DTA measure 1pb3 Test Date: 20231123:1247 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1018.93 s Mass = 1128.900 mg data_number = 1253 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1238 -1.8825 274.7396 276.6222 264.2173 2.7340 -1.8797 274.7301 276.6098 264.2028 3.4938 -1.8815 274.7446 276.6262 264.2141 5.1370 -1.8811 274.7392 276.6203 264.2102 5.8985 -1.8817 274.7507 276.6324 264.2068 7.5128 -1.8819 274.7489 276.6308 264.2433 8.3348 -1.8821 274.7350 276.6171 264.2534 9.9185 -1.8802 274.7494 276.6295 264.2892 10.7710 -1.8805 274.7484 276.6289 264.3338 12.3548 -1.8837 274.7688 276.6525 264.3950 13.1503 -1.8848 274.7794 276.6642 264.4450 14.7948 -1.8844 274.7797 276.6640 264.5568 15.5565 -1.8841 274.7797 276.6638 264.6190 16.3788 -1.8804 274.7835 276.6640 264.6870 17.1705 -1.8845 274.7793 276.6638 264.7713 17.9625 -1.8858 274.7787 276.6644 264.8503 18.8148 -1.8860 274.7961 276.6821 264.9546 19.5765 -1.8851 274.7973 276.6824 265.0507 20.3985 -1.8848 274.7976 276.6824 265.1329 21.2205 -1.8859 274.7868 276.6727 265.2227 21.9825 -1.8894 274.7842 276.6736 265.3180 22.8345 -1.8894 274.8054 276.6948 265.4154 23.6265 -1.8894 274.8093 276.6987 265.5225 24.4185 -1.8908 274.8123 276.7031 265.6335 25.2408 -1.8926 274.8185 276.7111 265.7399 26.0035 -1.8932 274.8270 276.7202 265.8531 26.8545 -1.8930 274.8362 276.7292 265.9888 27.6425 -1.8933 274.8293 276.7226 266.1073 28.4303 -1.8933 274.8300 276.7233 266.2457 29.2490 -1.8967 274.8520 276.7488 266.3667 30.0080 -1.8976 274.8550 276.7525 266.4902 30.8568 -1.8961 274.8698 276.7659 266.6302 31.6450 -1.8992 274.8666 276.7658 266.7622 32.4340 -1.8994 274.8621 276.7616 266.8981 33.3553 -1.9014 274.8698 276.7712 267.0624 34.2180 -1.9044 274.8532 276.7576 267.2013 35.0685 -1.9078 274.8679 276.7758 267.3459 35.8598 -1.9082 274.8858 276.7940 267.4817 36.6515 -1.9122 274.8965 276.8087 267.6323 37.4735 -1.9111 274.9054 276.8165 267.7718 38.2355 -1.9139 274.9150 276.8289 267.8992 39.0875 -1.9172 274.9309 276.8481 268.0586 39.8795 -1.9210 274.9281 276.8491 268.1958 40.6715 -1.9258 274.9437 276.8694 268.3339 41.4935 -1.9262 274.9390 276.8652 268.4540 42.2555 -1.9266 274.9622 276.8889 268.5958 43.1073 -1.9287 274.9620 276.8907 268.7375 43.8993 -1.9301 274.9680 276.8981 268.8821 44.6908 -1.9325 274.9844 276.9169 269.0205 45.5130 -1.9356 274.9768 276.9124 269.1498 46.2745 -1.9381 275.0116 276.9497 269.2782 47.1270 -1.9402 275.0263 276.9665 269.4116 47.9190 -1.9425 275.0246 276.9671 269.5590 48.7105 -1.9446 275.0258 276.9704 269.6711 49.5330 -1.9459 275.0446 276.9905 269.7985 50.2945 -1.9489 275.0508 276.9996 269.9370 51.1470 -1.9514 275.0753 277.0267 270.0792 51.9088 -1.9529 275.0927 277.0457 270.2094 52.7315 -1.9562 275.1052 277.0615 270.3339 53.5540 -1.9566 275.1201 277.0767 270.4615 54.3165 -1.9590 275.1331 277.0921 270.5817 55.1688 -1.9617 275.1414 277.1031 270.7215 55.9305 -1.9657 275.1679 277.1336 270.8274 56.7528 -1.9675 275.1897 277.1572 270.9652 57.5745 -1.9712 275.1866 277.1578 271.1004 58.3365 -1.9726 275.1992 277.1718 271.2111 59.1885 -1.9731 275.2153 277.1884 271.3519 59.9783 -1.9765 275.2265 277.2030 271.4584 60.7678 -1.9790 275.2556 277.2346 271.5927 61.5860 -1.9793 275.2789 277.2581 271.7241 62.3440 -1.9829 275.3105 277.2934 271.8399 63.1925 -1.9867 275.3307 277.3174 271.9582 63.9523 -1.9861 275.3301 277.3161 272.0695 64.7760 -1.9859 275.3558 277.3417 272.1900 65.5940 -1.9902 275.3799 277.3701 272.3235 66.3520 -1.9925 275.3935 277.3860 272.4421 67.2008 -1.9966 275.4267 277.4232 272.5528 67.9618 -1.9994 275.4422 277.4417 272.6851 68.7815 -2.0011 275.4647 277.4658 272.7790 69.6038 -2.0044 275.4837 277.4882 272.8994 70.3655 -2.0078 275.4976 277.5054 273.0152 71.2175 -2.0083 275.5338 277.5422 273.1452 71.9795 -2.0091 275.5672 277.5763 273.2575 72.8015 -2.0114 275.5810 277.5924 273.3708 73.5935 -2.0179 275.6013 277.6193 273.4891 74.3855 -2.0185 275.6286 277.6471 273.6178 75.2375 -2.0200 275.6530 277.6730 273.7346 75.9995 -2.0197 275.6792 277.6989 273.8413 76.8215 -2.0240 275.6836 277.7077 273.9397 77.6135 -2.0287 275.7260 277.7547 274.0460 78.4055 -2.0290 275.7529 277.7820 274.1731 79.2275 -2.0282 275.7881 277.8163 274.2964 80.0195 -2.0325 275.8285 277.8610 274.4328 80.8415 -2.0350 275.8346 277.8697 274.5576 81.6335 -2.0335 275.8682 277.9017 274.6679 82.4253 -2.0376 275.9116 277.9492 274.7880 83.2475 -2.0404 275.9451 277.9855 274.9322 84.0390 -2.0421 275.9714 278.0136 275.0567 85.0635 -2.0454 275.9911 278.0366 275.1829 85.8560 -2.0460 276.0259 278.0719 275.3164 86.6475 -2.0473 276.0588 278.1061 275.4381 87.4700 -2.0497 276.0964 278.1461 275.5822 88.2315 -2.0529 276.1123 278.1652 275.7086 89.0840 -2.0542 276.1445 278.1988 275.8313 89.8760 -2.0556 276.1949 278.2504 275.9537 90.6685 -2.0562 276.2173 278.2735 276.0727 91.4910 -2.0580 276.2591 278.3171 276.2051 92.2810 -2.0593 276.2936 278.3529 276.3257 93.0990 -2.0600 276.3043 278.3643 276.4503 93.8870 -2.0593 276.3421 278.4014 276.5564 94.6750 -2.0611 276.3798 278.4409 276.6929 95.4933 -2.0647 276.4164 278.4811 276.8241 96.2510 -2.0677 276.4473 278.5150 276.9368 97.1008 -2.0681 276.4913 278.5595 277.0716 97.8895 -2.0682 276.5351 278.6033 277.1887 98.6780 -2.0696 276.5794 278.6489 277.2873 99.4973 -2.0715 276.6129 278.6844 277.4187 100.2575 -2.0748 276.6482 278.7231 277.5446 101.1090 -2.0774 276.6739 278.7513 277.6685 101.9013 -2.0805 276.7241 278.8047 277.7956 102.6925 -2.0821 276.7636 278.8457 277.8960 103.5150 -2.0826 276.7903 278.8729 278.0208 104.2765 -2.0827 276.8226 278.9053 278.1549 105.1290 -2.0834 276.8732 278.9566 278.2854 105.8908 -2.0863 276.9018 278.9880 278.4032 106.7128 -2.0875 276.9384 279.0259 278.5322 107.5348 -2.0899 276.9982 279.0881 278.6746 108.2965 -2.0905 277.0380 279.1285 278.8188 109.1488 -2.0908 277.1012 279.1920 278.9503 109.9105 -2.0949 277.1427 279.2376 279.0736 110.7328 -2.0933 277.1808 279.2741 279.2024 111.5548 -2.0972 277.2127 279.3098 279.3440 112.3165 -2.0982 277.2539 279.3521 279.4494 113.1688 -2.0995 277.3037 279.4032 279.6185 113.9305 -2.1020 277.3288 279.4308 279.7352 114.7525 -2.1029 277.3788 279.4816 279.8728 115.5475 -2.1073 277.4397 279.5470 279.9924 116.3415 -2.1100 277.4717 279.5817 280.1440 117.1940 -2.1105 277.5210 279.6315 280.2749 117.9565 -2.1133 277.5769 279.6902 280.3817 118.7785 -2.1133 277.6118 279.7251 280.5183 119.5705 -2.1127 277.6662 279.7789 280.6487 120.3625 -2.1141 277.7322 279.8464 280.7645 121.2150 -2.1147 277.7721 279.8868 280.9285 121.9775 -2.1141 277.8194 279.9335 281.0527 122.7998 -2.1151 277.8647 279.9798 281.1719 123.5923 -2.1177 277.9193 280.0369 281.3070 124.3813 -2.1169 277.9644 280.0813 281.4441 125.2293 -2.1201 278.0167 280.1368 281.5570 125.9873 -2.1187 278.0590 280.1777 281.6943 126.8058 -2.1195 278.1166 280.2361 281.8063 127.5940 -2.1225 278.1715 280.2941 281.9457 128.3818 -2.1233 278.2309 280.3541 282.0730 129.2305 -2.1233 278.2638 280.3871 282.1882 129.9890 -2.1267 278.3185 280.4452 282.3049 130.8078 -2.1267 278.3861 280.5128 282.4451 131.6263 -2.1259 278.4282 280.5542 282.5682 132.3860 -2.1295 278.4846 280.6141 282.6858 133.2375 -2.1340 278.5400 280.6740 282.7962 134.0288 -2.1315 278.6069 280.7384 282.9301 134.8205 -2.1329 278.6598 280.7926 283.0367 135.7460 -2.1344 278.7154 280.8497 283.1982 136.6123 -2.1356 278.7681 280.9036 283.3216 137.4645 -2.1387 278.8350 280.9737 283.4524 138.2265 -2.1397 278.8848 281.0245 283.5657 139.0478 -2.1381 278.9558 281.0939 283.6801 139.8405 -2.1401 279.0045 281.1446 283.8135 140.6315 -2.1420 279.0639 281.2059 283.9245 141.4843 -2.1422 279.1240 281.2661 284.0447 142.2458 -2.1487 279.1788 281.3275 284.1597 143.0678 -2.1499 279.2519 281.4018 284.2653 143.8900 -2.1488 279.2929 281.4418 284.3993 144.6518 -2.1496 279.3503 281.4999 284.5066 145.5050 -2.1499 279.4263 281.5762 284.6482 146.2668 -2.1505 279.4756 281.6261 284.7680 147.0888 -2.1546 279.5271 281.6817 284.9239 147.9110 -2.1545 279.5743 281.7289 285.0508 148.6725 -2.1541 279.6420 281.7961 285.1711 149.5250 -2.1561 279.7267 281.8828 285.3189 150.2865 -2.1586 279.7842 281.9428 285.4435 151.1088 -2.1611 279.8475 282.0086 285.5684 151.9308 -2.1602 279.9090 282.0691 285.6979 152.6925 -2.1600 279.9614 282.1214 285.8418 153.5445 -2.1600 280.0450 282.2050 285.9877 154.3365 -2.1636 280.1040 282.2677 286.1146 155.1285 -2.1655 280.1675 282.3331 286.2303 155.9498 -2.1647 280.2233 282.3881 286.4022 156.7380 -2.1662 280.2960 282.4622 286.5325 157.5568 -2.1657 280.3768 282.5425 286.6582 158.3450 -2.1656 280.4308 282.5964 286.7980 159.1330 -2.1644 280.4855 282.6499 286.9397 159.9518 -2.1676 280.5529 282.7205 287.0687 160.7400 -2.1683 280.6281 282.7964 287.1959 161.5588 -2.1701 280.6883 282.8583 287.3338 162.3475 -2.1706 280.7655 282.9361 287.4633 163.1370 -2.1727 280.8457 283.0184 287.5995 163.9568 -2.1717 280.9076 283.0793 287.7464 164.7468 -2.1732 280.9767 283.1499 287.8689 165.5678 -2.1770 281.0443 283.2213 287.9995 166.3595 -2.1792 281.1213 283.3005 288.1310 167.1515 -2.1799 281.1928 283.3727 288.2593 167.9735 -2.1798 281.2708 283.4506 288.4128 168.7655 -2.1783 281.3201 283.4984 288.5443 169.5875 -2.1807 281.3830 283.5636 288.6611 170.3795 -2.1825 281.4393 283.6218 288.8025 171.1715 -2.1830 281.5373 283.7202 288.9193 171.9935 -2.1849 281.6292 283.8142 289.0661 172.7855 -2.1848 281.6926 283.8774 289.1915 173.6075 -2.1878 281.7624 283.9502 289.3295 174.3995 -2.1849 281.8378 284.0227 289.4527 175.1915 -2.1856 281.9075 284.0931 289.5817 176.0135 -2.1875 281.9848 284.1724 289.6937 176.8055 -2.1886 282.0471 284.2357 289.8238 177.6275 -2.1893 282.1211 284.3104 289.9581 178.4195 -2.1926 282.1970 284.3896 290.0859 179.2113 -2.1937 282.2720 284.4657 290.2082 180.0630 -2.1939 282.3704 284.5643 290.3496 180.8253 -2.1957 282.4346 284.6303 290.4651 181.6478 -2.1950 282.5050 284.7000 290.5851 182.4400 -2.1948 282.5967 284.7915 290.7043 183.2315 -2.1957 282.6638 284.8595 290.8089 184.0840 -2.1979 282.7391 284.9369 290.9708 184.8458 -2.1990 282.8267 285.0257 291.1042 185.6678 -2.1983 282.8985 285.0967 291.2059 186.4903 -2.1996 282.9806 285.1802 291.3249 187.2525 -2.2025 283.0486 285.2511 291.4314 188.1048 -2.2021 283.1508 285.3529 291.5754 188.8665 -2.2025 283.2292 285.4317 291.7025 189.6860 -2.2039 283.3039 285.5077 291.8209 190.5048 -2.2036 283.3665 285.5701 291.9317 191.2630 -2.2035 283.4536 285.6570 292.0498 192.1100 -2.2063 283.5432 285.7495 292.1845 192.8693 -2.2074 283.6341 285.8415 292.2954 193.6880 -2.2091 283.7161 285.9252 292.4285 194.5065 -2.2091 283.7823 285.9914 292.5316 195.2650 -2.2106 283.8399 286.0504 292.6393 196.1158 -2.2113 283.9491 286.1604 292.8045 196.8760 -2.2135 284.0071 286.2205 292.9213 197.6978 -2.2126 284.0994 286.3120 293.0341 198.4900 -2.2131 284.1877 286.4008 293.1647 199.2815 -2.2127 284.2607 286.4735 293.2799 200.1040 -2.2145 284.3604 286.5749 293.4008 200.8958 -2.2158 284.4440 286.6599 293.5442 201.7178 -2.2170 284.5437 286.7607 293.6985 202.5100 -2.2178 284.6157 286.8335 293.8042 203.3015 -2.2183 284.6938 286.9121 293.9462 204.1238 -2.2204 284.7817 287.0021 294.0995 204.8855 -2.2210 284.8635 287.0845 294.2110 205.7378 -2.2227 284.9610 287.1837 294.3530 206.5298 -2.2213 285.0340 287.2553 294.4700 207.3215 -2.2239 285.1213 287.3452 294.6164 208.1435 -2.2234 285.2188 287.4422 294.7641 208.9055 -2.2245 285.2948 287.5192 294.8932 209.7575 -2.2268 285.4007 287.6275 295.0387 210.5195 -2.2247 285.4852 287.7100 295.1632 211.3415 -2.2255 285.5667 287.7922 295.3094 212.1635 -2.2268 285.6673 287.8942 295.4409 212.9255 -2.2303 285.7447 287.9749 295.5686 213.7775 -2.2329 285.8240 288.0569 295.7105 214.5395 -2.2315 285.9158 288.1473 295.8387 215.3615 -2.2289 286.0145 288.2434 295.9880 216.1585 -2.2288 286.0971 288.3259 296.1306 216.9525 -2.2301 286.1835 288.4137 296.2451 217.9545 -2.2320 286.2986 288.5306 296.4117 218.7660 -2.2351 286.3976 288.6327 296.5516 219.5878 -2.2350 286.4895 288.7245 296.7029 220.3800 -2.2382 286.5689 288.8071 296.8182 221.1680 -2.2402 286.6703 288.9105 296.9444 222.0178 -2.2392 286.7505 288.9896 297.0886 222.7753 -2.2394 286.8340 289.0734 297.2241 223.5933 -2.2418 286.9359 289.1777 297.3747 224.3815 -2.2435 287.0228 289.2664 297.4913 225.1708 -2.2422 287.1109 289.3531 297.6163 225.9903 -2.2444 287.2143 289.4587 297.7518 226.7795 -2.2464 287.3147 289.5611 297.8699 227.5993 -2.2473 287.3852 289.6325 298.0151 228.3895 -2.2496 287.4946 289.7442 298.1521 229.1800 -2.2525 287.5900 289.8425 298.2807 229.9998 -2.2530 287.6719 289.9249 298.4134 230.7615 -2.2538 287.7647 290.0185 298.5305 231.6133 -2.2528 287.8633 290.1161 298.6777 232.4050 -2.2542 287.9717 290.2259 298.8115 233.1968 -2.2582 288.0817 290.3399 298.9115 234.0190 -2.2584 288.1556 290.4140 299.0568 234.7808 -2.2585 288.2474 290.5059 299.1776 235.6333 -2.2598 288.3576 290.6174 299.3167 236.3950 -2.2628 288.4368 290.6995 299.4293 237.2168 -2.2632 288.5446 290.8079 299.5667 238.0090 -2.2632 288.6275 290.8907 299.6896 238.8005 -2.2647 288.7198 290.9845 299.8139 239.6530 -2.2629 288.8345 291.0973 299.9334 240.4148 -2.2636 288.9339 291.1975 300.0683 241.2368 -2.2634 289.0228 291.2862 300.1953 242.0290 -2.2661 289.1165 291.3826 300.3164 242.8205 -2.2683 289.2178 291.4861 300.4375 243.6730 -2.2660 289.3219 291.5879 300.5786 244.4348 -2.2676 289.4351 291.7027 300.6976 245.2568 -2.2704 289.5113 291.7816 300.8161 246.0488 -2.2723 289.6136 291.8859 300.9399 246.8405 -2.2742 289.7131 291.9872 301.0817 247.6928 -2.2735 289.8154 292.0889 301.2177 248.4545 -2.2757 289.9171 292.1928 301.3368 249.2765 -2.2793 290.0162 292.2954 301.4539 250.0685 -2.2783 290.1031 292.3814 301.5680 250.8605 -2.2787 290.1935 292.4721 301.6945 251.7130 -2.2778 290.3053 292.5831 301.8255 252.4755 -2.2799 290.4234 292.7033 301.9597 253.2950 -2.2817 290.5390 292.8207 302.0709 254.0830 -2.2805 290.6274 292.9079 302.1919 254.8710 -2.2810 290.7182 292.9991 302.3163 255.7190 -2.2823 290.8478 293.1300 302.4489 256.4770 -2.2831 290.9307 293.2138 302.5638 257.2950 -2.2831 291.0421 293.3252 302.6898 258.0830 -2.2856 291.1329 293.4185 302.7945 258.8720 -2.2886 291.2418 293.5303 302.9200 259.7208 -2.2892 291.3581 293.6473 303.0608 260.4800 -2.2890 291.4476 293.7366 303.1914 261.2995 -2.2899 291.5390 293.8290 303.3062 262.1198 -2.2904 291.6592 293.9496 303.4133 262.8815 -2.2924 291.7676 294.0601 303.5288 263.7335 -2.2962 291.8640 294.1602 303.6632 264.4955 -2.2977 291.9653 294.2630 303.7834 265.3175 -2.2980 292.0626 294.3607 303.9099 266.1395 -2.2974 292.1771 294.4746 304.0670 266.9015 -2.2993 292.2733 294.5726 304.1893 267.7535 -2.2998 292.3866 294.6865 304.3202 268.5155 -2.3016 292.4891 294.7907 304.4702 269.3375 -2.3036 292.5982 294.9018 304.6060 270.1295 -2.3033 292.6948 294.9981 304.7369 270.9215 -2.3033 292.8066 295.1099 304.8720 271.7735 -2.3047 292.9106 295.2152 305.0158 272.5355 -2.3064 293.0065 295.3128 305.1461 273.3575 -2.3069 293.1268 295.4337 305.3050 274.1795 -2.3100 293.2307 295.5406 305.4571 274.9410 -2.3084 293.3439 295.6523 305.5730 275.7938 -2.3076 293.4513 295.7589 305.7249 276.5560 -2.3083 293.5589 295.8671 305.8690 277.3778 -2.3117 293.6746 295.9863 305.9989 278.2003 -2.3150 293.7880 296.1031 306.1405 278.9625 -2.3170 293.8733 296.1903 306.2753 279.8155 -2.3187 293.9890 296.3077 306.4421 280.5778 -2.3221 294.0998 296.4219 306.5898 281.4005 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