1.4952 295.9688 297.4640 312.8722 246.1425 -1.4984 296.1158 297.6142 313.1432 246.8978 -1.5077 296.2471 297.7548 313.4165 247.7255 -1.5135 296.4064 297.9199 313.7367 248.5220 -1.5131 296.5701 298.0832 314.0058 249.3185 -1.5170 296.7440 298.2610 314.2815 250.1153 -1.5225 296.9336 298.4561 314.5484 250.9015 -1.5303 297.1028 298.6330 314.7894 251.7390 -1.5361 297.2628 298.7989 315.0674 252.4948 -1.5408 297.4169 298.9576 315.2962 253.3528 -1.5472 297.5989 299.1461 315.5186 254.1188 -1.5510 297.7593 299.3102 315.6936 254.9565 -1.5607 297.9261 299.4868 315.8891 255.7425 -1.5676 298.0897 299.6573 316.0481 256.5393 -1.5746 298.2723 299.8469 316.1698 257.3668 -1.5820 298.4682 300.0502 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