DTA measure 1lassu Date: 2026224:1153 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.22 s Mass = 1367.600 mg data_number = 1581 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2205 -1.8359 213.0284 214.8643 248.3968 1.9870 -1.8413 213.1521 214.9934 248.3410 2.8355 -1.8435 213.2934 215.1370 248.2707 3.6123 -1.8403 213.3941 215.2344 248.2336 4.4300 -1.8410 213.4925 215.3334 248.1813 5.2170 -1.8388 213.6123 215.4511 248.1331 6.0143 -1.8364 213.7459 215.5823 248.0721 6.8423 -1.8347 213.8459 215.6806 248.0471 7.5985 -1.8401 213.9809 215.8210 248.0225 8.4573 -1.8399 214.0859 215.9258 247.9924 9.2238 -1.8409 214.1985 216.0394 247.9365 10.0420 -1.8387 214.3011 216.1398 247.8844 10.8398 -1.8379 214.4265 216.2644 247.8270 11.6370 -1.8342 214.5326 216.3668 247.7984 12.4240 -1.8287 214.6850 216.5137 247.7691 13.2315 -1.8284 214.8149 216.6433 247.7206 14.0493 -1.8281 214.9589 216.7871 247.6947 14.8158 -1.8272 215.0759 216.9031 247.6461 15.6745 -1.8267 215.2160 217.0427 247.6316 16.4410 -1.8253 215.3153 217.1407 247.5803 17.2690 -1.8246 215.4114 217.2360 247.5566 18.0565 -1.8223 215.5310 217.3533 247.5195 18.8645 -1.8189 215.6561 217.4750 247.4891 19.6823 -1.8144 215.7624 217.5768 247.4768 20.4488 -1.8158 215.8240 217.6397 247.4798 21.3075 -1.8128 215.9554 217.7682 247.4808 22.0740 -1.8090 216.0749 217.8840 247.5083 22.9020 -1.8112 216.2295 218.0407 247.5438 23.6890 -1.8088 216.3771 218.1859 247.5367 24.4965 -1.8094 216.4934 218.3028 247.5551 25.3145 -1.8071 216.6021 218.4091 247.5755 26.0818 -1.8044 216.7097 218.5141 247.6006 26.9405 -1.8035 216.8564 218.6600 247.6049 27.7070 -1.8008 216.9780 218.7788 247.6382 28.5350 -1.8037 217.0886 218.8922 247.6755 29.3323 -1.8030 217.2279 219.0309 247.7011 30.1295 -1.7975 217.3779 219.1754 247.7513 30.9575 -1.7931 217.4635 219.2566 247.7723 31.7240 -1.7865 217.5697 219.3562 247.8241 32.5725 -1.7854 217.6597 219.4451 247.8883 33.3495 -1.7840 217.7846 219.5686 247.9156 34.1680 -1.7803 217.9161 219.6964 247.9819 34.9653 -1.7792 218.0355 219.8146 248.0310 35.7625 -1.7752 218.1660 219.9412 248.1331 36.5803 -1.7698 218.2859 220.0556 248.2106 37.3365 -1.7648 218.3854 220.1503 248.2831 38.1645 -1.7556 218.5019 220.2575 248.3387 38.9515 -1.7484 218.5837 220.3321 248.4082 39.7795 -1.7465 218.7078 220.4542 248.4940 40.5768 -1.7491 218.8333 220.5825 248.5777 41.3740 -1.7451 218.9674 220.7126 248.6363 42.1918 -1.7445 219.0992 220.8438 248.7183 42.9685 -1.7380 219.1697 220.9077 248.8301 43.8170 -1.7353 219.3141 221.0494 248.9716 44.5733 -1.7346 219.4277 221.1622 249.0591 45.4120 -1.7351 219.5754 221.3104 249.2006 46.1995 -1.7340 219.6955 221.4295 249.2976 46.9865 -1.7321 219.7910 221.5231 249.3806 47.8248 -1.7308 219.9301 221.6610 249.4978 48.5810 -1.7298 220.0486 221.7784 249.5901 49.4398 -1.7320 220.1458 221.8778 249.7007 50.2063 -1.7289 220.2286 221.9575 249.8006 51.0343 -1.7289 220.3058 222.0347 249.9635 51.8008 -1.7270 220.4065 222.1335 250.0856 52.6185 -1.7258 220.5464 222.2722 250.1796 53.4568 -1.7176 220.6629 222.3806 250.2843 54.2130 -1.7145 220.7522 222.4667 250.4065 55.0718 -1.7152 220.8492 222.5644 250.5608 55.8385 -1.7137 220.9013 222.6150 250.6578 56.6673 -1.7120 221.0038 222.7158 250.7758 57.4645 -1.7063 221.1216 222.8279 250.8938 58.2515 -1.7106 221.2540 222.9646 250.9879 59.0590 -1.7070 221.4161 223.1231 251.1331 59.8460 -1.7020 221.5375 223.2395 251.2511 60.7150 -1.7005 221.6499 223.3503 251.3967 61.4405 -1.7040 221.7649 223.4690 251.5337 62.3095 -1.7027 221.8834 223.5860 251.7065 63.0658 -1.7080 222.0069 223.7148 251.8471 63.8938 -1.7078 222.1483 223.8560 252.0111 64.7218 -1.7047 222.2771 223.9817 252.1437 65.4883 -1.6996 222.3822 224.0818 252.2950 66.3378 -1.6934 222.4945 224.1879 252.4692 67.1043 -1.6909 222.5665 224.2574 252.6146 67.9220 -1.6893 222.6605 224.3498 252.7819 68.7193 -1.6869 222.7470 224.4338 252.8946 69.5165 -1.6830 222.8974 224.5805 253.0401 70.3343 -1.6807 223.0278 224.7085 253.1778 71.0905 -1.6799 223.1452 224.8251 253.3202 71.9595 -1.6760 223.2861 224.9620 253.4630 72.6850 -1.6753 223.4260 225.1013 253.5921 73.5438 -1.6735 223.5456 225.2191 253.7588 74.3103 -1.6768 223.6369 225.3137 253.9019 75.1393 -1.6782 223.7308 225.4090 254.0714 75.9365 -1.6807 223.8336 225.5143 254.2215 76.7235 -1.6785 223.9525 225.6310 254.3600 77.5618 -1.6856 224.0378 225.7235 254.5031 78.3180 -1.6864 224.1526 225.8389 254.6319 79.1665 -1.6826 224.2716 225.9543 254.7900 79.9433 -1.6798 224.3500 226.0298 254.9304 80.7610 -1.6768 224.4851 226.1620 255.0711 81.5583 -1.6765 224.5711 226.2476 255.2194 82.3555 -1.6726 224.7015 226.3741 255.3469 83.1528 -1.6730 224.8298 226.5028 255.4786 83.9508 -1.6738 224.9909 226.6647 255.6027 84.7688 -1.6787 225.1064 226.7851 255.7291 85.5455 -1.6825 225.1990 226.8815 255.8579 86.3940 -1.6830 225.2959 226.9789 255.9813 87.1605 -1.6809 225.3747 227.0556 256.1102 87.9885 -1.6793 225.5363 227.2156 256.2568 88.7858 -1.6816 225.6709 227.3525 256.3986 89.5830 -1.6835 225.7542 227.4377 256.5380 90.4110 -1.6789 225.8468 227.5257 256.6608 91.1785 -1.6797 225.9699 227.6496 256.7812 92.0373 -1.6821 226.1096 227.7917 256.9352 92.8038 -1.6789 226.1797 227.8587 257.0568 93.6318 -1.6782 226.2812 227.9594 257.1938 94.3983 -1.6820 226.4159 228.0980 257.3458 95.2263 -1.6893 226.5283 228.2176 257.4489 96.0235 -1.6893 226.6343 228.3237 257.5685 96.8105 -1.6873 226.7086 228.3959 257.6580 97.6488 -1.6836 226.8296 228.5133 257.7531 98.4050 -1.6874 226.9014 228.5888 257.8615 99.2638 -1.6870 227.0309 228.7179 257.9923 100.0303 -1.6871 227.1454 228.8324 258.0683 100.8480 -1.6861 227.2921 228.9781 258.1971 101.6355 -1.6821 227.4387 229.1209 258.3273 102.4435 -1.6810 227.5632 229.2442 258.4079 103.2613 -1.6834 227.6828 229.3663 258.5291 104.0175 -1.6842 227.7981 229.4823 258.6368 104.8763 -1.6867 227.9038 229.5905 258.7779 105.6428 -1.6882 228.0125 229.7007 258.8857 106.4605 -1.6892 228.1199 229.8091 258.9809 107.2578 -1.6912 228.2147 229.9059 259.0778 108.0550 -1.6830 228.3645 230.0475 259.1373 108.8728 -1.6823 228.4697 230.1520 259.2729 109.6495 -1.6819 228.5797 230.2616 259.4109 110.4673 -1.6812 228.6713 230.3524 259.5332 111.2343 -1.6834 228.7609 230.4443 259.6307 112.0935 -1.6890 228.8834 230.5724 259.7299 112.8600 -1.6927 228.9985 230.6912 259.8636 113.6880 -1.6948 229.1303 230.8251 259.9796 114.4750 -1.6939 229.2536 230.9474 260.0866 115.2825 -1.6882 229.3526 231.0408 260.1774 116.1003 -1.6855 229.5118 231.1973 260.2785 116.8668 -1.6864 229.6186 231.3051 260.3469 117.7255 -1.6880 229.7203 231.4083 260.4788 118.4920 -1.6881 229.8095 231.4976 260.5187 119.3203 -1.6932 229.9283 231.6214 260.5597 120.1075 -1.6933 230.0428 231.7361 260.6083 120.9155 -1.6866 230.1406 231.8273 260.7152 121.7435 -1.6800 230.2709 231.9509 260.8308 122.5100 -1.6787 230.3937 232.0725 260.9193 123.3278 -1.6779 230.4812 232.1591 261.0481 124.1353 -1.6756 230.6044 232.2800 261.1166 124.9530 -1.6755 230.7060 232.3815 261.1958 125.7195 -1.6743 230.8273 232.5016 261.2945 126.5475 -1.6795 230.9712 232.6507 261.4054 127.3448 -1.6859 231.1127 232.7986 261.5335 128.1420 -1.6903 231.2205 232.9108 261.6445 128.9598 -1.6918 231.3137 233.0056 261.7483 129.7365 -1.6891 231.4189 233.1080 261.8522 130.5858 -1.6886 231.5301 233.2187 261.9913 131.3625 -1.6931 231.6344 233.3274 262.1021 132.1698 -1.6946 231.7245 233.4191 262.1940 132.9675 -1.7002 231.8233 233.5235 262.2548 133.7850 -1.7021 231.9388 233.6408 262.3493 134.5415 -1.7031 232.0425 233.7456 262.4391 135.4105 -1.7054 232.1451 233.8505 262.5196 136.1668 -1.7076 232.2639 233.9715 262.5968 136.9845 -1.7059 232.3620 234.0679 262.6831 137.7818 -1.7040 232.5016 234.2056 262.7764 138.5790 -1.7058 232.6193 234.3251 262.8856 139.3968 -1.7024 232.7671 234.4695 262.9981 140.1735 -1.7010 232.8859 234.5870 263.0684 140.9913 -1.7002 232.9878 234.6879 263.1538 141.7578 -1.6988 233.1099 234.8087 263.2303 142.6165 -1.6988 233.2258 234.9246 263.3412 143.3730 -1.7027 233.3403 235.0430 263.4043 144.2018 -1.7069 233.4369 235.1438 263.4618 144.9990 -1.7025 233.5358 235.2383 263.5617 145.7963 -1.6993 233.6411 235.3404 263.6320 146.6243 -1.6983 233.7772 235.4755 263.7154 147.3805 -1.6976 233.8981 235.5958 263.8064 148.2495 -1.6960 234.0096 235.7056 263.9050 149.0058 -1.6996 234.1125 235.8120 263.9962 149.8338 -1.7006 234.1871 235.8877 264.0673 150.6313 -1.6992 234.3036 236.0029 264.1429 151.4285 -1.7054 234.4013 236.1067 264.2552 152.2570 -1.7093 234.5286 236.2379 264.3649 153.0238 -1.7096 234.6324 236.3420 264.4764 153.8825 -1.7038 234.7665 236.4703 264.5424 154.6490 -1.7039 234.8683 236.5722 264.6191 155.4770 -1.6984 234.9943 236.6927 264.7075 156.2640 -1.6991 235.0986 236.7977 264.7800 157.0715 -1.7008 235.2269 236.9277 264.8565 157.8893 -1.7006 235.3120 237.0126 264.9855 158.6558 -1.6951 235.4191 237.1142 265.0519 159.5153 -1.6951 235.5286 237.2237 265.1782 160.2818 -1.6964 235.6100 237.3064 265.2817 161.1100 -1.6952 235.7272 237.4223 265.3807 161.8970 -1.6964 235.8263 237.5227 265.5146 162.7045 -1.6968 235.9460 237.6427 265.6074 163.5223 -1.6988 236.0905 237.7894 265.7187 164.2785 -1.6999 236.2074 237.9074 265.8294 165.1373 -1.7002 236.3175 238.0177 265.9533 165.9040 -1.6994 236.4031 238.1024 266.0137 166.7225 -1.6984 236.5295 238.2279 266.0647 167.5198 -1.7017 236.6564 238.3582 266.1701 168.3170 -1.6982 236.7838 238.4820 266.2965 169.1040 -1.6980 236.8994 238.5974 266.4105 169.9013 -1.7003 237.0272 238.7274 266.5150 170.7293 -1.7050 237.1402 238.8452 266.6216 171.4855 -1.7070 237.1887 238.8956 266.7002 172.3545 -1.7068 237.2885 238.9953 266.8004 173.1108 -1.7074 237.3672 239.0746 266.9089 173.9285 -1.7062 237.4742 239.1804 267.0239 174.7360 -1.7083 237.5668 239.2752 267.1318 175.5238 -1.7128 237.7077 239.4205 267.2514 176.3520 -1.7122 237.8285 239.5407 267.3199 177.1185 -1.7163 237.9525 239.6689 267.4378 177.9773 -1.7217 238.1003 239.8220 267.5424 178.7130 -1.7190 238.1928 239.9118 267.6054 179.5615 -1.7132 238.3180 240.0312 267.7086 180.3383 -1.7116 238.4443 240.1559 267.8122 181.1560 -1.7084 238.5276 240.2360 267.9343 181.9533 -1.7093 238.6482 240.3574 268.0501 182.7505 -1.7104 238.7861 240.4965 268.1396 183.5790 -1.7089 238.9095 240.6184 268.2225 184.3460 -1.7081 239.0326 240.7406 268.3156 185.1945 -1.7038 239.1780 240.8818 268.4308 185.9405 -1.7053 239.2692 240.9745 268.4965 186.7890 -1.7060 239.4003 241.1063 268.6001 187.5555 -1.7058 239.5179 241.2237 268.7261 188.3835 -1.7066 239.6022 241.3088 268.8455 189.1910 -1.7098 239.7142 241.4240 268.9634 189.9780 -1.7146 239.7933 241.5078 269.0683 190.8060 -1.7186 239.9132 241.6319 269.1272 191.5725 -1.7193 240.0144 241.7338 269.2365 192.4318 -1.7165 240.0636 241.7801 269.3759 193.1988 -1.7162 240.1584 241.8746 269.4916 194.0165 -1.7164 240.2792 241.9955 269.6044 194.8240 -1.7179 240.3613 242.0791 269.7410 195.6110 -1.7218 240.4878 242.2096 269.8643 196.4083 -1.7216 240.6186 242.3402 269.9590 197.2055 -1.7234 240.7532 242.4766 270.0517 198.0233 -1.7176 240.8862 242.6038 270.1522 198.7898 -1.7123 241.0046 242.7169 270.2751 199.6488 -1.7116 241.1350 242.8466 270.3855 200.4050 -1.7110 241.2214 242.9324 270.4745 201.2338 -1.7115 241.3379 243.0495 270.5756 202.0310 -1.7095 241.4356 243.1451 270.6906 202.8180 -1.7077 241.5523 243.2600 270.8183 203.6460 -1.7089 241.6599 243.3689 270.8951 204.4125 -1.7100 241.7480 243.4579 270.9939 205.2405 -1.7119 241.8525 243.5645 271.0946 206.0070 -1.7121 241.9295 243.6417 271.2248 206.8555 -1.7154 242.0616 243.7770 271.3208 207.6323 -1.7198 242.1811 243.9008 271.4274 208.4500 -1.7212 242.2895 244.0107 271.5276 209.2473 -1.7219 242.3907 244.1126 271.6130 210.0445 -1.7217 242.4679 244.1896 271.7001 210.8725 -1.7178 242.5822 244.3000 271.8449 211.6398 -1.7151 242.7112 244.4263 271.9381 212.4885 -1.7203 242.8361 244.5564 272.0323 213.2550 -1.7219 242.9352 244.6571 272.1403 214.0728 -1.7251 243.0428 244.7678 272.2309 214.8495 -1.7317 243.1534 244.8850 272.3039 215.6980 -1.7263 243.2787 245.0050 272.4287 216.4645 -1.7313 243.4106 245.1419 272.5298 217.2925 -1.7267 243.5415 245.2682 272.6421 218.0898 -1.7246 243.6385 245.3631 272.7440 218.8870 -1.7209 243.7797 245.5006 272.8269 219.7048 -1.7234 243.9034 245.6269 272.9170 220.4815 -1.7227 244.0067 245.7293 273.0051 221.3300 -1.7231 244.1011 245.8242 273.1122 222.0965 -1.7196 244.1915 245.9111 273.2434 222.9248 -1.7200 244.2998 246.0198 273.3317 223.6920 -1.7190 244.4020 246.1210 273.4498 224.5405 -1.7211 244.5520 246.2731 273.5338 225.3173 -1.7241 244.6742 246.3983 273.6471 226.1350 -1.7245 244.7570 246.4815 273.7354 226.9323 -1.7222 244.8202 246.5424 273.8066 227.7295 -1.7244 244.9434 246.6678 273.9052 228.5575 -1.7252 245.0404 246.7656 273.9957 229.3240 -1.7258 245.1202 246.8460 274.0481 230.1725 -1.7283 245.2205 246.9487 274.1466 230.9390 -1.7312 245.3219 247.0531 274.2734 231.7568 -1.7342 245.3916 247.1258 274.3821 232.5540 -1.7322 245.4933 247.2255 274.4879 233.3513 -1.7326 245.5928 247.3254 274.5942 234.1698 -1.7324 245.7307 247.4631 274.7001 234.9365 -1.7342 245.8456 247.5797 274.7911 235.7645 -1.7272 245.9885 247.7157 274.9080 236.5310 -1.7269 246.1024 247.8292 275.0002 237.3795 -1.7281 246.2475 247.9756 275.0975 238.1460 -1.7284 246.4008 248.1292 275.1788 238.9740 -1.7240 246.5309 248.2548 275.2786 239.7610 -1.7247 246.6263 248.3509 275.3916 240.5685 -1.7277 246.7103 248.4380 275.4916 241.3863 -1.7283 246.8106 248.5389 275.5817 242.1528 -1.7356 246.9123 248.6480 275.6792 243.0115 -1.7414 247.0024 248.7438 275.8192 243.7780 -1.7385 247.1142 248.8527 275.9406 244.6060 -1.7365 247.2565 248.9930 276.0408 245.4040 -1.7344 247.3943 249.1287 276.1471 246.2015 -1.7309 247.4754 249.2063 276.2710 247.0295 -1.7317 247.5891 249.3208 276.4244 247.7960 -1.7298 247.6928 249.4225 276.5323 248.6445 -1.7323 247.7747 249.5070 276.6486 249.4213 -1.7341 247.9134 249.6475 276.7899 250.2390 -1.7356 248.0428 249.7783 276.9048 251.0363 -1.7392 248.1471 249.8864 276.9684 251.8335 -1.7438 248.2757 250.0195 277.0554 252.6623 -1.7463 248.4025 250.1488 277.2062 253.4290 -1.7486 248.5097 250.2583 277.3145 254.2468 -1.7462 248.6306 250.3767 277.4089 255.0235 -1.7429 248.7093 250.4523 277.5204 255.8720 -1.7393 248.8043 250.5436 277.6460 256.6385 -1.7410 248.9227 250.6637 277.7324 257.4665 -1.7428 249.0276 250.7704 277.8924 258.2740 -1.7437 249.1354 250.8791 277.9712 259.0610 -1.7464 249.2550 251.0014 278.0758 259.8898 -1.7472 249.3639 251.1111 278.1878 260.6565 -1.7489 249.4934 251.2423 278.2994 261.5050 -1.7498 249.6031 251.3530 278.4211 262.2715 -1.7492 249.6987 251.4478 278.5368 263.0995 -1.7601 249.8114 251.5714 278.6648 263.8865 -1.7577 249.8861 251.6439 278.7698 264.6735 -1.7555 249.9891 251.7445 278.8729 265.5118 -1.7545 250.1021 251.8566 278.9730 266.2680 -1.7549 250.1758 251.9307 279.0760 267.1165 -1.7579 250.2704 252.0282 279.1788 267.8625 -1.7593 250.3859 252.1451 279.2780 268.7110 -1.7614 250.4206 252.1820 279.3827 269.4775 -1.7602 250.5186 252.2788 279.5186 270.3055 -1.7574 250.6459 252.4033 279.6462 271.1028 -1.7571 250.7683 252.5254 279.7799 271.9000 -1.7573 250.8859 252.6432 279.8770 272.7178 -1.7546 250.9988 252.7534 279.9766 273.4945 -1.7528 251.0995 252.8523 280.0687 274.3430 -1.7552 251.2353 252.9904 280.1680 275.0795 -1.7553 251.3635 253.1188 280.2632 275.9385 -1.7581 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