DTA measure 1pb_updown Date: 202634:857 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.05 s Mass = 1164.300 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2093 0.4726 242.3964 241.9238 275.3235 1.9750 0.4759 242.6273 242.1514 275.2045 2.7923 0.4794 242.8578 242.3785 275.0717 3.5888 0.4843 243.0729 242.5886 274.9348 4.3855 0.4901 243.3077 242.8176 274.7908 5.2028 0.4905 243.5531 243.0625 274.6108 5.9785 0.4900 243.8049 243.3149 274.4821 6.8265 0.4914 244.0592 243.5678 274.3012 7.5925 0.4903 244.2715 243.7811 274.1392 8.4195 0.4937 244.5220 244.0282 273.9845 9.2060 0.4970 244.7321 244.2351 273.8223 10.0028 0.4948 244.9626 244.4678 273.6795 10.8300 0.4971 245.1947 244.6976 273.5666 11.5960 0.4973 245.4053 244.9080 273.4542 12.4540 0.5039 245.6822 245.1784 273.4069 13.2095 0.5076 245.9073 245.3997 273.3813 14.0473 0.5143 246.1578 245.6434 273.3992 14.8028 0.5164 246.3626 245.8462 273.4314 15.6403 0.5176 246.5973 246.0797 273.5318 16.4268 0.5189 246.8441 246.3252 273.6382 17.2335 0.5181 247.0728 246.5548 273.7598 18.0505 0.5196 247.3341 246.8145 273.9088 18.8168 0.5212 247.5441 247.0229 274.0932 19.6745 0.5229 247.7928 247.2699 274.3600 20.4408 0.5276 248.0004 247.4728 274.6395 21.2680 0.5328 248.2061 247.6733 274.9788 22.0645 0.5334 248.4262 247.8927 275.3406 22.8615 0.5359 248.6371 248.1012 275.7376 23.6885 0.5378 248.8522 248.3144 276.1467 24.4548 0.5377 249.0476 248.5099 276.5228 25.3025 0.5354 249.3085 248.7731 276.9683 26.0785 0.5336 249.5269 248.9934 277.3867 26.9060 0.5325 249.7628 249.2303 277.8312 27.7025 0.5322 249.9510 249.4188 278.2198 28.4890 0.5297 250.1671 249.6375 278.6102 29.3268 0.5272 250.3909 249.8637 278.9857 30.0820 0.5373 250.6076 250.0703 279.3316 30.9505 0.5793 250.8296 250.2503 279.7013 31.7063 0.5884 251.0533 250.4649 279.9691 32.5438 0.5745 251.2746 250.7000 280.2460 33.3305 0.5606 251.4876 250.9270 280.5027 34.1370 0.5521 251.6967 251.1446 280.7349 34.9543 0.5430 251.9089 251.3660 280.9299 35.7203 0.5365 252.1100 251.5734 281.0789 36.5678 0.5256 252.3514 251.8258 281.2140 37.3338 0.5176 252.5732 252.0557 281.3169 38.1613 0.5129 252.7798 252.2669 281.4046 38.9268 0.5273 252.9620 252.4348 281.4354 39.7440 0.5280 253.1650 252.6370 281.4372 40.5510 0.5186 253.4062 252.8876 281.4300 41.3370 0.5171 253.6595 253.1423 281.4057 42.1648 0.5104 253.8694 253.3590 281.3681 42.9305 0.5050 254.0636 253.5586 281.3384 43.7885 0.4961 254.2780 253.7819 281.2607 44.5545 0.4853 254.4878 254.0026 281.1544 45.3715 0.4767 254.7086 254.2320 281.0562 46.1785 0.4723 254.9101 254.4379 280.9852 46.9650 0.4726 255.1103 254.6377 280.8938 47.7920 0.4682 255.3275 254.8593 280.7893 48.5580 0.4676 255.5065 255.0389 280.6952 49.4163 0.4620 255.7297 255.2677 280.6096 50.1818 0.4631 255.9534 255.4903 280.5180 50.9990 0.4623 256.1985 255.7362 280.4491 51.8060 0.4710 256.3989 255.9279 280.4087 52.5923 0.4857 256.5999 256.1141 280.3793 53.4198 0.4837 256.7843 256.3006 280.3643 54.1855 0.4709 256.9767 256.5058 280.3873 55.0435 0.4644 257.2131 256.7487 280.4592 55.8098 0.4620 257.4236 256.9616 280.5631 56.6368 0.4566 257.6572 257.2006 280.6796 57.4335 0.4517 257.8787 257.4271 280.8261 58.2303 0.4498 258.0560 257.6061 281.0003 59.0573 0.4491 258.2789 257.8298 281.1874 59.8133 0.4451 258.4926 258.0475 281.4006 60.6815 0.4384 258.6893 258.2509 281.6771 61.4473 0.4509 258.8959 258.4450 281.9599 62.2748 0.4719 259.0980 258.6261 282.2985 63.0610 0.4668 259.2905 258.8237 282.6156 63.8680 0.4547 259.5073 259.0525 282.9812 64.6853 0.4434 259.6915 259.2481 283.3533 65.4610 0.4330 259.8753 259.4423 283.7011 66.3090 0.4291 260.0804 259.6514 284.0800 67.0750 0.4240 260.2749 259.8509 284.4145 67.9020 0.4166 260.4802 260.0636 284.7857 68.6888 0.4081 260.6897 260.2816 285.1205 69.4853 0.4057 260.8690 260.4633 285.4373 70.3125 0.3978 261.0501 260.6523 285.7576 71.0683 0.3865 261.2282 260.8417 286.0487 71.9058 0.3806 261.4573 261.0767 286.3319 72.6615 0.3721 261.6306 261.2584 286.5827 73.5198 0.3641 261.8385 261.4744 286.8192 74.2853 0.3568 262.0299 261.6731 287.0041 75.1128 0.3486 262.2025 261.8540 287.1558 75.9095 0.3419 262.3934 262.0515 287.2778 76.6955 0.3359 262.6132 262.2773 287.3919 77.5335 0.3343 262.8047 262.4704 287.4880 78.2890 0.3260 263.0006 262.6745 287.5390 79.1473 0.3427 263.2371 262.8944 287.5999 79.9133 0.3571 263.4215 263.0644 287.6377 80.7405 0.3603 263.6078 263.2475 287.6086 81.5373 0.3632 263.7964 263.4332 287.5746 82.3338 0.3640 263.9907 263.6267 287.5695 83.1613 0.3561 264.1833 263.8271 287.5432 83.9273 0.3464 264.3859 264.0396 287.5023 84.7850 0.3305 264.5882 264.2577 287.4509 85.5513 0.3161 264.7755 264.4594 287.3985 86.3785 0.3033 264.9749 264.6716 287.3399 87.1750 0.2986 265.1926 264.8940 287.2599 87.9718 0.2924 265.4031 265.1107 287.1926 88.7888 0.2878 265.6182 265.3304 287.1686 89.5648 0.2832 265.8315 265.5483 287.1407 90.4130 0.2749 266.0692 265.7943 287.1338 91.1888 0.2685 266.2462 265.9776 287.1482 92.0060 0.2554 266.4488 266.1934 287.1873 92.8130 0.2485 266.6546 266.4061 287.2565 93.5993 0.2443 266.8217 266.5774 287.3248 94.4370 0.2384 267.0019 266.7634 287.3893 95.1925 0.2341 267.1831 266.9490 287.4774 96.0608 0.2305 267.3843 267.1538 287.6044 96.7858 0.2287 267.5692 267.3405 287.7203 97.6438 0.2272 267.7923 267.5651 287.8868 98.4405 0.2270 267.9892 267.7622 288.0821 99.2475 0.2185 268.1852 267.9667 288.2924 100.0335 0.2138 268.3599 268.1461 288.5302 100.8200 0.2103 268.5150 268.3047 288.8028 101.6578 0.2040 268.6976 268.4936 289.0809 102.4130 0.2013 268.8838 268.6825 289.3410 103.2405 0.1971 269.0754 268.8782 289.6274 104.0065 0.1955 269.2527 269.0572 289.9202 104.8540 0.1938 269.4408 269.2470 290.2479 105.6203 0.1842 269.6096 269.4254 290.5589 106.4475 0.1741 269.7911 269.6171 290.8790 107.2440 0.1692 269.9749 269.8057 291.1809 108.0410 0.1620 270.1602 269.9982 291.4719 108.8578 0.1563 270.3408 270.1844 291.7541 109.6340 0.1507 270.5051 270.3544 292.0130 110.4820 0.1453 270.7038 270.5584 292.3049 111.2270 0.1463 270.8927 270.7464 292.5271 112.0753 0.1451 271.0987 270.9536 292.7608 112.8513 0.1367 271.2915 271.1548 292.9443 113.6683 0.1259 271.4963 271.3703 293.1292 114.4650 0.1198 271.6671 271.5473 293.3019 115.2615 0.1123 271.8341 271.7218 293.4415 116.0888 0.1009 272.0032 271.9023 293.5673 116.8550 0.0964 272.1684 272.0720 293.6490 117.7025 0.0951 272.3935 272.2984 293.7441 118.4790 0.0901 272.5697 272.4797 293.8052 119.3063 0.0844 272.7402 272.6558 293.8762 120.0720 0.0764 272.9238 272.8475 293.9086 120.8895 0.0685 273.1528 273.0844 293.8978 121.6960 0.0611 273.3482 273.2871 293.8912 122.4925 0.0525 273.5138 273.4613 293.8807 123.3203 0.0479 273.6974 273.6495 293.8861 124.0755 0.0388 273.8420 273.8032 293.8614 124.9440 0.0332 274.0538 274.0205 293.8243 125.7098 0.0310 274.2378 274.2069 293.7994 126.5370 0.0320 274.4088 274.3768 293.7650 127.3233 0.0272 274.5742 274.5470 293.7331 128.1303 0.0242 274.7186 274.6944 293.7228 128.9268 0.0145 274.8815 274.8670 293.7317 129.7233 0.0123 275.0577 275.0454 293.7991 130.5405 0.0083 275.2684 275.2601 293.8159 131.3165 0.0027 275.4665 275.4639 293.8295 132.1645 -0.0044 275.6177 275.6221 293.8801 132.9203 -0.0057 275.7953 275.8010 293.9449 133.7575 -0.0074 275.9956 276.0030 294.0436 134.5440 -0.0061 276.1747 276.1808 294.1453 135.3305 -0.0103 276.3594 276.3697 294.2393 136.1678 -0.0155 276.5439 276.5594 294.4251 136.9238 -0.0217 276.7247 276.7465 294.5782 137.7510 -0.0268 276.9075 276.9343 294.7534 138.5168 -0.0340 277.1038 277.1378 294.9777 139.3750 -0.0375 277.3146 277.3522 295.2056 140.1408 -0.0429 277.4978 277.5406 295.4444 140.9578 -0.0481 277.6639 277.7120 295.7050 141.7648 -0.0536 277.8274 277.8810 295.9717 142.5510 -0.0595 277.9867 278.0462 296.2468 143.3785 -0.0614 278.1635 278.2249 296.5321 144.1445 -0.0625 278.3487 278.4112 296.8024 145.0023 -0.0704 278.5395 278.6099 297.1098 145.7683 -0.0773 278.6886 278.7659 297.3881 146.5855 -0.0819 278.8560 278.9379 297.6696 147.3923 -0.0876 279.0492 279.1368 297.9516 148.1788 -0.0931 279.2247 279.3178 298.2031 149.0060 -0.1012 279.4052 279.5064 298.4554 149.7720 -0.1073 279.5646 279.6719 298.6434 150.6303 -0.1125 279.7675 279.8800 298.8650 151.3958 -0.1207 279.9344 280.0551 299.0846 152.2133 -0.1283 280.1172 280.2455 299.2723 153.0200 -0.1345 280.2958 280.4303 299.4387 153.8163 -0.1406 280.4529 280.5935 299.6030 154.6438 -0.1502 280.6375 280.7877 299.7518 155.3995 -0.1531 280.8259 280.9789 299.8672 156.2678 -0.1538 281.0161 281.1699 299.9938 157.0235 -0.1624 281.1801 281.3426 300.0740 157.8610 -0.1675 281.3341 281.5016 300.1361 158.6475 -0.1756 281.5177 281.6933 300.1899 159.4545 -0.1806 281.7261 281.9067 300.2143 160.2713 -0.1853 281.8960 282.0813 300.2223 161.0478 -0.1917 282.0527 282.2444 300.2331 161.8955 -0.1929 282.2390 282.4319 300.2599 162.6715 -0.1981 282.4221 282.6203 300.2590 163.4888 -0.2032 282.6097 282.8129 300.2577 164.2853 -0.2054 282.7809 282.9864 300.2701 165.0818 -0.2055 282.9463 283.1518 300.2706 165.8990 -0.2093 283.1112 283.3205 300.3019 166.6648 -0.2116 283.2831 283.4947 300.3024 167.5230 -0.2169 283.4664 283.6833 300.3119 168.2788 -0.2196 283.6111 283.8307 300.2907 169.1058 -0.2228 283.7889 284.0118 300.3183 169.8720 -0.2292 283.9436 284.1728 300.3621 170.6993 -0.2330 284.1228 284.3558 300.3952 171.4958 -0.2383 284.3006 284.5389 300.4535 172.2823 -0.2424 284.4578 284.7002 300.5634 173.1198 -0.2437 284.6095 284.8532 300.6629 173.8753 -0.2442 284.7911 285.0353 300.7496 174.7335 -0.2483 284.9973 285.2455 300.9055 175.4993 -0.2513 285.1599 285.4112 301.0625 176.3268 -0.2520 285.3355 285.5875 301.2205 177.1235 -0.2569 285.5067 285.7637 301.3201 177.9098 -0.2633 285.6788 285.9421 301.4963 178.7475 -0.2705 285.8594 286.1298 301.7617 179.5133 -0.2740 285.9891 286.2631 302.0045 180.3713 -0.2801 286.1618 286.4419 302.2719 181.1270 -0.2854 286.3242 286.6095 302.5157 181.9645 -0.2923 286.5081 286.8004 302.7950 182.7613 -0.3002 286.6812 286.9813 303.0417 183.5580 -0.3098 286.8325 287.1423 303.2944 184.3748 -0.3160 287.0056 287.3217 303.5654 185.1510 -0.3169 287.1700 287.4869 303.8249 185.9990 -0.3225 287.3507 287.6733 304.1348 186.7645 -0.3280 287.5186 287.8466 304.3881 187.5923 -0.3327 287.7129 288.0455 304.6647 188.3888 -0.3377 287.9011 288.2389 304.9095 189.1853 -0.3425 288.0453 288.3878 305.1313 190.0028 -0.3476 288.2043 288.5519 305.3370 190.7785 -0.3529 288.3710 288.7239 305.5346 191.6265 -0.3631 288.5427 288.9058 305.7237 192.4028 -0.3730 288.7246 289.0977 305.8730 193.2195 -0.3764 288.9074 289.2838 306.0307 194.0265 -0.3860 289.0785 289.4645 306.1567 194.8130 -0.3939 289.2447 289.6385 306.2807 195.6400 -0.3989 289.4287 289.8276 306.3747 196.4060 -0.3998 289.5780 289.9778 306.4316 197.2540 -0.4021 289.7537 290.1558 306.5275 197.9890 -0.4101 289.9075 290.3176 306.5710 198.8473 -0.4161 290.0895 290.5057 306.6250 199.6130 -0.4185 290.2272 290.6457 306.6678 200.4300 -0.4267 290.3794 290.8061 306.6882 201.2268 -0.4335 290.5711 291.0046 306.6977 202.0233 -0.4392 290.7408 291.1800 306.6628 202.8508 -0.4457 290.9157 291.3614 306.6900 203.6065 -0.4518 291.0736 291.5254 306.7092 204.4745 -0.4532 291.2471 291.7003 306.7048 205.2098 -0.4536 291.4078 291.8614 306.7085 206.0680 -0.4557 291.5886 292.0443 306.7179 206.8233 -0.4564 291.7531 292.2094 306.7422 207.6610 -0.4617 291.9405 292.4022 306.7797 208.4475 -0.4617 292.1045 292.5663 306.8299 209.2440 -0.4648 292.2701 292.7349 306.9002 210.0715 -0.4707 292.4603 292.9309 306.9530 210.8373 -0.4784 292.5935 293.0718 307.0119 211.6955 -0.4816 292.7420 293.2236 307.1476 212.4205 -0.4853 292.8857 293.3710 307.2535 213.2885 -0.4887 293.0688 293.5575 307.3998 214.0545 -0.4926 293.2354 293.7281 307.5583 214.8820 -0.4953 293.4159 293.9112 307.7312 215.6785 -0.4959 293.5732 294.0691 307.8784 216.4753 -0.4994 293.7414 294.2408 308.0315 217.3025 -0.5049 293.9118 294.4167 308.2717 218.0683 -0.5108 294.0796 294.5904 308.4852 218.9163 -0.5148 294.2546 294.7694 308.7280 219.6615 -0.5204 294.4088 294.9291 308.9461 220.5095 -0.5245 294.5850 295.1096 309.2036 221.2858 -0.5312 294.7575 295.2887 309.4188 222.1028 -0.5402 294.9310 295.4712 309.6983 222.9098 -0.5443 295.1090 295.6533 309.9578 223.6960 -0.5475 295.3050 295.8525 310.1812 224.5335 -0.5526 295.4941 296.0467 310.4738 225.2893 -0.5559 295.6265 296.1823 310.7025 226.1575 -0.5635 295.8085 296.3720 310.9344 226.9130 -0.5688 295.9512 296.5200 311.1547 227.7508 -0.5756 296.0885 296.6641 311.3513 228.5370 -0.5774 296.2332 296.8105 311.5521 229.3335 -0.5804 296.3986 296.9791 311.7640 230.1200 -0.5840 296.5501 297.1341 311.9533 230.9165 -0.5911 296.7186 297.3097 312.1016 231.7438 -0.5950 296.8483 297.4433 312.2489 232.5100 -0.5978 297.0091 297.6069 312.3717 233.3575 -0.6042 297.1724 297.7766 312.5269 234.1338 -0.6108 297.3032 297.9140 312.6377 234.9510 -0.6187 297.4655 298.0842 312.7499 235.7473 -0.6256 297.6441 298.2697 312.8544 236.5440 -0.6286 297.8310 298.4596 312.8849 237.3408 -0.6333 298.0065 298.6398 312.9388 238.1373 -0.6350 298.1562 298.7912 312.9851 238.9545 -0.6369 298.3319 298.9689 313.0228 239.7305 -0.6402 298.4890 299.1293 313.0646 240.5785 -0.6458 298.6467 299.2925 313.1106 241.3445 -0.6513 298.7902 299.4415 313.1318 242.1715 -0.6528 298.9597 299.6124 313.1420 242.9685 -0.6565 299.1125 299.7690 313.1885 243.7650 -0.6620 299.2786 299.9406 313.2128 244.5615 -0.6718 299.4799 300.1516 313.2400 245.3585 -0.6778 299.6420 300.3198 313.2722 246.1855 -0.6836 299.8233 300.5069 313.3112 246.9515 -0.6900 299.9812 300.6712 313.3543 247.7995 -0.6981 300.1574 300.8556 313.4109 248.5755 -0.7060 300.2986 301.0046 313.4759 249.3928 -0.7076 300.4750 301.1826 313.5569 250.1995 -0.7074 300.6585 301.3659 313.6512 250.9858 -0.7103 300.8106 301.5209 313.7451 251.8235 -0.7086 300.9941 301.7027 313.8432 252.5790 -0.7084 301.1653 301.8737 313.9574 253.4473 -0.7147 301.3276 302.0422 314.1361 254.2033 -0.7182 301.4643 302.1824 314.3177 255.0405 -0.7224 301.6239 302.3463 314.5081 255.8270 -0.7262 301.8015 302.5277 314.6857 256.6340 -0.7309 301.9754 302.7063 314.8854 257.4510 -0.7394 302.1387 302.8782 315.1205 258.2273 -0.7445 302.2855 303.0299 315.3176 259.0545 -0.7476 302.4778 303.2255 315.5628 259.8200 -0.7495 302.6305 303.3800 315.7853 260.6683 -0.7503 302.7429 303.4932 316.0492 261.4443 -0.7541 302.8860 303.6401 316.2881 262.2610 -0.7586 303.0216 303.7802 316.5466 263.0478 -0.7614 303.1438 303.9052 316.7943 263.8545 -0.7673 303.3204 304.0877 317.0367 264.6715 -0.7722 303.4978 304.2700 317.2544 265.4273 -0.7774 303.6639 304.4413 317.4566 266.2955 -0.7853 303.8265 304.6118 317.6765 267.0513 -0.7926 303.9572 304.7498 317.8929 267.8788 -0.7937 304.1220 304.9156 318.0785 268.6750 -0.7973 304.3144 305.1117 318.2436 269.4718 -0.8029 304.4984 305.3014 318.4051 270.2993 -0.8094 304.6766 305.4861 318.5600 271.0545 -0.8168 304.8557 305.6725 318.6925 271.9230 -0.8220 305.0249 305.8468 318.8401 272.6788 -0.8238 305.1808 306.0046 318.9471 273.5058 -0.8278 305.3569 306.1847 319.0862 274.3028 -0.8323 305.5315 306.3638 319.1923 275.0993 -0.8375 305.6622 306.4998 319.2814 275.9268 -0.8445 305.8112 306.6557 319.3491 276.6825 -0.8464 305.9617 306.8081 319.4367 277.5508 -0.8528 306.1295 306.9823 319.4821 278.3168 -0.8597 306.2854 307.1451 319.5228 279.1440 -0.8633 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