DTA measure 1on_1.dat Date: 2025915:1449 Lower limit = 100.0 C Upper limit = 340.0 C Rate = 10.00 C/min Mtime = 1439.57 s Mass = 100.000 mg data_number = 1788 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1478 -0.8013 100.7043 101.5056 96.0786 1.9033 -0.7979 100.7384 101.5363 96.1059 2.7615 -0.7992 100.7568 101.5559 96.1425 3.5273 -0.7979 100.7534 101.5513 96.1769 4.3548 -0.7966 100.7533 101.5499 96.1818 5.1515 -0.7954 100.7517 101.5471 96.1938 5.9375 -0.7982 100.7507 101.5489 96.1847 6.7753 -0.7977 100.7106 101.5083 96.2295 7.5310 -0.7967 100.6971 101.4938 96.2329 8.3888 -0.7931 100.6734 101.4665 96.2661 9.1548 -0.7970 100.6808 101.4778 96.2678 9.9823 -0.7961 100.6674 101.4635 96.2973 10.7785 -0.7929 100.6545 101.4474 96.3255 11.5653 -0.7881 100.6511 101.4392 96.3791 12.4028 -0.7836 100.6847 101.4683 96.4472 13.1583 -0.7802 100.6653 101.4455 96.4485 14.0168 -0.7773 100.6509 101.4282 96.4769 14.7823 -0.7781 100.6448 101.4229 96.6147 15.6095 -0.7772 100.6562 101.4334 96.7081 16.4063 -0.7745 100.6628 101.4372 96.7922 17.1925 -0.7705 100.6704 101.4410 96.9117 18.0300 -0.7691 100.6900 101.4591 97.0517 18.7960 -0.7655 100.6618 101.4273 97.1429 19.6540 -0.7639 100.6477 101.4116 97.2630 20.3788 -0.7676 100.6229 101.3905 97.3493 21.2473 -0.7658 100.5318 101.2977 97.5155 22.0028 -0.7662 100.5046 101.2708 97.6795 22.8303 -0.7641 100.5325 101.2966 97.8321 23.6578 -0.7671 100.5518 101.3189 98.0198 24.4335 -0.7680 100.5436 101.3115 98.2227 25.2508 -0.7707 100.5450 101.3158 98.4230 26.0168 -0.7691 100.5127 101.2818 98.5862 26.8745 -0.7693 100.4908 101.2600 98.7769 27.6303 -0.7637 100.5196 101.2832 98.9515 28.4578 -0.7600 100.5188 101.2788 99.1685 29.2543 -0.7588 100.5303 101.2891 99.3617 30.0408 -0.7591 100.5399 101.2990 99.5489 30.8680 -0.7592 100.5416 101.3008 99.7620 31.6340 -0.7620 100.5667 101.3287 99.9483 32.4923 -0.7601 100.5842 101.3444 100.1882 33.2580 -0.7598 100.6170 101.3767 100.3569 34.0753 -0.7631 100.6245 101.3876 100.5542 34.8513 -0.7628 100.6291 101.3919 100.7487 35.6683 -0.7609 100.6212 101.3820 100.9405 36.4753 -0.7636 100.5965 101.3601 101.1502 37.2615 -0.7681 100.5870 101.3551 101.3235 38.0993 -0.7724 100.5513 101.3237 101.5167 38.8550 -0.7714 100.5339 101.3054 101.6622 39.7128 -0.7741 100.5480 101.3221 101.8376 40.4788 -0.7790 100.5215 101.3005 101.9721 41.3063 -0.7739 100.5205 101.2944 102.1316 42.1028 -0.7730 100.4951 101.2681 102.2633 42.8995 -0.7704 100.5046 101.2750 102.4080 43.7268 -0.7726 100.5051 101.2777 102.5365 44.4925 -0.7744 100.5436 101.3180 102.6553 45.3510 -0.7771 100.5503 101.3274 102.8080 46.1165 -0.7818 100.5072 101.2890 102.9105 46.9438 -0.7878 100.5232 101.3110 103.0422 47.7405 -0.7905 100.5134 101.3039 103.1340 48.5370 -0.7924 100.5749 101.3673 103.2212 49.3540 -0.7930 100.5911 101.3841 103.3262 50.1303 -0.7940 100.6111 101.4050 103.4435 50.9780 -0.7944 100.6268 101.4212 103.5361 51.7543 -0.7932 100.6082 101.4014 103.6069 52.5715 -0.7979 100.6036 101.4015 103.6790 53.3780 -0.8034 100.6124 101.4158 103.7853 54.1645 -0.8055 100.6037 101.4092 103.8565 55.0023 -0.8089 100.5738 101.3827 103.9483 55.7575 -0.8116 100.5754 101.3870 104.0342 56.6260 -0.8099 100.5671 101.3769 104.1416 57.3818 -0.8146 100.5555 101.3702 104.2423 58.2088 -0.8162 100.5621 101.3783 104.3343 59.0055 -0.8226 100.5381 101.3607 104.4306 59.7920 -0.8214 100.5041 101.3255 104.5136 60.6088 -0.8197 100.5150 101.3347 104.6049 61.3850 -0.8226 100.5535 101.3761 104.6806 62.2330 -0.8251 100.5538 101.3789 104.7516 62.9678 -0.8255 100.5342 101.3597 104.8202 63.8260 -0.8311 100.5835 101.4146 104.8978 64.5818 -0.8303 100.5916 101.4219 104.9539 65.4088 -0.8303 100.5836 101.4139 105.0736 66.2055 -0.8282 100.5811 101.4093 105.1962 67.0023 -0.8308 100.5909 101.4217 105.2908 67.8293 -0.8358 100.6144 101.4502 105.4254 68.5850 -0.8377 100.6238 101.4614 105.5521 69.4535 -0.8427 100.6246 101.4672 105.7299 70.2088 -0.8446 100.6017 101.4463 105.8475 71.0365 -0.8506 100.6183 101.4689 105.9865 71.8330 -0.8527 100.6435 101.4962 106.1377 72.6293 -0.8571 100.6377 101.4947 106.2972 73.4570 -0.8611 100.6454 101.5065 106.4475 74.2228 -0.8638 100.6581 101.5219 106.5759 75.0808 -0.8663 100.6498 101.5160 106.7675 75.8160 -0.8677 100.6683 101.5360 106.9128 76.6740 -0.8666 100.6617 101.5283 107.0575 77.4298 -0.8676 100.6795 101.5472 107.2305 78.2675 -0.8697 100.6652 101.5350 107.3989 79.0638 -0.8746 100.6412 101.5158 107.5249 79.8608 -0.8810 100.6670 101.5479 107.6867 80.6778 -0.8867 100.6668 101.5535 107.8755 81.4538 -0.8893 100.6911 101.5804 108.0244 82.3018 -0.8908 100.7243 101.6151 108.2266 83.0675 -0.8939 100.7278 101.6217 108.3838 83.8950 -0.9066 100.7052 101.6117 108.5747 84.6918 -0.9099 100.7034 101.6133 108.7487 85.4880 -0.9094 100.7190 101.6284 108.8922 86.3055 -0.9116 100.7242 101.6358 109.0546 87.0815 -0.9131 100.7127 101.6257 109.2134 87.9293 -0.9182 100.7498 101.6680 109.3682 88.7055 -0.9204 100.7573 101.6777 109.5120 89.5225 -0.9253 100.7646 101.6898 109.6576 90.3190 -0.9310 100.7690 101.7001 109.7687 91.1158 -0.9356 100.7601 101.6956 109.8915 91.9328 -0.9422 100.7712 101.7133 110.0149 92.6985 -0.9461 100.7869 101.7330 110.1496 93.5570 -0.9498 100.8093 101.7591 110.3240 94.3123 -0.9548 100.8143 101.7690 110.4402 95.1398 -0.9624 100.8254 101.7879 110.5417 95.9365 -0.9623 100.8557 101.8180 110.6486 96.7228 -0.9651 100.8959 101.8610 110.7625 97.5295 -0.9666 100.9281 101.8948 110.8848 98.3160 -0.9710 100.9587 101.9298 111.0134 99.1433 -0.9771 100.9253 101.9024 111.1252 99.9093 -0.9797 100.9252 101.9049 111.2420 100.7673 -0.9808 100.9728 101.9535 111.3345 101.5330 -0.9838 101.0034 101.9872 111.4421 102.3505 -0.9916 101.0036 101.9952 111.5693 103.1570 -0.9959 100.9847 101.9806 111.6867 103.9435 -0.9966 101.0113 102.0080 111.7852 104.7710 -1.0006 101.0515 102.0521 111.8815 105.5365 -1.0026 101.0677 102.0703 112.0072 106.3745 -1.0070 101.0772 102.0842 112.1126 107.1300 -1.0111 101.0946 102.1056 112.2199 107.9880 -1.0122 101.0552 102.0674 112.3140 108.7543 -1.0150 101.1113 102.1263 112.4214 109.5813 -1.0194 101.1657 102.1850 112.5416 110.3780 -1.0264 101.1922 102.2186 112.6683 111.1645 -1.0307 101.1949 102.2256 112.7595 112.0020 -1.0365 101.1851 102.2216 112.8445 112.7580 -1.0383 101.1977 102.2360 112.9563 113.6158 -1.0443 101.2094 102.2537 113.1176 114.3818 -1.0520 101.2588 102.3108 113.2181 115.2093 -1.0583 101.2682 102.3265 113.3628 116.0058 -1.0629 101.2690 102.3319 113.4850 116.7923 -1.0658 101.3178 102.3835 113.6172 117.6298 -1.0697 101.3713 102.4410 113.7387 118.3955 -1.0753 101.3777 102.4530 113.8503 119.2538 -1.0797 101.3623 102.4420 113.9639 120.0093 -1.0849 101.3881 102.4730 114.0968 120.8468 -1.0904 101.4084 102.4988 114.2202 121.6435 -1.0980 101.4361 102.5342 114.3269 122.4400 -1.1012 101.4751 102.5763 114.4804 123.2570 -1.1057 101.5250 102.6307 114.6390 124.0333 -1.1113 101.5451 102.6564 114.7847 124.8810 -1.1147 101.5411 102.6558 114.9496 125.6470 -1.1230 101.5659 102.6889 115.1191 126.4745 -1.1311 101.6056 102.7368 115.2527 127.2605 -1.1364 101.6126 102.7490 115.4099 128.0570 -1.1409 101.6414 102.7822 115.5672 128.8845 -1.1448 101.6536 102.7983 115.7121 129.6400 -1.1463 101.6733 102.8196 115.8822 130.4983 -1.1496 101.7106 102.8602 116.0206 131.2643 -1.1536 101.7065 102.8601 116.1677 132.0913 -1.1587 101.7300 102.8888 116.3743 132.8880 -1.1668 101.7713 102.9381 116.5456 133.6745 -1.1713 101.8099 102.9812 116.7116 134.5118 -1.1762 101.8747 103.0509 116.8933 135.2675 -1.1804 101.9071 103.0875 117.0154 136.1258 -1.1819 101.9460 103.1279 117.1170 136.8915 -1.1898 101.9666 103.1564 117.2494 137.7190 -1.1918 101.9650 103.1569 117.4341 138.5155 -1.1980 101.9975 103.1956 117.5646 139.3018 -1.2038 102.0221 103.2259 117.7002 140.1398 -1.2128 102.0471 103.2600 117.8368 140.8950 -1.2198 102.0599 103.2796 117.9934 141.7533 -1.2269 102.0770 103.3039 118.1237 142.5193 -1.2299 102.1188 103.3487 118.2489 143.3465 -1.2359 102.1279 103.3639 118.3726 144.2663 -1.2448 102.1961 103.4410 118.4867 145.1448 -1.2494 102.2324 103.4819 118.6040 145.9210 -1.2557 102.2683 103.5240 118.7036 146.7690 -1.2595 102.2869 103.5463 118.8176 147.5345 -1.2646 102.3040 103.5686 118.9145 148.3620 -1.2708 102.3344 103.6052 119.0212 149.1588 -1.2737 102.4104 103.6841 119.1554 149.9550 -1.2773 102.4334 103.7107 119.2912 150.7725 -1.2824 102.4612 103.7437 119.4023 151.5485 -1.2893 102.4851 103.7745 119.4648 152.4065 -1.2998 102.5135 103.8132 119.5485 153.1725 -1.3067 102.5622 103.8689 119.6600 153.9895 -1.3120 102.6027 103.9146 119.8117 154.7963 -1.3152 102.6610 103.9762 119.9265 155.5830 -1.3224 102.7029 104.0253 120.0304 156.3998 -1.3293 102.7499 104.0793 120.1599 157.1763 -1.3324 102.7810 104.1135 120.2510 158.0240 -1.3355 102.8280 104.1634 120.3869 158.7898 -1.3433 102.8599 104.2032 120.4733 159.6173 -1.3494 102.9208 104.2702 120.5793 160.3830 -1.3548 102.9250 104.2798 120.7039 161.2103 -1.3568 102.9266 104.2834 120.8167 161.9970 -1.3651 102.9397 104.3048 120.9242 162.8035 -1.3718 102.9894 104.3612 121.1005 163.6208 -1.3771 103.0616 104.4387 121.2344 164.3868 -1.3828 103.1156 104.4985 121.3532 165.2448 -1.3864 103.1265 104.5129 121.5245 166.0108 -1.3943 103.1503 104.5446 121.6651 166.8380 -1.4039 103.1925 104.5964 121.8590 167.5938 -1.4088 103.2441 104.6529 121.9918 168.4315 -1.4166 103.2703 104.6870 122.1433 169.2175 -1.4195 103.3183 104.7378 122.2960 170.0245 -1.4199 103.3382 104.7581 122.4387 170.8415 -1.4275 103.3896 104.8171 122.5617 171.6175 -1.4357 103.3965 104.8322 122.6799 172.4653 -1.4407 103.4328 104.8736 122.8354 173.2110 -1.4480 103.4858 104.9338 122.9789 174.0585 -1.4558 103.5439 104.9997 123.1333 174.8348 -1.4630 103.5557 105.0187 123.2785 175.6623 -1.4709 103.5869 105.0578 123.4280 176.4585 -1.4786 103.5701 105.0488 123.6006 177.2450 -1.4871 103.6243 105.1115 123.7597 178.0825 -1.4914 103.6946 105.1861 123.9283 178.8483 -1.4903 103.7433 105.2336 124.0685 179.7063 -1.4964 103.7701 105.2665 124.2083 180.4623 -1.5040 103.8170 105.3210 124.3446 181.2995 -1.5114 103.8539 105.3653 124.4961 182.0655 -1.5182 103.8973 105.4155 124.6389 182.8930 -1.5234 103.9621 105.4855 124.7902 183.6790 -1.5279 104.0329 105.5608 124.8935 184.4860 -1.5307 104.0936 105.6243 125.0412 185.3033 -1.5383 104.1525 105.6908 125.1915 186.0790 -1.5423 104.1816 105.7239 125.3283 186.9270 -1.5454 104.2303 105.7758 125.4118 187.6930 -1.5573 104.2942 105.8515 125.5218 188.5100 -1.5660 104.3001 105.8661 125.6502 189.3068 -1.5736 104.3639 105.9375 125.8075 190.0930 -1.5812 104.4324 106.0135 125.9333 190.9098 -1.5876 104.4962 106.0838 126.0479 191.6860 -1.5901 104.4910 106.0810 126.1679 192.5340 -1.5933 104.5188 106.1121 126.2790 193.2893 -1.5970 104.5850 106.1820 126.4073 194.1273 -1.6028 104.6578 106.2605 126.5270 194.9135 -1.6065 104.6991 106.3056 126.6745 195.7100 -1.6124 104.7499 106.3623 126.8086 196.5068 -1.6169 104.7977 106.4146 126.9186 197.3033 -1.6218 104.8785 106.5003 127.0508 198.1308 -1.6277 104.9453 106.5729 127.1461 198.8865 -1.6351 104.9849 106.6200 127.2650 199.7545 -1.6432 105.0222 106.6653 127.3752 200.5105 -1.6463 105.0709 106.7172 127.4882 201.3685 -1.6515 105.0934 106.7448 127.6273 202.2573 -1.6648 105.1383 106.8031 127.7325 203.0540 -1.6749 105.2098 106.8847 127.8086 203.8813 -1.6778 105.2773 106.9551 127.9354 204.7598 -1.6835 105.3446 107.0281 128.0530 205.5975 -1.6893 105.3896 107.0789 128.1826 206.3530 -1.6978 105.4342 107.1320 128.2645 207.2213 -1.7069 105.4920 107.1989 128.3892 207.9463 -1.7107 105.5517 107.2624 128.5084 208.8145 -1.7175 105.6103 107.3278 128.6450 209.5700 -1.7251 105.6505 107.3756 128.7613 210.3978 -1.7327 105.7104 107.4431 128.8929 211.1940 -1.7351 105.7872 107.5224 129.0448 212.0010 -1.7358 105.8393 107.5751 129.1727 212.8183 -1.7410 105.8809 107.6220 129.3228 213.5840 -1.7455 105.9403 107.6858 129.4760 214.4423 -1.7512 106.0216 107.7727 129.6629 215.2183 -1.7584 106.0852 107.8436 129.7832 216.0353 -1.7662 106.1168 107.8830 129.9253 216.8320 -1.7745 106.1730 107.9475 130.0957 217.6285 -1.7847 106.1886 107.9733 130.2495 218.4353 -1.7942 106.2010 107.9952 130.4029 219.2218 -1.7976 106.2131 108.0107 130.5403 220.0388 -1.8020 106.2958 108.0978 130.7096 220.8148 -1.8059 106.3745 108.1804 130.8691 221.6628 -1.8086 106.4613 108.2699 131.0078 222.4285 -1.8161 106.5610 108.3771 131.1531 223.2558 -1.8231 106.6138 108.4368 131.3019 224.0423 -1.8259 106.6453 108.4712 131.4325 224.8388 -1.8322 106.7107 108.5429 131.5717 225.6353 -1.8376 106.7971 108.6347 131.7202 226.4320 -1.8443 106.8224 108.6666 131.8908 227.2593 -1.8473 106.8669 108.7142 132.0537 228.0150 -1.8495 106.9428 108.7922 132.1765 228.8835 -1.8625 107.0415 108.9039 132.3168 229.6388 -1.8691 107.1202 108.9893 132.4284 230.4665 -1.8763 107.1851 109.0613 132.5967 231.2630 -1.8799 107.2489 109.1288 132.7588 232.0595 -1.8861 107.2706 109.1568 132.8992 232.8873 -1.8927 107.3116 109.2043 133.0246 233.6425 -1.8964 107.3722 109.2687 133.1307 234.5110 -1.9012 107.4518 109.3529 133.2602 235.2463 -1.9049 107.4895 109.3944 133.3620 236.1043 -1.9140 107.5671 109.4811 133.4924 236.8600 -1.9218 107.6158 109.5376 133.6188 237.6975 -1.9300 107.7035 109.6335 133.7169 238.4943 -1.9374 107.7637 109.7011 133.8268 239.2910 -1.9426 107.8056 109.7482 133.9647 240.1078 -1.9511 107.8772 109.8283 134.1012 240.8840 -1.9590 107.9562 109.9152 134.2133 241.7320 -1.9699 108.0182 109.9880 134.3611 242.5078 -1.9753 108.1024 110.0778 134.4812 243.3353 -1.9846 108.1621 110.1467 134.6009 244.1320 -1.9836 108.2172 110.2008 134.6782 244.9283 -1.9863 108.2569 110.2432 134.7496 245.7558 -1.9951 108.3375 110.3326 134.8366 246.5218 -2.0031 108.4022 110.4052 134.9276 247.3488 -2.0092 108.4556 110.4648 135.0123 248.1453 -2.0113 108.4877 110.4990 135.1138 249.0345 -2.0186 108.5848 110.6034 135.2375 249.8205 -2.0228 108.6607 110.6835 135.3375 250.6890 -2.0269 108.7448 110.7718 135.4860 251.4550 -2.0320 108.8134 110.8454 135.6150 252.2820 -2.0363 108.9019 110.9382 135.7428 253.0685 -2.0422 108.9844 111.0266 135.8914 253.9883 -2.0506 109.0761 111.1266 136.0417 254.8053 -2.0607 109.1741 111.2348 136.1527 255.5713 -2.0671 109.2792 111.3463 136.2772 256.4293 -2.0729 109.3296 111.4025 136.4301 257.1950 -2.0787 109.3898 111.4686 136.5694 258.0123 -2.0879 109.4729 111.5608 136.7371 258.8088 -2.0927 109.5412 111.6339 136.8919 259.6670 -2.0990 109.6082 111.7072 137.0708 260.4843 -2.1048 109.6815 111.7863 137.2305 261.3215 -2.1095 109.7484 111.8579 137.3873 262.1083 -2.1154 109.8222 111.9375 137.5605 262.9048 -2.1206 109.8723 111.9928 137.6985 263.7323 -2.1309 109.9350 112.0660 137.8756 264.4983 -2.1361 110.0327 112.1688 138.0305 265.3563 -2.1401 110.0810 112.2211 138.1928 266.1120 -2.1469 110.1410 112.2879 138.3512 266.9495 -2.1543 110.2107 112.3650 138.4978 267.7050 -2.1584 110.2818 112.4402 138.6474 268.5428 -2.1620 110.3602 112.5222 138.8097 269.3290 -2.1676 110.4216 112.5893 138.9437 270.1358 -2.1715 110.4987 112.6701 139.1058 270.9530 -2.1777 110.5980 112.7757 139.2640 271.7290 -2.1827 110.6625 112.8452 139.4183 272.5768 -2.1853 110.7073 112.8926 139.5505 273.3530 -2.1899 110.7872 112.9771 139.6867 274.1700 -2.1991 110.8770 113.0761 139.8211 274.9358 -2.2030 110.9459 113.1488 139.9237 275.7635 -2.2064 111.0199 113.2263 140.0603 276.5700 -2.2161 111.0982 113.3143 140.1971 277.3565 -2.2239 111.1593 113.3831 140.3260 278.1840 -2.2330 111.2292 113.4622 140.4495 278.9495 -2.2382 111.3259 113.5642 140.5645 279.8078 -2.2431 111.4296 113.6727 140.7053 280.5738 -2.2429 111.5097 113.7526 140.7975 281.4010 -2.2448 111.6020 113.8468 140.9302 282.1978 -2.2499 111.6677 113.9176 141.0287 283.0045 -2.2544 111.6978 113.9522 141.1379 283.7803 -2.2587 111.7950 114.0537 141.2096 284.6080 -2.2698 111.8965 114.1663 141.3250 285.4045 -2.2805 111.9940 114.2745 141.4272 286.1908 -2.2928 112.0879 114.3807 141.5561 287.0183 -2.2978 112.1689 114.4667 141.6846 287.7840 -2.2983 112.2012 114.4994 141.8043 288.6318 -2.3002 112.2929 114.5931 141.9092 289.3773 -2.3055 112.3599 114.6654 142.0310 290.2250 -2.3108 112.4452 114.7559 142.1629 290.9908 -2.3157 112.5345 114.8502 142.2576 291.8183 -2.3210 112.6023 114.9233 142.3821 292.6148 -2.3303 112.6662 114.9965 142.4884 293.4113 -2.3370 112.7416 115.0786 142.6356 294.2288 -2.3427 112.8313 115.1740 142.7653 295.0045 -2.3487 112.9177 115.2664 142.9101 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