DTA measure 251104_on+5.dat Date: 2025114:1110 Lower limit = 100.0 C Upper limit = 350.0 C Rate = 5.00 C/min Mtime = 2817.06 s Mass = 100.000 mg data_number = 1752 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3541 -2.2508 29.6704 31.9212 74.7849 3.9484 -2.2702 29.8675 32.1377 74.7244 5.5675 -2.2897 30.1142 32.4039 74.7064 7.1719 -2.3042 30.3289 32.6331 74.7012 8.7863 -2.3197 30.5135 32.8332 74.6604 10.3901 -2.3325 30.7258 33.0583 74.6410 12.0045 -2.3410 30.9237 33.2647 74.6095 13.6086 -2.3491 31.1002 33.4493 74.5612 15.2228 -2.3715 31.3083 33.6798 74.4893 16.8219 -2.3867 31.5086 33.8953 74.4715 18.4158 -2.3923 31.7200 34.1123 74.4543 20.0248 -2.4015 31.9228 34.3243 74.4547 21.6288 -2.4129 32.1515 34.5644 74.4414 23.2279 -2.4190 32.3696 34.7886 74.4444 24.8370 -2.4235 32.6088 35.0323 74.3743 26.4514 -2.4290 32.8627 35.2918 74.3885 28.0609 -2.4279 33.0368 35.4647 74.4072 29.6646 -2.4314 33.2227 35.6541 74.4288 31.2689 -2.4346 33.3947 35.8293 74.4232 32.8783 -2.4404 33.5841 36.0245 74.4829 34.4821 -2.4468 33.7634 36.2102 74.5066 36.0916 -2.4486 33.9961 36.4447 74.5063 37.7110 -2.4509 34.2088 36.6597 74.5401 39.3200 -2.4552 34.4344 36.8895 74.5605 40.9245 -2.4584 34.6420 37.1004 74.6601 42.5335 -2.4586 34.8647 37.3233 74.7651 44.1430 -2.4580 35.0512 37.5092 74.7892 45.7471 -2.4554 35.2516 37.7070 74.8509 47.3561 -2.4579 35.4514 37.9094 74.9556 48.9604 -2.4632 35.6763 38.1396 75.0095 50.5594 -2.4626 35.8905 38.3531 75.0828 52.1633 -2.4548 36.1086 38.5634 75.2060 53.7674 -2.4534 36.3468 38.8002 75.3155 55.3614 -2.4519 36.5414 38.9933 75.3766 56.9704 -2.4536 36.7738 39.2274 75.4756 58.5798 -2.4480 37.0312 39.4792 75.6472 60.1839 -2.4447 37.2025 39.6472 75.7752 61.7930 -2.4432 37.3889 39.8322 75.9312 63.3819 -2.4463 37.6512 40.0975 76.0392 65.0013 -2.4416 37.8319 40.2735 76.1801 66.6104 -2.4332 37.9872 40.4204 76.3098 68.2148 -2.4331 38.1632 40.5963 76.4563 69.8238 -2.4304 38.3425 40.7729 76.6048 71.4280 -2.4292 38.5648 40.9939 76.7272 73.0424 -2.4249 38.7909 41.2158 76.8409 74.6463 -2.4237 38.9589 41.3826 77.0758 76.2555 -2.4219 39.1776 41.5995 77.3005 77.8649 -2.4136 39.4039 41.8176 77.4711 79.4739 -2.4115 39.6270 42.0385 77.6258 81.0730 -2.4066 39.8793 42.2859 77.8129 82.6773 -2.4095 40.1229 42.5324 77.9855 84.2759 -2.4111 40.3423 42.7533 78.1320 85.8648 -2.4089 40.5241 42.9330 78.3150 87.4639 -2.4074 40.7139 43.1212 78.4663 89.0728 -2.4129 40.9090 43.3219 78.6041 90.6925 -2.4170 41.1037 43.5208 78.8112 92.2966 -2.4161 41.3341 43.7501 79.0036 93.9056 -2.4085 41.5489 43.9575 79.1849 95.5098 -2.4088 41.7538 44.1626 79.3587 97.1036 -2.4079 41.9626 44.3705 79.5460 98.7075 -2.4029 42.1632 44.5661 79.6885 100.3169 -2.3967 42.3487 44.7454 79.8654 101.9211 -2.3927 42.5730 44.9656 80.0513 103.5404 -2.3875 42.8140 45.2015 80.2149 105.1498 -2.3852 42.9785 45.3636 80.3647 106.7590 -2.3839 43.1939 45.5779 80.5525 108.3680 -2.3862 43.4135 45.7997 80.7227 109.9721 -2.3873 43.6421 46.0295 80.8741 111.5815 -2.3853 43.8571 46.2424 81.0051 113.1853 -2.3809 44.0585 46.4394 81.1259 114.7996 -2.3778 44.2921 46.6698 81.2722 116.4040 -2.3755 44.5105 46.8860 81.4506 118.0026 -2.3725 44.7236 47.0961 81.5833 119.5865 -2.3612 44.9200 47.2812 81.7324 121.1958 -2.3547 45.1061 47.4608 81.9115 122.7996 -2.3508 45.3226 47.6735 82.0530 124.4093 -2.3391 45.5103 47.8494 82.2352 126.0131 -2.3341 45.6897 48.0239 82.3726 127.6325 -2.3281 45.8845 48.2126 82.5513 129.2419 -2.3253 46.0833 48.4086 82.6373 130.8459 -2.3296 46.2575 48.5872 82.7659 132.4551 -2.3254 46.4631 48.7885 82.9099 134.0593 -2.3226 46.6569 48.9795 83.0250 135.6684 -2.3205 46.8429 49.1634 83.1478 137.2728 -2.3167 47.0815 49.3981 83.2637 138.9025 -2.3192 47.2919 49.6112 83.3878 140.5063 -2.3187 47.5315 49.8502 83.5433 142.1208 -2.3141 47.7230 50.0371 83.6506 143.7250 -2.3115 47.9188 50.2303 83.7857 145.3236 -2.3083 48.1348 50.4431 83.9116 146.9281 -2.3056 48.3280 50.6336 84.0440 148.5270 -2.3037 48.4890 50.7927 84.2029 150.1413 -2.2965 48.7044 51.0009 84.3309 151.7506 -2.2951 48.9331 51.2282 84.4759 153.3546 -2.2981 49.1330 51.4311 84.6182 154.9535 -2.2936 49.3423 51.6359 84.7416 156.5476 -2.2843 49.5516 51.8359 84.8775 158.1515 -2.2885 49.7434 52.0319 85.0108 159.7609 -2.2825 49.9138 52.1963 85.1049 161.3649 -2.2780 50.0947 52.3727 85.1903 162.9843 -2.2732 50.3211 52.5943 85.3047 164.5934 -2.2672 50.5244 52.7916 85.4140 166.1978 -2.2632 50.7245 52.9878 85.5263 167.8119 -2.2520 50.9437 53.1957 85.6682 169.4160 -2.2443 51.1292 53.3736 85.7970 171.0304 -2.2368 51.3668 53.6036 85.9227 172.6190 -2.2314 51.5797 53.8111 86.0660 174.2284 -2.2275 51.7286 53.9561 86.2123 175.8480 -2.2237 51.9581 54.1817 86.2856 177.4570 -2.2214 52.1502 54.3716 86.3872 179.0559 -2.2151 52.3356 54.5507 86.5822 180.6551 -2.2160 52.5423 54.7583 86.7254 182.2538 -2.2123 52.7724 54.9847 86.8050 183.8476 -2.2058 52.9880 55.1938 86.9141 185.4466 -2.2037 53.1788 55.3825 87.0504 187.0558 -2.1948 53.3787 55.5735 87.1498 188.6751 -2.1912 53.5251 55.7164 87.2631 190.2795 -2.1893 53.6775 55.8668 87.3636 191.8783 -2.1890 53.8701 56.0591 87.4608 193.4820 -2.1852 54.0994 56.2846 87.6019 195.0915 -2.1787 54.2983 56.4770 87.7514 196.7008 -2.1707 54.5067 56.6773 87.8933 198.2943 -2.1621 54.6928 56.8549 88.0474 199.8984 -2.1587 54.8582 57.0169 88.1681 201.5079 -2.1554 55.0102 57.1656 88.2730 203.1321 -2.1466 55.1861 57.3327 88.4277 204.7416 -2.1403 55.3792 57.5195 88.5701 206.3458 -2.1313 55.6141 57.7454 88.6745 207.9548 -2.1215 55.8233 57.9448 88.7878 209.5590 -2.1109 56.0123 58.1232 88.8937 211.1580 -2.1050 56.2044 58.3094 89.0507 212.7619 -2.0974 56.3624 58.4598 89.1984 214.3456 -2.0939 56.5780 58.6719 89.3430 215.9651 -2.0859 56.7690 58.8549 89.4964 217.5741 -2.0830 56.9876 59.0706 89.6745 219.1731 -2.0784 57.1684 59.2468 89.8551 220.7773 -2.0758 57.3170 59.3928 90.0523 222.3863 -2.0686 57.5041 59.5727 90.2366 223.9905 -2.0616 57.6700 59.7316 90.3625 225.5999 -2.0518 57.8538 59.9056 90.5093 227.2190 -2.0507 58.0852 60.1359 90.6702 228.8284 -2.0446 58.3190 60.3635 90.8047 230.4326 -2.0424 58.5606 60.6030 90.9471 232.0418 -2.0374 58.7384 60.7758 91.0756 233.6513 -2.0329 58.8733 60.9063 91.2098 235.2603 -2.0283 59.0339 61.0621 91.3581 236.8695 -2.0299 59.2152 61.2451 91.5182 238.4890 -2.0275 59.4601 61.4876 91.6898 240.0879 -2.0245 59.6695 61.6940 91.8761 241.6919 -2.0203 59.8210 61.8413 91.9901 243.2963 -2.0141 60.0182 62.0323 92.1231 244.9001 -2.0048 60.2076 62.2124 92.2470 246.4993 -2.0055 60.3933 62.3988 92.3945 248.1035 -2.0020 60.5524 62.5544 92.5111 249.7073 -1.9986 60.7443 62.7429 92.6263 251.3219 -1.9935 60.9194 62.9129 92.7916 252.9311 -1.9905 61.0824 63.0729 92.9445 254.5350 -1.9810 61.2847 63.2658 93.0744 256.1444 -1.9765 61.4803 63.4568 93.2327 257.7536 -1.9761 61.6877 63.6637 93.3970 259.3626 -1.9670 61.8808 63.8479 93.5149 260.9515 -1.9603 62.0690 64.0293 93.6333 262.5915 -1.9544 62.2409 64.1954 93.7665 264.1954 -1.9474 62.4170 64.3645 93.8764 265.8049 -1.9426 62.5759 64.5185 93.9953 267.4140 -1.9440 62.7637 64.7076 94.0990 269.0026 -1.9370 62.9817 64.9188 94.2366 270.6273 -1.9278 63.1879 65.1157 94.3699 272.2365 -1.9255 63.3847 65.3102 94.5184 273.8404 -1.9175 63.5306 65.4481 94.6049 275.4395 -1.9145 63.6967 65.6112 94.7087 277.0436 -1.9090 63.8281 65.7372 94.8313 278.6475 -1.9075 64.0321 65.9396 94.9745 280.2466 -1.9045 64.2209 66.1254 95.1354 281.8456 -1.8936 64.3847 66.2783 95.2766 283.4494 -1.8834 64.5485 66.4319 95.3530 285.0536 -1.8806 64.7214 66.6020 95.4460 286.6476 -1.8775 64.9232 66.8007 95.5681 288.2514 -1.8757 65.0844 66.9601 95.7149 289.8761 -1.8676 65.2577 67.1253 95.8380 291.4804 -1.8690 65.4164 67.2855 95.9751 293.0894 -1.8682 65.5912 67.4594 96.0960 294.6990 -1.8632 65.7827 67.6459 96.2082 296.3080 -1.8555 65.9512 67.8068 96.2834 297.9121 -1.8529 66.1154 67.9683 96.4027 299.5113 -1.8508 66.2634 68.1142 96.5351 301.1151 -1.8416 66.4429 68.2845 96.6964 302.7348 -1.8399 66.6034 68.4433 96.8404 304.3493 -1.8344 66.7927 68.6272 97.0196 305.9530 -1.8315 67.0086 68.8401 97.1432 307.5573 -1.8208 67.1685 68.9893 97.2496 309.1513 -1.8164 67.3722 69.1886 97.3512 310.7550 -1.8085 67.5276 69.3361 97.4390 312.3593 -1.8014 67.6979 69.4994 97.5510 313.9481 -1.7967 67.8375 69.6342 97.6695 315.5673 -1.7934 68.0594 69.8528 97.8075 317.1765 -1.7892 68.2311 70.0203 97.9706 318.7808 -1.7859 68.4271 70.2130 98.0698 320.3898 -1.7811 68.6069 70.3880 98.1491 321.9938 -1.7746 68.7620 70.5366 98.2789 323.6031 -1.7728 68.9317 70.7045 98.4053 325.1969 -1.7643 69.1254 70.8896 98.5395 326.8060 -1.7532 69.2654 71.0186 98.6689 328.4255 -1.7506 69.4276 71.1782 98.7668 330.0348 -1.7455 69.6363 71.3818 98.8706 331.6285 -1.7330 69.8244 71.5574 98.9915 333.2481 -1.7311 69.9947 71.7257 99.1023 334.8521 -1.7279 70.1705 71.8984 99.2588 336.4613 -1.7251 70.3428 72.0679 99.4298 338.0655 -1.7212 70.4977 72.2189 99.5952 339.6644 -1.7123 70.6316 72.3439 99.7520 341.2890 -1.7098 70.8565 72.5664 99.8966 342.8883 -1.7094 71.0048 72.7142 100.0299 344.4869 -1.7081 71.1980 72.9061 100.1609 346.0963 -1.7055 71.3518 73.0573 100.3295 347.7005 -1.7034 71.5449 73.2483 100.4562 349.3094 -1.7013 71.6970 73.3983 100.6221 350.9136 -1.6941 71.8316 73.5258 100.7875 352.5126 -1.6884 71.9850 73.6733 100.8998 354.1319 -1.6867 72.1370 73.8237 101.0299 355.7360 -1.6808 72.3000 73.9808 101.1741 357.3455 -1.6689 72.4515 74.1204 101.3326 358.9494 -1.6644 72.6538 74.3182 101.4823 360.5589 -1.6658 72.8075 74.4733 101.6374 362.1629 -1.6628 72.9948 74.6576 101.7606 363.7770 -1.6709 73.2042 74.8750 101.9087 365.3966 -1.6699 73.3181 74.9879 102.0793 367.0059 -1.6637 73.4515 75.1152 102.2529 368.6150 -1.6608 73.5996 75.2603 102.4332 370.2244 -1.6570 73.7666 75.4235 102.5659 371.8233 -1.6577 73.9412 75.5989 102.6721 373.4220 -1.6541 74.0981 75.7522 102.7989 375.0264 -1.6456 74.2529 75.8985 102.9100 376.6150 -1.6372 74.4232 76.0603 103.0654 378.2189 -1.6396 74.5985 76.2382 103.2020 379.8385 -1.6354 74.7492 76.3846 103.3369 381.4426 -1.6271 74.9024 76.5295 103.4538 383.0516 -1.6241 75.1009 76.7250 103.5737 384.6408 -1.6181 75.2428 76.8609 103.7608 386.2498 -1.6154 75.4221 77.0375 103.8756 387.8539 -1.6172 75.5821 77.1993 103.9888 389.4633 -1.6163 75.7099 77.3262 104.1393 391.0671 -1.6149 75.8603 77.4752 104.2746 392.6868 -1.6130 76.0457 77.6587 104.3728 394.2961 -1.6080 76.2158 77.8238 104.5133 395.8999 -1.6094 76.4088 78.0182 104.6279 397.5141 -1.6012 76.5704 78.1715 104.7327 399.1031 -1.5985 76.7033 78.3018 104.7992 400.7121 -1.6011 76.8432 78.4443 104.9122 402.3214 -1.6040 76.9921 78.5962 105.0413 403.9256 -1.6026 77.1202 78.7228 105.1330 405.5398 -1.5905 77.2575 78.8480 105.2644 407.1439 -1.5841 77.4026 78.9867 105.4075 408.7481 -1.5839 77.6030 79.1869 105.5492 410.3520 -1.5792 77.8102 79.3894 105.6669 411.9406 -1.5831 78.0242 79.6074 105.8193 413.5500 -1.5803 78.1971 79.7775 105.9307 415.1540 -1.5736 78.3453 79.9188 106.0006 416.7633 -1.5679 78.5117 80.0797 106.1185 418.3830 -1.5661 78.6607 80.2268 106.2211 419.9970 -1.5594 78.8551 80.4145 106.3934 421.6011 -1.5549 79.0113 80.5662 106.5129 423.2158 -1.5466 79.1856 80.7322 106.6540 424.8196 -1.5370 79.2916 80.8287 106.8252 426.4293 -1.5376 79.4206 80.9583 106.9987 428.0331 -1.5350 79.5475 81.0824 107.1281 429.6578 -1.5301 79.6785 81.2085 107.2246 431.2673 -1.5285 79.8456 81.3741 107.3449 432.8710 -1.5253 80.0108 81.5361 107.4815 434.4803 -1.5208 80.1370 81.6577 107.6504 436.0794 -1.5149 80.3757 81.8906 107.7624 437.6833 -1.5160 80.5786 82.0946 107.9056 439.2824 -1.5153 80.7185 82.2338 108.0746 440.8713 -1.5113 80.8419 82.3532 108.2355 442.4904 -1.5066 80.9836 82.4903 108.4157 444.0946 -1.4986 81.1576 82.6562 108.5406 445.6989 -1.4953 81.2398 82.7351 108.6641 447.3079 -1.4937 81.4195 82.9132 108.8110 448.9123 -1.4941 81.5961 83.0902 108.9271 450.5214 -1.4960 81.7485 83.2445 109.0327 452.1254 -1.4950 81.9087 83.4037 109.1729 453.7451 -1.4871 82.0596 83.5467 109.3089 455.3541 -1.4781 82.2143 83.6924 109.4800 456.9583 -1.4806 82.4125 83.8931 109.6076 458.5678 -1.4813 82.5642 84.0455 109.7195 460.1766 -1.4761 82.7193 84.1954 109.8560 461.7860 -1.4728 82.8907 84.3635 109.9990 463.3901 -1.4731 83.0121 84.4852 110.1156 465.0145 -1.4708 83.1759 84.6466 110.2570 466.6188 -1.4701 83.3383 84.8084 110.3950 468.2230 -1.4637 83.4733 84.9370 110.5417 469.8269 -1.4577 83.6224 85.0800 110.7041 471.4260 -1.4617 83.7774 85.2392 110.8000 473.0250 -1.4615 83.9424 85.4039 110.9435 474.6340 -1.4579 84.1332 85.5910 111.0614 476.2536 -1.4527 84.3233 85.7760 111.2049 477.8629 -1.4475 84.4503 85.8978 111.3958 479.4668 -1.4480 84.6003 86.0484 111.5430 481.0609 -1.4520 84.7607 86.2126 111.6681 482.6700 -1.4501 84.9356 86.3857 111.7991 484.2738 -1.4418 85.0700 86.5119 111.9191 485.8833 -1.4386 85.2019 86.6405 112.0405 487.4874 -1.4420 85.3406 86.7826 112.1690 489.1119 -1.4423 85.5139 86.9562 112.3415 490.7163 -1.4408 85.6715 87.1124 112.5013 492.3253 -1.4340 85.8121 87.2460 112.6333 493.9345 -1.4319 85.9417 87.3736 112.7554 495.5440 -1.4271 86.1206 87.5477 112.8995 497.1529 -1.4255 86.2346 87.6601 113.0363 498.7623 -1.4274 86.3518 87.7792 113.1226 500.3819 -1.4257 86.5267 87.9524 113.2460 501.9805 -1.4276 86.7096 88.1373 113.3897 503.5694 -1.4271 86.8392 88.2663 113.5333 505.1736 -1.4260 86.9691 88.3951 113.6684 506.7775 -1.4247 87.1033 88.5280 113.7966 508.3816 -1.4199 87.2420 88.6619 113.9496 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205.9094 207.4363 226.5758 1918.5481 -1.5318 206.0081 207.5399 226.6907 1920.1524 -1.5265 206.1287 207.6552 226.8230 1921.7513 -1.5261 206.2906 207.8166 226.9691 1923.3706 -1.5252 206.3992 207.9245 227.1274 1924.9750 -1.5190 206.5589 208.0780 227.2466 1926.5635 -1.5068 206.7045 208.2112 227.3355 1928.1729 -1.5018 206.8424 208.3442 227.4751 1929.7771 -1.4831 207.0069 208.4900 227.6302 1931.3860 -1.4798 207.1604 208.6402 227.7533 1932.9904 -1.4804 207.2770 208.7573 227.8560 1934.5894 -1.4826 207.4119 208.8945 227.9980 1936.2138 -1.4883 207.5265 209.0148 228.1449 1937.8181 -1.4961 207.6395 209.1356 228.2864 1939.4119 -1.5038 207.8162 209.3200 228.4724 1941.0210 -1.5052 207.9919 209.4971 228.6008 1942.6306 -1.5044 208.0927 209.5971 228.7307 1944.2344 -1.5045 208.2115 209.7160 228.8734 1945.8390 -1.5047 208.3629 209.8676 228.9892 1947.4480 -1.4988 208.4671 209.9659 229.0961 1949.0676 -1.4987 208.5754 210.0741 229.1966 1950.6770 -1.5071 208.6592 210.1663 229.3032 1952.2809 -1.5009 208.8177 210.3186 229.4194 1953.8903 -1.4872 208.9812 210.4684 229.5569 1955.4944 -1.4918 209.1399 210.6316 229.6963 1957.1033 -1.4990 209.2747 210.7738 229.8197 1958.7128 -1.5093 209.3981 210.9074 229.9137 1960.3323 -1.5209 209.5494 211.0703 230.1093 1961.9413 -1.5231 209.6553 211.1784 230.2634 1963.5458 -1.5208 209.7938 211.3146 230.4173 1965.1548 -1.5212 209.9343 211.4555 230.5215 1966.7591 -1.5233 210.0248 211.5481 230.5693 1968.3735 -1.5237 210.1388 211.6624 230.7249 1969.9774 -1.5318 210.2673 211.7992 230.8949 1971.6074 -1.5296 210.4015 211.9311 231.0648 1973.2114 -1.5345 210.5466 212.0812 231.2070 1974.8206 -1.5402 210.6694 212.2096 231.3485 1976.4249 -1.5378 210.7654 212.3032 231.4868 1978.0390 -1.5382 210.9632 212.5014 231.6553 1979.6431 -1.5455 211.1233 212.6688 231.7760 1981.2474 -1.5444 211.2755 212.8199 231.8451 1982.8666 -1.5435 211.4091 212.9526 231.9792 1984.4708 -1.5406 211.5163 213.0569 232.0904 1986.0750 -1.5402 211.6322 213.1724 232.2311 1987.6789 -1.5361 211.7377 213.2738 232.4041 1989.2675 -1.5383 211.9222 213.4605 232.5398 1990.8768 -1.5392 212.0549 213.5941 232.6819 1992.4758 -1.5402 212.1933 213.7335 232.8250 1994.0799 -1.5366 212.3022 213.8387 232.9574 1995.7048 -1.5407 212.4012 213.9419 233.0830 1997.3085 -1.5347 212.5013 214.0360 233.2169 1998.9178 -1.5383 212.5968 214.1352 233.3585 2000.5170 -1.5406 212.7513 214.2919 233.5016 2002.1208 -1.5442 212.9018 214.4460 233.6548 2003.7303 -1.5514 213.0669 214.6183 233.7899 2005.3344 -1.5527 213.1949 214.7476 233.8948 2006.9588 -1.5539 213.2991 214.8530 234.0496 2008.5630 -1.5559 213.4292 214.9852 234.2153 2010.1723 -1.5563 213.5262 215.0826 234.3766 2011.7763 -1.5527 213.6948 215.2475 234.5102 2013.3805 -1.5543 213.8572 215.4115 234.6081 2014.9896 -1.5631 213.9821 215.5452 234.7087 2016.5936 -1.5626 214.1150 215.6776 234.8417 2018.2183 -1.5639 214.2231 215.7870 234.9467 2019.8224 -1.5729 214.3885 215.9614 235.0305 2021.4318 -1.5746 214.5515 216.1262 235.1856 2023.0360 -1.5734 214.6809 216.2542 235.3753 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