DTA measure 1gyors Date: 2026224:1053 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.68 s Mass = 1367.600 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2605 -4.4360 182.0990 186.5350 246.9525 2.1193 -4.4268 182.3769 186.8037 246.8741 2.8858 -4.4228 182.6319 187.0547 246.8473 3.7028 -4.4106 182.9049 187.3155 246.7930 4.5100 -4.3975 183.1886 187.5861 246.7139 5.2970 -4.3883 183.4544 187.8427 246.6508 6.1240 -4.3808 183.7324 188.1132 246.5694 6.8905 -4.3693 184.0114 188.3807 246.5158 7.7493 -4.3521 184.2884 188.6405 246.4477 8.5148 -4.3411 184.5260 188.8671 246.3709 9.3325 -4.3294 184.7553 189.0847 246.2804 10.1400 -4.3231 184.9958 189.3189 246.2049 10.9260 -4.3144 185.2526 189.5670 246.1383 11.7540 -4.3024 185.5077 189.8102 246.0881 12.5205 -4.2904 185.7280 190.0184 246.0645 13.3785 -4.2734 186.0041 190.2776 246.0172 14.1448 -4.2656 186.2432 190.5087 245.9774 14.9625 -4.2578 186.5227 190.7805 245.9419 15.7698 -4.2429 186.8077 191.0506 245.8918 16.5560 -4.2316 187.0616 191.2932 245.8141 17.3943 -4.2212 187.2829 191.5041 245.7826 18.1500 -4.2061 187.5161 191.7222 245.7570 19.0185 -4.1955 187.7751 191.9706 245.7677 19.7748 -4.1804 188.0042 192.1846 245.7217 20.5920 -4.1695 188.2590 192.4285 245.7150 21.3888 -4.1587 188.4744 192.6331 245.7146 22.1860 -4.1459 188.7203 192.8662 245.7183 23.0033 -4.1323 188.9852 193.1175 245.7099 23.7693 -4.1200 189.2205 193.3404 245.7318 24.6280 -4.1020 189.4662 193.5683 245.7280 25.3843 -4.0956 189.7143 193.8099 245.7221 26.2113 -4.0832 189.9413 194.0245 245.7608 26.9778 -4.0737 190.1604 194.2342 245.8014 27.8058 -4.0604 190.4067 194.4670 245.7886 28.6020 -4.0498 190.6567 194.7065 245.8555 29.3993 -4.0351 190.8771 194.9122 245.9209 30.2270 -4.0261 191.1132 195.1393 245.9897 30.9825 -4.0131 191.3430 195.3562 246.0268 31.8515 -4.0030 191.6334 195.6365 246.0915 32.6073 -3.9892 191.8654 195.8546 246.1766 33.4348 -3.9770 192.1107 196.0877 246.2860 34.2320 -3.9631 192.3228 196.2859 246.3846 35.0288 -3.9543 192.5537 196.5080 246.5209 35.8563 -3.9366 192.7598 196.6963 246.6346 36.6125 -3.9226 192.9675 196.8901 246.7429 37.4813 -3.9095 193.2352 197.1447 246.8531 38.2368 -3.8935 193.4469 197.3404 246.9607 39.0648 -3.8813 193.6893 197.5706 247.0631 39.8618 -3.8728 193.9301 197.8029 247.1712 40.6583 -3.8638 194.1869 198.0507 247.2988 41.4863 -3.8544 194.3970 198.2514 247.4434 42.2425 -3.8456 194.6211 198.4667 247.5804 43.1108 -3.8322 194.8578 198.6900 247.7139 43.8668 -3.8196 195.0985 198.9181 247.8490 44.6948 -3.8057 195.3506 199.1563 247.9791 45.4918 -3.7920 195.5569 199.3489 248.0861 46.2985 -3.7736 195.7788 199.5524 248.2197 47.1163 -3.7656 196.0185 199.7841 248.3973 47.8825 -3.7537 196.2217 199.9755 248.5635 48.7405 -3.7393 196.4465 200.1859 248.7351 49.5070 -3.7292 196.6624 200.3916 248.9307 50.3350 -3.7220 196.8549 200.5768 249.1215 51.1213 -3.7160 197.0806 200.7966 249.3238 51.9285 -3.7073 197.2774 200.9847 249.5203 52.7463 -3.7006 197.4924 201.1930 249.7050 53.5020 -3.6902 197.7040 201.3942 249.8496 54.3603 -3.6749 197.9472 201.6221 250.0727 55.1165 -3.6648 198.1362 201.8010 250.2300 55.9440 -3.6582 198.3547 202.0129 250.4242 56.7408 -3.6445 198.5738 202.2184 250.6143 57.5380 -3.6266 198.8304 202.4570 250.8379 58.3243 -3.6206 199.0475 202.6681 250.9772 59.1213 -3.6129 199.2317 202.8446 251.1830 59.9493 -3.6077 199.4968 203.1045 251.4005 60.7048 -3.6054 199.6957 203.3010 251.5714 61.5735 -3.5939 199.9400 203.5339 251.7441 62.3298 -3.5858 200.1401 203.7259 251.9229 63.1568 -3.5754 200.3494 203.9248 252.1594 63.9540 -3.5678 200.5541 204.1219 252.3705 64.7513 -3.5600 200.7863 204.3463 252.5898 65.5783 -3.5557 201.0310 204.5867 252.8249 66.3345 -3.5490 201.2259 204.7750 252.9953 67.2035 -3.5426 201.4446 204.9872 253.1828 67.9588 -3.5379 201.6537 205.1916 253.3404 68.7868 -3.5291 201.8595 205.3886 253.5376 69.5840 -3.5209 202.0431 205.5640 253.7514 70.3805 -3.5105 202.2390 205.7495 253.9610 71.2083 -3.5064 202.4806 205.9870 254.1379 71.9645 -3.4977 202.6738 206.1716 254.3191 72.8333 -3.4853 202.8892 206.3745 254.5267 73.5888 -3.4791 203.0928 206.5720 254.7087 74.4168 -3.4714 203.3392 206.8106 254.9180 75.2138 -3.4591 203.5680 207.0271 255.0481 76.0103 -3.4540 203.7596 207.2136 255.2205 76.8383 -3.4488 203.9576 207.4065 255.4177 77.5943 -3.4438 204.1407 207.5845 255.5830 78.4625 -3.4377 204.3794 207.8171 255.7972 79.2290 -3.4330 204.5670 208.0000 255.9675 80.0570 -3.4260 204.8004 208.2264 256.1882 80.8123 -3.4194 205.0176 208.4370 256.3648 81.6505 -3.4127 205.2514 208.6640 256.5023 82.4375 -3.4073 205.4557 208.8630 256.6439 83.2338 -3.4045 205.6670 209.0714 256.8043 84.0618 -3.4007 205.8752 209.2759 256.9923 84.8180 -3.3962 206.0758 209.4720 257.1732 85.6658 -3.3898 206.3091 209.6989 257.3257 86.4423 -3.3817 206.5209 209.9026 257.4569 87.2600 -3.3729 206.7462 210.1191 257.5845 88.0465 -3.3684 206.9422 210.3106 257.7213 88.8535 -3.3625 207.1341 210.4966 257.8702 89.6405 -3.3585 207.3020 210.6605 258.0479 90.4370 -3.3513 207.5039 210.8553 258.1645 91.2648 -3.3497 207.6851 211.0348 258.3025 92.0210 -3.3449 207.8536 211.1984 258.4690 92.8788 -3.3377 208.0787 211.4164 258.6229 93.6453 -3.3321 208.2798 211.6119 258.7503 94.4733 -3.3279 208.5006 211.8285 258.8932 95.2695 -3.3186 208.6893 212.0079 259.0077 96.0565 -3.3131 208.8704 212.1836 259.1530 96.8945 -3.3080 209.1033 212.4113 259.3098 97.6500 -3.2981 209.2900 212.5881 259.4305 98.4780 -3.2948 209.5143 212.8091 259.5635 99.2443 -3.2906 209.6833 212.9739 259.6983 100.1023 -3.2856 209.8851 213.1707 259.8339 100.8688 -3.2855 210.0781 213.3636 259.9636 101.6865 -3.2853 210.2654 213.5508 260.1435 102.4930 -3.2796 210.4680 213.7475 260.2977 103.2903 -3.2699 210.6669 213.9368 260.3988 104.1183 -3.2630 210.8446 214.1076 260.5434 104.8735 -3.2598 211.0656 214.3254 260.6507 105.7425 -3.2610 211.2993 214.5603 260.7646 106.4988 -3.2579 211.4761 214.7340 260.8607 107.3258 -3.2530 211.6446 214.8977 260.9611 108.1230 -3.2444 211.8499 215.0943 261.0335 108.9305 -3.2398 212.0420 215.2819 261.1512 109.7165 -3.2365 212.1977 215.4343 261.2340 110.5138 -3.2287 212.3682 215.5969 261.2839 111.3418 -3.2253 212.5861 215.8115 261.3807 112.1078 -3.2211 212.7902 216.0113 261.5012 112.9660 -3.2134 212.9924 216.2058 261.6134 113.7325 -3.2058 213.1809 216.3867 261.7062 114.5603 -3.2008 213.3653 216.5662 261.8218 115.3568 -3.1971 213.5641 216.7612 261.9246 116.1540 -3.1903 213.7576 216.9479 262.0158 116.9715 -3.1871 213.9471 217.1342 262.1473 117.7373 -3.1808 214.1305 217.3113 262.2690 118.5858 -3.1743 214.3629 217.5372 262.3976 119.3520 -3.1730 214.5262 217.6992 262.5141 120.1690 -3.1738 214.7013 217.8750 262.6288 120.9663 -3.1680 214.9059 218.0739 262.7203 121.7635 -3.1628 215.0754 218.2382 262.8408 122.5803 -3.1596 215.2575 218.4171 262.9690 123.3468 -3.1586 215.4377 218.5963 263.0382 124.2055 -3.1558 215.6516 218.8074 263.1667 124.9610 -3.1490 215.8371 218.9861 263.2902 125.7888 -3.1431 216.0421 219.1852 263.3859 126.5860 -3.1398 216.1866 219.3264 263.4842 127.3830 -3.1296 216.3881 219.5177 263.5938 128.2103 -3.1247 216.5872 219.7120 263.7120 128.9665 -3.1205 216.7353 219.8557 263.8336 129.8353 -3.1180 216.9325 220.0506 263.9676 130.5908 -3.1147 217.1098 220.2245 264.0666 131.4188 -3.1053 217.3412 220.4464 264.1553 132.2160 -3.0998 217.5366 220.6364 264.2927 133.0123 -3.0949 217.7231 220.8180 264.4344 133.8403 -3.0924 217.9404 221.0327 264.5724 134.5963 -3.0894 218.1146 221.2040 264.6581 135.4645 -3.0807 218.3414 221.4221 264.7668 136.2208 -3.0796 218.5280 221.6076 264.8820 137.0485 -3.0758 218.7082 221.7840 264.9957 137.8450 -3.0719 218.9094 221.9813 265.1106 138.6525 -3.0645 219.0718 222.1362 265.2498 139.4700 -3.0643 219.2522 222.3165 265.3897 140.2358 -3.0666 219.4210 222.4876 265.5303 141.0945 -3.0606 219.6182 222.6788 265.6549 141.8610 -3.0587 219.7513 222.8100 265.7605 142.6883 -3.0556 219.9527 223.0083 265.8613 143.4853 -3.0484 220.1762 223.2246 265.9942 144.2825 -3.0413 220.3423 223.3836 266.1473 145.1100 -3.0349 220.5068 223.5417 266.2795 145.8760 -3.0285 220.6832 223.7116 266.3791 146.6938 -3.0235 220.8887 223.9122 266.4859 147.4703 -3.0202 221.0653 224.0855 266.6126 148.3180 -3.0139 221.2580 224.2719 266.7732 149.0845 -3.0092 221.4192 224.4284 266.9008 149.9125 -3.0048 221.5934 224.5982 267.0490 150.6985 -3.0039 221.7795 224.7834 267.1950 151.4855 -3.0027 221.9521 224.9548 267.3293 152.3238 -2.9978 222.1032 225.1010 267.4488 153.0790 -2.9908 222.2534 225.2441 267.5521 153.9275 -2.9905 222.4300 225.4205 267.6674 154.7038 -2.9827 222.5913 225.5740 267.8154 155.5210 -2.9761 222.7718 225.7479 267.9355 156.3183 -2.9739 222.9674 225.9414 268.0540 157.1153 -2.9762 223.1635 226.1397 268.1971 157.9425 -2.9739 223.3749 226.3488 268.3964 158.7090 -2.9679 223.5715 226.5394 268.5507 159.5573 -2.9687 223.7818 226.7505 268.6612 160.3333 -2.9653 223.9852 226.9505 268.7821 161.1510 -2.9619 224.1772 227.1391 268.9348 161.9483 -2.9578 224.3449 227.3026 269.0495 162.7445 -2.9544 224.5459 227.5003 269.1559 163.5725 -2.9455 224.7362 227.6817 269.3071 164.3388 -2.9399 224.9093 227.8492 269.4381 165.1865 -2.9355 225.0997 228.0352 269.6034 165.9633 -2.9353 225.2585 228.1937 269.7063 166.7810 -2.9350 225.4555 228.3905 269.8739 167.5773 -2.9309 225.6695 228.6004 270.0310 168.3745 -2.9322 225.8635 228.7957 270.1566 169.2025 -2.9260 226.0222 228.9482 270.2798 169.9685 -2.9247 226.1528 229.0776 270.4112 170.7960 -2.9216 226.3275 229.2491 270.5618 171.5625 -2.9174 226.4923 229.4097 270.7244 172.4310 -2.9108 226.6918 229.6026 270.9114 173.1868 -2.9073 226.8403 229.7476 271.0606 174.0148 -2.9019 227.0454 229.9473 271.2142 174.8113 -2.9010 227.2283 230.1293 271.3221 175.6083 -2.8957 227.4060 230.3017 271.4091 176.4363 -2.8934 227.5844 230.4778 271.5280 177.2025 -2.8937 227.7694 230.6631 271.6892 178.0605 -2.8939 227.9799 230.8738 271.8385 178.8270 -2.8903 228.1966 231.0869 271.9847 179.6548 -2.8865 228.3695 231.2560 272.1480 180.4410 -2.8825 228.5436 231.4262 272.3119 181.2383 -2.8784 228.7064 231.5848 272.4639 182.0253 -2.8775 228.8518 231.7293 272.6021 182.8218 -2.8728 229.0218 231.8946 272.7304 183.6495 -2.8658 229.2140 232.0798 272.8864 184.4058 -2.8607 229.3530 232.2137 273.0139 185.2638 -2.8559 229.5135 232.3694 273.1555 186.0198 -2.8565 229.6603 232.5168 273.2633 186.8478 -2.8523 229.8483 232.7006 273.4094 187.6443 -2.8535 229.9896 232.8430 273.5214 188.4413 -2.8478 230.1388 232.9866 273.6756 189.2385 -2.8446 230.3302 233.1748 273.8015 190.0248 -2.8460 230.5099 233.3560 273.9360 190.8628 -2.8488 230.6972 233.5460 274.0756 191.6190 -2.8474 230.8435 233.6909 274.2018 192.4770 -2.8453 231.0301 233.8754 274.3517 193.2433 -2.8430 231.1843 234.0273 274.5154 194.0713 -2.8410 231.3304 234.1713 274.6518 194.8370 -2.8379 231.4789 234.3168 274.7802 195.6545 -2.8387 231.6657 234.5044 274.9310 196.4620 -2.8338 231.8309 234.6647 275.1101 197.2483 -2.8263 232.0137 234.8400 275.2589 198.0760 -2.8242 232.1776 235.0018 275.4201 198.8425 -2.8287 232.3551 235.1838 275.5801 199.7110 -2.8261 232.5696 235.3957 275.6922 200.4668 -2.8231 232.7183 235.5414 275.8326 201.2948 -2.8199 232.9126 235.7324 275.9938 202.0913 -2.8166 233.0776 235.8942 276.1301 202.8883 -2.8155 233.2367 236.0522 276.2685 203.7163 -2.8141 233.4011 236.2152 276.4412 204.4725 -2.8137 233.5667 236.3805 276.5349 205.3098 -2.8151 233.7593 236.5745 276.6790 206.0968 -2.8099 233.9170 236.7269 276.8343 206.9248 -2.8090 234.1155 236.9245 276.9603 207.7210 -2.8073 234.2808 237.0881 277.1105 208.5183 -2.8018 234.4517 237.2535 277.2367 209.3463 -2.7960 234.6582 237.4542 277.3765 210.1018 -2.7998 234.7769 237.5768 277.4878 210.9705 -2.7966 234.9557 237.7523 277.6575 211.7268 -2.7954 235.1195 237.9148 277.7900 212.5545 -2.7920 235.2956 238.0876 277.8848 213.3203 -2.7891 235.4408 238.2299 278.0265 214.1380 -2.7880 235.6190 238.4070 278.1885 214.9348 -2.7861 235.7770 238.5631 278.3043 215.7315 -2.7840 235.9370 238.7210 278.4333 216.5493 -2.7795 236.1268 238.9063 278.5524 217.3150 -2.7752 236.2997 239.0749 278.6601 218.1735 -2.7703 236.5193 239.2896 278.7844 218.9298 -2.7692 236.6837 239.4529 278.9175 219.7570 -2.7712 236.8520 239.6233 279.0590 220.5540 -2.7708 237.0180 239.7888 279.2121 221.3513 -2.7712 237.1764 239.9476 279.3437 222.1783 -2.7675 237.3304 240.0979 279.4407 222.9345 -2.7623 237.4761 240.2384 279.5779 223.8035 -2.7591 237.6463 240.4054 279.7247 224.5283 -2.7616 237.8093 240.5709 279.8194 225.3868 -2.7629 237.9717 240.7345 279.9248 226.1533 -2.7609 238.1262 240.8870 280.0372 226.9808 -2.7578 238.2983 241.0561 280.1563 227.7775 -2.7540 238.4465 241.2005 280.2704 228.5645 -2.7570 238.6021 241.3590 280.3943 229.4020 -2.7590 238.8165 241.5755 280.5348 230.1683 -2.7625 238.9821 241.7446 280.6157 231.0270 -2.7575 239.1258 241.8833 280.7273 231.7825 -2.7530 239.2101 241.9631 280.8390 232.6205 -2.7486 239.3857 242.1344 280.9741 233.4075 -2.7441 239.5730 242.3171 281.0746 234.2043 -2.7370 239.7306 242.4676 281.1533 235.0318 -2.7341 239.9195 242.6536 281.2783 235.8085 -2.7370 240.0636 242.8007 281.4060 236.6565 -2.7403 240.2446 242.9849 281.5436 237.4225 -2.7400 240.4015 243.1415 281.6743 238.2505 -2.7344 240.5591 243.2934 281.7860 239.0473 -2.7341 240.7330 243.4671 281.9048 239.8440 -2.7349 240.8996 243.6345 281.9918 240.6618 -2.7320 241.0660 243.7980 282.1220 241.4380 -2.7286 241.2169 243.9455 282.2654 242.2963 -2.7302 241.4021 244.1322 282.3920 243.0628 -2.7323 241.5871 244.3194 282.4804 243.8803 -2.7330 241.7725 244.5055 282.6070 244.6870 -2.7311 241.9543 244.6854 282.7423 245.4740 -2.7268 242.1172 244.8440 282.8920 246.2915 -2.7264 242.2297 244.9560 283.0175 247.0675 -2.7289 242.3632 245.0922 283.1328 247.9160 -2.7313 242.5176 245.2489 283.2634 248.6720 -2.7391 242.7236 245.4627 283.3863 249.4993 -2.7383 242.9153 245.6536 283.5325 250.2965 -2.7390 243.0497 245.7888 283.6163 251.0833 -2.7371 243.2242 245.9613 283.7342 251.8900 -2.7278 243.4208 246.1486 283.8647 252.6770 -2.7217 243.5900 246.3117 283.9751 253.5050 -2.7177 243.7643 246.4820 284.1254 254.2708 -2.7162 243.9246 246.6407 284.2694 255.1190 -2.7141 244.0454 246.7594 284.4003 255.8855 -2.7110 244.1725 246.8835 284.5302 256.7130 -2.7105 244.3351 247.0456 284.6685 257.5098 -2.7123 244.4896 247.2019 284.7748 258.3070 -2.7092 244.6469 247.3561 284.8860 259.1245 -2.7082 244.7742 247.4825 285.0168 259.9005 -2.7046 244.9296 247.6342 285.1446 260.7490 -2.6994 245.1096 247.8089 285.2846 261.5153 -2.6973 245.2933 247.9906 285.4117 262.3425 -2.6979 245.4567 248.1545 285.5274 263.1398 -2.7033 245.6044 248.3077 285.6690 263.9370 -2.7014 245.7564 248.4578 285.8081 264.7538 -2.7020 245.9425 248.6445 285.9199 265.5305 -2.7015 246.1077 248.8091 286.0782 266.3790 -2.6967 246.2978 248.9946 286.2225 267.1448 -2.6944 246.4522 249.1466 286.3312 267.9725 -2.6926 246.6301 249.3227 286.4289 268.7698 -2.6937 246.8054 249.4991 286.5529 269.5665 -2.6905 246.9673 249.6578 286.6780 270.3838 -2.6874 247.0973 249.7847 286.7916 271.1913 -2.6826 247.2219 249.9045 286.9160 272.0188 -2.6826 247.3963 250.0789 287.0398 272.7848 -2.6819 247.5528 250.2347 287.1183 273.6230 -2.6836 247.7119 250.3955 287.2465 274.4095 -2.6830 247.8717 250.5547 287.3737 275.2165 -2.6814 248.0383 250.7197 287.5029 276.0343 -2.6790 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748.6550 -8.6050 327.1458 335.7509 364.3740 749.4210 -8.6771 327.2011 335.8782 364.5300 750.2490 -8.7585 327.2472 336.0058 364.6843 751.0358 -8.8323 327.3128 336.1451 364.8445 751.8425 -8.9067 327.3638 336.2706 364.9868 752.6603 -8.9815 327.4314 336.4128 365.1145 753.4268 -9.0552 327.5170 336.5722 365.2383 754.2848 -9.1424 327.5497 336.6921 365.3940 755.0510 -9.2198 327.6271 336.8470 365.5470 755.8790 -9.2984 327.6884 336.9868 365.7272 756.6655 -9.3743 327.7351 337.1094 365.8670 757.4725 -9.4521 327.8009 337.2530 366.0095 758.2903 -9.5308 327.8707 337.4015 366.2141 759.0563 -9.6002 327.9313 337.5315 366.3568 759.9145 -9.6777 327.9555 337.6333 366.4898 760.6810 -9.7520 327.9951 337.7472 366.6356 761.5088 -9.8341 328.0341 337.8682 366.7792 762.2950 -9.9080 328.1080 338.0161 366.8824 763.0923 -9.9814 328.1687 338.1501 366.9938 763.9093 -10.0601 328.2390 338.2991 367.1294 764.6755 -10.1340 328.3116 338.4456 367.2745 765.5343 -10.2161 328.3631 338.5793 367.4288 766.2903 -10.2878 328.4239 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