DTA measure 1DTA1_PB3 Date: 202623:1256 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.04 s Mass = 1173.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1485 0.5995 235.3983 234.7988 274.9315 1.9655 0.5995 235.6888 235.0892 274.9611 2.7723 0.5980 235.9780 235.3800 274.9603 3.5693 0.5956 236.2536 235.6580 274.9112 4.3963 0.5967 236.5280 235.9313 274.8875 5.1520 0.5954 236.7913 236.1959 274.8744 6.0205 0.5935 237.0654 236.4719 274.8147 6.7860 0.5950 237.2985 236.7034 274.7542 7.6133 0.5948 237.5635 236.9687 274.6977 8.4000 0.5927 237.8187 237.2260 274.5994 9.2065 0.5935 238.0933 237.4999 274.5256 10.0238 0.5943 238.3546 237.7603 274.4638 10.7898 0.5920 238.6467 238.0547 274.4207 11.6170 0.5917 238.9176 238.3259 274.3585 12.3728 0.5905 239.1452 238.5547 274.2850 13.2205 0.5908 239.3975 238.8067 274.2378 13.9965 0.5885 239.6314 239.0429 274.2147 14.8138 0.5909 239.9422 239.3513 274.2175 15.6103 0.5930 240.2117 239.6187 274.2188 16.4070 0.5916 240.4751 239.8835 274.2474 17.2038 0.5933 240.7230 240.1298 274.3176 18.0000 0.5965 241.0101 240.4136 274.4178 18.8173 0.5987 241.2845 240.6858 274.5796 19.5935 0.6012 241.5253 240.9241 274.6916 20.4413 0.5995 241.7546 241.1551 274.8924 21.2073 0.5963 242.0031 241.4068 275.0993 22.0345 0.5958 242.2693 241.6735 275.3361 22.8313 0.5934 242.5082 241.9148 275.6071 23.6280 0.5900 242.7668 242.1768 275.8667 24.4448 0.5903 243.0227 242.4324 276.1515 25.2213 0.5924 243.2831 242.6907 276.4568 26.0485 0.5924 243.5461 242.9537 276.7715 26.8143 0.5905 243.7704 243.1799 277.0961 27.6625 0.5854 244.0546 243.4692 277.4767 28.4383 0.5830 244.2878 243.7048 277.8443 29.2555 0.5823 244.5451 243.9628 278.1850 30.0523 0.5796 244.8035 244.2239 278.5156 30.8488 0.5756 245.0817 244.5060 278.8417 31.6763 0.5735 245.3264 244.7529 279.1521 32.4420 0.5660 245.5499 244.9839 279.4344 33.2900 0.5581 245.8124 245.2543 279.7369 34.0663 0.5527 246.0369 245.4842 279.9676 34.8933 0.5507 246.2844 245.7336 280.1929 35.6903 0.5495 246.5382 245.9887 280.4206 36.4765 0.5473 246.7757 246.2284 280.5943 37.3140 0.5437 247.0378 246.4940 280.7400 38.0803 0.5414 247.2988 246.7573 280.8881 38.9073 0.5359 247.5426 247.0067 281.0060 39.6633 0.5318 247.7940 247.2623 281.1122 40.5315 0.5221 248.0413 247.5191 281.1979 41.2973 0.5165 248.3086 247.7921 281.2530 42.1250 0.5101 248.5397 248.0296 281.3021 42.9110 0.5048 248.7560 248.2512 281.3296 43.7078 0.5016 248.9870 248.4854 281.3152 44.5353 0.4952 249.2290 248.7338 281.2896 45.2908 0.4907 249.4560 248.9653 281.2766 46.1183 0.4901 249.7083 249.2181 281.2392 46.8840 0.4902 249.9458 249.4556 281.1693 47.7318 0.4873 250.1666 249.6793 281.1283 48.5080 0.4811 250.3983 249.9172 281.0817 49.3250 0.4768 250.6407 250.1639 281.0413 50.1215 0.4663 250.8861 250.4198 280.9968 50.9183 0.4613 251.1422 250.6810 280.9619 51.7455 0.4568 251.3756 250.9188 280.9536 52.5115 0.4541 251.5860 251.1319 280.9646 53.3595 0.4507 251.8244 251.3737 280.9616 54.1353 0.4483 252.0378 251.5894 280.9648 54.9525 0.4426 252.2695 251.8269 280.9814 55.7493 0.4406 252.4856 252.0450 281.0237 56.5455 0.4417 252.6983 252.2566 281.0906 57.3730 0.4436 252.9432 252.4997 281.2144 58.1390 0.4386 253.1814 252.7428 281.3320 58.9868 0.4393 253.4081 252.9688 281.4580 59.7630 0.4345 253.6277 253.1932 281.6403 60.5800 0.4295 253.8664 253.4369 281.8159 61.3768 0.4267 254.1066 253.6798 282.0281 62.1735 0.4191 254.3115 253.8924 282.2661 63.0005 0.4130 254.5256 254.1126 282.5189 63.7665 0.4120 254.7471 254.3350 282.7815 64.6248 0.4092 255.0168 254.6076 283.0991 65.3905 0.4027 255.2315 254.8287 283.3683 66.2180 0.3959 255.4387 255.0428 283.6935 67.0145 0.3929 255.6558 255.2628 284.0274 67.8110 0.3878 255.8649 255.4771 284.3656 68.6080 0.3819 256.0759 255.6940 284.6718 69.4043 0.3762 256.2860 255.9098 284.9966 70.2628 0.3670 256.5398 256.1728 285.3329 71.0183 0.3602 256.7447 256.3846 285.5969 71.8558 0.3534 256.9743 256.6209 285.9071 72.6425 0.3448 257.1755 256.8307 286.1634 73.4490 0.3393 257.3736 257.0343 286.3632 74.2665 0.3319 257.6085 257.2766 286.5696 75.0425 0.3306 257.8347 257.5041 286.7431 75.8595 0.3253 258.0504 257.7251 286.8855 76.6255 0.3161 258.2647 257.9486 287.0413 77.4835 0.3080 258.5205 258.2125 287.1968 78.2390 0.3010 258.7231 258.4221 287.3118 79.0665 0.2957 258.9365 258.6408 287.4013 79.8630 0.2886 259.1590 258.8704 287.4579 80.6595 0.2844 259.3900 259.1056 287.5193 81.4768 0.2819 259.5949 259.3130 287.6063 82.2425 0.2801 259.7860 259.5059 287.6582 83.1005 0.2726 260.0220 259.7494 287.6829 83.8668 0.2682 260.2592 259.9910 287.6922 84.6835 0.2610 260.4806 260.2196 287.7089 85.4905 0.2556 260.6887 260.4331 287.6943 86.2770 0.2497 260.9290 260.6793 287.6677 87.1040 0.2467 261.1798 260.9331 287.6361 87.8700 0.2410 261.3841 261.1431 287.6065 88.7283 0.2328 261.6249 261.3922 287.5689 89.4940 0.2281 261.8219 261.5937 287.5462 90.3113 0.2230 262.0228 261.7998 287.5296 91.1180 0.2186 262.2428 262.0243 287.5194 91.9148 0.2134 262.4559 262.2425 287.5098 92.7423 0.2051 262.7030 262.4979 287.5016 93.4975 0.2009 262.9023 262.7014 287.5444 94.3663 0.1938 263.1475 262.9537 287.5886 95.1218 0.1915 263.3383 263.1468 287.6719 95.9490 0.1876 263.5364 263.3488 287.7682 96.7460 0.1870 263.7540 263.5670 287.8679 97.5423 0.1849 263.9612 263.7763 287.9818 98.3700 0.1812 264.1757 263.9945 288.1369 99.1255 0.1767 264.3463 264.1697 288.3092 99.9938 0.1749 264.5742 264.3993 288.4817 100.7598 0.1702 264.7570 264.5868 288.6730 101.5870 0.1661 264.9557 264.7896 288.9323 102.3735 0.1624 265.1439 264.9815 289.1842 103.1805 0.1500 265.3281 265.1781 289.4485 104.0078 0.1416 265.5427 265.4011 289.7037 104.7738 0.1354 265.7570 265.6216 289.9799 105.6215 0.1282 265.9833 265.8551 290.2985 106.3975 0.1231 266.1727 266.0496 290.5843 107.2148 0.1175 266.3858 266.2684 290.8799 108.0113 0.1139 266.5824 266.4685 291.1777 108.8080 0.1095 266.7664 266.6569 291.5033 109.6253 0.1021 266.9912 266.8891 291.8011 110.3908 0.0974 267.1932 267.0958 292.0686 111.2185 0.0922 267.4093 267.3171 292.3650 111.9843 0.0928 267.6277 267.5350 292.6115 112.8320 0.0837 267.8399 267.7562 292.8508 113.5980 0.0758 268.0347 267.9589 293.0616 114.4253 0.0706 268.2460 268.1755 293.2441 115.2220 0.0618 268.4384 268.3766 293.4380 116.0085 0.0536 268.6297 268.5761 293.6147 116.8458 0.0405 268.8458 268.8053 293.7524 117.6015 0.0315 269.0195 268.9880 293.8512 118.4598 0.0257 269.2442 269.2185 293.9372 119.1948 0.0198 269.4210 269.4012 293.9868 120.0533 0.0083 269.6282 269.6199 294.0467 120.8188 0.0033 269.7950 269.7917 294.0420 121.6360 -0.0052 269.9838 269.9890 294.0626 122.4430 -0.0101 270.1895 270.1996 294.0559 123.2290 -0.0133 270.3885 270.4018 294.0659 124.0568 -0.0156 270.6201 270.6358 294.0664 124.8225 -0.0193 270.8075 270.8269 294.0536 125.6908 -0.0251 270.9859 271.0110 294.0261 126.4465 -0.0310 271.1557 271.1867 293.9865 127.2738 -0.0408 271.3788 271.4196 293.9455 128.0700 -0.0448 271.5501 271.5948 293.9369 128.8670 -0.0515 271.7349 271.7864 293.9206 129.6943 -0.0570 271.9684 272.0254 293.9391 130.4600 -0.0661 272.1474 272.2136 293.9494 131.2875 -0.0698 272.3572 272.4270 293.9692 132.0533 -0.0725 272.5525 272.6249 293.9847 132.9113 -0.0773 272.7375 272.8149 294.0555 133.6673 -0.0848 272.9235 273.0084 294.1269 134.5045 -0.0908 273.1345 273.2254 294.1995 135.3013 -0.0959 273.3318 273.4277 294.3106 136.0980 -0.0981 273.5439 273.6420 294.4330 136.9148 -0.1036 273.7598 273.8634 294.5856 137.6910 -0.1108 273.9523 274.0630 294.7420 138.5390 -0.1182 274.1460 274.2642 294.9447 139.3045 -0.1246 274.3185 274.4431 295.1396 140.1320 -0.1290 274.4990 274.6281 295.3994 140.8980 -0.1318 274.7035 274.8353 295.6256 141.7148 -0.1348 274.9360 275.0708 295.8879 142.5115 -0.1393 275.1272 275.2665 296.1492 143.3083 -0.1466 275.3119 275.4585 296.4100 144.1353 -0.1539 275.5096 275.6636 296.7274 144.8910 -0.1608 275.6885 275.8494 296.9921 145.7595 -0.1696 275.9019 276.0714 297.2879 146.5148 -0.1754 276.0916 276.2670 297.5856 147.3425 -0.1835 276.2983 276.4818 297.9038 148.1083 -0.1892 276.4888 276.6780 298.1528 148.9353 -0.1943 276.6796 276.8739 298.4328 149.7320 -0.2009 276.8713 277.0722 298.6789 150.5185 -0.2084 277.0482 277.2566 298.9006 151.3558 -0.2152 277.2579 277.4731 299.1203 152.1115 -0.2206 277.4511 277.6717 299.3234 152.9698 -0.2234 277.6479 277.8713 299.5111 153.7353 -0.2238 277.8000 278.0239 299.6565 154.5730 -0.2297 278.0140 278.2438 299.8046 155.3595 -0.2358 278.2057 278.4415 299.9098 156.1560 -0.2401 278.3898 278.6299 300.0291 156.9835 -0.2441 278.5857 278.8297 300.1291 157.7493 -0.2510 278.7696 279.0206 300.2056 158.6075 -0.2537 278.9532 279.2069 300.2805 159.3735 -0.2590 279.1302 279.3892 300.3292 160.2005 -0.2653 279.3125 279.5778 300.3855 160.9973 -0.2739 279.4819 279.7558 300.4043 161.7940 -0.2792 279.6779 279.9571 300.4116 162.6108 -0.2848 279.8819 280.1668 300.3924 163.3873 -0.2912 280.0703 280.3615 300.3939 164.2248 -0.2983 280.2793 280.5776 300.3919 164.9803 -0.3065 280.4525 280.7590 300.3925 165.8388 -0.3145 280.6842 280.9988 300.3874 166.6043 -0.3206 280.8548 281.1754 300.3922 167.4420 -0.3217 281.0355 281.3572 300.3930 168.2285 -0.3245 281.2371 281.5616 300.3892 169.0248 -0.3309 281.4255 281.7564 300.4028 169.8525 -0.3351 281.6200 281.9551 300.4466 170.6285 -0.3398 281.8066 282.1464 300.4814 171.4765 -0.3438 281.9878 282.3316 300.5430 172.2323 -0.3462 282.1604 282.5066 300.6123 173.0595 -0.3499 282.3645 282.7143 300.7045 173.8460 -0.3568 282.5491 282.9060 300.8394 174.6425 -0.3661 282.7267 283.0928 300.9557 175.4698 -0.3660 282.9011 283.2672 301.1041 176.2360 -0.3673 283.0553 283.4227 301.2681 177.0835 -0.3691 283.2354 283.6045 301.4673 177.8495 -0.3777 283.3978 283.7754 301.6391 178.6770 -0.3865 283.5598 283.9462 301.8662 179.4630 -0.3906 283.7324 284.1229 302.0931 180.2700 -0.3983 283.9164 284.3147 302.3248 181.0873 -0.4111 284.1185 284.5296 302.5706 181.8530 -0.4125 284.2907 284.7033 302.8227 182.7113 -0.4169 284.4665 284.8834 303.1107 183.4770 -0.4200 284.6413 285.0613 303.3544 184.3043 -0.4234 284.8325 285.2559 303.6350 185.0908 -0.4296 285.0438 285.4734 303.9037 185.8975 -0.4371 285.2227 285.6598 304.1678 186.7148 -0.4426 285.4045 285.8471 304.4317 187.4808 -0.4463 285.5960 286.0422 304.6794 188.3388 -0.4508 285.8031 286.2539 304.9207 189.1150 -0.4569 285.9747 286.4316 305.1477 189.9320 -0.4641 286.1611 286.6252 305.3741 190.7285 -0.4694 286.3519 286.8213 305.5742 191.5255 -0.4755 286.5271 287.0025 305.7392 192.3525 -0.4828 286.7108 287.1935 305.9088 193.1185 -0.4880 286.8496 287.3376 306.0570 193.9665 -0.4952 287.0391 287.5343 306.1784 194.7425 -0.5010 287.1841 287.6851 306.3015 195.5598 -0.5098 287.3761 287.8859 306.4185 196.3665 -0.5165 287.5690 288.0855 306.5104 197.1530 -0.5250 287.7395 288.2645 306.5603 197.9908 -0.5299 287.8997 288.4297 306.6310 198.7463 -0.5363 288.0655 288.6018 306.6885 199.6148 -0.5440 288.2226 288.7666 306.7356 200.3703 -0.5461 288.4037 288.9498 306.7700 201.2078 -0.5517 288.5960 289.1477 306.7896 201.9945 -0.5577 288.7694 289.3270 306.7892 202.8010 -0.5643 288.9579 289.5222 306.7899 203.6183 -0.5679 289.1491 289.7170 306.7888 204.3843 -0.5756 289.3036 289.8792 306.7876 205.2423 -0.5827 289.5063 290.0890 306.8070 205.9673 -0.5890 289.6735 290.2625 306.7870 206.8253 -0.5915 289.8103 290.4017 306.7979 207.5910 -0.5952 289.9805 290.5757 306.8297 208.4085 -0.5998 290.1662 290.7660 306.8910 209.2048 -0.6037 290.3456 290.9493 306.9573 210.0015 -0.6061 290.5378 291.1439 307.0330 210.8188 -0.6084 290.7207 291.3292 307.0962 211.5948 -0.6118 290.8884 291.5002 307.1711 212.4428 -0.6172 291.0935 291.7107 307.3022 213.2085 -0.6203 291.2709 291.8912 307.4112 214.0358 -0.6253 291.4709 292.0962 307.5733 214.8328 -0.6293 291.6487 292.2781 307.7447 215.6290 -0.6373 291.8216 292.4589 307.9158 216.4463 -0.6392 291.9869 292.6261 308.1281 217.2225 -0.6444 292.1692 292.8136 308.3486 218.0700 -0.6504 292.3526 293.0030 308.6082 218.8363 -0.6540 292.5120 293.1660 308.8260 219.6635 -0.6566 292.6898 293.3463 309.0886 220.4600 -0.6585 292.8402 293.4987 309.3286 221.2568 -0.6614 293.0247 293.6861 309.5678 222.0738 -0.6656 293.1922 293.8578 309.8023 222.8500 -0.6699 293.3671 294.0370 310.0719 223.6980 -0.6769 293.5564 294.2332 310.3526 224.4635 -0.6817 293.7167 294.3983 310.5583 225.2913 -0.6854 293.8862 294.5716 310.8326 226.0878 -0.6896 294.0557 294.7453 311.0884 226.8843 -0.6958 294.2237 294.9195 311.3097 227.7015 -0.7019 294.3808 295.0826 311.5400 228.4775 -0.7086 294.5333 295.2419 311.7444 229.3255 -0.7192 294.7211 295.4403 311.9633 230.1018 -0.7250 294.8767 295.6017 312.1409 230.9185 -0.7284 295.0404 295.7687 312.2894 231.7255 -0.7331 295.2223 295.9555 312.4438 232.5120 -0.7347 295.3904 296.1251 312.5834 233.3493 -0.7369 295.5820 296.3190 312.6924 234.1050 -0.7442 295.7553 296.4995 312.8032 234.9735 -0.7500 295.9769 296.7269 312.8796 235.6980 -0.7508 296.1752 296.9260 312.9296 236.5563 -0.7585 296.3516 297.1100 312.9567 237.3223 -0.7628 296.5201 297.2829 312.9666 238.1393 -0.7658 296.6813 297.4471 313.0090 238.9360 -0.7702 296.8369 297.6071 313.0358 239.7325 -0.7787 296.9908 297.7695 313.0593 240.5293 -0.7819 297.1552 297.9371 313.0652 241.3260 -0.7899 297.3132 298.1031 313.1030 242.1428 -0.7954 297.5118 298.3072 313.1212 242.9190 -0.7982 297.6832 298.4813 313.1243 243.7670 -0.7996 297.8628 298.6624 313.0978 244.5328 -0.8042 298.0169 298.8212 313.1065 245.3603 -0.8109 298.1591 298.9700 313.1221 246.1260 -0.8185 298.3318 299.1503 313.1407 246.9535 -0.8244 298.5041 299.3285 313.2118 247.7503 -0.8286 298.6474 299.4759 313.2704 248.5468 -0.8335 298.8261 299.6596 313.3546 249.3743 -0.8380 299.0170 299.8549 313.4309 250.1400 -0.8397 299.1713 300.0111 313.5111 250.9878 -0.8405 299.3533 300.1938 313.6444 251.7643 -0.8461 299.5180 300.3641 313.8086 252.5810 -0.8524 299.6943 300.5466 314.0049 253.3470 -0.8546 299.8659 300.7205 314.1665 254.1745 -0.8607 300.0502 300.9109 314.3651 254.9810 -0.8639 300.2360 301.0999 314.5655 255.7675 -0.8689 300.3693 301.2382 314.7443 256.5950 -0.8753 300.5219 301.3972 314.9786 257.3608 -0.8756 300.6618 301.5374 315.2150 258.2293 -0.8798 300.8629 301.7427 315.5205 258.9848 -0.8851 301.0405 301.9256 315.7819 259.8120 -0.8900 301.2138 302.1038 316.0493 260.6088 -0.8946 301.4175 302.3121 316.3288 261.4155 -0.8977 301.5969 302.4946 316.5892 262.2018 -0.9002 301.7317 302.6319 316.8438 262.9985 -0.9065 301.9093 302.8158 317.0838 263.8565 -0.9078 302.1200 303.0278 317.3505 264.6020 -0.9136 302.2661 303.1797 317.5531 265.4500 -0.9191 302.4208 303.3399 317.7485 266.2155 -0.9284 302.5740 303.5025 317.9410 267.0433 -0.9337 302.7305 303.6641 318.1362 267.8398 -0.9335 302.9041 303.8376 318.3192 268.6363 -0.9388 303.0681 304.0069 318.4450 269.4535 -0.9456 303.2427 304.1883 318.5911 270.2193 -0.9508 303.3887 304.3395 318.7088 271.0775 -0.9540 303.5446 304.4986 318.8427 271.8333 -0.9567 303.7126 304.6693 318.9183 272.6603 -0.9616 303.8687 304.8303 319.0078 273.4570 -0.9667 304.0330 304.9997 319.0856 274.2435 -0.9709 304.2083 305.1792 319.1405 275.0503 -0.9753 304.4022 305.3775 319.1777 275.8370 -0.9819 304.5800 305.5619 319.2180 276.6640 -0.9857 304.7413 305.7270 319.2302 277.4300 -0.9927 304.8902 305.8829 319.2543 278.2780 -0.9999 305.0440 306.0438 319.2581 279.0435 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