DTA measure 2pb_updown4 Date: 202634:954 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1514.01 s Mass = 1164.300 mg data_number = 1884 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2820 -1.0903 254.0258 255.1161 243.8446 2.0475 -1.0831 254.0563 255.1394 243.6326 2.8755 -1.0741 254.0567 255.1309 243.4038 3.6625 -1.0621 254.0933 255.1554 243.1982 4.4495 -1.0488 254.1085 255.1573 242.9976 5.2775 -1.0356 254.1449 255.1805 242.8308 6.0438 -1.0244 254.1770 255.2014 242.6670 6.8923 -1.0124 254.1936 255.2061 242.4799 7.6273 -0.9985 254.2206 255.2191 242.3492 8.4860 -0.9846 254.2746 255.2592 242.2262 9.2423 -0.9711 254.3046 255.2757 242.1012 10.0703 -0.9603 254.3198 255.2801 241.9977 10.8675 -0.9515 254.3377 255.2892 241.9111 11.6545 -0.9475 254.3626 255.3101 241.8655 12.4825 -0.9382 254.4061 255.3443 241.8610 13.2485 -0.9287 254.4263 255.3551 241.8673 14.0965 -0.9185 254.4341 255.3526 241.8998 14.8733 -0.9082 254.4783 255.3865 241.9746 15.6910 -0.8977 254.4901 255.3878 242.0602 16.4780 -0.8874 254.5188 255.4062 242.1798 17.2855 -0.8769 254.5291 255.4061 242.3571 18.1033 -0.8686 254.5556 255.4242 242.5577 18.8693 -0.8628 254.5712 255.4340 242.7855 19.7275 -0.8538 254.6203 255.4741 243.0465 20.4633 -0.8480 254.6302 255.4782 243.3293 21.3220 -0.8423 254.6429 255.4852 243.6661 22.0783 -0.8347 254.6460 255.4807 243.9505 22.9165 -0.8250 254.6758 255.5008 244.2865 23.7035 -0.8184 254.7026 255.5210 244.6426 24.4998 -0.8144 254.7038 255.5182 245.0044 25.3278 -0.8097 254.7202 255.5299 245.3665 26.0943 -0.8023 254.7250 255.5273 245.6952 26.9530 -0.7904 254.7498 255.5401 246.0629 27.7093 -0.7849 254.7823 255.5672 246.3419 28.5475 -0.7804 254.8246 255.6050 246.6382 29.3345 -0.7764 254.8592 255.6356 246.9499 30.1310 -0.7721 254.8746 255.6467 247.2738 30.9588 -0.7691 254.9076 255.6767 247.5573 31.7253 -0.7651 254.9368 255.7019 247.8173 32.5840 -0.7641 254.9686 255.7327 248.0556 33.3403 -0.7612 254.9733 255.7345 248.2341 34.1785 -0.7536 254.9983 255.7519 248.4051 34.9655 -0.7498 255.0413 255.7911 248.5530 35.7725 -0.7477 255.0338 255.7815 248.6771 36.5590 -0.7477 255.0358 255.7835 248.7997 37.3665 -0.7415 255.0792 255.8207 248.8872 38.1843 -0.7404 255.1108 255.8512 248.9268 38.9508 -0.7392 255.1364 255.8756 248.9547 39.8093 -0.7328 255.1778 255.9105 249.0021 40.5750 -0.7299 255.2120 255.9419 249.0200 41.4030 -0.7253 255.2474 255.9726 249.0241 42.2003 -0.7214 255.2398 255.9612 249.0002 42.9975 -0.7238 255.2900 256.0137 248.9663 43.8255 -0.7177 255.3431 256.0608 248.9535 44.5920 -0.7146 255.3737 256.0883 248.9283 45.4405 -0.7082 255.4179 256.1262 248.8472 46.2165 -0.7072 255.4387 256.1459 248.7863 47.0340 -0.7032 255.4530 256.1562 248.7263 47.8313 -0.7004 255.4791 256.1795 248.6563 48.6285 -0.6975 255.4993 256.1968 248.5815 49.4565 -0.6941 255.5205 256.2146 248.4889 50.2230 -0.6903 255.5575 256.2478 248.4257 51.0715 -0.6872 255.5807 256.2679 248.3679 51.8483 -0.6831 255.6203 256.3034 248.3365 52.6753 -0.6848 255.6415 256.3264 248.3527 53.4725 -0.6812 255.6913 256.3724 248.3107 54.2595 -0.6782 255.7201 256.3983 248.3018 55.0978 -0.6763 255.7456 256.4219 248.3269 55.8540 -0.6736 255.7599 256.4335 248.3420 56.7128 -0.6711 255.7885 256.4597 248.3541 57.4485 -0.6662 255.8421 256.5083 248.4105 58.3065 -0.6652 255.8988 256.5640 248.4644 59.0728 -0.6586 255.9428 256.6014 248.5181 59.8905 -0.6514 255.9687 256.6201 248.6351 60.6980 -0.6528 255.9669 256.6197 248.7423 61.4850 -0.6485 255.9779 256.6264 248.8880 62.3130 -0.6454 256.0230 256.6684 249.0460 63.0795 -0.6443 256.0808 256.7252 249.2158 63.9485 -0.6427 256.1126 256.7553 249.4285 64.7045 -0.6413 256.1350 256.7762 249.6384 65.5318 -0.6433 256.1735 256.8168 249.8757 66.3290 -0.6398 256.2082 256.8481 250.1008 67.1263 -0.6371 256.2620 256.8991 250.3093 67.9440 -0.6344 256.3064 256.9408 250.5675 68.7105 -0.6342 256.3406 256.9748 250.8070 69.5385 -0.6322 256.3649 256.9972 251.0813 70.2945 -0.6308 256.3777 257.0085 251.3575 71.1535 -0.6296 256.4175 257.0471 251.6266 71.9090 -0.6302 256.4594 257.0895 251.8643 72.7470 -0.6280 256.4756 257.1036 252.0960 73.5033 -0.6293 256.4845 257.1138 252.3079 74.3415 -0.6258 256.5057 257.1315 252.5303 75.1285 -0.6258 256.5480 257.1738 252.7313 75.9155 -0.6247 256.5842 257.2090 252.9104 76.7538 -0.6269 256.6251 257.2521 253.0889 77.5098 -0.6253 256.6654 257.2907 253.2755 78.3678 -0.6286 256.7003 257.3290 253.4200 79.1343 -0.6274 256.7223 257.3497 253.5290 79.9520 -0.6293 256.7589 257.3882 253.6307 80.7185 -0.6307 256.7856 257.4162 253.7298 81.5465 -0.6313 256.8195 257.4508 253.8282 82.3438 -0.6298 256.8523 257.4821 253.8849 83.1403 -0.6284 256.9104 257.5388 253.9305 83.9578 -0.6294 256.9608 257.5903 253.9465 84.7345 -0.6222 256.9901 257.6123 253.9790 85.5830 -0.6229 257.0166 257.6394 253.9804 86.3495 -0.6247 257.0429 257.6676 254.0241 87.1775 -0.6264 257.1135 257.7399 254.0606 87.9748 -0.6291 257.1733 257.8024 254.0803 88.7710 -0.6288 257.2180 257.8468 254.0777 89.5888 -0.6285 257.2869 257.9154 254.0661 90.3655 -0.6250 257.3178 257.9428 254.0519 91.1833 -0.6227 257.3491 257.9718 254.0576 91.9498 -0.6237 257.3887 258.0124 254.0439 92.8085 -0.6226 257.4312 258.0538 254.0317 93.5750 -0.6199 257.4914 258.1113 254.0168 94.4030 -0.6210 257.5309 258.1518 254.0107 95.2003 -0.6204 257.5909 258.2114 254.0254 95.9965 -0.6229 257.6413 258.2642 254.0514 96.8245 -0.6193 257.6789 258.2982 254.0750 97.5910 -0.6186 257.7039 258.3225 254.1114 98.4395 -0.6166 257.7488 258.3654 254.1392 99.2163 -0.6156 257.7715 258.3872 254.1974 100.0340 -0.6122 257.8174 258.4296 254.2899 100.8005 -0.6104 257.8898 258.5003 254.3757 101.6280 -0.6107 257.9328 258.5435 254.4758 102.4248 -0.6071 257.9999 258.6070 254.5887 103.2220 -0.6080 258.0711 258.6792 254.6700 104.0398 -0.6071 258.1372 258.7443 254.8109 104.8165 -0.6075 258.1780 258.7855 254.9561 105.6650 -0.6067 258.2073 258.8140 255.1136 106.4315 -0.6023 258.2537 258.8560 255.2568 107.2590 -0.5994 258.2878 258.8872 255.4377 108.0558 -0.5940 258.3274 258.9213 255.6354 108.8530 -0.5911 258.3556 258.9467 255.8394 109.6708 -0.5900 258.4106 259.0006 256.0602 110.4475 -0.5881 258.4565 259.0446 256.2706 111.2960 -0.5872 258.5229 259.1101 256.4775 112.0625 -0.5887 258.5779 259.1667 256.6830 112.8905 -0.5872 258.6233 259.2105 256.8829 113.6980 -0.5916 258.6858 259.2774 257.0258 114.4840 -0.5957 258.7042 259.2999 257.2016 115.3120 -0.5940 258.7402 259.3341 257.3953 116.0785 -0.5937 258.7874 259.3811 257.5880 116.9373 -0.5906 258.8237 259.4143 257.7852 117.7038 -0.5876 258.8540 259.4416 257.9564 118.5215 -0.5868 258.9013 259.4881 258.1372 119.3290 -0.5872 258.9540 259.5412 258.2744 120.1160 -0.5883 259.0143 259.6026 258.4156 120.9438 -0.5878 259.0785 259.6664 258.5558 121.7095 -0.5873 259.1259 259.7132 258.6944 122.5683 -0.5858 259.1441 259.7300 258.8490 123.3348 -0.5820 259.1916 259.7736 258.9496 124.1525 -0.5850 259.2642 259.8492 259.0557 124.9600 -0.5838 259.3243 259.9080 259.1199 125.7470 -0.5814 259.3866 259.9680 259.2020 126.5750 -0.5791 259.4491 260.0283 259.2944 127.3415 -0.5812 259.5043 260.0855 259.3549 128.1995 -0.5818 259.5759 260.1577 259.3578 128.9658 -0.5816 259.6308 260.2124 259.3998 129.7835 -0.5823 259.7081 260.2904 259.4418 130.5910 -0.5822 259.7476 260.3298 259.4551 131.3780 -0.5868 259.8001 260.3868 259.4925 132.1958 -0.5870 259.8829 260.4699 259.5387 132.9725 -0.5887 259.9468 260.5355 259.5904 133.8205 -0.5876 260.0028 260.5904 259.6040 134.5763 -0.5844 260.0772 260.6616 259.6187 135.4043 -0.5843 260.1784 260.7628 259.6311 136.1913 -0.5858 260.2210 260.8068 259.6469 136.9885 -0.5870 260.2696 260.8566 259.6671 137.8165 -0.5872 260.3391 260.9263 259.7103 138.5728 -0.5870 260.4047 260.9917 259.7651 139.4313 -0.5835 260.4879 261.0714 259.8048 140.1970 -0.5832 260.5385 261.1218 259.8455 141.0148 -0.5852 260.5809 261.1662 259.9120 141.7813 -0.5828 260.6376 261.2204 259.9807 142.6093 -0.5848 260.6821 261.2669 260.0685 143.3963 -0.5857 260.7263 261.3120 260.1424 144.1935 -0.5850 260.7970 261.3820 260.2240 145.0215 -0.5821 260.8758 261.4579 260.3063 145.7880 -0.5804 260.9183 261.4987 260.4063 146.6360 -0.5817 260.9751 261.5568 260.5363 147.4123 -0.5824 260.9969 261.5793 260.6454 148.2300 -0.5840 261.0595 261.6435 260.7929 148.9965 -0.5844 261.1267 261.7111 260.9303 149.8245 -0.5848 261.1587 261.7435 261.0830 150.6218 -0.5817 261.2281 261.8098 261.2740 151.4188 -0.5810 261.2980 261.8790 261.4676 152.2360 -0.5772 261.3623 261.9396 261.6138 153.0125 -0.5774 261.4143 261.9917 261.7814 153.8610 -0.5750 261.4827 262.0577 261.9898 154.6275 -0.5721 261.5551 262.1272 262.1635 155.4555 -0.5746 261.6370 262.2115 262.3649 156.2528 -0.5767 261.7309 262.3076 262.5568 157.0500 -0.5768 261.7834 262.3602 262.7672 157.8363 -0.5747 261.8116 262.3863 262.9586 158.6435 -0.5748 261.8573 262.4321 263.1267 159.4613 -0.5735 261.9285 262.5020 263.3034 160.2278 -0.5739 262.0037 262.5776 263.4298 161.0865 -0.5744 262.0735 262.6478 263.5896 161.8530 -0.5770 262.1538 262.7308 263.7197 162.6810 -0.5803 262.2185 262.7988 263.8421 163.4680 -0.5817 262.2850 262.8666 263.9419 164.2745 -0.5853 262.3681 262.9534 264.0525 165.0923 -0.5856 262.4319 263.0175 264.1712 165.8588 -0.5901 262.4828 263.0729 264.2690 166.7175 -0.5934 262.5478 263.1412 264.3695 167.4533 -0.5962 262.6446 263.2408 264.4616 168.3120 -0.5976 262.7245 263.3221 264.5586 169.0683 -0.6024 262.7825 263.3848 264.6238 169.9063 -0.6036 262.8313 263.4349 264.6998 170.6925 -0.6060 262.8659 263.4719 264.7701 171.4898 -0.6072 262.9162 263.5234 264.8326 172.3178 -0.6060 262.9991 263.6051 264.8713 173.0843 -0.6042 263.0956 263.6998 264.8983 173.9430 -0.6065 263.1825 263.7890 264.9481 174.7095 -0.6083 263.2371 263.8454 265.0031 175.5375 -0.6081 263.3075 263.9156 265.0578 176.3338 -0.6067 263.3743 263.9811 265.0878 177.1310 -0.6043 263.4535 264.0578 265.1179 177.9488 -0.6058 263.5437 264.1495 265.1858 178.7255 -0.6049 263.6260 264.2309 265.2357 179.5740 -0.6039 263.7129 264.3168 265.3081 180.3200 -0.6032 263.7929 264.3961 265.3699 181.1685 -0.6016 263.8684 264.4701 265.3997 181.9443 -0.6031 263.9311 264.5341 265.4643 182.7620 -0.6042 264.0006 264.6048 265.5276 183.5593 -0.6066 264.0751 264.6817 265.6207 184.3565 -0.6065 264.1380 264.7445 265.7076 185.1845 -0.6097 264.1940 264.8038 265.8297 185.9510 -0.6082 264.2592 264.8675 265.9139 186.7995 -0.6048 264.3534 264.9582 266.0092 187.5763 -0.6034 264.4328 265.0362 266.1430 188.3930 -0.6045 264.5063 265.1107 266.2755 189.1903 -0.6017 264.5610 265.1627 266.4125 189.9875 -0.6018 264.6431 265.2448 266.5492 190.8155 -0.6013 264.7291 265.3304 266.6895 191.5820 -0.6001 264.8085 265.4085 266.8236 192.4305 -0.5991 264.8957 265.4949 266.9681 193.2073 -0.6021 264.9691 265.5712 267.1173 194.0250 -0.6032 265.0414 265.6447 267.2689 194.8218 -0.6009 265.1065 265.7073 267.4231 195.6185 -0.6027 265.1191 265.7218 267.5721 196.4465 -0.6065 265.2174 265.8240 267.7214 197.2028 -0.6078 265.2965 265.9042 267.8293 198.0615 -0.6065 265.3540 265.9605 267.9880 198.8178 -0.6047 265.4192 266.0239 268.1430 199.6355 -0.6046 265.5153 266.1199 268.3075 200.4425 -0.6073 265.6074 266.2148 268.4701 201.2290 -0.6069 265.6852 266.2921 268.6200 202.0468 -0.6040 265.7708 266.3748 268.7724 202.8235 -0.6029 265.8567 266.4596 268.9108 203.6413 -0.6067 265.9334 266.5401 269.0631 204.4078 -0.6068 266.0020 266.6088 269.1778 205.2663 -0.6082 266.0593 266.6675 269.3098 206.0218 -0.6065 266.1242 266.7308 269.4124 206.8498 -0.6077 266.2032 266.8109 269.5251 207.6470 -0.6079 266.2907 266.8986 269.6341 208.4443 -0.6044 266.3814 266.9858 269.7386 209.2620 -0.6007 266.4610 267.0617 269.8470 210.0285 -0.5973 266.5462 267.1435 269.9255 210.8873 -0.5992 266.6546 267.2538 270.0431 211.6528 -0.5992 266.7530 267.3521 270.1268 212.4705 -0.5985 266.8458 267.4443 270.1965 213.2780 -0.5984 266.9264 267.5248 270.2656 214.0650 -0.5986 266.9844 267.5830 270.3218 214.8828 -0.6021 267.0714 267.6736 270.3740 215.6595 -0.6071 267.1523 267.7594 270.4270 216.5080 -0.6059 267.2460 267.8519 270.4902 217.2745 -0.6081 267.3234 267.9315 270.5438 218.1018 -0.6085 267.3991 268.0076 270.5926 218.8988 -0.6119 267.4881 268.1000 270.6424 219.6960 -0.6117 267.5798 268.1916 270.6732 220.5138 -0.6129 267.6724 268.2853 270.7092 221.2905 -0.6138 267.7358 268.3497 270.7725 222.1390 -0.6164 267.8129 268.4293 270.8373 222.9055 -0.6132 267.8768 268.4900 270.8799 223.7325 -0.6144 267.9819 268.5963 270.9513 224.5298 -0.6177 268.0752 268.6929 271.0301 225.3270 -0.6157 268.1784 268.7941 271.1244 226.1448 -0.6186 268.2795 268.8980 271.2253 226.9215 -0.6167 268.3643 268.9810 271.3267 227.7700 -0.6132 268.4349 269.0481 271.4432 228.5365 -0.6125 268.5047 269.1172 271.5572 229.3645 -0.6110 268.5865 269.1975 271.6711 230.1608 -0.6123 268.6659 269.2781 271.7967 230.9580 -0.6116 268.7652 269.3768 271.9099 231.7758 -0.6087 268.8633 269.4720 272.0285 232.5525 -0.6062 268.9370 269.5432 272.1525 233.4010 -0.6064 269.0189 269.6253 272.2754 234.1675 -0.6050 269.1031 269.7082 272.4139 234.9948 -0.6054 269.1869 269.7924 272.5668 235.7918 -0.6021 269.2448 269.8469 272.7362 236.5890 -0.6041 269.3346 269.9387 272.9075 237.4068 -0.6117 269.4185 270.0302 273.0575 238.1835 -0.6137 269.4907 270.1044 273.2234 239.0320 -0.6136 269.5849 270.1985 273.4070 239.8088 -0.6112 269.6701 270.2813 273.5514 240.6258 -0.6118 269.7772 270.3889 273.6899 241.4330 -0.6148 269.8688 270.4837 273.8578 242.2200 -0.6165 269.9813 270.5977 274.0195 243.0480 -0.6167 270.0833 270.7000 274.1602 243.8145 -0.6150 270.1716 270.7866 274.2919 244.6425 -0.6124 270.2584 270.8708 274.4374 245.4393 -0.6118 270.3248 270.9367 274.5673 246.2565 -0.6154 270.4101 271.0255 274.6932 247.0333 -0.6173 270.4977 271.1149 274.8125 247.8510 -0.6188 270.5991 271.2179 274.9151 248.6585 -0.6180 270.6953 271.3133 275.0357 249.4455 -0.6181 270.7804 271.3985 275.1456 250.2833 -0.6196 270.8830 271.5026 275.2375 251.0390 -0.6175 270.9484 271.5659 275.3080 251.8978 -0.6153 271.0388 271.6540 275.3959 252.6643 -0.6163 271.1058 271.7221 275.4818 253.4923 -0.6192 271.2402 271.8594 275.5551 254.2895 -0.6232 271.3196 271.9428 275.6240 255.0765 -0.6200 271.4021 272.0221 275.6981 255.9148 -0.6170 271.4928 272.1098 275.7556 256.6710 -0.6170 271.5810 272.1981 275.7991 257.5298 -0.6195 271.6878 272.3072 275.8620 258.2955 -0.6207 271.7819 272.4026 275.8930 259.1233 -0.6222 271.8593 272.4815 275.9456 259.9205 -0.6215 271.9253 272.5468 275.9952 260.7075 -0.6257 272.0024 272.6281 276.0553 261.5048 -0.6284 272.0714 272.6998 276.1194 262.2918 -0.6275 272.1201 272.7476 276.2005 263.1198 -0.6292 272.1736 272.8028 276.2724 263.8863 -0.6284 272.2823 272.9107 276.3518 264.7340 -0.6246 272.4032 273.0278 276.4463 265.5003 -0.6247 272.5102 273.1349 276.5260 266.3180 -0.6211 272.6078 273.2288 276.6188 267.1153 -0.6176 272.7477 273.3652 276.7126 267.9125 -0.6164 272.8222 273.4385 276.7889 268.7405 -0.6140 272.9109 273.5249 276.8979 269.4968 -0.6151 272.9771 273.5921 277.0183 270.3240 -0.6153 273.0836 273.6989 277.1375 271.0903 -0.6189 273.1625 273.7813 277.2381 271.9490 -0.6173 273.2700 273.8872 277.3620 272.7053 -0.6199 273.3435 273.9634 277.4769 273.5435 -0.6217 273.4477 274.0694 277.6103 274.3305 -0.6213 273.5368 274.1582 277.7545 275.1278 -0.6191 273.6436 274.2627 277.8880 275.9250 -0.6235 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