DTA measure 2Pb_1 Date: 2025916:1154 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.00 s Mass = 100.000 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3785 -5.0936 451.4093 456.5030 433.1258 3.9665 -5.1019 451.4035 456.5054 433.3316 5.5751 -5.1148 451.3858 456.5007 433.4844 7.1734 -5.1291 451.4257 456.5548 433.5398 8.7768 -5.1552 451.4239 456.5791 433.4588 10.3853 -5.1629 451.4302 456.5931 433.2891 12.0040 -5.1718 451.4596 456.6314 433.0689 13.6125 -5.1762 451.4612 456.6374 432.7692 15.2160 -5.1784 451.4644 456.6428 432.3389 16.8245 -5.1789 451.5115 456.6905 431.8838 18.4176 -5.1791 451.5316 456.7108 431.4092 20.0263 -5.1786 451.5586 456.7372 430.8319 21.6346 -5.1788 451.5704 456.7492 430.2557 23.2431 -5.1770 451.5436 456.7206 429.7537 24.8620 -5.1829 451.6110 456.7939 429.2134 26.4705 -5.1794 451.5635 456.7429 428.7630 28.0689 -5.1710 451.5267 456.6977 428.3661 29.6724 -5.1651 451.5263 456.6914 428.0511 31.2911 -5.1635 451.5265 456.6900 427.8205 32.8996 -5.1639 451.5211 456.6850 427.6263 34.4775 -5.1615 451.4837 456.6452 427.5610 36.0808 -5.1616 451.4709 456.6326 427.5281 37.6843 -5.1614 451.4616 456.6230 427.5264 39.3031 -5.1623 451.4266 456.5889 427.5628 40.9064 -5.1603 451.3894 456.5497 427.6250 42.5150 -5.1609 451.3146 456.4755 427.6809 44.1184 -5.1680 451.3045 456.4726 427.7134 45.7114 -5.1771 451.2687 456.4458 427.7200 47.3149 -5.1853 451.2439 456.4292 427.6540 48.9236 -5.1853 451.2112 456.3965 427.5484 50.5269 -5.1884 451.1919 456.3803 427.3449 52.1456 -5.1934 451.1640 456.3574 427.1754 53.7544 -5.1954 451.0841 456.2795 426.9081 55.3575 -5.1962 450.9910 456.1871 426.5579 56.9713 -5.1979 450.9897 456.1877 426.2134 58.5746 -5.2011 450.9750 456.1762 425.8270 60.1883 -5.1998 450.9533 456.1532 425.4068 61.7918 -5.1994 450.9040 456.1034 425.0292 63.4156 -5.2016 450.8196 456.0211 424.6623 65.0189 -5.1993 450.7744 455.9737 424.3200 66.6173 -5.1989 450.7114 455.9103 423.9637 68.2204 -5.1950 450.6457 455.8406 423.6370 69.8239 -5.1920 450.5757 455.7676 423.4000 71.4324 -5.1945 450.5119 455.7064 423.1339 73.0358 -5.1948 450.4509 455.6456 422.9094 74.6341 -5.1942 450.3548 455.5490 422.7551 76.2529 -5.1904 450.3062 455.4966 422.6073 77.8561 -5.1916 450.2462 455.4378 422.4892 79.4648 -5.1963 450.1667 455.3630 422.4158 81.0781 -5.1966 450.0963 455.2929 422.3602 82.6868 -5.1970 450.0263 455.2232 422.3169 84.2950 -5.1982 449.9264 455.1246 422.1686 85.9036 -5.1974 449.8536 455.0510 422.0750 87.5123 -5.1949 449.7607 454.9556 421.9169 89.1256 -5.1945 449.6971 454.8916 421.7193 90.7343 -5.2010 449.6194 454.8204 421.5996 92.3376 -5.2048 449.5113 454.7161 421.4175 93.9461 -5.2036 449.4133 454.6169 421.2095 95.5548 -5.2061 449.3331 454.5393 420.9916 97.1579 -5.2050 449.2299 454.4349 420.7932 98.7614 -5.2021 449.1475 454.3496 420.5044 100.3598 -5.2020 449.0435 454.2455 420.1947 101.9629 -5.1982 448.9587 454.1568 419.8828 103.5664 -5.1951 448.8597 454.0549 419.6356 105.1749 -5.1959 448.7622 453.9581 419.3701 106.7783 -5.1987 448.6415 453.8402 419.0824 108.3818 -5.1949 448.4997 453.6946 418.7819 109.9903 -5.1903 448.4171 453.6074 418.5543 111.5936 -5.1884 448.3329 453.5213 418.3347 113.1869 -5.1880 448.2122 453.4002 418.1016 114.7954 -5.1846 448.0832 453.2678 417.8700 116.4193 -5.1865 447.9295 453.1160 417.6412 118.0226 -5.1866 447.8236 453.0102 417.4387 119.6310 -5.1874 447.7216 452.9090 417.2266 121.2398 -5.1881 447.6182 452.8063 417.0471 122.8483 -5.1842 447.4347 452.6188 416.8991 124.4566 -5.1823 447.3495 452.5318 416.7103 126.0654 -5.1831 447.2423 452.4254 416.5819 127.6534 -5.1809 447.1424 452.3233 416.4610 129.2721 -5.1809 447.0313 452.2122 416.2604 130.8755 -5.1829 446.9251 452.1080 416.0593 132.4791 -5.1833 446.7909 451.9743 415.9026 134.0773 -5.1776 446.6382 451.8158 415.7777 135.6858 -5.1728 446.5459 451.7187 415.6035 137.2894 -5.1730 446.4330 451.6060 415.4211 138.8825 -5.1710 446.2936 451.4646 415.1920 140.4859 -5.1681 446.1083 451.2764 415.0087 142.1150 -5.1647 445.9935 451.1581 414.7702 143.7236 -5.1635 445.8633 451.0268 414.4781 145.3168 -5.1654 445.7469 450.9123 414.2262 146.9203 -5.1604 445.6559 450.8163 413.9898 148.5443 -5.1599 445.5199 450.6799 413.7260 150.1373 -5.1601 445.3722 450.5323 413.4690 151.7510 -5.1590 445.1508 450.3098 413.2142 153.3648 -5.1546 445.0018 450.1564 412.9428 154.9680 -5.1528 444.8791 450.0319 412.7344 156.5920 -5.1520 444.7356 449.8876 412.5111 158.1955 -5.1533 444.5386 449.6919 412.2632 159.7989 -5.1484 444.4125 449.5610 412.0647 161.3921 -5.1471 444.3221 449.4692 411.8650 163.0059 -5.1456 444.2353 449.3809 411.6878 164.6040 -5.1429 444.0904 449.2333 411.5022 166.2074 -5.1422 443.9492 449.0914 411.3482 167.8109 -5.1335 443.8039 448.9374 411.1370 169.4141 -5.1242 443.6150 448.7392 410.9817 171.0330 -5.1203 443.4134 448.5336 410.8279 172.6364 -5.1195 443.2228 448.3422 410.6122 174.2396 -5.1201 443.0570 448.1771 410.4195 175.8483 -5.1125 442.9338 448.0463 410.2636 177.4516 -5.1074 442.8086 447.9160 410.0889 179.0601 -5.1087 442.6455 447.7542 409.8809 180.6636 -5.1100 442.5174 447.6274 409.6505 182.2875 -5.1119 442.3669 447.4788 409.4373 183.8960 -5.1111 442.2272 447.3384 409.2527 185.5046 -5.1105 442.0661 447.1767 409.0364 187.1130 -5.1080 441.8612 446.9692 408.8089 188.7215 -5.1047 441.6882 446.7929 408.5868 190.3250 -5.1019 441.5500 446.6520 408.3477 191.9385 -5.1030 441.3708 446.4738 408.0760 193.5574 -5.0952 441.2292 446.3245 407.8342 195.1558 -5.0947 441.0890 446.1837 407.5635 196.7643 -5.0929 440.9522 446.0451 407.3316 198.3473 -5.0911 440.7976 445.8887 407.1021 199.9506 -5.0871 440.6488 445.7359 406.8721 201.5540 -5.0774 440.4690 445.5464 406.6662 203.1676 -5.0733 440.2982 445.3715 406.4386 204.7609 -5.0731 440.1169 445.1901 406.2359 206.3643 -5.0661 439.9236 444.9897 405.9931 207.9934 -5.0582 439.7735 444.8318 405.7222 209.5969 -5.0482 439.6060 444.6541 405.5400 211.1900 -5.0465 439.4430 444.4895 405.3623 212.7934 -5.0452 439.2722 444.3173 405.2063 214.4020 -5.0402 439.0721 444.1124 405.0133 216.0054 -5.0406 438.8795 443.9201 404.8197 217.6139 -5.0416 438.7247 443.7663 404.6723 219.2225 -5.0402 438.5548 443.5949 404.4971 220.8413 -5.0386 438.4040 443.4427 404.2991 222.4394 -5.0349 438.2911 443.3260 404.1199 224.0531 -5.0300 438.1348 443.1647 403.9306 225.6564 -5.0236 437.9600 442.9837 403.7288 227.2549 -5.0253 437.8008 442.8261 403.5311 228.8584 -5.0227 437.5492 442.5719 403.3358 230.4616 -5.0195 437.3717 442.3912 403.1190 232.0496 -5.0169 437.2635 442.2804 402.8611 233.6531 -5.0222 437.0694 442.0916 402.6043 235.2718 -5.0149 436.8747 441.8897 402.4083 236.8804 -5.0043 436.7307 441.7350 402.1802 238.4839 -5.0012 436.5383 441.5395 401.9766 240.0871 -5.0014 436.3554 441.3568 401.7670 241.7009 -4.9946 436.1849 441.1795 401.4993 243.3043 -4.9893 435.9848 440.9741 401.2684 244.9179 -4.9840 435.7945 440.7785 401.0404 246.5368 -4.9835 435.6102 440.5936 400.7678 248.1300 -4.9793 435.4051 440.3845 400.5771 249.7384 -4.9761 435.2047 440.1809 400.3760 251.3470 -4.9751 435.0605 440.0355 400.1158 252.9505 -4.9730 434.8881 439.8611 399.9225 254.5640 -4.9664 434.7008 439.6672 399.7357 256.1675 -4.9601 434.5727 439.5328 399.5735 257.7761 -4.9532 434.3632 439.3164 399.3762 259.3896 -4.9472 434.1418 439.0890 399.1560 260.9931 -4.9485 433.9516 438.9002 398.9247 262.5964 -4.9424 433.8078 438.7502 398.7195 264.1998 -4.9330 433.6784 438.6114 398.5955 265.8084 -4.9315 433.4938 438.4252 398.4199 267.4118 -4.9284 433.3057 438.2341 398.2328 269.0151 -4.9227 433.0866 438.0093 398.0408 270.6393 -4.9181 432.9098 437.8279 397.7952 272.2428 -4.9151 432.6885 437.6036 397.5559 273.8409 -4.9144 432.4963 437.4107 397.3437 275.4598 -4.9076 432.3325 437.2400 397.1150 277.0633 -4.9024 432.1616 437.0640 396.9154 278.6716 -4.9026 431.9440 436.8466 396.6981 280.2803 -4.8970 431.7128 436.6098 396.4868 281.8889 -4.8934 431.5327 436.4260 396.2491 283.4920 -4.8915 431.3898 436.2813 396.0142 285.1211 -4.8881 431.1856 436.0737 395.7488 286.7248 -4.8780 431.0083 435.8863 395.5499 288.3383 -4.8752 430.7834 435.6585 395.3553 289.9418 -4.8767 430.6191 435.4958 395.1179 291.5350 -4.8687 430.4374 435.3062 394.9254 293.1280 -4.8644 430.2594 435.1238 394.7091 294.7315 -4.8573 430.0536 434.9110 394.5157 296.3401 -4.8558 429.8774 434.7332 394.3147 297.9539 -4.8498 429.6582 434.5080 394.0883 299.5419 -4.8428 429.4831 434.3259 393.8953 301.1504 -4.8416 429.3277 434.1693 393.6756 302.7536 -4.8395 429.1340 433.9735 393.4767 304.3623 -4.8332 428.9265 433.7597 393.2994 305.9656 -4.8241 428.7721 433.5962 393.1066 307.5741 -4.8172 428.6259 433.4431 392.8733 309.1776 -4.8148 428.3981 433.2129 392.6873 310.7965 -4.8149 428.1352 432.9501 392.4931 312.4100 -4.8118 427.9279 432.7397 392.2645 314.0135 -4.8076 427.7908 432.5984 392.0238 315.6270 -4.7997 427.6188 432.4186 391.8207 317.2150 -4.7933 427.4143 432.2076 391.6343 318.8288 -4.7943 427.2321 432.0265 391.4433 320.4321 -4.7907 427.0060 431.7967 391.2672 322.0406 -4.7921 426.7822 431.5744 391.0713 323.6595 -4.7853 426.5780 431.3633 390.8681 325.2578 -4.7773 426.4092 431.1865 390.6292 326.8458 -4.7647 426.2272 430.9919 390.4422 328.4493 -4.7657 426.0324 430.7981 390.1580 330.0576 -4.7591 425.8164 430.5755 389.8982 331.6610 -4.7547 425.5863 430.3410 389.6977 333.2696 -4.7509 425.3533 430.1042 389.5026 334.8728 -4.7507 425.1441 429.8948 389.2634 336.4814 -4.7448 424.9804 429.7252 389.0226 338.1000 -4.7318 424.7832 429.5150 388.7748 339.7085 -4.7260 424.5739 429.3000 388.5570 341.3120 -4.7234 424.3852 429.1087 388.3581 342.9254 -4.7207 424.1798 428.9005 388.1633 344.5289 -4.7167 424.0252 428.7419 387.9513 346.1374 -4.7179 423.8306 428.5485 387.7201 347.7304 -4.7071 423.6642 428.3712 387.5502 349.3390 -4.7022 423.4419 428.1441 387.3307 350.9628 -4.6948 423.2584 427.9532 387.1408 352.5713 -4.6874 423.0773 427.7647 386.9537 354.1798 -4.6847 422.8751 427.5598 386.6973 355.7780 -4.6800 422.6557 427.3358 386.4953 357.3815 -4.6802 422.4186 427.0988 386.3111 358.9849 -4.6762 422.2488 426.9250 386.1383 360.5934 -4.6722 422.1185 426.7906 385.9553 362.2123 -4.6747 421.8936 426.5683 385.7505 363.8105 -4.6709 421.7089 426.3798 385.5450 365.4190 -4.6644 421.4919 426.1562 385.3054 367.0225 -4.6577 421.2890 425.9467 385.0489 368.6311 -4.6478 421.1335 425.7813 384.8636 370.2344 -4.6398 420.9198 425.5596 384.6390 371.8430 -4.6316 420.6826 425.3142 384.4702 373.4669 -4.6236 420.4641 425.0877 384.2498 375.0704 -4.6213 420.2556 424.8770 383.9861 376.6790 -4.6225 420.1082 424.7307 383.7793 378.2876 -4.6173 419.9337 424.5510 383.5979 379.8960 -4.6163 419.7243 424.3406 383.3596 381.4994 -4.6112 419.4899 424.1011 383.1356 383.1130 -4.6034 419.2399 423.8433 382.9069 384.7318 -4.5997 419.0317 423.6315 382.6877 386.3404 -4.5911 418.8433 423.4344 382.4602 387.9438 -4.5878 418.6088 423.1966 382.2391 389.5214 -4.5839 418.3424 422.9263 382.0453 391.1301 -4.5814 418.1808 422.7622 381.8246 392.7334 -4.5703 418.0031 422.5735 381.6367 394.3419 -4.5617 417.8287 422.3905 381.4460 395.9454 -4.5569 417.6302 422.1871 381.2249 397.5639 -4.5512 417.4397 421.9909 381.0161 399.1725 -4.5458 417.2350 421.7808 380.8349 400.7756 -4.5443 417.0197 421.5640 380.6040 402.3895 -4.5408 416.8100 421.3508 380.3799 403.9929 -4.5418 416.6257 421.1675 380.2022 405.5859 -4.5415 416.4008 420.9423 380.0292 407.1893 -4.5362 416.1942 420.7304 379.8289 408.8029 -4.5261 415.9851 420.5111 379.6264 410.4216 -4.5222 415.7887 420.3109 379.4831 412.0303 -4.5219 415.6146 420.1365 379.2729 413.6386 -4.5201 415.3954 419.9155 379.0699 415.2471 -4.5166 415.1790 419.6956 378.8226 416.8505 -4.5068 414.9967 419.5034 378.5933 418.4641 -4.5054 414.8291 419.3345 378.3723 420.0624 -4.4981 414.6389 419.1370 378.1140 421.6811 -4.4892 414.4463 418.9355 377.8906 423.2691 -4.4866 414.2475 418.7341 377.7056 424.8725 -4.4804 413.9717 418.4521 377.4809 426.4759 -4.4757 413.7103 418.1861 377.2262 428.0844 -4.4663 413.5381 418.0045 377.0252 429.6879 -4.4571 413.3821 417.8392 376.7920 431.2961 -4.4509 413.1929 417.6438 376.5571 432.8996 -4.4456 412.9864 417.4321 376.3397 434.5235 -4.4389 412.7472 417.1862 376.1450 436.1269 -4.4338 412.5530 416.9868 375.9429 437.7304 -4.4375 412.3610 416.7985 375.6983 439.3391 -4.4348 412.1857 416.6204 375.4998 440.9424 -4.4252 411.9892 416.4144 375.2688 442.5561 -4.4144 411.7863 416.2007 375.0480 444.1595 -4.4091 411.5272 415.9363 374.8432 445.7834 -4.4046 411.3379 415.7425 374.6248 447.3869 -4.3948 411.1187 415.5135 374.4127 449.0006 -4.3916 410.9119 415.3035 374.2079 450.6039 -4.3919 410.7114 415.1033 373.9894 452.2075 -4.3840 410.5135 414.8975 373.7917 453.8059 -4.3802 410.2604 414.6406 373.6254 455.4039 -4.3798 410.0733 414.4531 373.4231 457.0229 -4.3756 409.9167 414.2923 373.1999 458.6315 -4.3676 409.7005 414.0681 373.0229 460.2193 -4.3673 409.4847 413.8520 372.8182 461.8330 -4.3705 409.2815 413.6520 372.6228 463.4365 -4.3650 409.0833 413.4483 372.4463 465.0449 -4.3548 408.8852 413.2400 372.2608 466.6483 -4.3477 408.6984 413.0461 372.0259 468.2570 -4.3419 408.5070 412.8489 371.7951 469.8756 -4.3393 408.3175 412.6568 371.5419 471.4894 -4.3359 408.0972 412.4331 371.3193 473.0929 -4.3321 407.9090 412.2411 371.1081 474.6961 -4.3232 407.7044 412.0276 370.9050 476.3099 -4.3256 407.4912 411.8168 370.6078 477.9134 -4.3201 407.2992 411.6193 370.3915 479.5218 -4.3182 407.1172 411.4355 370.1878 481.1406 -4.3079 406.9000 411.2079 370.0017 482.7544 -4.2996 406.6549 410.9545 369.8403 484.3524 -4.2935 406.4233 410.7168 369.6456 485.9559 -4.2968 406.2360 410.5328 369.4673 487.5593 -4.2886 406.0214 410.3100 369.2697 489.1421 -4.2788 405.8610 410.1398 369.0279 490.7508 -4.2739 405.6448 409.9186 368.7838 492.3541 -4.2747 405.4179 409.6926 368.5390 493.9729 -4.2651 405.1553 409.4204 368.3192 495.5815 -4.2526 404.9212 409.1738 368.0681 497.1851 -4.2436 404.7204 408.9641 367.8665 498.7935 -4.2377 404.5632 408.8009 367.6622 500.3970 -4.2365 404.3578 408.5943 367.4686 502.0056 -4.2320 404.1458 408.3778 367.2372 503.6089 -4.2252 403.9431 408.1683 367.0483 505.2379 -4.2235 403.7699 407.9934 366.8865 506.8413 -4.2216 403.5524 407.7739 366.7113 508.4498 -4.2200 403.2986 407.5186 366.5026 510.0585 -4.2157 403.0947 407.3104 366.2794 511.6620 -4.2079 402.8826 407.0905 366.0996 513.2755 -4.1959 402.6221 406.8180 365.8738 514.8790 -4.1917 402.4241 406.6158 365.6453 516.4979 -4.1915 402.2281 406.4196 365.4358 518.0909 -4.1874 402.0301 406.2175 365.2016 519.6944 -4.1856 401.8413 406.0269 364.9754 521.3031 -4.1822 401.5934 405.7756 364.7802 522.8963 -4.1677 401.3957 405.5634 364.5499 524.5046 -4.1687 401.2015 405.3702 364.3283 526.1081 -4.1587 401.0135 405.1721 364.0781 527.7165 -4.1527 400.8530 405.0057 363.8514 529.3354 -4.1473 400.6685 404.8158 363.6563 530.9386 -4.1399 400.4409 404.5808 363.4707 532.5473 -4.1319 400.2516 404.3834 363.3091 534.1559 -4.1261 400.0608 404.1869 363.0747 535.7644 -4.1234 399.8413 403.9647 362.8478 537.3676 -4.1241 399.6332 403.7572 362.6616 538.9814 -4.1246 399.4059 403.5305 362.4596 540.5999 -4.1161 399.1656 403.2817 362.2503 542.2136 -4.1103 398.9851 403.0954 362.0257 543.8171 -4.1030 398.7718 402.8748 361.8063 545.4255 -4.0943 398.5583 402.6526 361.5824 547.0289 -4.0893 398.3627 402.4520 361.4050 548.6373 -4.0871 398.1604 402.2475 361.2324 550.2406 -4.0809 397.9121 401.9930 361.0312 551.8541 -4.0766 397.6671 401.7437 360.8280 553.4473 -4.0689 397.4778 401.5467 360.6309 555.0506 -4.0621 397.2979 401.3600 360.4243 556.6590 -4.0604 397.0982 401.1586 360.2214 558.2625 -4.0600 396.8929 400.9529 359.9830 559.8659 -4.0594 396.6795 400.7389 359.7542 561.4743 -4.0596 396.5134 400.5730 359.5199 563.0778 -4.0549 396.3289 400.3839 359.2686 564.7016 -4.0471 396.1273 400.1743 359.0896 566.3050 -4.0459 395.9120 399.9580 358.8722 567.9138 -4.0371 395.6886 399.7257 358.6090 569.5223 -4.0356 395.4489 399.4845 358.3832 571.1306 -4.0292 395.2149 399.2440 358.2093 572.7393 -4.0230 394.9820 399.0050 357.9857 574.3478 -4.0130 394.6996 398.7126 357.7645 575.9665 -4.0053 394.5326 398.5379 357.5293 577.5753 -3.9972 394.3858 398.3830 357.2747 579.1839 -3.9966 394.1666 398.1632 357.0458 580.7820 -3.9887 393.9408 397.9296 356.8362 582.3905 -3.9810 393.7146 397.6957 356.6107 583.9941 -3.9776 393.5248 397.5023 356.3952 585.5923 -3.9716 393.3332 397.3048 356.1539 587.2010 -3.9681 393.1180 397.0861 355.9464 588.8045 -3.9619 392.9343 396.8962 355.7483 590.4128 -3.9519 392.7287 396.6806 355.5416 592.0163 -3.9524 392.5009 396.4532 355.3666 593.6248 -3.9471 392.3036 396.2507 355.1459 595.2281 -3.9398 392.1308 396.0706 354.9409 596.8316 -3.9370 391.9162 395.8532 354.7769 598.4400 -3.9316 391.6780 395.6096 354.5534 600.0588 -3.9250 391.4190 395.3440 354.3837 601.6725 -3.9198 391.1853 395.1051 354.1790 603.2759 -3.9181 390.9775 394.8957 354.0077 604.8843 -3.9168 390.7802 394.6970 353.8077 606.4878 -3.9162 390.5949 394.5111 353.6044 608.1013 -3.9116 390.4066 394.3183 353.3646 609.6894 -3.9049 390.2493 394.1541 353.1336 611.3185 -3.9008 390.0510 393.9519 352.9605 612.9218 -3.8889 389.8055 393.6945 352.7179 614.5201 -3.8811 389.5795 393.4606 352.5270 616.1288 -3.8788 389.3844 393.2632 352.3473 617.7320 -3.8758 389.1672 393.0430 352.1476 619.3201 -3.8681 388.9551 392.8231 351.9152 620.9236 -3.8669 388.7566 392.6235 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