DTA measure 1pb4 Test Date: 20231123:1412 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.20 s Mass = 1128.900 mg data_number = 1576 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.8652 -1.9466 274.4843 276.4309 264.2894 2.9005 -1.9478 274.4966 276.4444 264.2857 3.7228 -1.9490 274.5096 276.4586 264.2799 5.3065 -1.9528 274.5242 276.4769 264.2676 6.1588 -1.9508 274.5171 276.4679 264.2801 7.7428 -1.9528 274.5527 276.5055 264.2977 8.5345 -1.9534 274.5579 276.5114 264.3152 9.3265 -1.9527 274.5405 276.4932 264.3237 10.9405 -1.9548 274.5423 276.4971 264.3680 11.7625 -1.9540 274.5549 276.5089 264.3861 13.3465 -1.9574 274.5742 276.5316 264.4368 14.1985 -1.9574 274.5916 276.5490 264.4718 15.7823 -1.9600 274.5831 276.5431 264.5723 16.5745 -1.9625 274.5909 276.5534 264.6144 17.3665 -1.9638 274.6003 276.5641 264.6649 18.2178 -1.9643 274.6026 276.5669 264.7339 19.7933 -1.9637 274.6052 276.5689 264.8546 20.5820 -1.9636 274.5993 276.5629 264.9222 21.3693 -1.9634 274.6080 276.5714 264.9921 22.2185 -1.9631 274.6085 276.5716 265.0632 22.9768 -1.9640 274.6323 276.5963 265.1472 23.7950 -1.9667 274.6229 276.5897 265.2274 24.6133 -1.9670 274.6302 276.5972 265.3103 25.3725 -1.9692 274.6465 276.6157 265.3789 26.2225 -1.9708 274.6415 276.6123 265.4789 26.9840 -1.9705 274.6500 276.6205 265.5631 27.8043 -1.9683 274.6535 276.6217 265.6512 28.5955 -1.9717 274.6693 276.6410 265.7459 29.3875 -1.9741 274.6735 276.6476 265.8260 30.2395 -1.9756 274.6705 276.6461 265.9426 31.0015 -1.9757 274.6891 276.6648 266.0324 31.8235 -1.9774 274.6977 276.6752 266.1467 32.6153 -1.9816 274.6945 276.6761 266.2474 33.4070 -1.9824 274.7109 276.6932 266.3368 34.2293 -1.9835 274.7178 276.7013 266.4554 35.0208 -1.9854 274.7249 276.7102 266.5607 35.8430 -1.9872 274.7314 276.7186 266.6674 36.6353 -1.9886 274.7283 276.7169 266.7755 37.4265 -1.9916 274.7280 276.7195 266.9004 38.2490 -1.9933 274.7425 276.7358 267.0160 39.0408 -1.9946 274.7426 276.7373 267.1279 39.8628 -1.9961 274.7629 276.7590 267.2485 40.6550 -1.9982 274.7728 276.7710 267.3446 41.4465 -1.9973 274.7845 276.7818 267.4655 42.2690 -1.9987 274.7921 276.7908 267.5637 43.0605 -2.0023 274.8029 276.8052 267.6815 43.8828 -2.0045 274.8113 276.8158 267.8119 44.6748 -2.0053 274.8222 276.8275 267.9312 45.4665 -2.0080 274.8223 276.8303 268.0468 46.3188 -2.0080 274.8439 276.8519 268.1583 47.0805 -2.0099 274.8478 276.8577 268.2657 47.9025 -2.0114 274.8597 276.8711 268.3786 48.6945 -2.0131 274.8645 276.8776 268.4833 49.4865 -2.0163 274.8901 276.9065 268.5978 50.3385 -2.0177 274.9064 276.9241 268.7283 51.0990 -2.0200 274.9115 276.9315 268.8312 51.9185 -2.0226 274.9146 276.9372 268.9260 52.7070 -2.0215 274.9100 276.9315 269.0460 53.4950 -2.0217 274.9358 276.9575 269.1671 54.3430 -2.0226 274.9590 276.9816 269.2708 55.1010 -2.0263 274.9647 276.9910 269.3817 55.9200 -2.0272 274.9908 277.0180 269.4884 56.7380 -2.0299 274.9996 277.0295 269.6030 57.4960 -2.0331 275.0284 277.0614 269.7006 58.3458 -2.0352 275.0268 277.0619 269.8106 59.1055 -2.0391 275.0387 277.0778 269.9133 59.9263 -2.0416 275.0622 277.1038 270.0272 60.7475 -2.0429 275.0752 277.1181 270.1165 61.5095 -2.0444 275.0847 277.1291 270.2198 62.3615 -2.0462 275.0937 277.1399 270.3214 63.1228 -2.0493 275.1391 277.1884 270.4281 63.9445 -2.0482 275.1510 277.1992 270.5527 64.7665 -2.0510 275.1707 277.2218 270.6330 65.5285 -2.0552 275.1962 277.2514 270.7224 66.3805 -2.0565 275.1970 277.2535 270.8347 67.1425 -2.0600 275.2039 277.2639 270.9290 67.9645 -2.0604 275.2439 277.3042 271.0410 68.7865 -2.0624 275.2515 277.3139 271.1322 69.5485 -2.0655 275.2810 277.3465 271.2274 70.4005 -2.0672 275.2982 277.3654 271.3322 71.1625 -2.0677 275.3307 277.3984 271.4136 71.9843 -2.0686 275.3421 277.4108 271.5139 72.8068 -2.0719 275.3543 277.4261 271.6140 73.5695 -2.0734 275.3819 277.4553 271.7026 74.4210 -2.0754 275.3987 277.4741 271.7996 75.1828 -2.0788 275.4180 277.4968 271.8926 76.0048 -2.0807 275.4354 277.5161 271.9858 76.8270 -2.0817 275.4575 277.5392 272.0746 77.5885 -2.0815 275.4704 277.5518 272.1649 78.4415 -2.0815 275.5053 277.5868 272.2790 79.2340 -2.0871 275.5301 277.6173 272.3800 80.0265 -2.0920 275.5490 277.6410 272.4696 80.8490 -2.0908 275.5864 277.6772 272.5408 81.6105 -2.0924 275.6125 277.7050 272.6366 82.4628 -2.0934 275.6321 277.7255 272.7201 83.2525 -2.0958 275.6596 277.7554 272.8117 84.0408 -2.0954 275.6850 277.7803 272.9129 84.8580 -2.0972 275.7190 277.8163 273.0151 85.6160 -2.0981 275.7342 277.8323 273.0984 86.4640 -2.0965 275.7655 277.8620 273.1879 87.2520 -2.0977 275.7943 277.8920 273.2759 88.0410 -2.0994 275.8153 277.9147 273.3591 88.8590 -2.1039 275.8397 277.9437 273.4391 89.6170 -2.1063 275.8651 277.9714 273.5443 90.4655 -2.1097 275.8922 278.0019 273.6466 91.2545 -2.1094 275.9315 278.0409 273.7244 92.0445 -2.1098 275.9547 278.0645 273.8036 92.8668 -2.1111 275.9905 278.1016 273.9086 93.6285 -2.1102 276.0211 278.1313 273.9953 94.4810 -2.1096 276.0282 278.1378 274.1218 95.2730 -2.1120 276.0607 278.1727 274.2139 96.0645 -2.1146 276.0812 278.1957 274.3186 96.8868 -2.1159 276.1277 278.2436 274.4159 97.6485 -2.1175 276.1463 278.2638 274.5025 98.5005 -2.1194 276.1878 278.3072 274.6146 99.2628 -2.1231 276.2244 278.3475 274.6992 100.0845 -2.1253 276.2568 278.3820 274.8139 100.9065 -2.1250 276.2970 278.4220 274.9206 101.6685 -2.1232 276.3309 278.4541 275.0224 102.5208 -2.1270 276.3525 278.4795 275.1339 103.2825 -2.1298 276.3936 278.5234 275.2584 104.1045 -2.1300 276.4268 278.5568 275.3349 104.9265 -2.1298 276.4425 278.5723 275.4353 105.6885 -2.1318 276.4918 278.6237 275.5375 106.5405 -2.1350 276.5174 278.6525 275.6537 107.3325 -2.1355 276.5602 278.6957 275.7767 108.1245 -2.1375 276.5916 278.7291 275.8535 108.9468 -2.1379 276.6242 278.7621 275.9650 109.7093 -2.1369 276.6701 278.8070 276.0672 110.5615 -2.1371 276.7067 278.8437 276.1784 111.3545 -2.1385 276.7373 278.8757 276.2769 112.1473 -2.1397 276.7689 278.9086 276.3788 112.9710 -2.1432 276.7957 278.9389 276.5018 113.7338 -2.1436 276.8339 278.9776 276.5963 114.5860 -2.1463 276.8915 279.0379 276.6989 115.3480 -2.1460 276.9352 279.0812 276.7845 116.1700 -2.1459 276.9641 279.1100 276.8913 116.9580 -2.1456 276.9982 279.1438 276.9911 117.7470 -2.1460 277.0283 279.1742 277.0863 118.5953 -2.1534 277.0602 279.2136 277.1759 119.3535 -2.1539 277.1194 279.2733 277.2710 120.1710 -2.1514 277.1623 279.3136 277.3734 120.9593 -2.1506 277.2036 279.3542 277.4711 121.7473 -2.1533 277.2388 279.3921 277.5752 122.5983 -2.1527 277.2795 279.4322 277.6590 123.3563 -2.1552 277.3097 279.4649 277.7722 124.1750 -2.1605 277.3539 279.5145 277.8713 124.9955 -2.1609 277.4007 279.5615 277.9764 125.7565 -2.1618 277.4404 279.6022 278.0568 126.6080 -2.1639 277.4851 279.6490 278.1745 127.3693 -2.1654 277.5259 279.6913 278.2737 128.1908 -2.1669 277.5576 279.7245 278.3576 128.9835 -2.1682 277.6128 279.7810 278.4646 129.7765 -2.1691 277.6615 279.8307 278.5502 130.6290 -2.1723 277.6993 279.8716 278.6508 131.3908 -2.1710 277.7448 279.9159 278.7282 132.2128 -2.1724 277.7833 279.9557 278.8198 133.0050 -2.1751 277.8142 279.9893 278.9241 133.7965 -2.1747 277.8694 280.0441 279.0325 134.6490 -2.1726 277.9198 280.0924 279.1407 135.4108 -2.1732 277.9703 280.1435 279.2290 136.2328 -2.1780 278.0181 280.1962 279.3447 137.0250 -2.1802 278.0765 280.2567 279.4476 137.8203 -2.1798 278.1216 280.3013 279.5552 138.6528 -2.1796 278.1455 280.3251 279.6686 139.4145 -2.1840 278.1847 280.3687 279.7580 140.2668 -2.1849 278.2380 280.4230 279.8647 141.0585 -2.1868 278.3147 280.5015 279.9765 141.8505 -2.1856 278.3503 280.5359 280.1010 142.6725 -2.1856 278.4000 280.5856 280.2079 143.4345 -2.1875 278.4436 280.6311 280.3222 144.2865 -2.1881 278.4893 280.6774 280.4316 145.0785 -2.1900 278.5432 280.7333 280.5606 145.8705 -2.1903 278.5928 280.7831 280.6757 146.6925 -2.1898 278.6421 280.8319 280.7727 147.4528 -2.1895 278.6889 280.8783 280.8649 148.3008 -2.1877 278.7368 280.9245 280.9859 149.0888 -2.1883 278.7860 280.9743 281.1045 149.8765 -2.1889 278.8520 281.0410 281.2205 150.6950 -2.1906 278.9068 281.0974 281.3379 151.4530 -2.1926 278.9466 281.1392 281.4422 152.3010 -2.1952 279.0046 281.1998 281.5510 153.0890 -2.1953 279.0492 281.2445 281.6621 153.8770 -2.1950 279.1098 281.3047 281.7716 154.6953 -2.1968 279.1567 281.3535 281.8893 155.4845 -2.1973 279.2018 281.3991 282.0020 156.3045 -2.1984 279.2623 281.4607 282.1045 157.0963 -2.2013 279.3152 281.5165 282.2179 157.8885 -2.2053 279.3678 281.5732 282.3256 158.7120 -2.2049 279.4408 281.6457 282.4445 159.4755 -2.2026 279.4910 281.6936 282.5385 160.3275 -2.2034 279.5536 281.7570 282.6529 161.0895 -2.2020 279.6024 281.8044 282.7487 161.9115 -2.2041 279.6466 281.8507 282.8370 162.7335 -2.2051 279.6863 281.8914 282.9598 163.4955 -2.2011 279.7448 281.9459 283.0657 164.3475 -2.2005 279.8061 282.0066 283.1892 165.1095 -2.2036 279.8740 282.0776 283.3028 165.9315 -2.2054 279.9351 282.1404 283.3863 166.7235 -2.2068 279.9763 282.1831 283.4881 167.5150 -2.2059 280.0408 282.2468 283.6127 168.3673 -2.2071 280.1237 282.3309 283.7044 169.1295 -2.2091 280.1745 282.3836 283.7988 169.9518 -2.2110 280.2427 282.4537 283.9171 170.7440 -2.2099 280.2823 282.4922 284.0037 171.5358 -2.2094 280.3511 282.5605 284.1010 172.3880 -2.2031 280.4033 282.6065 284.2110 173.1498 -2.2073 280.4657 282.6731 284.3184 173.9718 -2.2081 280.5186 282.7267 284.4247 174.7943 -2.2080 280.5918 282.7998 284.5198 175.5565 -2.2054 280.6466 282.8521 284.6068 176.4090 -2.2079 280.7139 282.9217 284.7146 177.1708 -2.2103 280.7707 282.9810 284.8110 177.9938 -2.2107 280.8338 283.0445 284.9133 178.7858 -2.2101 280.8955 283.1056 285.0253 179.5785 -2.2109 280.9486 283.1595 285.1135 180.4298 -2.2120 281.0159 283.2280 285.2291 181.1910 -2.2101 281.0823 283.2924 285.3280 182.0130 -2.2116 281.1351 283.3467 285.4430 182.8015 -2.2115 281.2031 283.4146 285.5523 183.5900 -2.2121 281.2810 283.4930 285.6217 184.4388 -2.2141 281.3492 283.5633 285.7284 185.1970 -2.2143 281.3998 283.6141 285.8125 186.0160 -2.2182 281.4759 283.6940 285.9143 186.8343 -2.2167 281.5557 283.7724 286.0301 187.5955 -2.2175 281.6065 283.8240 286.1190 188.4458 -2.2188 281.6844 283.9032 286.2233 189.1803 -2.2209 281.7304 283.9513 286.3023 190.0453 -2.2176 281.7872 284.0048 286.4010 190.8375 -2.2173 281.8513 284.0686 286.4885 191.6295 -2.2163 281.9221 284.1384 286.5706 192.4520 -2.2165 281.9819 284.1984 286.6600 193.2145 -2.2169 282.0428 284.2597 286.7599 194.0668 -2.2164 282.1242 284.3407 286.8758 194.8588 -2.2171 282.1844 284.4016 286.9691 195.6505 -2.2175 282.2532 284.4706 287.0754 196.4728 -2.2174 282.3327 284.5501 287.1608 197.2345 -2.2187 282.3915 284.6102 287.2407 198.0865 -2.2194 282.4456 284.6650 287.3443 198.8785 -2.2202 282.5340 284.7541 287.4387 199.6705 -2.2198 282.6121 284.8319 287.5270 200.4925 -2.2178 282.6695 284.8873 287.6131 201.2845 -2.2215 282.7202 284.9416 287.6887 202.1065 -2.2207 282.7972 285.0179 287.7840 202.8985 -2.2201 282.8709 285.0910 287.8850 203.6905 -2.2204 282.9383 285.1587 287.9873 204.5140 -2.2196 283.0276 285.2471 288.0823 205.3065 -2.2171 283.0977 285.3148 288.1714 206.1283 -2.2196 283.1714 285.3910 288.2717 206.9205 -2.2213 283.2213 285.4425 288.3605 207.7115 -2.2209 283.2882 285.5091 288.4674 208.5343 -2.2211 283.3658 285.5869 288.5885 209.3258 -2.2231 283.4324 285.6556 288.6937 210.1488 -2.2216 283.5063 285.7279 288.8001 210.9410 -2.2225 283.5749 285.7974 288.9084 211.7325 -2.2233 283.6504 285.8738 289.0135 212.5520 -2.2251 283.7314 285.9565 289.1050 213.3110 -2.2252 283.7801 286.0054 289.2047 214.1593 -2.2255 283.8637 286.0892 289.3151 214.9475 -2.2247 283.9372 286.1619 289.4173 215.7353 -2.2231 284.0200 286.2431 289.5310 216.5538 -2.2233 284.1002 286.3235 289.6394 217.3123 -2.2227 284.1579 286.3806 289.7385 218.1613 -2.2219 284.2301 286.4519 289.8723 218.9495 -2.2247 284.2992 286.5239 289.9750 219.7380 -2.2240 284.3766 286.6007 290.0731 220.5575 -2.2260 284.4567 286.6827 290.1827 221.3175 -2.2266 284.5341 286.7608 290.2949 222.1690 -2.2253 284.5997 286.8250 290.4124 222.9610 -2.2280 284.6835 286.9115 290.5179 223.7528 -2.2299 284.7517 286.9816 290.6346 224.5750 -2.2287 284.8265 287.0552 290.7381 225.3368 -2.2304 284.9017 287.1321 290.8282 226.1895 -2.2296 284.9750 287.2046 290.9517 226.9518 -2.2277 285.0330 287.2607 291.0427 227.7738 -2.2282 285.1125 287.3407 291.1509 228.5960 -2.2344 285.2080 287.4424 291.2729 229.3575 -2.2333 285.2762 287.5096 291.3822 230.2215 -2.2294 285.3509 287.5803 291.4761 230.9635 -2.2298 285.4263 287.6560 291.5752 231.8158 -2.2303 285.5223 287.7526 291.7060 232.5778 -2.2325 285.5811 287.8136 291.7928 233.3998 -2.2327 285.6733 287.9059 291.9064 234.2215 -2.2329 285.7505 287.9835 292.0054 234.9835 -2.2323 285.8080 288.0403 292.1139 235.8363 -2.2319 285.8811 288.1130 292.2215 236.5985 -2.2337 285.9673 288.2010 292.3282 237.4205 -2.2355 286.0580 288.2935 292.4290 238.2425 -2.2387 286.1368 288.3755 292.5472 239.0045 -2.2403 286.2003 288.4406 292.6502 239.8565 -2.2393 286.2672 288.5065 292.7450 240.6210 -2.2392 286.3473 288.5865 292.8560 241.4455 -2.2408 286.4300 288.6707 292.9647 242.2675 -2.2397 286.5265 288.7662 293.0730 243.0295 -2.2403 286.5996 288.8399 293.1854 243.8813 -2.2397 286.6950 288.9346 293.2872 244.6393 -2.2386 286.7611 288.9997 293.3778 245.4578 -2.2417 286.8518 289.0935 293.4954 246.2760 -2.2410 286.9370 289.1780 293.5989 247.0333 -2.2404 286.9913 289.2317 293.6974 247.8818 -2.2385 287.0754 289.3139 293.8142 248.6400 -2.2407 287.1553 289.3960 293.9130 249.4580 -2.2421 287.2322 289.4743 294.0172 250.2763 -2.2413 287.3173 289.5585 294.1339 251.0355 -2.2449 287.3997 289.6446 294.2231 251.8858 -2.2480 287.4876 289.7356 294.3208 252.6755 -2.2487 287.5629 289.8115 294.4216 253.4665 -2.2509 287.6452 289.8962 294.5237 254.2880 -2.2538 287.7354 289.9892 294.6333 255.0495 -2.2529 287.8117 290.0646 294.7364 255.9023 -2.2528 287.8944 290.1471 294.8153 256.6945 -2.2568 287.9760 290.2328 294.9132 257.4865 -2.2572 288.0569 290.3141 295.0257 258.3085 -2.2566 288.1488 290.4054 295.1384 259.0705 -2.2577 288.2336 290.4913 295.2239 259.9225 -2.2568 288.3007 290.5575 295.3261 260.7145 -2.2592 288.3831 290.6422 295.4135 261.5055 -2.2590 288.4744 290.7333 295.5190 262.3283 -2.2620 288.5619 290.8238 295.6127 263.0898 -2.2607 288.6403 290.9010 295.7087 263.9425 -2.2590 288.7294 290.9885 295.8158 264.7350 -2.2631 288.8085 291.0715 295.9147 265.5568 -2.2608 288.8997 291.1605 296.0197 266.3788 -2.2616 288.9764 291.2380 296.1163 267.1720 -2.2606 289.0570 291.3176 296.1944 267.9645 -2.2605 289.1397 291.4001 296.3079 268.7890 -2.2621 289.2536 291.5156 296.4098 269.5818 -2.2644 289.3345 291.5990 296.5009 270.4045 -2.2662 289.4115 291.6777 296.5951 271.1968 -2.2684 289.4906 291.7591 296.6989 271.9885 -2.2674 289.5766 291.8440 296.8005 272.8113 -2.2644 289.6628 291.9272 296.8973 273.6045 -2.2647 289.7343 291.9991 296.9801 274.4268 -2.2717 289.8337 292.1054 297.0801 275.2185 -2.2687 289.9293 292.1980 297.1691 276.0103 -2.2702 290.0067 292.2768 297.2777 276.8273 -2.2710 290.0955 292.3666 297.3653 277.6155 -2.2703 290.1874 292.4577 297.4691 278.4340 -2.2712 290.2687 292.5399 297.5710 279.2215 -2.2706 290.3514 292.6220 297.6779 280.0110 -2.2759 290.4440 292.7199 297.7962 280.8293 -2.2757 290.5288 292.8045 297.8850 281.5890 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