DTA measure 2Pb_1-ud3.dat Date: 2026827:1536 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1648.06 s Mass = 100.000 mg data_number = 1024 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4463 -4.2268 405.9190 410.1458 404.1561 4.0504 -4.2273 406.1008 410.3281 404.1656 5.6598 -4.2323 406.3126 410.5449 404.1803 7.2640 -4.2330 406.4729 410.7060 404.1574 8.8734 -4.2351 406.6489 410.8839 404.1210 10.4720 -4.2363 406.7970 411.0333 404.1226 12.0921 -4.2402 406.9584 411.1987 404.0802 13.7010 -4.2407 407.1345 411.3753 404.0346 15.3054 -4.2436 407.2844 411.5280 403.9983 16.9044 -4.2489 407.4487 411.6976 403.9621 18.5139 -4.2516 407.6114 411.8630 403.9087 20.1129 -4.2519 407.7995 412.0514 403.8185 21.7223 -4.2529 407.9643 412.2172 403.7404 23.3419 -4.2542 408.1216 412.3758 403.6564 24.9460 -4.2595 408.2743 412.5338 403.5558 26.5555 -4.2636 408.4443 412.7079 403.4393 28.1443 -4.2655 408.5780 412.8435 403.3223 29.7538 -4.2679 408.7226 412.9905 403.2115 31.3578 -4.2689 408.8729 413.1418 403.1216 32.9673 -4.2666 409.0209 413.2875 402.9737 34.5711 -4.2658 409.1787 413.4445 402.8473 36.1909 -4.2706 409.3136 413.5842 402.6984 37.7848 -4.2714 409.4307 413.7021 402.5437 39.3836 -4.2686 409.5543 413.8229 402.3946 40.9984 -4.2677 409.7070 413.9748 402.2208 42.6024 -4.2674 409.8551 414.1225 402.0803 44.2016 -4.2659 409.9901 414.2560 401.9248 45.8106 -4.2677 410.1176 414.3853 401.7774 47.4103 -4.2707 410.2478 414.5185 401.5886 49.0346 -4.2733 410.3499 414.6231 401.3976 50.6235 -4.2771 410.4586 414.7356 401.2349 52.2276 -4.2788 410.5883 414.8672 401.0457 53.8369 -4.2803 410.7015 414.9818 400.8622 55.4361 -4.2811 410.8097 415.0908 400.6865 57.0400 -4.2793 410.9294 415.2087 400.5112 58.6445 -4.2817 411.0183 415.3000 400.3434 60.2484 -4.2823 411.1091 415.3913 400.2029 61.8681 -4.2814 411.1945 415.4760 400.0502 63.4723 -4.2792 411.3041 415.5832 399.8891 65.0713 -4.2803 411.4016 415.6820 399.7362 66.6808 -4.2796 411.4811 415.7607 399.6042 68.2848 -4.2804 411.5832 415.8636 399.4352 69.8790 -4.2819 411.6701 415.9520 399.2734 71.4830 -4.2836 411.7503 416.0339 399.0922 73.0823 -4.2828 411.8364 416.1192 398.8996 74.7068 -4.2820 411.9195 416.2015 398.7173 76.3110 -4.2841 411.9767 416.2608 398.5356 77.9151 -4.2865 412.0387 416.3253 398.3789 79.5190 -4.2887 412.1068 416.3956 398.2241 81.1133 -4.2900 412.1715 416.4616 398.0684 82.7171 -4.2916 412.2243 416.5159 397.9110 84.3265 -4.2910 412.2791 416.5700 397.7358 85.9308 -4.2917 412.3518 416.6435 397.5714 87.5348 -4.2927 412.4046 416.6973 397.3775 89.1544 -4.2898 412.4492 416.7390 397.2039 90.7584 -4.2889 412.4962 416.7851 397.0171 92.3576 -4.2909 412.5482 416.8392 396.8449 93.9669 -4.2933 412.5817 416.8750 396.6787 95.5659 -4.2987 412.6313 416.9300 396.5186 97.1651 -4.3000 412.6987 416.9987 396.3205 98.7640 -4.2980 412.7386 417.0366 396.1448 100.3685 -4.2999 412.7571 417.0569 395.9719 101.9878 -4.3025 412.7806 417.0831 395.7946 103.5923 -4.3041 412.8236 417.1277 395.6160 105.1910 -4.3056 412.8387 417.1443 395.4547 106.8006 -4.3103 412.8766 417.1868 395.2846 108.4046 -4.3116 412.9079 417.2196 395.1256 110.0086 -4.3103 412.9140 417.2244 394.9582 111.6130 -4.3111 412.9256 417.2366 394.7750 113.2015 -4.3104 412.9360 417.2464 394.5908 114.8263 -4.3133 412.9331 417.2464 394.3926 116.4305 -4.3136 412.9715 417.2852 394.2297 118.0399 -4.3154 413.0004 417.3159 394.0747 119.6390 -4.3148 412.9918 417.3066 393.8773 121.2428 -4.3188 412.9587 417.2775 393.6548 122.8473 -4.3187 412.9701 417.2888 393.4759 124.4513 -4.3195 412.9809 417.3005 393.3171 126.0708 -4.3218 412.9819 417.3036 393.1431 127.6751 -4.3239 412.9586 417.2825 392.9635 129.2636 -4.3285 412.9495 417.2780 392.7867 130.8733 -4.3304 412.9461 417.2764 392.6216 132.4771 -4.3328 412.9331 417.2659 392.4399 134.0916 -4.3350 412.9299 417.2649 392.2714 135.6805 -4.3366 412.9194 417.2560 392.0934 137.2845 -4.3392 412.8958 417.2350 391.9341 138.9044 -4.3392 412.8620 417.2012 391.7568 140.5081 -4.3379 412.8614 417.1993 391.5897 142.1124 -4.3403 412.8518 417.1921 391.4241 143.7218 -4.3399 412.8261 417.1660 391.2381 145.3258 -4.3428 412.7932 417.1360 391.0802 146.9250 -4.3410 412.7797 417.1207 390.9043 148.5340 -4.3430 412.7400 417.0830 390.7276 150.1538 -4.3429 412.6858 417.0287 390.5524 151.7579 -4.3433 412.6553 416.9987 390.3469 153.3619 -4.3441 412.6236 416.9677 390.1569 154.9613 -4.3462 412.5710 416.9172 389.9787 156.5704 -4.3475 412.5304 416.8779 389.7956 158.1748 -4.3469 412.4969 416.8437 389.6292 159.7838 -4.3471 412.4473 416.7943 389.4494 161.3984 -4.3521 412.3877 416.7398 389.2551 163.0025 -4.3522 412.3131 416.6653 389.0870 164.6065 -4.3529 412.2586 416.6115 388.9117 166.2110 -4.3526 412.2091 416.5617 388.7416 167.8148 -4.3567 412.1595 416.5162 388.5550 169.4241 -4.3564 412.1072 416.4636 388.3689 171.0284 -4.3536 412.0492 416.4027 388.1924 172.6476 -4.3577 411.9801 416.3378 387.9985 174.2521 -4.3576 411.9438 416.3014 387.8222 175.8509 -4.3571 411.8923 416.2494 387.6165 177.4604 -4.3614 411.8192 416.1806 387.4138 179.0645 -4.3642 411.7440 416.1081 387.2291 180.6739 -4.3651 411.6913 416.0565 387.0542 182.2730 -4.3653 411.6184 415.9837 386.8737 183.8925 -4.3633 411.5481 415.9114 386.6752 185.4864 -4.3587 411.4740 415.8328 386.4850 187.0853 -4.3577 411.3906 415.7483 386.2957 188.6898 -4.3580 411.3082 415.6662 386.1111 190.2989 -4.3585 411.2511 415.6096 385.9242 191.8978 -4.3608 411.1988 415.5596 385.7377 193.5074 -4.3598 411.1268 415.4865 385.5489 195.1111 -4.3606 411.0768 415.4374 385.3468 196.7309 -4.3598 410.9974 415.3572 385.1687 198.3350 -4.3617 410.9021 415.2638 384.9953 199.9239 -4.3609 410.8257 415.1867 384.8151 201.5281 -4.3614 410.7207 415.0821 384.6466 203.1321 -4.3621 410.6463 415.0084 384.4748 204.7366 -4.3628 410.5557 414.9185 384.3013 206.3455 -4.3616 410.4507 414.8123 384.1197 207.9451 -4.3625 410.3688 414.7313 383.9341 209.5643 -4.3628 410.2790 414.6418 383.7473 211.1740 -4.3632 410.1868 414.5500 383.5492 212.7779 -4.3617 410.0889 414.4506 383.3588 214.3720 -4.3606 409.9838 414.3444 383.1840 215.9761 -4.3598 409.8968 414.2566 383.0114 217.5853 -4.3588 409.8053 414.1641 382.8309 219.1846 -4.3569 409.6945 414.0514 382.6433 220.7885 -4.3519 409.5941 413.9460 382.4394 222.4134 -4.3530 409.4961 413.8491 382.2499 224.0123 -4.3495 409.3891 413.7386 382.0610 225.6165 -4.3467 409.2879 413.6345 381.8682 227.2208 -4.3453 409.1902 413.5355 381.6963 228.8248 -4.3444 409.0856 413.4301 381.4945 230.4344 -4.3441 408.9828 413.3269 381.2908 232.0381 -4.3456 408.8773 413.2229 381.1043 233.6528 -4.3433 408.7598 413.1031 380.9334 235.2466 -4.3431 408.6462 412.9893 380.7382 236.8510 -4.3401 408.5452 412.8853 380.5769 238.4603 -4.3404 408.4289 412.7693 380.3965 240.0590 -4.3399 408.3078 412.6477 380.2078 241.6636 -4.3344 408.1783 412.5127 380.0329 243.2725 -4.3311 408.0479 412.3790 379.8540 244.8719 -4.3329 407.9552 412.2881 379.6724 246.4913 -4.3291 407.8458 412.1749 379.4817 248.1005 -4.3241 407.7189 412.0431 379.2868 249.7049 -4.3250 407.6042 411.9292 379.1127 251.3139 -4.3210 407.4888 411.8098 378.9131 252.9184 -4.3157 407.3625 411.6782 378.7198 254.5274 -4.3125 407.2496 411.5621 378.5540 256.1268 -4.3104 407.1373 411.4477 378.3601 257.7461 -4.3110 407.0332 411.3442 378.1623 259.3555 -4.3113 406.9181 411.2295 377.9584 260.9598 -4.3091 406.8054 411.1144 377.7686 262.5638 -4.3046 406.6812 410.9858 377.5628 264.1683 -4.3000 406.5330 410.8330 377.3620 265.7670 -4.2971 406.3977 410.6948 377.1701 267.3768 -4.2940 406.2805 410.5746 376.9842 268.9806 -4.2921 406.1650 410.4571 376.8160 270.6003 -4.2934 406.0363 410.3297 376.6292 272.1941 -4.2911 405.9066 410.1978 376.4400 273.7981 -4.2883 405.7726 410.0609 376.2628 275.4025 -4.2850 405.6417 409.9268 376.0888 277.0013 -4.2847 405.4969 409.7816 375.9095 278.6056 -4.2820 405.3538 409.6358 375.7373 280.2098 -4.2788 405.2182 409.4970 375.5695 281.8293 -4.2788 405.0809 409.3597 375.3801 283.4336 -4.2759 404.9566 409.2325 375.2133 285.0425 -4.2730 404.8289 409.1019 375.0200 286.6470 -4.2700 404.6927 408.9627 374.8095 288.2510 -4.2669 404.5580 408.8249 374.6051 289.8551 -4.2645 404.4206 408.6851 374.3987 291.4595 -4.2617 404.2690 408.5307 374.1981 293.0786 -4.2580 404.1246 408.3826 373.9978 294.6678 -4.2544 404.0015 408.2558 373.8016 296.2769 -4.2523 403.8670 408.1193 373.6017 297.8811 -4.2492 403.7454 407.9945 373.4035 299.4803 -4.2432 403.6143 407.8575 373.2080 301.0899 -4.2400 403.4692 407.7092 373.0064 302.6939 -4.2391 403.3486 407.5878 372.7996 304.3034 -4.2334 403.1888 407.4222 372.5905 305.9178 -4.2286 403.0418 407.2704 372.3838 307.5218 -4.2257 402.8971 407.1228 372.2027 309.1263 -4.2227 402.7534 406.9760 372.0280 310.7146 -4.2205 402.6061 406.8266 371.8403 312.3140 -4.2213 402.4399 406.6612 371.6388 313.9231 -4.2193 402.2826 406.5019 371.4381 315.5275 -4.2148 402.1551 406.3698 371.2580 317.1368 -4.2098 402.0093 406.2191 371.0743 318.7561 -4.2042 401.8711 406.0753 370.8852 320.3606 -4.2027 401.7123 405.9151 370.7002 321.9541 -4.2006 401.5732 405.7738 370.5318 323.5585 -4.1999 401.4260 405.6260 370.3416 325.1678 -4.1961 401.2812 405.4774 370.1407 326.7718 -4.1907 401.1236 405.3143 369.9506 328.3711 -4.1871 400.9468 405.1339 369.7505 329.9801 -4.1798 400.7929 404.9728 369.5533 331.6000 -4.1764 400.6745 404.8509 369.3706 333.2039 -4.1725 400.5191 404.6916 369.1814 334.8084 -4.1697 400.3403 404.5100 368.9960 336.4124 -4.1686 400.1744 404.3430 368.8071 338.0164 -4.1667 400.0197 404.1864 368.6045 339.6209 -4.1641 399.8580 404.0221 368.3997 341.2300 -4.1586 399.7112 403.8698 368.1851 342.8445 -4.1557 399.5494 403.7051 367.9759 344.4485 -4.1545 399.3967 403.5512 367.8035 346.0578 -4.1519 399.2489 403.4008 367.6178 347.6621 -4.1467 399.1104 403.2571 367.4209 349.2608 -4.1410 398.9414 403.0824 367.2195 350.8704 -4.1398 398.7806 402.9204 367.0190 352.4539 -4.1348 398.6214 402.7561 366.8281 354.0941 -4.1275 398.4475 402.5750 366.6171 355.6829 -4.1251 398.2892 402.4143 366.4180 357.2870 -4.1225 398.1264 402.2489 366.2275 358.8964 -4.1168 397.9679 402.0847 366.0336 360.5003 -4.1127 397.8210 401.9337 365.8373 362.1096 -4.1138 397.6593 401.7731 365.6322 363.7088 -4.1104 397.5124 401.6228 365.4445 365.3128 -4.1054 397.3482 401.4536 365.2407 366.9376 -4.1012 397.2038 401.3050 365.0506 368.5415 -4.0979 397.0271 401.1251 364.8818 370.1459 -4.0952 396.8568 400.9520 364.6900 371.7449 -4.0894 396.6982 400.7875 364.4928 373.3490 -4.0855 396.5142 400.5997 364.3092 374.9585 -4.0799 396.3512 400.4311 364.1030 376.5574 -4.0759 396.2005 400.2765 363.9144 378.1773 -4.0692 396.0357 400.1049 363.7226 379.7861 -4.0659 395.8629 399.9288 363.5397 381.3904 -4.0611 395.7017 399.7628 363.3522 382.9998 -4.0601 395.5440 399.6041 363.1646 384.5884 -4.0602 395.3783 399.4384 362.9706 386.1878 -4.0540 395.1953 399.2493 362.7770 387.7966 -4.0516 395.0248 399.0763 362.5724 389.3960 -4.0477 394.8426 398.8903 362.3741 391.0205 -4.0435 394.6818 398.7253 362.1761 392.6246 -4.0381 394.5130 398.5511 361.9556 394.2239 -4.0344 394.3556 398.3900 361.7484 395.8329 -4.0320 394.1669 398.1989 361.5531 397.4374 -4.0294 394.0173 398.0467 361.3627 399.0464 -4.0250 393.8545 397.8795 361.1572 400.6506 -4.0195 393.6794 397.6989 360.9769 402.2445 -4.0169 393.4936 397.5105 360.7727 403.8689 -4.0147 393.3138 397.3284 360.5501 405.4681 -4.0128 393.1538 397.1666 360.3535 407.0774 -4.0083 392.9853 396.9936 360.1490 408.6815 -4.0020 392.8073 396.8092 359.9568 410.2859 -3.9989 392.6310 396.6299 359.7630 411.8899 -3.9967 392.4577 396.4543 359.5834 413.4944 -3.9926 392.2886 396.2811 359.3840 415.1189 -3.9886 392.1495 396.1381 359.1783 416.7233 -3.9859 391.9710 395.9570 358.9841 418.3220 -3.9834 391.7874 395.7708 358.8003 419.9315 -3.9783 391.6041 395.5824 358.6165 421.5305 -3.9711 391.4085 395.3796 358.4208 423.1396 -3.9662 391.2458 395.2120 358.2160 424.7440 -3.9618 391.0903 395.0521 358.0381 426.3581 -3.9591 390.9054 394.8644 357.8297 427.9680 -3.9540 390.7436 394.6976 357.6535 429.5666 -3.9482 390.5701 394.5183 357.4723 431.1711 -3.9442 390.3915 394.3358 357.2623 432.7751 -3.9426 390.2124 394.1550 357.0621 434.3795 -3.9413 390.0610 394.0022 356.8678 435.9888 -3.9350 389.8850 393.8201 356.6891 437.6080 -3.9298 389.7089 393.6388 356.5177 439.2126 -3.9302 389.5353 393.4655 356.3365 440.8215 -3.9262 389.3713 393.2975 356.1603 442.4260 -3.9232 389.1700 393.0932 355.9709 444.0300 -3.9190 388.9878 392.9068 355.7651 445.6341 -3.9137 388.8025 392.7162 355.5722 447.2334 -3.9096 388.6194 392.5289 355.3870 448.8580 -3.9050 388.4419 392.3469 355.1631 450.4624 -3.9008 388.2731 392.1739 354.9418 452.0663 -3.8942 388.0882 391.9824 354.7361 453.6709 -3.8870 387.9429 391.8299 354.5308 455.2746 -3.8840 387.7889 391.6729 354.3449 456.8841 -3.8797 387.5915 391.4712 354.1535 458.4831 -3.8759 387.4168 391.2927 353.9461 460.0874 -3.8718 387.2174 391.0893 353.7580 461.6968 -3.8689 387.0356 390.9045 353.5753 463.3110 -3.8622 386.8703 390.7325 353.3870 464.9206 -3.8603 386.6916 390.5519 353.2074 466.5193 -3.8526 386.5280 390.3807 352.9935 468.1239 -3.8460 386.3502 390.1961 352.7846 469.7329 -3.8414 386.1779 390.0193 352.6064 471.3474 -3.8394 385.9706 389.8100 352.3815 472.9516 -3.8353 385.7999 389.6352 352.1761 474.5608 -3.8314 385.6277 389.4591 351.9920 476.1653 -3.8269 385.4229 389.2498 351.7982 477.7741 -3.8222 385.2499 389.0721 351.6060 479.3736 -3.8173 385.1039 388.9212 351.4254 480.9775 -3.8130 384.9171 388.7301 351.2310 482.6025 -3.8064 384.7091 388.5155 351.0343 484.2065 -3.8010 384.5082 388.3092 350.8712 485.8108 -3.7960 384.3430 388.1391 350.6985 487.4099 -3.7910 384.1501 387.9410 350.4847 489.0139 -3.7907 383.9745 387.7652 350.2926 490.6235 -3.7886 383.8001 387.5887 350.1009 492.2221 -3.7838 383.6057 387.3896 349.9263 493.8421 -3.7797 383.4028 387.1825 349.7236 495.4511 -3.7732 383.2333 387.0065 349.5147 497.0555 -3.7686 383.0558 386.8243 349.3161 498.6648 -3.7641 382.8865 386.6506 349.1180 500.2688 -3.7579 382.6991 386.4570 348.9249 501.8681 -3.7532 382.5023 386.2555 348.7296 503.4719 -3.7495 382.3163 386.0658 348.5086 505.0920 -3.7459 382.1364 385.8823 348.2856 506.7009 -3.7411 381.9742 385.7153 348.0910 508.2898 -3.7357 381.7871 385.5228 347.8929 509.8889 -3.7320 381.6116 385.3436 347.6790 511.5133 -3.7280 381.4111 385.1391 347.4710 513.1178 -3.7250 381.2081 384.9332 347.2624 514.7216 -3.7199 381.0143 384.7342 347.0643 516.3414 -3.7169 380.8168 384.5336 346.8655 517.9455 -3.7123 380.6440 384.3563 346.6471 519.5498 -3.7088 380.4637 384.1725 346.4474 521.1540 -3.7034 380.2725 383.9758 346.2492 522.7428 -3.6987 380.0917 383.7904 346.0675 524.3523 -3.6959 379.9045 383.6004 345.8803 525.9510 -3.6922 379.7239 383.4161 345.6962 527.5608 -3.6892 379.5491 383.2382 345.4964 529.2824 -3.6874 379.3532 383.0406 345.2945 530.9023 -3.6813 379.1868 382.8681 345.1001 532.5114 -3.6739 378.9970 382.6709 344.9104 534.1155 -3.6683 378.7943 382.4627 344.7131 535.7148 -3.6665 378.6095 382.2760 344.5113 537.3854 -3.6639 378.4362 382.1001 344.2929 539.0051 -3.6559 378.2738 381.9296 344.0804 540.6141 -3.6510 378.0728 381.7238 343.9027 542.3006 -3.6462 377.8654 381.5116 343.7014 544.0840 -3.6403 377.6541 381.2944 343.4942 545.6935 -3.6368 377.4732 381.1099 343.3111 547.2976 -3.6300 377.2890 380.9190 343.1086 548.9018 -3.6232 377.1054 380.7286 342.9266 550.5061 -3.6179 376.9191 380.5370 342.7396 552.1099 -3.6168 376.7385 380.3553 342.5431 553.7193 -3.6140 376.5502 380.1642 342.3309 555.3081 -3.6082 376.3517 379.9600 342.1427 556.9274 -3.6028 376.1291 379.7319 341.9511 558.5368 -3.5959 375.9235 379.5194 341.7515 560.1409 -3.5902 375.7446 379.3348 341.5602 561.7500 -3.5844 375.5660 379.1505 341.3876 563.3544 -3.5788 375.3863 378.9651 341.1895 564.9480 -3.5739 375.2052 378.7791 340.9766 566.5470 -3.5723 375.0101 378.5824 340.7537 568.1514 -3.5675 374.8051 378.3726 340.5504 569.7760 -3.5602 374.6095 378.1696 340.3558 571.3804 -3.5543 374.4362 377.9905 340.1498 572.9794 -3.5494 374.2476 377.7970 339.9613 574.6504 -3.5470 374.0603 377.6073 339.7407 576.2493 -3.5428 373.8754 377.4182 339.5334 577.8589 -3.5362 373.6930 377.2292 339.3224 579.5191 -3.5312 373.4985 377.0297 339.1306 581.1699 -3.5249 373.3015 376.8265 338.9448 582.7789 -3.5199 373.1209 376.6408 338.7655 584.3831 -3.5150 372.9297 376.4447 338.5646 585.9873 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