DTA measure 1260217_SN_3.dat Date: 2026217:1143 Lower limit = 100.0 C Upper limit = 340.0 C Rate = 10.00 C/min Mtime = 1439.24 s Mass = 918.200 mg data_number = 1791 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3240 -1.8977 23.0141 24.9117 74.5607 2.0803 -1.8989 23.1405 25.0394 74.5387 2.9180 -1.9015 23.3162 25.2176 74.5065 3.7045 -1.9015 23.4623 25.3639 74.4803 4.5018 -1.9090 23.6231 25.5322 74.4702 5.3295 -1.9105 23.7800 25.6905 74.4196 6.0953 -1.9091 23.9080 25.8171 74.3692 6.9540 -1.9100 24.0375 25.9475 74.2856 7.7100 -1.9099 24.1531 26.0630 74.2423 8.5373 -1.9096 24.2978 26.2073 74.1845 9.3243 -1.9099 24.4205 26.3304 74.1549 10.1213 -1.9075 24.5470 26.4545 74.1533 10.9178 -1.9029 24.7015 26.6044 74.1243 11.7048 -1.9034 24.8093 26.7127 74.1041 12.5325 -1.9136 24.9432 26.8569 74.0643 13.2880 -1.9122 25.0773 26.9895 74.0441 14.1468 -1.9139 25.2383 27.1522 74.0708 14.9133 -1.9129 25.3828 27.2957 74.0719 15.7300 -1.9115 25.5277 27.4391 74.0431 16.5273 -1.9091 25.6575 27.5666 74.0198 17.3245 -1.9055 25.7719 27.6773 74.0067 18.1413 -1.9083 25.9109 27.8192 73.9764 18.9078 -1.9077 26.0640 27.9718 73.9741 19.7665 -1.9060 26.2122 28.1182 73.9510 20.5323 -1.9036 26.2852 28.1888 73.9493 21.3498 -1.9052 26.4281 28.3333 73.9340 22.1470 -1.9024 26.5753 28.4777 73.8922 22.9433 -1.9031 26.6645 28.5676 73.8689 23.7405 -1.8971 26.8143 28.7114 73.8480 24.5275 -1.8966 26.9154 28.8120 73.8630 25.3550 -1.8954 27.0731 28.9684 73.8912 26.1210 -1.8947 27.1899 29.0846 73.9016 26.9695 -1.8939 27.3222 29.2161 73.9398 27.7458 -1.8922 27.4358 29.3280 73.9482 28.5630 -1.8897 27.5783 29.4679 73.9753 29.3603 -1.8927 27.6950 29.5877 73.9903 30.1573 -1.8899 27.8516 29.7415 73.9920 30.9845 -1.8904 28.0320 29.9224 74.0149 31.7510 -1.8904 28.1667 30.0571 74.0380 32.5993 -1.8895 28.3117 30.2012 74.0449 33.3753 -1.8851 28.4281 30.3132 74.1018 34.1930 -1.8852 28.5502 30.4354 74.1310 34.9903 -1.8775 28.6826 30.5601 74.1876 35.7865 -1.8775 28.8253 30.7028 74.2585 36.6145 -1.8754 28.9575 30.8328 74.3428 37.3808 -1.8727 29.1149 30.9876 74.4216 38.2285 -1.8711 29.2614 31.1325 74.4988 39.0053 -1.8654 29.3838 31.2492 74.5677 39.8230 -1.8579 29.4969 31.3548 74.6672 40.6193 -1.8517 29.6514 31.5030 74.7303 41.4165 -1.8502 29.8108 31.6610 74.8118 42.2445 -1.8494 29.9339 31.7833 74.8995 43.0100 -1.8528 30.0416 31.8944 74.9678 43.8585 -1.8510 30.2054 32.0564 75.0608 44.6353 -1.8499 30.3345 32.1843 75.1138 45.4523 -1.8494 30.4434 32.2928 75.1898 46.2493 -1.8461 30.5723 32.4184 75.2834 47.0465 -1.8434 30.7315 32.5749 75.3872 47.8738 -1.8427 30.8868 32.7295 75.4740 48.6400 -1.8391 30.9519 32.7910 75.5302 49.4885 -1.8391 31.0904 32.9295 75.6447 50.2645 -1.8366 31.2197 33.0563 75.8131 51.0820 -1.8322 31.3335 33.1658 75.9427 51.8793 -1.8306 31.4620 33.2927 76.0720 52.6760 -1.8267 31.6122 33.4389 76.2426 53.5035 -1.8230 31.7488 33.5718 76.4105 54.2700 -1.8245 31.8769 33.7014 76.5317 55.1183 -1.8191 32.0274 33.8465 76.6821 55.8943 -1.8170 32.1752 33.9922 76.7824 56.7120 -1.8133 32.2954 34.1087 76.9718 57.5190 -1.8097 32.4384 34.2481 77.0797 58.3055 -1.8038 32.5777 34.3815 77.2427 59.1438 -1.8031 32.6482 34.4513 77.3864 59.8995 -1.7994 32.7745 34.5739 77.5275 60.7578 -1.8007 32.8979 34.6986 77.6933 61.5243 -1.7989 33.0261 34.8250 77.8410 62.3523 -1.7969 33.1423 34.9392 78.0158 63.1485 -1.7951 33.2449 35.0400 78.1900 63.9355 -1.7956 33.3876 35.1832 78.3633 64.7738 -1.7922 33.5761 35.3683 78.5593 65.5295 -1.7886 33.7081 35.4967 78.6996 66.3878 -1.7835 33.8165 35.6000 78.8704 67.1543 -1.7822 33.9333 35.7156 79.0291 67.9818 -1.7861 34.0610 35.8470 79.1914 68.8093 -1.7841 34.1934 35.9775 79.3536 69.5655 -1.7854 34.3376 36.1230 79.4867 70.4035 -1.7844 34.4577 36.2421 79.6661 71.1693 -1.7851 34.6120 36.3971 79.8144 72.0280 -1.7842 34.8019 36.5862 79.9710 72.7835 -1.7831 34.8958 36.6790 80.1330 73.6113 -1.7831 35.0032 36.7862 80.3352 74.3983 -1.7833 35.1068 36.8901 80.5237 75.1948 -1.7862 35.2283 37.0145 80.6872 76.0123 -1.7851 35.3728 37.1579 80.8649 76.7788 -1.7807 35.5435 37.3242 80.9820 77.6063 -1.7794 35.6593 37.4387 81.1423 78.3620 -1.7778 35.7684 37.5462 81.2913 79.2105 -1.7762 35.8961 37.6724 81.5296 79.9868 -1.7707 36.0097 37.7804 81.7014 80.8040 -1.7701 36.1501 37.9202 81.8604 81.6013 -1.7665 36.3033 38.0698 82.0349 82.3978 -1.7669 36.4288 38.1957 82.2262 83.2153 -1.7661 36.5570 38.3231 82.3859 83.9818 -1.7657 36.6775 38.4432 82.5540 84.8093 -1.7646 36.8228 38.5874 82.7127 85.5753 -1.7551 36.9322 38.6873 82.8454 86.4238 -1.7574 37.0748 38.8322 83.0125 87.1895 -1.7607 37.2255 38.9861 83.2020 88.0173 -1.7621 37.3731 39.1352 83.3843 88.8145 -1.7606 37.4841 39.2447 83.5551 89.6008 -1.7611 37.6063 39.3674 83.7362 90.4388 -1.7587 37.7374 39.4962 83.9170 91.1950 -1.7607 37.8444 39.6051 84.0742 92.0225 -1.7654 37.9800 39.7454 84.2578 92.7885 -1.7625 38.1062 39.8687 84.4232 93.6370 -1.7618 38.2344 39.9962 84.5717 94.4035 -1.7609 38.3660 40.1269 84.7312 95.2305 -1.7574 38.5020 40.2594 84.8905 96.0278 -1.7547 38.6208 40.3755 85.0670 96.8250 -1.7579 38.7308 40.4887 85.2486 97.6418 -1.7562 38.8557 40.6119 85.4118 98.4185 -1.7568 38.9935 40.7503 85.5509 99.2670 -1.7578 39.1519 40.9097 85.7387 100.0120 -1.7573 39.3054 41.0626 85.8653 100.8605 -1.7562 39.4210 41.1773 85.9912 101.6373 -1.7615 39.5358 41.2973 86.0879 102.4540 -1.7660 39.6572 41.4231 86.2409 103.2513 -1.7641 39.8036 41.5676 86.3884 104.0485 -1.7669 39.9306 41.6975 86.5412 104.8755 -1.7629 40.0709 41.8338 86.7012 105.6420 -1.7649 40.1891 41.9540 86.8273 106.4905 -1.7668 40.2896 42.0563 86.9926 107.2665 -1.7673 40.4197 42.1870 87.1448 108.0943 -1.7652 40.5687 42.3339 87.3027 108.8608 -1.7624 40.7121 42.4744 87.4404 109.6778 -1.7599 40.8588 42.6187 87.5781 110.4850 -1.7568 40.9801 42.7369 87.7615 111.2720 -1.7545 41.1180 42.8725 87.9153 112.0995 -1.7537 41.2851 43.0387 88.0440 112.8655 -1.7494 41.4008 43.1502 88.1459 113.7243 -1.7475 41.5413 43.2888 88.2846 114.4903 -1.7502 41.6750 43.4252 88.4123 115.3178 -1.7515 41.8430 43.5944 88.5359 116.1150 -1.7532 42.0081 43.7614 88.6849 116.9115 -1.7543 42.1362 43.8905 88.7823 117.7393 -1.7533 42.2717 44.0250 88.9245 118.4955 -1.7537 42.3901 44.1438 89.0766 119.3640 -1.7567 42.5303 44.2870 89.2532 120.0993 -1.7554 42.6482 44.4036 89.3262 120.9580 -1.7557 42.7957 44.5514 89.4659 121.7135 -1.7585 42.9100 44.6685 89.6282 122.5515 -1.7592 43.0014 44.7606 89.7857 123.3385 -1.7591 43.1295 44.8887 89.9248 124.1453 -1.7551 43.3027 45.0578 90.0534 124.9628 -1.7570 43.4694 45.2264 90.1522 125.7395 -1.7617 43.6048 45.3665 90.2829 126.5873 -1.7637 43.7327 45.4965 90.4020 127.3535 -1.7667 43.8635 45.6302 90.4967 128.1815 -1.7712 44.0243 45.7955 90.6327 128.9883 -1.7716 44.1519 45.9235 90.7377 129.7750 -1.7696 44.2786 46.0482 90.8565 130.6030 -1.7641 44.4233 46.1874 90.9888 131.3690 -1.7603 44.5544 46.3147 91.0709 132.2273 -1.7578 44.7140 46.4718 91.2203 132.9938 -1.7570 44.8222 46.5792 91.3407 133.8213 -1.7561 44.9318 46.6878 91.4860 134.6180 -1.7544 45.0663 46.8207 91.5940 135.4153 -1.7514 45.2044 46.9558 91.7118 136.2020 -1.7470 45.3371 47.0841 91.8405 136.9985 -1.7489 45.4827 47.2316 91.9593 137.8265 -1.7540 45.6221 47.3761 92.0876 138.5823 -1.7598 45.7351 47.4949 92.1920 139.4405 -1.7612 45.8773 47.6384 92.3372 140.1968 -1.7635 46.0074 47.7710 92.4356 141.0245 -1.7706 46.1423 47.9129 92.5479 141.8210 -1.7718 46.2695 48.0413 92.6529 142.6080 -1.7687 46.3938 48.1625 92.7664 143.4255 -1.7695 46.5418 48.3113 92.8546 144.2015 -1.7720 46.6930 48.4650 92.9736 145.0500 -1.7730 46.8403 48.6133 93.0822 145.8165 -1.7695 46.9283 48.6978 93.1903 146.6435 -1.7662 47.0246 48.7908 93.3043 147.4408 -1.7660 47.1180 48.8840 93.4431 148.2278 -1.7687 47.2148 48.9835 93.6124 149.0548 -1.7689 47.3548 49.1236 93.7597 149.8213 -1.7685 47.4873 49.2558 93.8774 150.6798 -1.7650 47.6657 49.4307 93.9791 151.4353 -1.7649 47.8070 49.5719 94.1307 152.2735 -1.7633 47.9018 49.6651 94.2861 153.0605 -1.7629 48.0359 49.7988 94.4045 153.8468 -1.7640 48.1615 49.9255 94.5362 154.6848 -1.7647 48.3448 50.1095 94.6549 155.4410 -1.7695 48.4606 50.2301 94.7606 156.2988 -1.7689 48.5922 50.3611 94.8471 157.0653 -1.7648 48.7272 50.4920 94.9768 157.8930 -1.7587 48.8731 50.6317 95.1303 158.6895 -1.7590 49.0257 50.7847 95.2385 159.4765 -1.7661 49.1756 50.9417 95.3535 160.2840 -1.7636 49.3337 51.0973 95.4721 161.0700 -1.7628 49.4815 51.2443 95.6417 161.9288 -1.7598 49.6252 51.3850 95.7580 162.6953 -1.7572 49.7690 51.5262 95.8874 163.5225 -1.7576 49.9000 51.6575 96.0034 164.3195 -1.7606 50.0406 51.8012 96.1035 165.1065 -1.7573 50.1698 51.9271 96.1808 165.9438 -1.7585 50.3036 52.0621 96.3041 166.7000 -1.7606 50.4260 52.1866 96.4187 167.5588 -1.7616 50.5571 52.3188 96.5278 168.3245 -1.7665 50.7074 52.4739 96.6358 169.1523 -1.7659 50.8568 52.6227 96.7560 169.9495 -1.7641 50.9703 52.7344 96.8556 170.7358 -1.7626 51.0927 52.8553 96.9332 171.5738 -1.7629 51.2281 52.9910 97.0550 172.3300 -1.7661 51.3293 53.0954 97.1918 173.1888 -1.7660 51.4348 53.2008 97.3159 173.9235 -1.7701 51.5535 53.3236 97.4489 174.7925 -1.7691 51.6888 53.4579 97.5580 175.5488 -1.7689 51.8167 53.5856 97.6631 176.3758 -1.7696 51.9657 53.7353 97.7966 177.1730 -1.7654 52.1208 53.8863 97.9087 177.9703 -1.7661 52.2431 54.0092 98.0134 178.7973 -1.7675 52.3817 54.1492 98.1572 179.5535 -1.7691 52.5270 54.2960 98.2971 180.4225 -1.7714 52.6390 54.4104 98.4115 181.1780 -1.7700 52.7675 54.5374 98.5375 182.0058 -1.7675 52.8976 54.6651 98.6420 182.8030 -1.7624 53.0330 54.7954 98.7404 183.5995 -1.7630 53.1639 54.9270 98.8542 184.4273 -1.7653 53.3308 55.0960 98.9975 185.1835 -1.7643 53.4906 55.2549 99.1508 186.0520 -1.7640 53.6371 55.4010 99.2793 186.8078 -1.7636 53.7494 55.5130 99.3502 187.6358 -1.7630 53.8769 55.6400 99.4785 188.4323 -1.7625 53.9695 55.7320 99.5957 189.2293 -1.7635 54.1276 55.8911 99.7409 190.0573 -1.7643 54.2798 56.0441 99.8839 190.8128 -1.7605 54.3814 56.1419 99.9985 191.6815 -1.7572 54.5335 56.2907 100.0868 192.4378 -1.7565 54.6674 56.4239 100.2040 193.2655 -1.7605 54.8000 56.5605 100.3215 194.0620 -1.7654 54.9257 56.6911 100.4389 194.8593 -1.7651 55.0378 56.8030 100.5559 195.6563 -1.7653 55.1831 56.9483 100.6820 196.4425 -1.7654 55.3310 57.0964 100.8123 197.2808 -1.7612 55.4675 57.2287 100.9618 198.0368 -1.7612 55.5902 57.3515 101.0762 198.8948 -1.7623 55.7371 57.4994 101.1928 199.6613 -1.7667 55.8898 57.6565 101.3235 200.4788 -1.7696 55.9933 57.7628 101.4358 201.2753 -1.7685 56.1582 57.9268 101.5732 202.0725 -1.7656 56.3311 58.0968 101.6881 202.8898 -1.7638 56.4780 58.2418 101.8276 203.6455 -1.7629 56.5675 58.3304 101.9639 204.5043 -1.7614 56.6870 58.4483 102.1131 205.2708 -1.7544 56.8310 58.5854 102.2295 206.0875 -1.7537 56.9599 58.7136 102.3508 206.8643 -1.7572 57.0963 58.8535 102.4864 207.6820 -1.7572 57.2245 58.9817 102.6233 208.4680 -1.7558 57.3219 59.0776 102.7403 209.2755 -1.7608 57.4577 59.2185 102.8896 210.0930 -1.7624 57.5848 59.3472 103.0282 210.8485 -1.7693 57.7113 59.4805 103.1607 211.7175 -1.7704 57.8184 59.5888 103.3813 212.4733 -1.7674 57.9465 59.7139 103.4680 213.2905 -1.7648 58.0723 59.8372 103.5825 214.0980 -1.7611 58.2191 59.9802 103.7093 214.8845 -1.7606 58.3306 60.0911 103.8431 215.6915 -1.7645 58.4673 60.2319 103.9414 216.4888 -1.7616 58.5909 60.3525 104.0750 217.3163 -1.7667 58.7512 60.5179 104.2025 218.0823 -1.7713 58.8993 60.6705 104.3179 218.9410 -1.7669 59.1012 60.8682 104.4762 219.6973 -1.7636 59.2226 60.9862 104.6037 220.5345 -1.7640 59.3250 61.0890 104.7460 221.2908 -1.7622 59.4630 61.2252 104.8765 222.1183 -1.7604 59.6282 61.3886 105.0070 222.9150 -1.7643 59.7715 61.5358 105.1232 223.7123 -1.7650 59.9258 61.6908 105.2398 224.5398 -1.7625 60.0919 61.8544 105.3547 225.2955 -1.7607 60.2111 61.9717 105.4590 226.1645 -1.7540 60.3173 62.0713 105.6182 226.9303 -1.7510 60.4514 62.2023 105.7520 227.7580 -1.7491 60.5943 62.3434 105.8929 228.5143 -1.7496 60.7164 62.4659 106.0405 229.3525 -1.7510 60.8726 62.6235 106.1658 230.1385 -1.7509 61.0076 62.7586 106.2695 230.9358 -1.7504 61.1110 62.8614 106.3777 231.7638 -1.7549 61.2392 62.9941 106.5171 232.5293 -1.7587 61.3524 63.1111 106.6440 233.3880 -1.7625 61.5013 63.2639 106.7479 234.1440 -1.7616 61.6218 63.3834 106.8575 234.9815 -1.7645 61.7453 63.5098 107.0184 235.7685 -1.7641 61.8826 63.6467 107.1778 236.5655 -1.7635 62.0195 63.7830 107.3074 237.3928 -1.7607 62.1352 63.8958 107.4195 238.1593 -1.7593 62.2378 63.9971 107.5472 239.0175 -1.7564 62.4013 64.1576 107.6626 239.7733 -1.7560 62.5365 64.2925 107.7965 240.6115 -1.7565 62.6536 64.4101 107.9331 241.3983 -1.7559 62.8227 64.5786 108.0693 242.1948 -1.7547 62.9879 64.7426 108.2189 243.0228 -1.7584 63.1426 64.9010 108.3672 243.7893 -1.7575 63.2881 65.0456 108.5078 244.6470 -1.7586 63.4288 65.1874 108.6688 245.4135 -1.7573 63.5523 65.3096 108.8255 246.2413 -1.7568 63.6785 65.4353 108.9592 247.0378 -1.7545 63.8229 65.5774 109.1018 247.8350 -1.7510 63.9719 65.7229 109.2461 248.6525 -1.7515 64.0588 65.8103 109.3757 249.4285 -1.7545 64.1387 65.8932 109.4692 250.2770 -1.7540 64.2783 66.0323 109.6214 251.0433 -1.7523 64.4294 66.1817 109.7508 251.8705 -1.7538 64.5932 66.3470 109.8987 252.6678 -1.7539 64.7233 66.4772 110.0386 253.4648 -1.7533 64.8665 66.6198 110.1791 254.2818 -1.7494 65.0323 66.7816 110.3228 255.0585 -1.7537 65.1258 66.8794 110.4246 255.9070 -1.7606 65.2507 67.0113 110.5763 256.6725 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