DTA measure 2pb_updown Date: 202634:926 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1606.80 s Mass = 1164.300 mg data_number = 999 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3789 -5.1289 460.1725 465.3015 433.3535 3.9823 -5.1388 460.2023 465.3410 433.5969 5.5754 -5.1475 460.2027 465.3502 433.7910 7.1941 -5.1556 460.2280 465.3836 433.8870 8.7974 -5.1645 460.2645 465.4290 433.8853 10.4111 -5.1731 460.2705 465.4436 433.7751 12.0146 -5.1830 460.2751 465.4581 433.5691 13.6281 -5.1863 460.2714 465.4576 433.2878 15.2315 -5.1852 460.2700 465.4552 432.9131 16.8451 -5.1913 460.3096 465.5008 432.4647 18.4639 -5.1971 460.3016 465.4987 431.9770 20.0725 -5.2024 460.3202 465.5226 431.5148 21.6813 -5.2041 460.3306 465.5347 431.0193 23.2896 -5.2049 460.3283 465.5332 430.5088 24.8930 -5.2010 460.3064 465.5074 430.0403 26.4864 -5.2008 460.2867 465.4875 429.5737 28.0845 -5.1977 460.2966 465.4943 429.1149 29.6829 -5.1969 460.2794 465.4763 428.7443 31.3069 -5.1951 460.2678 465.4629 428.4406 32.9101 -5.1946 460.2423 465.4369 428.2171 34.5188 -5.1956 460.2103 465.4059 428.0901 36.1221 -5.1946 460.1992 465.3939 427.9386 37.7254 -5.1949 460.1369 465.3318 427.9219 39.3340 -5.1967 460.0662 465.2629 427.9293 40.9476 -5.1951 460.0420 465.2371 427.9636 42.5510 -5.1967 459.9901 465.1868 427.9928 44.1751 -5.1997 459.9393 465.1390 427.9777 45.7838 -5.2030 459.8912 465.0942 427.9858 47.3921 -5.2164 459.8879 465.1043 427.9036 49.0008 -5.2167 459.8411 465.0578 427.7989 50.5991 -5.2102 459.8112 465.0214 427.6707 52.2178 -5.2139 459.7645 464.9784 427.5127 53.8059 -5.2179 459.7221 464.9399 427.2832 55.4299 -5.2164 459.6586 464.8750 427.0059 57.0331 -5.2186 459.5837 464.8023 426.7290 58.6213 -5.2178 459.5089 464.7267 426.4122 60.2296 -5.2166 459.4902 464.7068 426.0656 61.8484 -5.2207 459.4765 464.6972 425.6915 63.4519 -5.2208 459.4202 464.6411 425.3240 65.0448 -5.2247 459.3699 464.5946 424.9836 66.6431 -5.2184 459.2807 464.4991 424.6227 68.2468 -5.2196 459.1812 464.4008 424.2855 69.8550 -5.2217 459.1274 464.3490 423.9887 71.4585 -5.2236 459.0566 464.2802 423.7274 73.0670 -5.2233 458.9193 464.1426 423.5013 74.6906 -5.2195 458.8041 464.0236 423.3007 76.2993 -5.2188 458.7098 463.9286 423.1615 77.9025 -5.2195 458.6376 463.8571 423.0422 79.5111 -5.2204 458.5750 463.7955 422.9154 81.1195 -5.2170 458.5155 463.7325 422.8369 82.7281 -5.2152 458.4420 463.6572 422.7197 84.3213 -5.2182 458.3766 463.5949 422.6617 85.9298 -5.2238 458.3087 463.5325 422.5727 87.5485 -5.2252 458.2067 463.4318 422.4673 89.1520 -5.2257 458.0821 463.3077 422.3306 90.7604 -5.2260 457.9922 463.2182 422.1767 92.3586 -5.2298 457.8903 463.1201 421.9758 93.9673 -5.2326 457.7710 463.0036 421.7676 95.5653 -5.2283 457.7135 462.9418 421.5366 97.1688 -5.2264 457.6384 462.8648 421.2740 98.7775 -5.2320 457.4996 462.7316 421.0071 100.3808 -5.2379 457.3832 462.6211 420.7376 101.9894 -5.2333 457.2917 462.5250 420.4583 103.5929 -5.2306 457.1880 462.4185 420.1790 105.1961 -5.2248 457.0780 462.3028 419.9029 106.8048 -5.2226 456.9740 462.1966 419.6168 108.4185 -5.2197 456.8535 462.0732 419.3251 110.0270 -5.2232 456.7751 461.9983 419.0327 111.6458 -5.2222 456.6302 461.8524 418.7818 113.2544 -5.2217 456.5061 461.7278 418.5313 114.8579 -5.2199 456.3821 461.6020 418.3415 116.4715 -5.2167 456.2461 461.4628 418.1449 118.0750 -5.2180 456.1300 461.3480 417.9433 119.6886 -5.2169 456.0308 461.2478 417.7762 121.2971 -5.2145 455.9085 461.1230 417.6071 122.8904 -5.2116 455.7826 460.9943 417.4627 124.4936 -5.2103 455.6362 460.8465 417.3302 126.1124 -5.2100 455.5233 460.7333 417.1993 127.7109 -5.2073 455.4117 460.6190 417.0336 129.3194 -5.2101 455.2948 460.5050 416.8412 130.9228 -5.2105 455.1177 460.3281 416.7180 132.5314 -5.2101 454.9573 460.1674 416.5455 134.1345 -5.2064 454.8118 460.0182 416.3822 135.7431 -5.2049 454.6910 459.8958 416.1916 137.3671 -5.2048 454.5894 459.7943 415.9367 138.9704 -5.1999 454.4519 459.6518 415.7055 140.5636 -5.1996 454.3283 459.5280 415.4598 142.1876 -5.1979 454.1624 459.3603 415.2119 143.7959 -5.1921 454.0331 459.2252 414.9546 145.3994 -5.1896 453.8953 459.0849 414.7503 147.0130 -5.1912 453.7310 458.9222 414.5099 148.6316 -5.1894 453.5977 458.7870 414.2575 150.2453 -5.1854 453.4322 458.6175 413.9772 151.8485 -5.1839 453.3042 458.4881 413.7236 153.4469 -5.1794 453.1641 458.3436 413.4775 155.0449 -5.1761 453.0147 458.1908 413.2528 156.6483 -5.1708 452.8929 458.0637 413.0513 158.2516 -5.1711 452.7424 457.9135 412.8420 159.8395 -5.1709 452.5380 457.7090 412.6513 161.4481 -5.1658 452.3603 457.5260 412.4526 163.0670 -5.1605 452.2207 457.3811 412.2416 164.6755 -5.1603 452.0706 457.2309 412.0388 166.2790 -5.1566 451.9477 457.1043 411.8654 167.8771 -5.1504 451.8016 456.9520 411.6765 169.4805 -5.1426 451.6360 456.7786 411.5136 171.0840 -5.1370 451.4576 456.5946 411.3259 172.6924 -5.1319 451.3157 456.4476 411.1406 174.2958 -5.1282 451.1295 456.2578 410.9490 175.9250 -5.1288 450.9514 456.0802 410.7583 177.5283 -5.1240 450.8098 455.9339 410.5335 179.1266 -5.1178 450.6401 455.7579 410.3217 180.7301 -5.1183 450.4756 455.5939 410.1352 182.3385 -5.1158 450.3055 455.4213 409.9425 183.9471 -5.1110 450.1129 455.2240 409.7359 185.5558 -5.1049 449.9169 455.0217 409.5163 187.1540 -5.1018 449.7700 454.8719 409.2716 188.7678 -5.1041 449.6167 454.7208 409.0484 190.3764 -5.0991 449.4766 454.5757 408.8339 191.9748 -5.0919 449.3445 454.4364 408.5825 193.5780 -5.0912 449.1918 454.2830 408.3387 195.1714 -5.0895 449.0402 454.1297 408.1220 196.7746 -5.0932 448.8532 453.9464 407.8720 198.3831 -5.0845 448.6514 453.7359 407.6115 199.9866 -5.0790 448.5090 453.5879 407.3752 201.6156 -5.0734 448.3054 453.3788 407.1840 203.2190 -5.0702 448.1170 453.1872 406.9880 204.8276 -5.0668 447.9582 453.0250 406.7960 206.4361 -5.0652 447.7987 452.8639 406.6082 208.0446 -5.0633 447.6322 452.6955 406.4194 209.6379 -5.0553 447.4539 452.5092 406.2215 211.2463 -5.0504 447.2821 452.3325 406.0198 212.8496 -5.0515 447.1221 452.1736 405.8282 214.4788 -5.0522 446.9608 452.0130 405.6470 216.0820 -5.0531 446.7788 451.8318 405.4443 217.6906 -5.0491 446.5660 451.6151 405.2383 219.2940 -5.0461 446.3761 451.4222 405.0420 220.8921 -5.0391 446.2085 451.2476 404.8467 222.5008 -5.0366 446.0561 451.0927 404.6564 224.0991 -5.0311 445.8857 450.9168 404.4501 225.7179 -5.0203 445.7028 450.7231 404.2478 227.3265 -5.0248 445.4949 450.5197 403.9789 228.9300 -5.0213 445.3339 450.3552 403.7535 230.5384 -5.0147 445.1506 450.1653 403.5367 232.1419 -5.0042 444.9636 449.9677 403.3162 233.7556 -4.9981 444.7551 449.7533 403.0783 235.3589 -4.9965 444.5517 449.5482 402.8852 236.9778 -4.9904 444.4008 449.3912 402.6494 238.5760 -4.9904 444.2235 449.2139 402.4635 240.1946 -4.9877 444.0407 449.0284 402.2534 241.8031 -4.9801 443.8482 448.8283 402.0328 243.4115 -4.9767 443.6583 448.6350 401.8288 245.0201 -4.9718 443.4637 448.4355 401.5382 246.6285 -4.9647 443.2683 448.2330 401.3403 248.2215 -4.9575 443.1097 448.0672 401.1586 249.8455 -4.9498 442.9076 447.8574 400.9621 251.4538 -4.9389 442.7629 447.7017 400.7857 253.0521 -4.9333 442.5493 447.4826 400.6036 254.6504 -4.9330 442.3810 447.3140 400.3897 256.2589 -4.9261 442.1778 447.1040 400.1859 257.8624 -4.9213 442.0212 446.9425 399.9796 259.4708 -4.9195 441.8474 446.7670 399.7368 261.0588 -4.9127 441.6125 446.5253 399.5234 262.6828 -4.9041 441.3874 446.2915 399.2923 264.2860 -4.9049 441.2283 446.1331 399.0771 265.8895 -4.9012 441.0620 445.9631 398.8581 267.4981 -4.8987 440.8681 445.7667 398.6591 269.1116 -4.8945 440.6937 445.5881 398.4887 270.7203 -4.8906 440.4830 445.3736 398.2854 272.3238 -4.8875 440.3173 445.2048 398.0803 273.9526 -4.8780 440.1099 444.9879 397.8828 275.5408 -4.8743 439.9021 444.7764 397.6363 277.1545 -4.8690 439.7026 444.5715 397.3716 278.7579 -4.8661 439.5199 444.3860 397.1424 280.3716 -4.8627 439.3252 444.1878 396.9224 281.9751 -4.8550 439.1223 443.9773 396.7207 283.5631 -4.8493 438.9081 443.7574 396.5403 285.1766 -4.8378 438.6971 443.5349 396.3095 286.7648 -4.8298 438.5200 443.3497 396.0804 288.3835 -4.8250 438.3246 443.1495 395.8803 289.9870 -4.8225 438.1474 442.9699 395.6420 291.5956 -4.8209 437.9302 442.7511 395.4244 293.1988 -4.8171 437.7310 442.5480 395.1836 294.8023 -4.8119 437.5377 442.3496 394.9461 296.4109 -4.8068 437.3425 442.1493 394.7621 297.9986 -4.8021 437.1407 441.9428 394.6032 299.6074 -4.7929 436.9437 441.7366 394.4227 301.2263 -4.7861 436.7540 441.5402 394.2286 302.8346 -4.7790 436.5488 441.3278 394.0342 304.4381 -4.7800 436.3519 441.1320 393.8611 306.0469 -4.7773 436.1590 440.9364 393.6301 307.6551 -4.7684 435.9183 440.6868 393.4373 309.2638 -4.7646 435.6919 440.4566 393.2277 310.8724 -4.7619 435.5117 440.2736 393.0373 312.4911 -4.7649 435.3238 440.0887 392.8291 314.0996 -4.7575 435.1082 439.8657 392.6276 315.7031 -4.7530 434.9090 439.6620 392.4110 317.2910 -4.7492 434.6966 439.4458 392.2040 318.8945 -4.7405 434.5003 439.2409 391.9490 320.4928 -4.7284 434.3298 439.0582 391.7237 322.1011 -4.7177 434.1563 438.8740 391.5074 323.7046 -4.7155 433.9291 438.6446 391.2664 325.3285 -4.7135 433.7290 438.4425 391.0622 326.9320 -4.7098 433.5106 438.2205 390.8704 328.5355 -4.7028 433.3057 438.0085 390.6645 330.1491 -4.6996 433.0897 437.7894 390.4468 331.7524 -4.6945 432.8977 437.5922 390.2178 333.3611 -4.6935 432.7368 437.4303 389.9988 334.9695 -4.6805 432.5394 437.2199 389.7632 336.5934 -4.6711 432.3210 436.9921 389.5305 338.2019 -4.6708 432.1072 436.7780 389.3242 339.8101 -4.6701 431.8845 436.5545 389.1228 341.4138 -4.6665 431.6944 436.3609 388.8966 343.0221 -4.6620 431.5127 436.1747 388.6915 344.6305 -4.6556 431.3156 435.9712 388.5079 346.2391 -4.6480 431.1378 435.7858 388.3051 347.8578 -4.6418 430.9126 435.5543 388.0744 349.4561 -4.6326 430.7159 435.3484 387.8789 351.0648 -4.6297 430.5145 435.1442 387.7376 352.6629 -4.6298 430.2835 434.9133 387.5635 354.2715 -4.6253 430.0833 434.7086 387.3721 355.8699 -4.6172 429.8586 434.4757 387.1802 357.4731 -4.6128 429.6540 434.2668 386.9553 359.0664 -4.6096 429.4714 434.0810 386.7174 360.6850 -4.6057 429.2372 433.8428 386.5146 362.2935 -4.6026 429.0590 433.6616 386.2839 363.8970 -4.6024 428.8747 433.4771 386.0548 365.5156 -4.5952 428.6753 433.2705 385.8002 367.1190 -4.5831 428.4759 433.0590 385.6156 368.7276 -4.5708 428.2622 432.8330 385.3841 370.3360 -4.5669 428.0362 432.6030 385.1246 371.9600 -4.5673 427.7725 432.3397 384.9031 373.5634 -4.5633 427.5761 432.1393 384.7252 375.1666 -4.5603 427.3410 431.9013 384.5290 376.7805 -4.5538 427.1436 431.6974 384.3050 378.3838 -4.5476 426.9587 431.5063 384.0858 379.9923 -4.5411 426.7713 431.3124 383.8520 381.5905 -4.5320 426.5830 431.1150 383.5982 383.2091 -4.5311 426.3229 430.8540 383.4042 384.8126 -4.5167 426.1368 430.6534 383.2307 386.4005 -4.5086 425.9636 430.4721 383.0534 388.0141 -4.4993 425.7552 430.2545 382.8141 389.6176 -4.4927 425.5443 430.0370 382.6272 391.2259 -4.4907 425.3379 429.8286 382.4246 392.8294 -4.4816 425.1322 429.6138 382.2118 394.4379 -4.4781 424.9378 429.4159 382.0013 396.0566 -4.4734 424.7149 429.1882 381.8051 397.6653 -4.4653 424.5435 429.0088 381.5648 399.2739 -4.4612 424.3724 428.8335 381.3590 400.8771 -4.4539 424.1396 428.5935 381.1928 402.4909 -4.4504 423.9191 428.3695 381.0094 404.0994 -4.4515 423.6973 428.1488 380.7999 405.7078 -4.4532 423.4723 427.9255 380.5857 407.3265 -4.4437 423.2539 427.6976 380.3518 408.9349 -4.4337 423.0184 427.4521 380.1163 410.5384 -4.4255 422.8048 427.2303 379.9058 412.1471 -4.4198 422.5967 427.0165 379.7116 413.7454 -4.4129 422.3678 426.7807 379.4874 415.3436 -4.4056 422.1861 426.5917 379.2715 416.9369 -4.3999 421.9678 426.3677 379.0633 418.5401 -4.3962 421.7540 426.1501 378.8790 420.1641 -4.3913 421.5931 425.9844 378.6468 421.7675 -4.3822 421.3761 425.7583 378.4288 423.3710 -4.3762 421.1399 425.5161 378.2076 424.9794 -4.3717 420.9544 425.3261 378.0122 426.5829 -4.3669 420.7577 425.1246 377.7988 428.1913 -4.3596 420.5894 424.9489 377.5986 429.7998 -4.3511 420.3840 424.7351 377.4140 431.4239 -4.3414 420.1619 424.5033 377.2298 433.0323 -4.3378 419.9402 424.2780 377.0224 434.6255 -4.3333 419.6935 424.0268 376.8169 436.2339 -4.3290 419.4576 423.7865 376.5962 437.8424 -4.3218 419.2470 423.5689 376.3828 439.4459 -4.3115 419.0388 423.3504 376.1350 441.0596 -4.2989 418.8576 423.1565 375.9122 442.6629 -4.2933 418.6610 422.9543 375.6738 444.2818 -4.2887 418.4512 422.7399 375.4421 445.8850 -4.2847 418.2559 422.5406 375.2184 447.4884 -4.2800 418.0698 422.3499 374.9958 449.0919 -4.2651 417.8343 422.0994 374.7584 450.6849 -4.2614 417.5914 421.8528 374.5455 452.2935 -4.2551 417.3819 421.6370 374.3695 453.8968 -4.2534 417.1648 421.4182 374.2079 455.5001 -4.2498 416.9569 421.2067 374.0101 457.1240 -4.2396 416.7563 420.9959 373.8224 458.7273 -4.2352 416.5391 420.7742 373.6047 460.3359 -4.2267 416.3409 420.5676 373.3765 461.9394 -4.2194 416.1207 420.3400 373.1393 463.5478 -4.2109 415.9208 420.1317 372.9184 465.1514 -4.2056 415.7378 419.9434 372.7434 466.7650 -4.2039 415.5275 419.7314 372.5292 468.3836 -4.2001 415.2776 419.4777 372.3098 469.9873 -4.1900 415.0813 419.2713 372.1169 471.6010 -4.1877 414.8601 419.0479 371.9088 473.2093 -4.1782 414.6604 418.8386 371.6871 474.8179 -4.1720 414.4457 418.6177 371.4610 476.4265 -4.1650 414.2364 418.4015 371.2588 478.0298 -4.1556 414.0009 418.1565 371.0841 479.6179 -4.1503 413.7769 417.9273 370.8768 481.2366 -4.1440 413.5543 417.6983 370.6534 482.8400 -4.1418 413.3608 417.5026 370.3894 484.4384 -4.1391 413.1947 417.3338 370.1482 486.0470 -4.1330 412.9706 417.1036 369.9564 487.6503 -4.1264 412.7563 416.8827 369.7887 489.2589 -4.1182 412.5548 416.6730 369.6046 490.8624 -4.1116 412.3346 416.4462 369.3840 492.4810 -4.1067 412.0970 416.2037 369.1242 494.0896 -4.0971 411.8897 415.9867 368.8868 495.6983 -4.0821 411.6674 415.7495 368.6753 497.3065 -4.0759 411.4472 415.5231 368.4642 498.9151 -4.0689 411.2107 415.2796 368.2913 500.5236 -4.0632 411.0130 415.0762 368.1044 502.1321 -4.0584 410.8177 414.8761 367.9071 503.7561 -4.0571 410.5952 414.6523 367.7196 505.3646 -4.0499 410.4280 414.4779 367.5309 506.9731 -4.0381 410.1915 414.2296 367.3074 508.5766 -4.0310 409.9776 414.0086 367.1004 510.1850 -4.0319 409.7630 413.7949 366.8784 511.7730 -4.0227 409.5805 413.6031 366.6597 513.3714 -4.0168 409.3687 413.3856 366.4437 514.9798 -4.0098 409.1555 413.1653 366.2000 516.5985 -4.0011 408.9521 412.9532 365.9913 518.2019 -3.9972 408.7238 412.7210 365.7575 519.8051 -3.9917 408.5141 412.5058 365.5255 521.4086 -3.9854 408.2932 412.2787 365.2806 523.0170 -3.9757 408.0434 412.0191 365.0768 524.6255 -3.9741 407.8319 411.8060 364.8617 526.2391 -3.9675 407.6182 411.5857 364.6403 527.8578 -3.9586 407.3813 411.3398 364.4323 529.4664 -3.9543 407.1605 411.1148 364.2342 531.0749 -3.9512 406.9467 410.8979 364.0287 532.6834 -3.9485 406.7290 410.6775 363.8415 534.2920 -3.9455 406.5454 410.4909 363.6496 535.9004 -3.9437 406.3664 410.3101 363.4387 537.5090 -3.9305 406.1649 410.0953 363.2517 539.1330 -3.9222 405.9668 409.8890 363.0630 540.7363 -3.9192 405.7312 409.6504 362.8636 542.3449 -3.9137 405.4990 409.4127 362.6757 543.9431 -3.9091 405.2791 409.1883 362.4706 545.5310 -3.9018 405.0570 408.9588 362.2141 547.1345 -3.8952 404.8302 408.7254 361.9796 548.7381 -3.8940 404.6327 408.5267 361.7585 550.3465 -3.8891 404.4222 408.3113 361.4979 551.9653 -3.8821 404.2140 408.0961 361.2748 553.5686 -3.8781 403.9829 407.8610 361.0620 555.1770 -3.8677 403.7681 407.6358 360.8646 556.7806 -3.8585 403.5560 407.4145 360.6422 558.3891 -3.8506 403.3599 407.2105 360.4325 559.9925 -3.8405 403.1218 406.9623 360.2133 561.6063 -3.8394 402.9250 406.7644 360.0235 563.2248 -3.8311 402.6995 406.5306 359.7985 564.8385 -3.8204 402.4936 406.3140 359.6229 566.4420 -3.8205 402.2823 406.1028 359.4274 568.0554 -3.8169 402.0825 405.8993 359.1968 569.6589 -3.8121 401.8908 405.7030 358.9549 571.2673 -3.8051 401.6938 405.4989 358.7696 572.8758 -3.7985 401.4761 405.2746 358.5487 574.4894 -3.7922 401.2295 405.0217 358.3392 576.0926 -3.7864 400.9780 404.7645 358.1305 577.6961 -3.7862 400.7917 404.5778 357.8888 579.2891 -3.7847 400.6186 404.4033 357.7079 580.9028 -3.7765 400.3838 404.1603 357.5525 582.4909 -3.7714 400.1590 403.9305 357.3395 584.0994 -3.7668 399.9421 403.7089 357.1400 585.7028 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