DTA measure 3pb3 Date: 20241211:950 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1649.20 s Mass = 955.700 mg data_number = 1026 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4086 -4.5822 436.5768 441.1590 424.2561 4.0230 -4.5933 436.6708 441.2641 424.2803 5.6226 -4.5989 436.7758 441.3747 424.2727 7.2216 -4.5959 436.8485 441.4444 424.2386 8.8508 -4.5916 436.9147 441.5063 424.1743 10.4508 -4.6077 437.0006 441.6083 424.0867 12.0505 -4.6167 437.0917 441.7083 423.9874 13.6495 -4.6152 437.1677 441.7829 423.8359 15.2635 -4.6200 437.2433 441.8633 423.6802 16.8739 -4.6251 437.3097 441.9349 423.4933 18.4646 -4.6605 437.3834 442.0439 423.3127 20.0701 -4.6660 437.4470 442.1130 423.1142 21.6614 -4.6724 437.5084 442.1808 422.9015 23.2523 -4.6785 437.5897 442.2682 422.6809 24.8885 -4.6784 437.6471 442.3256 422.4410 26.4949 -4.6838 437.6874 442.3712 422.1982 28.0878 -4.6905 437.7635 442.4539 421.9484 29.6806 -4.6899 437.8121 442.5020 421.7030 31.3044 -4.6838 437.8440 442.5278 421.4620 32.8988 -4.6953 437.9030 442.5983 421.2324 34.5098 -4.6806 437.9372 442.6178 421.0183 36.1068 -4.6875 437.9718 442.6593 420.8072 37.7069 -4.6967 438.0152 442.7119 420.6070 39.3045 -4.7133 438.0549 442.7682 420.3955 40.9326 -4.7231 438.0910 442.8141 420.1982 42.5316 -4.7279 438.1127 442.8405 420.0094 44.1305 -4.7295 438.1337 442.8632 419.8298 45.7295 -4.7311 438.1418 442.8728 419.6443 47.3435 -4.7337 438.1752 442.9089 419.4530 48.9575 -4.7530 438.1956 442.9486 419.2756 50.5565 -4.8040 438.2015 443.0054 419.0878 52.1705 -4.8030 438.2304 443.0333 418.8959 53.7695 -4.8071 438.2338 443.0409 418.7023 55.3685 -4.8134 438.2244 443.0378 418.5222 56.9819 -4.8166 438.2369 443.0535 418.3316 58.5959 -4.8032 438.2398 443.0430 418.1236 60.1946 -4.7574 438.2404 442.9978 417.9230 61.8086 -4.7858 438.2422 443.0281 417.7145 63.4081 -4.8100 438.2263 443.0363 417.5203 65.0226 -4.8307 438.2208 443.0516 417.3233 66.6366 -4.8362 438.2004 443.0366 417.1210 68.2355 -4.8330 438.1927 443.0257 416.9192 69.8495 -4.8179 438.1842 443.0021 416.7342 71.4485 -4.8262 438.1812 443.0075 416.5516 73.0625 -4.8167 438.1423 442.9589 416.3604 74.6775 -4.8246 438.1316 442.9562 416.1664 76.2785 -4.8021 438.0913 442.8934 415.9814 77.8771 -4.8025 438.0638 442.8663 415.7631 79.4908 -4.8397 438.0474 442.8871 415.5508 81.0854 -4.8528 438.0081 442.8609 415.3648 82.7061 -4.8583 437.9679 442.8262 415.1546 84.2970 -4.8425 437.9327 442.7751 414.9313 85.8884 -4.8723 437.8955 442.7678 414.7333 87.4801 -4.8762 437.8439 442.7201 414.5288 89.0868 -4.8757 437.7974 442.6730 414.3287 90.6939 -4.8684 437.7620 442.6304 414.1289 92.3014 -4.8834 437.7212 442.6046 413.9292 93.8959 -4.8900 437.6551 442.5450 413.7382 95.4900 -4.8913 437.6166 442.5079 413.5330 97.0990 -4.8954 437.5581 442.4535 413.3450 98.7113 -4.8971 437.4965 442.3936 413.1559 100.3095 -4.8877 437.4490 442.3366 412.9631 101.9085 -4.8945 437.3895 442.2840 412.7689 103.5075 -4.8917 437.3198 442.2115 412.5589 105.1215 -4.8947 437.2444 442.1391 412.3558 106.7205 -4.8934 437.1973 442.0907 412.1560 108.3345 -4.8941 437.1306 442.0247 411.9508 109.9335 -4.8788 437.0567 441.9355 411.7238 111.5475 -4.8857 436.9789 441.8646 411.5273 113.1463 -4.8871 436.9139 441.8009 411.2929 114.7449 -4.8802 436.8414 441.7215 411.0789 116.3439 -4.8926 436.7573 441.6499 410.8734 117.9604 -4.9087 436.6702 441.5789 410.6510 119.5748 -4.9169 436.6126 441.5295 410.4504 121.1736 -4.9177 436.5181 441.4358 410.2203 122.7726 -4.9176 436.4200 441.3376 410.0196 124.3866 -4.9166 436.3408 441.2573 409.8140 126.0006 -4.9264 436.2651 441.1915 409.6165 127.5995 -4.9253 436.1763 441.1016 409.4260 129.2135 -4.9257 436.0687 440.9945 409.2230 130.8125 -4.9243 435.9790 440.9033 409.0281 132.4115 -4.9227 435.9021 440.8248 408.8215 134.0255 -4.9341 435.7975 440.7315 408.6450 135.6394 -4.9301 435.6991 440.6292 408.4327 137.2380 -4.9212 435.6075 440.5288 408.2340 138.8398 -4.9083 435.4933 440.4016 408.0578 140.4406 -4.9088 435.3959 440.3047 407.8723 142.0546 -4.9098 435.2890 440.1988 407.6723 143.6694 -4.9115 435.1908 440.1023 407.4800 145.2674 -4.9082 435.0849 439.9931 407.2672 146.8740 -4.9049 434.9766 439.8815 407.0641 148.4650 -4.8993 434.8757 439.7750 406.8579 150.0560 -4.8888 434.7554 439.6442 406.6572 151.6620 -4.9058 434.6511 439.5569 406.4543 153.2689 -4.8939 434.5375 439.4315 406.2239 154.8619 -4.8970 434.4271 439.3240 406.0040 156.4688 -4.9023 434.3095 439.2118 405.8107 158.0638 -4.9025 434.1984 439.1009 405.6090 159.6586 -4.9158 434.0755 438.9913 405.4048 161.2833 -4.9214 433.9494 438.8709 405.1652 162.8788 -4.9180 433.8420 438.7599 404.9662 164.4749 -4.9130 433.7180 438.6310 404.7595 166.0885 -4.9032 433.5942 438.4973 404.5613 167.6875 -4.8984 433.4574 438.3558 404.3525 169.3015 -4.8946 433.3336 438.2282 404.1658 170.9001 -4.8955 433.2121 438.1076 403.9653 172.5139 -4.8994 433.0768 437.9762 403.7617 174.1128 -4.9090 432.9557 437.8648 403.5601 175.7121 -4.9129 432.8232 437.7361 403.3639 177.3424 -4.9080 432.6880 437.5959 403.1679 178.9418 -4.9048 432.5587 437.4635 402.9815 180.5406 -4.9013 432.4258 437.3271 402.7915 182.1546 -4.9035 432.2898 437.1933 402.5990 183.7535 -4.8787 432.1713 437.0501 402.3959 185.3675 -4.8696 432.0250 436.8946 402.2012 186.9825 -4.8646 431.8780 436.7426 402.0007 188.5815 -4.8606 431.7554 436.6160 401.7828 190.1820 -4.8557 431.5937 436.4494 401.5722 191.7980 -4.8519 431.4546 436.3065 401.3600 193.3973 -4.8551 431.3166 436.1717 401.1207 195.0121 -4.8506 431.1783 436.0289 400.9221 196.6290 -4.8480 431.0304 435.8785 400.7111 198.2276 -4.8578 430.8973 435.7551 400.4939 199.8266 -4.8559 430.7444 435.6003 400.2750 201.4413 -4.8486 430.6132 435.4618 400.0867 203.0564 -4.8536 430.4499 435.3035 399.8715 204.6709 -4.8582 430.3042 435.1624 399.6605 206.2706 -4.8580 430.1503 435.0083 399.4434 207.8695 -4.8458 430.0068 434.8527 399.2414 209.4815 -4.8455 429.8639 434.7094 399.0413 211.0889 -4.8465 429.7290 434.5756 398.8300 212.6800 -4.8501 429.5546 434.4047 398.6418 214.2865 -4.8386 429.4056 434.2442 398.4240 215.8790 -4.8334 429.2461 434.0795 398.2250 217.4705 -4.8315 429.1173 433.9488 398.0330 219.0803 -4.8234 428.9650 433.7883 397.8361 220.6783 -4.8148 428.7913 433.6061 397.6448 222.2909 -4.8140 428.6342 433.4483 397.4389 223.8863 -4.8121 428.4816 433.2938 397.2561 225.4803 -4.8101 428.3171 433.1272 397.0561 227.0774 -4.8096 428.1590 432.9686 396.8685 228.7051 -4.8086 427.9957 432.8044 396.6576 230.3039 -4.8055 427.8447 432.6502 396.4546 231.9026 -4.8017 427.7033 432.5050 396.2593 233.5016 -4.7981 427.5288 432.3269 396.0423 235.1006 -4.7916 427.3505 432.1421 395.8327 236.6996 -4.7813 427.2002 431.9816 395.6033 238.3286 -4.7813 427.0312 431.8126 395.3893 239.9278 -4.7762 426.8747 431.6509 395.1730 241.5266 -4.7774 426.7112 431.4886 394.9585 243.1410 -4.7764 426.5443 431.3207 394.7374 244.7405 -4.7714 426.3883 431.1597 394.5245 246.3395 -4.7689 426.2251 430.9939 394.3148 247.9685 -4.7708 426.0438 430.8146 394.0909 249.5675 -4.7757 425.8836 430.6593 393.8733 251.1661 -4.7733 425.7182 430.4915 393.6507 252.7650 -4.7693 425.5452 430.3145 393.4452 254.3788 -4.7708 425.3913 430.1621 393.2475 255.9928 -4.7561 425.2006 429.9567 393.0207 257.5918 -4.7532 425.0346 429.7878 392.8247 259.2056 -4.7458 424.8633 429.6092 392.6112 260.8046 -4.7443 424.6999 429.4441 392.3998 262.4036 -4.7433 424.5202 429.2635 392.1984 264.0334 -4.7376 424.3441 429.0816 391.9986 265.6335 -4.7307 424.1984 428.9291 391.7870 267.2325 -4.7273 424.0171 428.7444 391.5937 268.8465 -4.7264 423.8305 428.5568 391.3912 270.4455 -4.7236 423.6585 428.3821 391.1895 272.0595 -4.7195 423.4878 428.2072 390.9924 273.6695 -4.7173 423.3164 428.0338 390.7856 275.2604 -4.7114 423.1342 427.8456 390.5927 276.8511 -4.7083 422.9582 427.6665 390.3937 278.4426 -4.7060 422.7918 427.4977 390.1998 280.0488 -4.6983 422.5938 427.2921 390.0220 281.6550 -4.6959 422.4253 427.1212 389.8165 283.2613 -4.6925 422.2530 426.9455 389.6280 284.8539 -4.6889 422.0716 426.7604 389.4269 286.4614 -4.6860 421.8944 426.5805 389.2187 288.0559 -4.6826 421.7245 426.4071 389.0218 289.6801 -4.6781 421.5511 426.2293 388.8235 291.2761 -4.6761 421.3748 426.0509 388.6007 292.8746 -4.6685 421.1821 425.8506 388.3764 294.4736 -4.6676 421.0001 425.6677 388.1577 296.0725 -4.6631 420.8302 425.4933 387.9445 297.7015 -4.6565 420.6507 425.3073 387.7407 299.3006 -4.6513 420.4681 425.1194 387.5316 300.8995 -4.6489 420.2889 424.9378 387.3161 302.5135 -4.6465 420.0962 424.7427 387.0959 304.1125 -4.6386 419.9090 424.5476 386.8659 305.7265 -4.6355 419.7370 424.3725 386.6577 307.3405 -4.6329 419.5493 424.1822 386.4496 308.9395 -4.6254 419.3777 424.0031 386.2301 310.5530 -4.6226 419.1766 423.7992 386.0355 312.1518 -4.6228 419.0095 423.6323 385.8151 313.7656 -4.6184 418.8282 423.4465 385.5904 315.3798 -4.6148 418.6476 423.2624 385.3929 316.9786 -4.6069 418.4498 423.0567 385.1824 318.5776 -4.6026 418.2826 422.8852 384.9835 320.1916 -4.6001 418.0891 422.6892 384.7715 321.7906 -4.5951 417.8877 422.4828 384.5622 323.4196 -4.5922 417.7005 422.2927 384.3556 325.0195 -4.5873 417.5167 422.1040 384.1519 326.6185 -4.5809 417.3558 421.9367 383.9611 328.2325 -4.5762 417.1393 421.7155 383.7564 329.8320 -4.5708 416.9569 421.5277 383.5563 331.4614 -4.5643 416.7683 421.3325 383.3473 333.0598 -4.5614 416.5809 421.1423 383.1536 334.6586 -4.5553 416.3836 420.9390 382.9561 336.2576 -4.5464 416.2115 420.7579 382.7680 337.8680 -4.5423 416.0224 420.5647 382.5845 339.4733 -4.5382 415.8287 420.3669 382.3730 341.0790 -4.5337 415.6387 420.1724 382.1583 342.6704 -4.5292 415.4549 419.9840 381.9689 344.2624 -4.5219 415.2765 419.7984 381.7440 345.8545 -4.5172 415.0847 419.6020 381.5242 347.4764 -4.5153 414.8904 419.4057 381.3090 349.0690 -4.5087 414.6874 419.1961 381.0983 350.6764 -4.5046 414.5055 419.0101 380.8668 352.2694 -4.5004 414.3119 418.8124 380.6448 353.8783 -4.4938 414.1285 418.6223 380.4207 355.4896 -4.4882 413.9395 418.4277 380.1966 357.0875 -4.4853 413.7523 418.2377 379.9818 358.6865 -4.4818 413.5590 418.0408 379.7561 360.2855 -4.4753 413.3726 417.8479 379.5343 361.8995 -4.4690 413.1732 417.6422 379.3233 363.4985 -4.4656 412.9670 417.4326 379.1210 365.1125 -4.4609 412.7848 417.2457 378.8862 366.7115 -4.4551 412.5916 417.0467 378.6843 368.3250 -4.4488 412.3918 416.8406 378.4689 369.9236 -4.4458 412.2152 416.6610 378.2601 371.5229 -4.4412 412.0192 416.4604 378.0504 373.1368 -4.4376 411.8234 416.2611 377.8557 374.7508 -4.4314 411.6305 416.0620 377.6297 376.3496 -4.4241 411.4286 415.8527 377.4079 377.9486 -4.4218 411.2381 415.6599 377.2168 379.5626 -4.4162 411.0397 415.4559 377.0072 381.1616 -4.4108 410.8565 415.2673 376.8139 382.7755 -4.4057 410.6570 415.0627 376.6172 384.3788 -4.4002 410.4524 414.8527 376.4029 385.9965 -4.3961 410.2678 414.6639 376.2125 387.5955 -4.3921 410.0735 414.4657 376.0086 389.1945 -4.3871 409.8676 414.2548 375.8080 390.8080 -4.3826 409.6675 414.0501 375.6215 392.4068 -4.3782 409.4860 413.8642 375.4276 394.0358 -4.3741 409.2836 413.6576 375.2111 395.6346 -4.3686 409.0742 413.4429 375.0140 397.2336 -4.3644 408.8828 413.2472 374.8180 398.8476 -4.3599 408.6911 413.0510 374.6224 400.4466 -4.3543 408.4810 412.8353 374.4352 402.0749 -4.3506 408.3012 412.6518 374.2271 403.6673 -4.3472 408.1125 412.4597 374.0372 405.2590 -4.3411 407.9115 412.2526 373.8424 406.8500 -4.3366 407.7093 412.0459 373.6445 408.4426 -4.3302 407.5131 411.8433 373.4525 410.0650 -4.3241 407.3139 411.6380 373.2487 411.6576 -4.3226 407.1088 411.4314 373.0672 413.2644 -4.3181 406.9171 411.2352 372.8545 414.8595 -4.3152 406.7249 411.0401 372.6499 416.4541 -4.3233 406.5310 410.8543 372.4342 418.0626 -4.3225 406.3363 410.6588 372.2238 419.6733 -4.3236 406.1289 410.4525 371.9987 421.2715 -4.3239 405.9220 410.2459 371.7976 422.8705 -4.3223 405.7374 410.0598 371.5763 424.4693 -4.3142 405.5418 409.8559 371.3663 426.0716 -4.3068 405.3422 409.6490 371.1396 427.6708 -4.2992 405.1464 409.4456 370.9092 429.2999 -4.2939 404.9554 409.2492 370.6915 430.8986 -4.2836 404.7508 409.0344 370.4712 432.4976 -4.2814 404.5445 408.8259 370.2604 434.0966 -4.2736 404.3592 408.6328 370.0631 435.7106 -4.2688 404.1588 408.4275 369.8526 437.3245 -4.2664 403.9564 408.2228 369.6254 438.9236 -4.2616 403.7798 408.0414 369.3916 440.5229 -4.2590 403.5563 407.8154 369.1841 442.1375 -4.2597 403.3547 407.6143 368.9828 443.7365 -4.2575 403.1572 407.4146 368.7754 445.3361 -4.2448 402.9650 407.2098 368.5687 446.9535 -4.2380 402.7596 406.9975 368.3545 448.5671 -4.2337 402.5450 406.7787 368.1498 450.1661 -4.2267 402.3537 406.5804 367.9424 451.7658 -4.2294 402.1572 406.3865 367.7435 453.3646 -4.2253 401.9509 406.1762 367.5281 454.9786 -4.2104 401.7536 405.9641 367.3241 456.5928 -4.2045 401.5568 405.7613 367.1265 458.1916 -4.2014 401.3559 405.5573 366.9154 459.7905 -4.1986 401.1618 405.3604 366.7233 461.4045 -4.1980 400.9488 405.1467 366.5246 463.0041 -4.1920 400.7503 404.9422 366.3082 464.6193 -4.1945 400.5470 404.7415 366.1187 466.2323 -4.1981 400.3444 404.5425 365.8928 467.8250 -4.1917 400.1569 404.3487 365.6900 469.4159 -4.1800 399.9597 404.1397 365.4970 471.0069 -4.1756 399.7571 403.9327 365.2947 472.6276 -4.1705 399.5495 403.7200 365.0859 474.2208 -4.1708 399.3391 403.5099 364.8819 475.8138 -4.1615 399.1514 403.3129 364.6724 477.4214 -4.1568 398.9380 403.0948 364.4788 479.0169 -4.1581 398.7442 402.9023 364.2934 480.6265 -4.1478 398.5473 402.6951 364.1033 482.2378 -4.1302 398.3484 402.4785 363.8913 483.8355 -4.1179 398.1263 402.2442 363.6803 485.4316 -4.1096 397.9390 402.0486 363.4849 487.0291 -4.1050 397.7405 401.8455 363.2856 488.6276 -4.0989 397.5434 401.6423 363.0728 490.2566 -4.0993 397.3356 401.4350 362.8519 491.8558 -4.0936 397.1286 401.2222 362.6463 493.4546 -4.0886 396.9441 401.0327 362.4322 495.0535 -4.0834 396.7332 400.8166 362.2127 496.6675 -4.0780 396.5457 400.6238 362.0043 498.2666 -4.0723 396.3350 400.4073 361.8011 499.8805 -4.0659 396.1416 400.2075 361.5915 501.4945 -4.0590 395.9270 399.9859 361.3725 503.0935 -4.0552 395.7249 399.7801 361.1664 504.6924 -4.0504 395.5332 399.5837 360.9490 506.2923 -4.0442 395.3329 399.3772 360.7364 507.9060 -4.0409 395.1337 399.1746 360.5320 509.5200 -4.0440 394.9240 398.9680 360.3312 511.1196 -4.0295 394.7229 398.7524 360.1204 512.7186 -4.0233 394.5171 398.5403 359.9043 514.3326 -4.0231 394.3035 398.3266 359.7100 515.9316 -4.0167 394.1218 398.1385 359.4990 517.5464 -4.0113 393.9224 397.9338 359.2879 519.1609 -4.0060 393.7148 397.7208 359.0867 520.7605 -3.9980 393.5153 397.5133 358.8808 522.3595 -3.9918 393.3214 397.3132 358.7016 523.9585 -3.9904 393.1058 397.0962 358.4985 525.5881 -3.9661 392.9065 396.8726 358.2836 527.1875 -3.9547 392.6993 396.6540 358.0905 528.8008 -3.9501 392.4987 396.4488 357.8744 530.3979 -3.9433 392.2984 396.2417 357.6761 531.9890 -3.9366 392.0902 396.0267 357.4873 533.5950 -3.9325 391.8903 395.8228 357.2870 535.2025 -3.9222 391.6882 395.6104 357.0987 536.7933 -3.9088 391.4977 395.4065 356.8915 538.3931 -3.9179 391.2943 395.2122 356.6854 539.9885 -3.9209 391.0881 395.0090 356.4823 541.5950 -3.9075 390.8805 394.7880 356.2641 543.2019 -3.9126 390.6827 394.5953 356.0595 544.8113 -3.9065 390.4884 394.3949 355.8351 546.4083 -3.9005 390.2699 394.1704 355.6323 548.0051 -3.8968 390.0619 393.9587 355.4033 549.6036 -3.8904 389.8790 393.7693 355.1813 551.2325 -3.8833 389.6686 393.5518 354.9649 552.8316 -3.8766 389.4561 393.3327 354.7433 554.4305 -3.8724 389.2537 393.1261 354.5263 556.0295 -3.8655 389.0562 392.9217 354.3145 557.6435 -3.8463 388.8448 392.6910 354.0904 559.2408 -3.8325 388.6607 392.4932 353.8778 560.8545 -3.8268 388.4273 392.2541 353.6616 562.4683 -3.8209 388.2330 392.0539 353.4589 564.0675 -3.8169 388.0360 391.8529 353.2472 565.6811 -3.8070 387.8404 391.6475 353.0328 567.2796 -3.8078 387.6476 391.4554 352.8142 568.8786 -3.8012 387.4363 391.2375 352.6111 570.4926 -3.8110 387.2320 391.0430 352.4006 572.1068 -3.8127 387.0176 390.8303 352.2027 573.7056 -3.8043 386.8126 390.6170 351.9860 575.3196 -3.7978 386.5991 390.3969 351.7799 576.9186 -3.7931 386.3986 390.1918 351.5739 578.5325 -3.7886 386.2090 389.9976 351.3699 580.1465 -3.7818 385.9922 389.7740 351.1661 581.7455 -3.7760 385.7780 389.5540 350.9634 583.3595 -3.7693 385.5804 389.3497 350.7569 584.9585 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