DTA measure 3_T250214.dat Date: 2025214:1359 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.12 s Mass = 100.000 mg data_number = 1024 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3680 -5.4124 441.0655 446.4779 421.4979 3.9751 -5.4237 441.0476 446.4713 421.7025 5.5979 -5.4353 441.0233 446.4585 421.9254 7.2103 -5.4476 441.0004 446.4479 422.1615 8.7919 -5.4595 440.9920 446.4515 422.3989 10.3885 -5.4718 440.9804 446.4522 422.6460 11.9908 -5.4854 440.9602 446.4456 422.9031 13.6029 -5.4992 440.9412 446.4404 423.1655 15.2050 -5.5132 440.9232 446.4365 423.4312 16.8121 -5.5263 440.9028 446.4291 423.6816 18.4346 -5.5395 440.8887 446.4282 423.9319 20.0368 -5.5523 440.8703 446.4226 424.1650 21.6490 -5.5654 440.8535 446.4189 424.3835 23.2511 -5.5783 440.8437 446.4220 424.5738 24.8636 -5.5910 440.8307 446.4217 424.7491 26.4658 -5.6030 440.8177 446.4207 424.8963 28.0729 -5.6153 440.8142 446.4295 425.0287 29.6959 -5.6263 440.8124 446.4387 425.1397 31.2979 -5.6368 440.8053 446.4421 425.2154 32.9105 -5.6464 440.8080 446.4544 425.2654 34.5229 -5.6560 440.8073 446.4633 425.2962 36.1095 -5.6650 440.8096 446.4745 425.2949 37.7218 -5.6732 440.8125 446.4857 425.2666 39.3240 -5.6808 440.8182 446.4991 425.2119 40.9260 -5.6877 440.8209 446.5085 425.1282 42.5435 -5.6931 440.8229 446.5160 425.0292 44.1458 -5.6978 440.8231 446.5209 424.8925 45.7426 -5.7041 440.8233 446.5274 424.7405 47.3550 -5.7087 440.8303 446.5391 424.5561 48.9569 -5.7131 440.8371 446.5502 424.3600 50.5639 -5.7153 440.8464 446.5617 424.1406 52.1710 -5.7173 440.8536 446.5709 423.8981 53.7781 -5.7192 440.8532 446.5724 423.6346 55.3853 -5.7213 440.8528 446.5742 423.3483 56.9871 -5.7236 440.8476 446.5712 423.0502 58.5995 -5.7252 440.8457 446.5709 422.7325 60.2119 -5.7254 440.8401 446.5656 422.3927 61.8139 -5.7254 440.8242 446.5497 422.0456 63.4210 -5.7253 440.8088 446.5340 421.6699 65.0281 -5.7240 440.7963 446.5203 421.2835 66.6510 -5.7221 440.7834 446.5055 420.9006 68.2583 -5.7198 440.7670 446.4869 420.4983 69.8551 -5.7168 440.7429 446.4597 420.0863 71.4573 -5.7151 440.7242 446.4393 419.6646 73.0541 -5.7119 440.6988 446.4107 419.2463 74.6613 -5.7086 440.6713 446.3799 418.8240 76.2685 -5.7062 440.6325 446.3388 418.3900 77.8654 -5.7027 440.5881 446.2909 417.9567 79.4881 -5.6997 440.5356 446.2352 417.5074 81.0903 -5.6953 440.4828 446.1781 417.0625 82.7026 -5.6908 440.4378 446.1286 416.6177 84.3048 -5.6865 440.3847 446.0712 416.1725 85.9068 -5.6819 440.3260 446.0079 415.7325 87.5140 -5.6774 440.2647 445.9420 415.2920 89.1213 -5.6741 440.1994 445.8735 414.8597 90.7389 -5.6697 440.1333 445.8030 414.4263 92.3356 -5.6645 440.0606 445.7251 414.0103 93.9429 -5.6592 439.9791 445.6383 413.5952 95.5503 -5.6547 439.9012 445.5559 413.1934 97.1625 -5.6503 439.8163 445.4666 412.7961 98.7645 -5.6457 439.7266 445.3723 412.4166 100.3719 -5.6410 439.6355 445.2765 412.0449 101.9791 -5.6361 439.5378 445.1740 411.6736 103.5966 -5.6329 439.4321 445.0650 411.3228 105.2035 -5.6294 439.3158 444.9452 410.9819 106.7951 -5.6266 439.2070 444.8337 410.6595 108.3921 -5.6250 439.1038 444.7288 410.3449 110.0044 -5.6222 438.9950 444.6171 410.0427 111.6013 -5.6187 438.8773 444.4960 409.7634 113.2085 -5.6158 438.7556 444.3714 409.4998 114.8158 -5.6151 438.6285 444.2436 409.2489 116.4385 -5.6150 438.5065 444.1216 409.0045 118.0405 -5.6132 438.3761 443.9893 408.7829 119.6528 -5.6128 438.2484 443.8611 408.5733 121.2548 -5.6122 438.1123 443.7245 408.3855 122.8669 -5.6117 437.9788 443.5905 408.2113 124.4743 -5.6120 437.8464 443.4584 408.0547 126.0659 -5.6122 437.7074 443.3196 407.9015 127.6734 -5.6132 437.5726 443.1858 407.7521 129.2961 -5.6145 437.4297 443.0441 407.6302 130.9031 -5.6159 437.2889 442.9048 407.5226 132.5104 -5.6182 437.1418 442.7600 407.4112 134.1223 -5.6200 436.9991 442.6191 407.3182 135.7193 -5.6225 436.8511 442.4737 407.2278 137.3213 -5.6252 436.7032 442.3285 407.1483 138.9285 -5.6269 436.5527 442.1796 407.0789 140.5459 -5.6292 436.4044 442.0336 407.0091 142.1428 -5.6321 436.2619 441.8940 406.9457 143.7553 -5.6341 436.1134 441.7475 406.8841 145.3416 -5.6360 435.9559 441.5919 406.8213 146.9540 -5.6387 435.8030 441.4417 406.7686 148.5559 -5.6410 435.6614 441.3025 406.7092 150.1630 -5.6426 435.5074 441.1500 406.6491 151.7703 -5.6440 435.3594 441.0034 406.5898 153.3621 -5.6465 435.2160 440.8624 406.5255 154.9846 -5.6501 435.0692 440.7193 406.4494 156.5919 -5.6525 434.9199 440.5724 406.3759 158.1989 -5.6548 434.7700 440.4247 406.3026 159.8113 -5.6578 434.6277 440.2855 406.2183 161.4135 -5.6603 434.4815 440.1418 406.1263 163.0206 -5.6627 434.3258 439.9885 406.0315 164.6174 -5.6646 434.1828 439.8474 405.9285 166.2245 -5.6661 434.0365 439.7026 405.8155 167.8421 -5.6668 433.8857 439.5525 405.6926 169.4441 -5.6674 433.7325 439.3999 405.5628 171.0411 -5.6677 433.5861 439.2537 405.4220 172.6534 -5.6676 433.4444 439.1120 405.2761 174.2504 -5.6687 433.2906 438.9593 405.1185 175.8523 -5.6689 433.1373 438.8062 404.9599 177.4648 -5.6690 432.9878 438.6568 404.7809 179.0515 -5.6686 432.8402 438.5087 404.5972 180.6741 -5.6669 432.6922 438.3591 404.4078 182.2815 -5.6649 432.5526 438.2175 404.2076 183.8938 -5.6628 432.4043 438.0670 404.0080 185.5009 -5.6604 432.2560 437.9164 403.7994 187.0923 -5.6584 432.1118 437.7702 403.5857 188.7045 -5.6565 431.9588 437.6153 403.3600 190.3116 -5.6549 431.8095 437.4643 403.1222 191.9188 -5.6527 431.6560 437.3087 402.8766 193.5468 -5.6497 431.5058 437.1554 402.6179 195.1541 -5.6476 431.3527 437.0003 402.3570 196.7561 -5.6455 431.2058 436.8513 402.0882 198.3686 -5.6429 431.0511 436.6940 401.8186 199.9709 -5.6401 430.8967 436.5368 401.5417 201.5779 -5.6370 430.7471 436.3841 401.2563 203.1643 -5.6326 430.5942 436.2269 400.9856 204.7664 -5.6283 430.4369 436.0652 400.7033 206.3889 -5.6243 430.2724 435.8966 400.4059 207.9858 -5.6209 430.1161 435.7369 400.1198 209.5983 -5.6170 429.9525 435.5695 399.8206 211.2001 -5.6118 429.7972 435.4090 399.5317 212.7969 -5.6056 429.6392 435.2448 399.2392 214.3989 -5.6012 429.4809 435.0822 398.9454 216.0060 -5.5962 429.3168 434.9130 398.6481 217.6184 -5.5910 429.1563 434.7472 398.3476 219.2410 -5.5857 428.9869 434.5726 398.0450 220.8429 -5.5807 428.8228 434.4035 397.7610 222.4554 -5.5753 428.6517 434.2270 397.4712 224.0573 -5.5704 428.4847 434.0552 397.1901 225.6698 -5.5655 428.3171 433.8826 396.9084 227.2720 -5.5609 428.1437 433.7046 396.6251 228.8790 -5.5554 427.9646 433.5201 396.3540 230.5016 -5.5506 427.7859 433.3366 396.0773 232.1036 -5.5451 427.6107 433.1558 395.8002 233.6900 -5.5390 427.4343 432.9732 395.5368 235.2868 -5.5336 427.2601 432.7937 395.2778 236.8943 -5.5284 427.0819 432.6103 395.0159 238.4964 -5.5221 426.9005 432.4227 394.7618 240.0985 -5.5174 426.7225 432.2400 394.5118 241.7110 -5.5132 426.5435 432.0567 394.2661 243.3288 -5.5067 426.3641 431.8708 394.0261 244.9360 -5.5016 426.1910 431.6926 393.7986 246.5435 -5.4970 426.0101 431.5071 393.5736 248.1458 -5.4916 425.8275 431.3191 393.3534 249.7580 -5.4872 425.6431 431.1303 393.1389 251.3600 -5.4836 425.4568 430.9404 392.9342 252.9724 -5.4800 425.2662 430.7462 392.7314 254.5950 -5.4760 425.0711 430.5471 392.5194 256.2073 -5.4714 424.8798 430.3512 392.3187 257.7939 -5.4672 424.6961 430.1633 392.1238 259.4064 -5.4635 424.5089 429.9724 391.9310 261.0083 -5.4595 424.3198 429.7792 391.7431 262.6154 -5.4553 424.1212 429.5765 391.5588 264.2278 -5.4521 423.9280 429.3801 391.3838 265.8298 -5.4476 423.7388 429.1865 391.2210 267.4423 -5.4433 423.5467 428.9900 391.0489 269.0443 -5.4398 423.3564 428.7961 390.8775 270.6360 -5.4372 423.1779 428.6151 390.7175 272.2383 -5.4342 422.9864 428.4206 390.5550 273.8453 -5.4301 422.7899 428.2200 390.4060 275.4473 -5.4271 422.5978 428.0249 390.2536 277.0595 -5.4233 422.3999 427.8233 390.1004 278.6463 -5.4201 422.2067 427.6267 389.9423 280.2535 -5.4174 422.0068 427.4243 389.7886 281.8761 -5.4152 421.8175 427.2328 389.6292 283.4835 -5.4119 421.6278 427.0396 389.4869 285.0906 -5.4089 421.4342 426.8431 389.3334 286.7031 -5.4064 421.2412 426.6476 389.1832 288.3050 -5.4042 421.0496 426.4538 389.0284 289.9174 -5.4015 420.8458 426.2473 388.8741 291.5041 -5.3982 420.6549 426.0531 388.7234 293.1165 -5.3936 420.4653 425.8589 388.5632 294.7393 -5.3900 420.2713 425.6612 388.4001 296.3461 -5.3860 420.0906 425.4766 388.2336 297.9535 -5.3822 419.8999 425.2821 388.0643 299.5501 -5.3786 419.7104 425.0890 387.9077 301.1473 -5.3757 419.5185 424.8942 387.7477 302.7493 -5.3733 419.3298 424.7030 387.5711 304.3518 -5.3695 419.1389 424.5084 387.3891 305.9744 -5.3665 418.9424 424.3089 387.2068 307.5816 -5.3616 418.7498 424.1114 387.0190 309.1835 -5.3565 418.5581 423.9146 386.8363 310.7959 -5.3528 418.3610 423.7138 386.6362 312.3823 -5.3501 418.1687 423.5187 386.4433 313.9948 -5.3461 417.9784 423.3245 386.2450 315.5970 -5.3417 417.7955 423.1371 386.0440 317.2091 -5.3364 417.5993 422.9357 385.8436 318.8316 -5.3322 417.4003 422.7324 385.6311 320.4390 -5.3272 417.2092 422.5364 385.4246 322.0413 -5.3233 417.0236 422.3469 385.2096 323.6538 -5.3191 416.8410 422.1601 384.9971 325.2558 -5.3151 416.6536 421.9687 384.7836 326.8684 -5.3107 416.4594 421.7700 384.5569 328.4705 -5.3055 416.2740 421.5795 384.3324 330.0933 -5.3001 416.0829 421.3830 384.1066 331.6900 -5.2957 415.8977 421.1934 383.8782 333.2923 -5.2915 415.7134 421.0049 383.6542 334.8894 -5.2871 415.5268 420.8139 383.4227 336.5016 -5.2825 415.3359 420.6184 383.1940 338.0884 -5.2777 415.1452 420.4229 382.9732 339.6956 -5.2722 414.9548 420.2270 382.7402 341.3028 -5.2668 414.7588 420.0256 382.5043 342.9255 -5.2609 414.5610 419.8220 382.2609 344.5326 -5.2564 414.3791 419.6355 382.0236 346.1345 -5.2519 414.1980 419.4499 381.7869 347.7469 -5.2459 414.0091 419.2551 381.5557 349.3489 -5.2410 413.8166 419.0576 381.3250 350.9561 -5.2362 413.6294 418.8656 381.0900 352.5634 -5.2307 413.4370 418.6677 380.8588 354.1863 -5.2254 413.2405 418.4660 380.6218 355.7986 -5.2191 413.0451 418.2642 380.3842 357.4059 -5.2126 412.8449 418.0574 380.1433 359.0079 -5.2063 412.6546 417.8610 379.9040 360.6203 -5.2008 412.4568 417.6576 379.6554 362.2169 -5.1948 412.2614 417.4561 379.4147 363.8033 -5.1889 412.0673 417.2561 379.1754 365.4158 -5.1827 411.8727 417.0555 378.9304 367.0281 -5.1762 411.6714 416.8476 378.6907 368.6355 -5.1700 411.4705 416.6405 378.4543 370.2374 -5.1640 411.2699 416.4339 378.2240 371.8240 -5.1575 411.0737 416.2312 377.9957 373.4363 -5.1513 410.8734 416.0248 377.7629 375.0384 -5.1454 410.6711 415.8166 377.5316 376.6456 -5.1396 410.4719 415.6115 377.3093 378.2531 -5.1330 410.2756 415.4086 377.0813 379.8811 -5.1261 410.0721 415.1982 376.8492 381.4831 -5.1206 409.8711 414.9917 376.6180 383.0956 -5.1142 409.6707 414.7849 376.3906 384.6978 -5.1093 409.4705 414.5798 376.1754 386.3101 -5.1044 409.2737 414.3781 375.9563 387.9171 -5.0988 409.0692 414.1680 375.7353 389.5090 -5.0925 408.8711 413.9636 375.5279 391.1163 -5.0863 408.6609 413.7472 375.3211 392.7390 -5.0805 408.4542 413.5347 375.1092 394.3410 -5.0758 408.2555 413.3313 374.9045 395.9428 -5.0706 408.0556 413.1262 374.6930 397.5501 -5.0658 407.8527 412.9184 374.4865 399.1364 -5.0604 407.6480 412.7084 374.2836 400.7384 -5.0554 407.4387 412.4941 374.0816 402.3458 -5.0502 407.2328 412.2830 373.8871 403.9476 -5.0459 407.0252 412.0711 373.6938 405.5703 -5.0420 406.8177 411.8597 373.4999 407.1724 -5.0379 406.6151 411.6529 373.3101 408.7849 -5.0319 406.4127 411.4446 373.1206 410.3871 -5.0268 406.2089 411.2356 372.9271 411.9944 -5.0226 406.0049 411.0275 372.7354 413.6016 -5.0177 405.7971 410.8148 372.5457 415.2140 -5.0125 405.5976 410.6101 372.3517 416.8056 -5.0076 405.3984 410.4060 372.1607 418.4281 -5.0027 405.1943 410.1970 371.9676 420.0303 -4.9973 404.9951 409.9924 371.7778 421.6426 -4.9923 404.7844 409.7767 371.5911 423.2549 -4.9868 404.5823 409.5691 371.4034 424.8569 -4.9813 404.3818 409.3631 371.2188 426.4640 -4.9750 404.1843 409.1593 371.0297 428.0663 -4.9694 403.9875 408.9570 370.8482 429.6838 -4.9661 403.7930 408.7591 370.6621 431.2909 -4.9611 403.5929 408.5540 370.4761 432.8878 -4.9563 403.3931 408.3495 370.2891 434.5001 -4.9517 403.1895 408.1412 370.0973 436.1023 -4.9457 402.9814 407.9271 369.9048 437.7146 -4.9406 402.7668 407.7074 369.7135 439.3011 -4.9372 402.5655 407.5027 369.5288 440.9084 -4.9324 402.3613 407.2936 369.3344 442.5311 -4.9273 402.1577 407.0850 369.1394 444.1329 -4.9217 401.9581 406.8799 368.9499 445.7453 -4.9172 401.7555 406.6727 368.7577 447.3474 -4.9119 401.5508 406.4627 368.5659 448.9598 -4.9065 401.3490 406.2555 368.3654 450.5620 -4.9004 401.1534 406.0538 368.1666 452.1693 -4.8957 400.9510 405.8466 367.9780 453.7916 -4.8919 400.7486 405.6405 367.7879 455.4040 -4.8871 400.5438 405.4309 367.5902 457.0059 -4.8817 400.3440 405.2257 367.3901 458.6080 -4.8775 400.1423 405.0198 367.1924 460.2153 -4.8728 399.9452 404.8180 366.9888 461.8174 -4.8684 399.7445 404.6129 366.7781 463.4143 -4.8635 399.5434 404.4068 366.5753 465.0371 -4.8575 399.3363 404.1938 366.3646 466.6443 -4.8520 399.1362 403.9882 366.1547 468.2359 -4.8457 398.9404 403.7861 365.9495 469.8376 -4.8404 398.7427 403.5831 365.7368 471.4501 -4.8357 398.5372 403.3729 365.5158 473.0519 -4.8305 398.3362 403.1668 365.2969 474.6591 -4.8246 398.1355 402.9601 365.0837 476.2664 -4.8198 397.9366 402.7564 364.8696 477.8893 -4.8132 397.7266 402.5398 364.6511 479.4964 -4.8064 397.5236 402.3300 364.4367 481.0984 -4.8000 397.3254 402.1254 364.2195 482.7110 -4.7952 397.1200 401.9152 363.9973 484.3129 -4.7909 396.9194 401.7103 363.7803 485.9254 -4.7859 396.7250 401.5109 363.5644 487.5325 -4.7798 396.5299 401.3097 363.3463 489.1554 -4.7750 396.3265 401.1015 363.1309 490.7625 -4.7708 396.1217 400.8925 362.9175 492.3440 -4.7659 395.9265 400.6924 362.7029 493.9564 -4.7614 395.7227 400.4841 362.4799 495.5533 -4.7565 395.5235 400.2799 362.2659 497.1655 -4.7513 395.3160 400.0673 362.0511 498.7674 -4.7458 395.1061 399.8519 361.8363 500.3796 -4.7402 394.9006 399.6408 361.6204 501.9818 -4.7361 394.6995 399.4357 361.4053 503.5891 -4.7311 394.4958 399.2268 361.1771 505.1964 -4.7247 394.2905 399.0152 360.9566 506.7984 -4.7182 394.0904 398.8086 360.7408 508.4108 -4.7118 393.8879 398.5997 360.5256 510.0128 -4.7051 393.6855 398.3906 360.3072 511.6253 -4.7000 393.4772 398.1772 360.0930 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-1.9240 255.3772 257.3012 221.8279 1598.2401 -1.9212 255.1714 257.0926 221.6405 1599.8421 -1.9190 254.9700 256.8890 221.4434 1601.4491 -1.9171 254.7682 256.6854 221.2522 1603.0564 -1.9147 254.5653 256.4800 221.0596 1604.6738 -1.9123 254.3666 256.2789 220.8681 1606.2859 -1.9099 254.1650 256.0749 220.6725 1607.8878 -1.9078 253.9678 255.8756 220.4776 1609.5003 -1.9059 253.7696 255.6754 220.2826 1611.1023 -1.9037 253.5698 255.4735 220.0935 1612.7094 -1.9013 253.3694 255.2707 219.9005 1614.3169 -1.8981 253.1622 255.0603 219.7111 1615.9344 -1.8951 252.9552 254.8503 219.5239 1617.5468 -1.8923 252.7475 254.6399 219.3248 1619.1488 -1.8900 252.5496 254.4397 219.1368 1620.7614 -1.8883 252.3466 254.2350 218.9475 1622.3635 -1.8861 252.1481 254.0341 218.7584 1623.9708 -1.8843 251.9389 253.8232 218.5612 1625.5829 -1.8818 251.7348 253.6166 218.3675 1627.2056 -1.8792 251.5363 253.4156 218.1761 1628.8129 -1.8769 251.3330 253.2099 217.9902 1630.4203 -1.8748 251.1329 253.0077 217.7943 1632.0323 -1.8720 250.9314 252.8033 217.6007 1633.6344 -1.8702 250.7303 252.6005 217.4050 1635.2470 -1.8690 250.5296 252.3986 217.2065 1636.8489 -1.8669 250.3263 252.1932 217.0159 1638.4716 -1.8639 250.1274 251.9913 216.8226 1640.0789 -1.8607 249.9278 251.7885 216.6404 1641.6808 -1.8579 249.7283 251.5862 216.4561 1643.2931 -1.8552 249.5347 251.3899 216.2651 1644.8953 -1.8518 249.3404 251.1922 216.0726 1646.5078 -1.8506 249.1455 250.9961 215.8767 1648.1200 -1.8491 248.9527 250.8018 215.6934