DTA measure 2pb4 Date: 20241211:1024 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.11 s Mass = 955.700 mg data_number = 1071 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4878 -0.9869 224.0412 225.0281 208.8759 4.0828 -0.9842 223.9812 224.9654 208.8692 5.6805 -0.9819 223.9184 224.9003 208.8729 7.2795 -0.9783 223.8576 224.8359 208.8828 8.9085 -0.9708 223.7953 224.7661 208.8950 10.5075 -0.9407 223.7484 224.6890 208.9425 12.1215 -0.8883 223.6888 224.5771 209.0076 13.7205 -0.8771 223.6363 224.5133 209.0908 15.3191 -0.9384 223.5816 224.5200 209.1809 16.9329 -0.9544 223.5183 224.4727 209.2971 18.5469 -0.9517 223.4580 224.4096 209.4383 20.1458 -0.9476 223.4158 224.3634 209.5780 21.7596 -0.9451 223.3620 224.3071 209.7681 23.3586 -0.9446 223.3026 224.2472 209.9463 24.9576 -0.9435 223.2628 224.2063 210.1325 26.5868 -0.9447 223.2338 224.1785 210.3561 28.1856 -0.9498 223.1821 224.1319 210.5597 29.7845 -0.9509 223.1297 224.0805 210.7724 31.3985 -0.9461 223.0817 224.0277 211.0000 32.9975 -0.9455 223.0304 223.9759 211.2194 34.6115 -0.9458 222.9937 223.9395 211.4321 36.2254 -0.9479 222.9556 223.9035 211.6467 37.8240 -0.9461 222.9046 223.8507 211.8667 39.4228 -0.9468 222.8843 223.8311 212.0848 41.0366 -0.9470 222.8372 223.7842 212.3157 42.6658 -0.9448 222.7952 223.7401 212.5316 44.2646 -0.9470 222.7644 223.7114 212.7477 45.8636 -0.9455 222.7306 223.6761 212.9577 47.4781 -0.9449 222.6938 223.6387 213.1664 49.0783 -0.9462 222.6671 223.6134 213.3844 50.7069 -0.9452 222.6456 223.5908 213.5885 52.3000 -0.9483 222.6268 223.5751 213.8017 53.8913 -0.9508 222.5863 223.5371 213.9979 55.4834 -0.9479 222.5785 223.5264 214.2213 57.0900 -0.9457 222.5288 223.4745 214.4252 58.7110 -0.9469 222.4913 223.4382 214.6174 60.3040 -0.9508 222.4917 223.4425 214.8152 61.8981 -0.9531 222.4818 223.4349 215.0160 63.5058 -0.9524 222.4784 223.4308 215.2108 65.0995 -0.9527 222.4560 223.4087 215.3988 66.7105 -0.9557 222.4416 223.3974 215.6071 68.3223 -0.9546 222.4222 223.3768 215.8188 69.9204 -0.9547 222.4101 223.3648 216.0297 71.5181 -0.9557 222.3991 223.3548 216.2383 73.1171 -0.9569 222.3960 223.3529 216.4427 74.7366 -0.9566 222.3929 223.3494 216.6575 76.3508 -0.9585 222.3807 223.3392 216.8801 77.9496 -0.9579 222.3882 223.3461 217.0857 79.5486 -0.9580 222.3875 223.3455 217.2767 81.1626 -0.9575 222.3829 223.3404 217.5024 82.7616 -0.9596 222.3945 223.3542 217.7014 84.3908 -0.9611 222.4006 223.3617 217.8958 85.9800 -0.9624 222.4086 223.3710 218.1041 87.5995 -0.9629 222.4181 223.3809 218.3107 89.1985 -0.9643 222.4263 223.3906 218.5044 90.7975 -0.9657 222.4376 223.4033 218.6975 92.4265 -0.9648 222.4496 223.4143 218.9102 94.0405 -0.9662 222.4661 223.4323 219.0987 95.6391 -0.9656 222.4871 223.4528 219.3021 97.2378 -0.9656 222.4963 223.4619 219.4858 98.8524 -0.9649 222.5229 223.4878 219.6837 100.4666 -0.9663 222.5260 223.4923 219.8587 102.0808 -0.9671 222.5430 223.5101 220.0462 103.6796 -0.9664 222.5878 223.5541 220.2436 105.2941 -0.9646 222.6170 223.5816 220.4323 106.8943 -0.9639 222.6363 223.6003 220.6280 108.5244 -0.9622 222.6729 223.6351 220.8407 110.1236 -0.9626 222.7124 223.6750 221.0583 111.7238 -0.9621 222.7413 223.7034 221.2498 113.3385 -0.9625 222.7719 223.7343 221.4684 114.9361 -0.9613 222.7982 223.7596 221.6654 116.5575 -0.9600 222.8465 223.8065 221.8861 118.1489 -0.9602 222.8690 223.8292 222.0916 119.7396 -0.9613 222.9079 223.8692 222.2884 121.3463 -0.9587 222.9621 223.9208 222.4991 122.9388 -0.9599 222.9905 223.9504 222.7063 124.5615 -0.9569 223.0495 224.0064 222.9024 126.1543 -0.9553 223.0982 224.0535 223.1094 127.7634 -0.9566 223.1455 224.1021 223.3033 129.3603 -0.9548 223.1801 224.1349 223.5041 130.9705 -0.9539 223.2345 224.1884 223.7086 132.5829 -0.9510 223.2872 224.2381 223.8871 134.1816 -0.9493 223.3385 224.2878 224.0932 135.7806 -0.9480 223.3802 224.3282 224.2887 137.3796 -0.9477 223.4451 224.3927 224.5044 138.9936 -0.9492 223.5141 224.4633 224.7226 140.6076 -0.9461 223.5771 224.5232 224.9408 142.2066 -0.9449 223.6329 224.5778 225.1514 143.8206 -0.9444 223.6881 224.6325 225.3811 145.4195 -0.9445 223.7575 224.7020 225.6056 147.0185 -0.9418 223.8107 224.7524 225.8300 148.6325 -0.9411 223.8750 224.8162 226.0448 150.2465 -0.9415 223.9481 224.8896 226.2872 151.8454 -0.9418 224.0220 224.9638 226.4988 153.4595 -0.9379 224.0976 225.0355 226.7260 155.0578 -0.9380 224.1715 225.1095 226.9313 156.6716 -0.9369 224.2370 225.1739 227.1488 158.2858 -0.9347 224.3180 225.2527 227.3839 159.8856 -0.9336 224.3811 225.3147 227.6016 161.4846 -0.9338 224.4529 225.3867 227.8332 163.0986 -0.9319 224.5504 225.4823 228.0624 164.6983 -0.9306 224.6314 225.5620 228.2804 166.3275 -0.9291 224.7328 225.6618 228.4838 167.9273 -0.9281 224.8136 225.7417 228.6883 169.5275 -0.9254 224.8983 225.8237 228.8898 171.1420 -0.9253 224.9736 225.8989 229.0628 172.7414 -0.9248 225.0585 225.9833 229.2388 174.3704 -0.9210 225.1554 226.0764 229.4245 175.9688 -0.9183 225.2398 226.1580 229.5908 177.5680 -0.9173 225.3364 226.2537 229.7775 179.1806 -0.9144 225.4305 226.3449 229.9742 180.7723 -0.9125 225.5200 226.4325 230.1668 182.3931 -0.9109 225.6297 226.5406 230.3541 183.9853 -0.9119 225.7163 226.6282 230.5339 185.5764 -0.9096 225.8179 226.7275 230.7212 187.1836 -0.9075 225.9143 226.8218 230.9347 188.7766 -0.9026 226.0041 226.9067 231.1273 190.3990 -0.9025 226.1131 227.0156 231.3287 191.9920 -0.8997 226.2148 227.1145 231.5402 193.5995 -0.8968 226.3118 227.2086 231.7289 195.1943 -0.8956 226.4282 227.3238 231.9538 196.8218 -0.8965 226.5477 227.4443 232.1774 198.4201 -0.8948 226.6439 227.5387 232.4001 200.0195 -0.8918 226.7583 227.6501 232.6246 201.6336 -0.8904 226.8557 227.7460 232.8552 203.2325 -0.8863 226.9583 227.8446 233.0782 204.8465 -0.8856 227.0828 227.9684 233.3101 206.4605 -0.8851 227.1975 228.0825 233.5268 208.0595 -0.8808 227.3125 228.1932 233.7540 209.6734 -0.8789 227.4229 228.3018 233.9765 211.2720 -0.8781 227.5303 228.4084 234.2087 212.8858 -0.8756 227.6689 228.5445 234.4352 214.4999 -0.8761 227.7953 228.6714 234.6652 216.1136 -0.8739 227.9057 228.7795 234.9035 217.7126 -0.8720 228.0264 228.8984 235.1030 219.3116 -0.8695 228.1515 229.0210 235.3143 220.9414 -0.8686 228.2707 229.1393 235.5165 222.5408 -0.8655 228.3986 229.2641 235.7043 224.1549 -0.8650 228.5221 229.3870 235.8903 225.7545 -0.8602 228.6450 229.5052 236.0753 227.3535 -0.8573 228.7710 229.6283 236.2516 228.9825 -0.8577 228.9039 229.7616 236.4392 230.5815 -0.8537 229.0323 229.8861 236.6390 232.1958 -0.8521 229.1593 230.0114 236.8202 233.7949 -0.8505 229.3021 230.1526 237.0215 235.4088 -0.8496 229.4267 230.2763 237.2320 237.0234 -0.8466 229.5697 230.4163 237.4188 238.6236 -0.8427 229.7106 230.5533 237.6265 240.2379 -0.8416 229.8390 230.6807 237.8427 241.8376 -0.8401 229.9702 230.8103 238.0444 243.4368 -0.8376 230.1154 230.9530 238.2507 245.0601 -0.8354 230.2559 231.0913 238.4571 246.6520 -0.8314 230.3840 231.2154 238.6608 248.2446 -0.8328 230.5341 231.3669 238.8702 249.8525 -0.8287 230.6739 231.5026 239.0763 251.4445 -0.8264 230.8177 231.6440 239.2691 253.0511 -0.8244 230.9666 231.7910 239.4780 254.6598 -0.8253 231.1173 231.9426 239.6731 256.2530 -0.8239 231.2266 232.0505 239.8909 257.8629 -0.8214 231.3893 232.2107 240.0836 259.4574 -0.8152 231.5498 232.3649 240.2877 261.0826 -0.8121 231.6946 232.5067 240.4982 262.6809 -0.8108 231.8423 232.6531 240.7066 264.2788 -0.8091 231.9755 232.7846 240.9439 265.8775 -0.8077 232.1254 232.9331 241.1655 267.4911 -0.8093 232.2727 233.0820 241.3983 269.0900 -0.8040 232.4285 233.2326 241.6350 270.7039 -0.8014 232.5848 233.3861 241.8609 272.3179 -0.8020 232.7407 233.5427 242.1076 273.9171 -0.8000 232.9001 233.7001 242.3476 275.5166 -0.7977 233.0522 233.8499 242.5822 277.1156 -0.7982 233.2063 234.0045 242.8106 278.7448 -0.7973 233.3608 234.1581 243.0324 280.3436 -0.7983 233.5125 234.3108 243.2281 281.9576 -0.7960 233.6857 234.4817 243.4240 283.5566 -0.7935 233.8409 234.6344 243.6348 285.1555 -0.7907 233.9904 234.7812 243.8392 286.7845 -0.7895 234.1509 234.9404 244.0307 288.3835 -0.7895 234.3314 235.1209 244.2132 289.9976 -0.7881 234.4863 235.2744 244.4125 291.5970 -0.7851 234.6373 235.4224 244.6016 293.1958 -0.7830 234.8119 235.5949 244.7817 294.8264 -0.7836 234.9794 235.7630 244.9587 296.4258 -0.7824 235.1403 235.9226 245.1393 298.0265 -0.7811 235.2887 236.0698 245.3365 299.6426 -0.7798 235.4709 236.2507 245.5390 301.2421 -0.7788 235.6464 236.4252 245.7582 302.8724 -0.7757 235.8066 236.5823 245.9601 304.4715 -0.7746 235.9663 236.7408 246.1714 306.0865 -0.7723 236.1462 236.9185 246.3878 307.6851 -0.7688 236.3107 237.0796 246.6117 309.2783 -0.7681 236.4705 237.2386 246.8358 310.9000 -0.7692 236.6369 237.4062 247.0624 312.4919 -0.7684 236.8196 237.5881 247.2808 314.0983 -0.7681 236.9855 237.7536 247.4940 315.6904 -0.7660 237.1589 237.9249 247.7169 317.2838 -0.7644 237.3378 238.1023 247.9378 318.9078 -0.7661 237.5153 238.2814 248.1721 320.5150 -0.7636 237.6739 238.4375 248.3933 322.1101 -0.7630 237.8454 238.6085 248.6085 323.7059 -0.7622 238.0305 238.7928 248.8414 325.3175 -0.7620 238.2012 238.9632 249.0575 326.9309 -0.7616 238.3804 239.1420 249.2735 328.5310 -0.7606 238.5633 239.3238 249.4832 330.1476 -0.7581 238.7257 239.4839 249.7049 331.7466 -0.7573 238.9084 239.6657 249.9277 333.3456 -0.7598 239.0836 239.8434 250.1375 334.9596 -0.7612 239.2580 240.0193 250.3715 336.5738 -0.7574 239.4331 240.1905 250.5770 338.1876 -0.7574 239.6198 240.3772 250.7988 339.7866 -0.7588 239.8022 240.5610 251.0131 341.3855 -0.7571 239.9870 240.7441 251.2202 342.9995 -0.7553 240.1762 240.9316 251.4339 344.6135 -0.7571 240.3584 241.1155 251.6372 346.2125 -0.7576 240.5427 241.3003 251.8538 347.8265 -0.7575 240.7317 241.4893 252.0826 349.4251 -0.7577 240.9004 241.6581 252.2758 351.0390 -0.7569 241.0876 241.8444 252.4852 352.6528 -0.7577 241.2743 242.0320 252.6931 354.2526 -0.7582 241.4641 242.2223 252.8965 355.8516 -0.7578 241.6557 242.4135 253.1125 357.4661 -0.7591 241.8461 242.6052 253.3222 359.0656 -0.7590 242.0355 242.7945 253.5138 360.6948 -0.7582 242.2136 242.9718 253.7166 362.2945 -0.7594 242.3993 243.1587 253.9245 363.8939 -0.7597 242.5829 243.3426 254.1136 365.5090 -0.7585 242.7806 243.5391 254.3271 367.1091 -0.7591 242.9718 243.7309 254.5224 368.7385 -0.7588 243.1617 243.9205 254.7275 370.3375 -0.7597 243.3593 244.1189 254.9258 371.9355 -0.7594 243.5517 244.3111 255.1114 373.5273 -0.7597 243.7445 244.5043 255.3071 375.1334 -0.7591 243.9271 244.6862 255.5022 376.7401 -0.7604 244.1084 244.8688 255.7045 378.3470 -0.7596 244.3113 245.0709 255.9095 379.9389 -0.7586 244.4984 245.2569 256.0972 381.5321 -0.7590 244.6920 245.4509 256.2789 383.1398 -0.7572 244.8944 245.6516 256.4805 384.7620 -0.7610 245.0812 245.8422 256.6907 386.3558 -0.7595 245.2739 246.0334 256.9016 387.9521 -0.7586 245.4693 246.2279 257.1151 389.5634 -0.7584 245.6647 246.4231 257.3436 391.1614 -0.7602 245.8668 246.6270 257.5560 392.7895 -0.7604 246.0486 246.8091 257.7877 394.4036 -0.7623 246.2426 247.0049 258.0199 396.0025 -0.7630 246.4450 247.2079 258.2552 397.6016 -0.7639 246.6457 247.4096 258.4830 399.2156 -0.7660 246.8451 247.6111 258.7202 400.8295 -0.7642 247.0362 247.8004 258.9382 402.4285 -0.7649 247.2397 248.0047 259.1652 404.0296 -0.7653 247.4315 248.1968 259.3857 405.6455 -0.7659 247.6435 248.4094 259.6252 407.2439 -0.7669 247.8349 248.6018 259.8337 408.8730 -0.7698 248.0375 248.8073 260.0632 410.4718 -0.7710 248.2428 249.0137 260.2674 412.0706 -0.7723 248.4346 249.2069 260.4614 413.6846 -0.7729 248.6441 249.4170 260.6698 415.2986 -0.7752 248.8441 249.6193 260.8452 416.9136 -0.7747 249.0510 249.8256 261.0287 418.5126 -0.7751 249.2515 250.0266 261.2098 420.1266 -0.7754 249.4437 250.2191 261.3916 421.7255 -0.7763 249.6495 250.4258 261.5910 423.3395 -0.7796 249.8402 250.6198 261.7718 424.9535 -0.7800 250.0582 250.8383 261.9704 426.5534 -0.7812 250.2487 251.0300 262.1780 428.1674 -0.7817 250.4630 251.2447 262.4043 429.7664 -0.7816 250.6575 251.4391 262.6122 431.3808 -0.7846 250.8771 251.6617 262.8220 432.9956 -0.7845 251.0838 251.8683 263.0401 434.5948 -0.7845 251.2801 252.0647 263.2503 436.2083 -0.7854 251.4903 252.2758 263.4606 437.8008 -0.7865 251.6910 252.4774 263.6741 439.4079 -0.7884 251.8892 252.6776 263.8706 441.0140 -0.7919 252.1040 252.8959 264.0813 442.6060 -0.7928 252.3079 253.1007 264.2914 444.2125 -0.7926 252.5025 253.2950 264.5054 445.8046 -0.7949 252.7103 253.5051 264.7122 447.4275 -0.7950 252.9109 253.7059 264.9438 449.0226 -0.7941 253.1249 253.9191 265.1549 450.6330 -0.7966 253.3320 254.1287 265.3536 452.2289 -0.8011 253.5428 254.3439 265.5498 453.8276 -0.8024 253.7561 254.5585 265.7589 455.4565 -0.8027 253.9571 254.7597 265.9819 457.0555 -0.8050 254.1652 254.9701 266.1685 458.6695 -0.8072 254.3574 255.1646 266.3754 460.2685 -0.8090 254.5853 255.3943 266.5988 461.8675 -0.8116 254.7892 255.6007 266.7914 463.4965 -0.8127 254.9886 255.8013 266.9838 465.0955 -0.8145 255.2205 256.0350 267.1905 466.7090 -0.8160 255.4140 256.2299 267.4108 468.3079 -0.8147 255.6153 256.4299 267.6451 469.9066 -0.8191 255.8314 256.6505 267.8559 471.5356 -0.8202 256.0556 256.8758 268.0889 473.1348 -0.8222 256.2692 257.0914 268.3430 474.7486 -0.8219 256.4670 257.2889 268.5738 476.3475 -0.8235 256.6812 257.5047 268.7994 477.9466 -0.8272 256.8886 257.7158 269.0269 479.5755 -0.8302 257.1070 257.9372 269.2464 481.1896 -0.8294 257.3217 258.1511 269.4723 482.7899 -0.8357 257.5392 258.3748 269.6703 484.3895 -0.8353 257.7345 258.5698 269.8676 486.0031 -0.8363 257.9517 258.7880 270.0733 487.6171 -0.8373 258.1676 259.0049 270.2695 489.2310 -0.8393 258.3739 259.2132 270.4637 490.8306 -0.8423 258.5895 259.4318 270.6560 492.4296 -0.8436 258.8034 259.6469 270.8583 494.0436 -0.8446 259.0138 259.8584 271.0484 495.6728 -0.8497 259.2455 260.0952 271.2487 497.2728 -0.8506 259.4479 260.2985 271.4341 498.8725 -0.8511 259.6606 260.5118 271.6130 500.4860 -0.8538 259.8694 260.7232 271.8303 502.0790 -0.8554 260.0852 260.9405 272.0573 503.7010 -0.8588 260.3015 261.1602 272.2726 505.2931 -0.8618 260.5173 261.3792 272.5104 506.8850 -0.8650 260.7428 261.6077 272.7275 508.4915 -0.8649 260.9492 261.8141 272.9571 510.0980 -0.8678 261.1633 262.0311 273.1893 511.7063 -0.8717 261.3787 262.2504 273.4146 513.3008 -0.8743 261.5845 262.4588 273.6427 514.9095 -0.8771 261.8037 262.6808 273.8798 516.5055 -0.8835 262.0098 262.8933 274.1049 518.1164 -0.8844 262.2177 263.1021 274.3266 519.7285 -0.8861 262.4471 263.3332 274.5464 521.3274 -0.8893 262.6695 263.5588 274.7857 522.9410 -0.8902 262.8877 263.7779 275.0149 524.5398 -0.8914 263.0967 263.9881 275.2433 526.1386 -0.8896 263.3318 264.2214 275.4561 527.8279 -0.8908 263.5444 264.4352 275.6445 529.5016 -0.8968 263.7616 264.6584 275.8519 531.1006 -0.8978 263.9934 264.8912 276.0388 532.6996 -0.9011 264.2100 265.1111 276.2240 534.3286 -0.9034 264.4175 265.3209 276.4046 535.9276 -0.9079 264.6361 265.5439 276.5747 537.5418 -0.9096 264.8637 265.7733 276.7591 539.1415 -0.9108 265.0894 266.0002 276.9511 540.7405 -0.9133 265.2992 266.2125 277.1533 542.3695 -0.9152 265.5136 266.4288 277.3598 543.9694 -0.9171 265.7283 266.6454 277.5610 545.5834 -0.9200 265.9480 266.8680 277.7736 547.1818 -0.9195 266.1740 267.0936 277.9877 548.8258 -0.9234 266.3888 267.3121 278.1928 550.4248 -0.9292 266.6281 267.5573 278.4096 552.0386 -0.9335 266.8465 267.7800 278.6130 553.6376 -0.9356 267.0626 267.9982 278.8241 555.2523 -0.9405 267.2854 268.2259 279.0359 556.8666 -0.9386 267.4907 268.4293 279.2560 558.4806 -0.9423 267.7219 268.6642 279.4728 560.0798 -0.9467 267.9563 268.9030 279.6886 561.6799 -0.9512 268.1710 269.1222 279.8923 563.2945 -0.9509 268.3794 269.3304 280.1166 564.9079 -0.9556 268.5987 269.5543 280.3063 566.5150 -0.9546 268.8111 269.7658 280.5235 568.1071 -0.9591 269.0338 269.9929 280.7398 569.6990 -0.9629 269.2536 270.2165 280.9534 571.3065 -0.9658 269.4762 270.4421 281.1502 572.9151 -0.9671 269.7122 270.6793 281.3445 574.5226 -0.9719 269.9118 270.8837 281.5631 576.1178 -0.9759 270.1355 271.1114 281.7651 577.7134 -0.9822 270.3518 271.3340 281.9792 579.3229 -0.9968 270.5723 271.5691 282.1929 580.9359 -1.0008 270.7991 271.7999 282.3860 582.5498 -1.0040 271.0239 272.0279 282.5894 584.1486 -1.0059 271.2368 272.2427 282.8017 585.7478 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