DTA measure 3gyors Date: 2026324:1538 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1647.96 s Mass = 1154.700 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4704 -5.0443 464.8151 469.8594 432.6087 4.0841 -5.0512 464.7732 469.8243 432.8761 5.6874 -5.0618 464.7332 469.7951 433.1065 7.2806 -5.0771 464.7139 469.7909 433.2969 8.8788 -5.0863 464.6755 469.7618 433.4365 10.4769 -5.0940 464.6416 469.7355 433.4929 12.0855 -5.1038 464.5887 469.6925 433.4734 13.6886 -5.1120 464.5326 469.6446 433.3447 15.2973 -5.1138 464.5151 469.6289 433.1438 16.9161 -5.1262 464.4805 469.6067 432.8100 18.5194 -5.1352 464.4229 469.5581 432.4424 20.1279 -5.1379 464.3609 469.4988 432.0649 21.7313 -5.1455 464.3228 469.4683 431.6232 23.3449 -5.1479 464.2761 469.4240 431.1748 24.9330 -5.1488 464.2495 469.3983 430.6907 26.5415 -5.1543 464.2303 469.3846 430.2124 28.1551 -5.1518 464.1768 469.3285 429.7787 29.7535 -5.1516 464.0977 469.2493 429.3617 31.3720 -5.1433 464.0391 469.1824 428.9493 32.9806 -5.1427 463.9550 469.0977 428.6047 34.5839 -5.1463 463.9039 469.0503 428.2982 36.1924 -5.1375 463.8460 468.9835 428.0616 37.8009 -5.1363 463.7883 468.9246 427.8806 39.4093 -5.1368 463.7459 468.8827 427.7599 41.0179 -5.1369 463.6675 468.8044 427.6971 42.6265 -5.1396 463.5791 468.7187 427.6330 44.2503 -5.1360 463.4740 468.6100 427.5760 45.8538 -5.1367 463.3846 468.5212 427.5396 47.4573 -5.1359 463.2775 468.4134 427.5209 49.0655 -5.1401 463.2139 468.3540 427.4417 50.6690 -5.1464 463.1564 468.3028 427.3750 52.2775 -5.1441 463.0831 468.2272 427.2983 53.8809 -5.1456 463.0071 468.1527 427.1568 55.5048 -5.1483 462.9174 468.0657 426.9977 57.1080 -5.1518 462.8107 467.9625 426.8234 58.7115 -5.1561 462.7348 467.8910 426.5992 60.3254 -5.1566 462.6460 467.8026 426.3119 61.9286 -5.1569 462.5183 467.6752 426.0170 63.5320 -5.1563 462.3996 467.5558 425.7048 65.1303 -5.1606 462.3148 467.4754 425.4063 66.7284 -5.1609 462.2060 467.3670 425.1041 68.3319 -5.1617 462.1426 467.3044 424.7905 69.9301 -5.1594 462.0661 467.2255 424.4948 71.5335 -5.1515 461.9919 467.1433 424.2116 73.1268 -5.1528 461.8969 467.0498 423.9263 74.7249 -5.1503 461.7594 466.9097 423.6528 76.3231 -5.1497 461.6184 466.7682 423.4049 77.9318 -5.1455 461.4898 466.6353 423.1741 79.5350 -5.1437 461.3663 466.5100 422.9823 81.1384 -5.1419 461.2550 466.3970 422.7734 82.7468 -5.1408 461.1621 466.3029 422.5862 84.3501 -5.1437 461.0285 466.1722 422.4148 85.9585 -5.1413 460.9050 466.0463 422.2771 87.5465 -5.1385 460.7862 465.9247 422.1856 89.1550 -5.1372 460.6970 465.8342 422.0282 90.7583 -5.1362 460.6022 465.7384 421.8708 92.3720 -5.1383 460.4792 465.6176 421.7253 93.9753 -5.1357 460.3987 465.5345 421.5938 95.5991 -5.1325 460.2715 465.4039 421.4330 97.1873 -5.1401 460.1419 465.2820 421.2818 98.7906 -5.1394 460.0119 465.1514 421.0851 100.3991 -5.1371 459.8411 464.9782 420.8790 102.0025 -5.1362 459.6995 464.8357 420.6530 103.6109 -5.1335 459.5955 464.7290 420.4309 105.2144 -5.1292 459.4469 464.5761 420.2111 106.8230 -5.1278 459.3066 464.4344 419.9593 108.4415 -5.1224 459.2220 464.3444 419.6864 110.0450 -5.1287 459.0943 464.2230 419.4141 111.6536 -5.1288 458.9560 464.0848 419.1649 113.2569 -5.1248 458.8160 463.9408 418.9265 114.8655 -5.1149 458.6970 463.8118 418.6685 116.4689 -5.1125 458.5416 463.6541 418.4345 118.0773 -5.1122 458.3924 463.5046 418.1601 119.6859 -5.1126 458.2504 463.3630 417.9509 121.3096 -5.1051 458.0714 463.1765 417.7560 122.9234 -5.1004 457.9392 463.0396 417.5218 124.5268 -5.0969 457.7641 462.8611 417.2891 126.1299 -5.0962 457.5914 462.6876 417.0551 127.7180 -5.0934 457.4373 462.5307 416.8587 129.3213 -5.0912 457.2859 462.3771 416.7053 130.9195 -5.0894 457.1272 462.2166 416.5427 132.5229 -5.0878 456.9906 462.0784 416.3340 134.1261 -5.0826 456.8633 461.9459 416.1776 135.7296 -5.0858 456.7035 461.7893 415.9878 137.3278 -5.0898 456.5738 461.6635 415.7937 138.9313 -5.0855 456.4113 461.4968 415.6576 140.5296 -5.0825 456.2603 461.3427 415.4941 142.1481 -5.0834 456.0949 461.1784 415.3158 143.7516 -5.0772 455.9519 461.0292 415.1041 145.3550 -5.0766 455.8310 460.9076 414.8943 146.9429 -5.0773 455.6648 460.7421 414.7256 148.5464 -5.0723 455.4742 460.5465 414.4858 150.1548 -5.0722 455.2752 460.3474 414.2739 151.7634 -5.0718 455.1074 460.1792 414.0480 153.3873 -5.0645 454.9393 460.0038 413.7911 154.9956 -5.0581 454.7829 459.8410 413.5494 156.5838 -5.0508 454.6225 459.6733 413.2986 158.1920 -5.0507 454.4482 459.4988 413.0763 159.8006 -5.0475 454.3080 459.3555 412.8226 161.4039 -5.0408 454.1575 459.1984 412.5570 163.0226 -5.0376 454.0012 459.0388 412.3012 164.6261 -5.0371 453.8054 458.8425 412.0773 166.2346 -5.0308 453.6625 458.6933 411.8257 167.8585 -5.0285 453.5052 458.5338 411.6081 169.4619 -5.0260 453.3505 458.3765 411.3576 171.1113 -5.0224 453.1336 458.1560 411.1649 172.8735 -5.0146 452.9368 457.9513 410.9997 174.4921 -5.0145 452.7824 457.7970 410.8076 176.1006 -5.0112 452.6180 457.6292 410.6198 177.7040 -5.0090 452.4319 457.4409 410.4463 179.3124 -5.0049 452.2518 457.2567 410.2855 180.9159 -4.9987 452.0927 457.0913 410.1296 182.5295 -4.9960 451.9326 456.9286 409.9879 184.1329 -4.9997 451.7483 456.7480 409.8104 185.7568 -4.9891 451.5285 456.5176 409.6124 187.3653 -4.9828 451.3484 456.3312 409.4385 188.9738 -4.9852 451.1563 456.1415 409.2864 190.5774 -4.9818 450.9877 455.9696 409.0637 192.1651 -4.9819 450.8065 455.7884 408.8158 193.7686 -4.9745 450.6307 455.6052 408.5773 195.3723 -4.9678 450.4383 455.4061 408.3285 196.9808 -4.9625 450.2606 455.2231 408.0968 198.5688 -4.9602 450.0701 455.0304 407.8568 200.1876 -4.9553 449.8536 454.8089 407.6074 201.7908 -4.9534 449.6837 454.6371 407.3667 203.3994 -4.9507 449.5162 454.4669 407.1271 205.0079 -4.9479 449.3492 454.2971 406.8951 206.6111 -4.9452 449.1727 454.1179 406.6878 208.2198 -4.9431 449.0010 453.9441 406.4493 209.8229 -4.9419 448.7912 453.7331 406.2406 211.4416 -4.9357 448.6140 453.5497 405.9928 213.0398 -4.9300 448.4186 453.3486 405.7711 214.6483 -4.9275 448.1802 453.1077 405.5878 216.2515 -4.9279 448.0014 452.9293 405.3699 217.8600 -4.9250 447.8332 452.7582 405.1703 219.4634 -4.9255 447.6811 452.6066 404.9587 221.0718 -4.9242 447.5274 452.4515 404.7280 222.6855 -4.9213 447.3038 452.2251 404.5474 224.2889 -4.9130 447.1056 452.0187 404.3860 225.8974 -4.9066 446.9371 451.8437 404.1827 227.5213 -4.8986 446.7390 451.6376 403.9966 229.1246 -4.8934 446.5391 451.4325 403.8091 230.7331 -4.8914 446.3742 451.2656 403.5739 232.3418 -4.8910 446.2005 451.0915 403.4056 233.9503 -4.8853 445.9978 450.8832 403.2457 235.5588 -4.8819 445.7944 450.6763 403.0133 237.1621 -4.8769 445.5716 450.4485 402.8276 238.7705 -4.8776 445.3715 450.2491 402.6085 240.3945 -4.8792 445.1851 450.0643 402.4096 242.0030 -4.8766 444.9864 449.8630 402.2127 243.6114 -4.8717 444.8333 449.7050 401.9821 245.2198 -4.8682 444.6542 449.5224 401.7596 246.8281 -4.8619 444.4636 449.3255 401.5420 248.4368 -4.8544 444.2534 449.1077 401.3028 250.0399 -4.8467 444.0308 448.8774 401.0647 251.6588 -4.8432 443.8483 448.6915 400.8331 253.2723 -4.8328 443.6576 448.4904 400.6008 254.8756 -4.8249 443.4389 448.2638 400.3680 256.4791 -4.8250 443.2532 448.0782 400.1363 258.0669 -4.8238 443.0938 447.9177 399.9219 259.6653 -4.8164 442.9329 447.7493 399.6934 261.2686 -4.8134 442.7517 447.5651 399.4566 262.8719 -4.8079 442.5117 447.3195 399.2571 264.4854 -4.8013 442.2829 447.0842 399.0749 266.0938 -4.7986 442.1157 446.9142 398.8815 267.6921 -4.7935 441.9048 446.6984 398.6718 269.3006 -4.7934 441.6952 446.4885 398.4963 270.9039 -4.7924 441.4967 446.2891 398.2890 272.5023 -4.7868 441.2913 446.0781 398.1029 274.1106 -4.7772 441.0842 445.8614 397.8857 275.7295 -4.7699 440.9050 445.6749 397.7197 277.3381 -4.7618 440.7135 445.4753 397.5173 278.9414 -4.7546 440.4767 445.2313 397.3384 280.5449 -4.7547 440.2519 445.0067 397.1533 282.1534 -4.7494 440.0652 444.8147 396.9391 283.7618 -4.7391 439.8982 444.6373 396.7222 285.3703 -4.7374 439.7043 444.4417 396.4902 286.9788 -4.7338 439.5218 444.2556 396.2396 288.6026 -4.7292 439.2783 444.0075 396.0509 290.2111 -4.7219 439.0778 443.7997 395.8576 291.8195 -4.7150 438.8669 443.5820 395.6496 293.4280 -4.7067 438.6973 443.4040 395.4669 295.0363 -4.7045 438.5173 443.2218 395.2270 296.6346 -4.7098 438.3040 443.0138 395.0279 298.2430 -4.7068 438.0901 442.7969 394.7914 299.8464 -4.6971 437.8921 442.5892 394.5645 301.4550 -4.6948 437.6895 442.3843 394.3471 303.0789 -4.6861 437.4621 442.1482 394.1196 304.6823 -4.6820 437.2399 441.9218 393.9055 306.3063 -4.6744 437.0586 441.7330 393.6752 307.9095 -4.6685 436.8702 441.5386 393.4708 309.5181 -4.6641 436.6827 441.3468 393.2379 311.1218 -4.6567 436.4892 441.1459 393.0319 312.7251 -4.6510 436.2724 440.9234 392.8303 314.3335 -4.6417 436.0370 440.6787 392.6456 315.9319 -4.6348 435.8111 440.4458 392.4303 317.5403 -4.6315 435.6312 440.2627 392.1941 319.1643 -4.6290 435.4448 440.0738 391.9669 320.7624 -4.6251 435.2428 439.8678 391.7738 322.3454 -4.6177 435.0251 439.6429 391.5615 323.9489 -4.6137 434.8151 439.4288 391.3576 325.5419 -4.6100 434.6257 439.2357 391.1537 327.1555 -4.6058 434.4311 439.0368 390.9024 328.7436 -4.5965 434.1964 438.7929 390.7032 330.3470 -4.5919 433.9924 438.5844 390.4973 331.9453 -4.5908 433.7805 438.3713 390.3160 333.5488 -4.5875 433.5793 438.1669 390.1261 335.1624 -4.5798 433.3923 437.9721 389.9258 336.7555 -4.5741 433.1826 437.7568 389.7857 338.3744 -4.5677 432.9512 437.5189 389.5693 339.9673 -4.5623 432.7212 437.2835 389.3427 341.5708 -4.5573 432.5317 437.0890 389.1324 343.1741 -4.5500 432.2951 436.8451 388.9094 344.7826 -4.5399 432.0965 436.6365 388.6722 346.3809 -4.5341 431.8706 436.4047 388.4331 347.9843 -4.5323 431.6767 436.2089 388.2161 349.5979 -4.5240 431.4860 436.0099 388.0057 351.2014 -4.5273 431.2844 435.8117 387.7622 352.8098 -4.5226 431.0792 435.6018 387.5443 354.3978 -4.5125 430.8827 435.3952 387.3475 356.0165 -4.5070 430.6900 435.1970 387.1372 357.6353 -4.4973 430.4723 434.9695 386.9242 359.2386 -4.4903 430.2802 434.7706 386.7003 360.8318 -4.4885 430.0875 434.5760 386.4522 362.4401 -4.4829 429.8682 434.3511 386.2307 364.0436 -4.4779 429.6489 434.1267 386.0303 365.6519 -4.4734 429.4321 433.9055 385.7965 367.2605 -4.4655 429.2048 433.6703 385.6082 368.8689 -4.4603 428.9957 433.4560 385.3982 370.4928 -4.4541 428.7712 433.2253 385.1963 372.0860 -4.4515 428.5960 433.0475 385.0141 373.6891 -4.4469 428.3993 432.8462 384.8339 375.2978 -4.4416 428.1738 432.6154 384.6163 376.9011 -4.4313 427.9379 432.3692 384.4096 378.5098 -4.4224 427.7245 432.1469 384.1568 380.1184 -4.4159 427.5080 431.9240 383.9696 381.7268 -4.4084 427.3095 431.7179 383.7691 383.3455 -4.4028 427.0999 431.5027 383.5641 384.9439 -4.3953 426.8966 431.2919 383.3981 386.5474 -4.3884 426.6873 431.0757 383.1898 388.1301 -4.3844 426.4790 430.8634 383.0142 389.7336 -4.3759 426.2779 430.6538 382.8096 391.3370 -4.3712 426.0855 430.4567 382.5662 392.9351 -4.3699 425.8562 430.2261 382.3159 394.5386 -4.3658 425.6454 430.0113 382.1002 396.1471 -4.3621 425.4458 429.8079 381.8587 397.7556 -4.3518 425.2312 429.5830 381.6264 399.3641 -4.3453 425.0125 429.3578 381.4356 400.9674 -4.3411 424.8141 429.1551 381.2374 402.5606 -4.3401 424.6172 428.9573 381.0144 404.1638 -4.3365 424.4094 428.7460 380.7328 405.7671 -4.3251 424.1909 428.5160 380.4808 407.3756 -4.3203 423.9928 428.3131 380.2791 408.9893 -4.3120 423.7872 428.0991 380.1116 410.5926 -4.3072 423.5670 427.8742 379.9360 412.2164 -4.3016 423.3401 427.6417 379.7370 413.8199 -4.2965 423.1256 427.4220 379.5388 415.4285 -4.2927 422.8693 427.1620 379.3229 417.0369 -4.2911 422.6781 426.9692 379.1463 418.6404 -4.2825 422.4725 426.7550 378.9632 420.2490 -4.2746 422.2397 426.5143 378.7569 421.8574 -4.2720 422.0399 426.3119 378.5473 423.4609 -4.2670 421.8779 426.1449 378.3578 425.0846 -4.2584 421.6758 425.9342 378.1288 426.6881 -4.2527 421.4441 425.6968 377.8811 428.3018 -4.2430 421.2599 425.5029 377.6568 429.9103 -4.2367 421.0387 425.2754 377.4511 431.5136 -4.2346 420.8133 425.0480 377.2518 433.1170 -4.2296 420.5720 424.8016 377.0544 434.7255 -4.2245 420.3640 424.5884 376.8525 436.3289 -4.2182 420.1781 424.3962 376.6296 437.9529 -4.2121 419.9667 424.1788 376.4688 439.5561 -4.2112 419.7457 423.9569 376.2472 441.1699 -4.2116 419.4848 423.6964 376.0394 442.7731 -4.2059 419.2863 423.4922 375.8661 444.3866 -4.1989 419.0612 423.2601 375.6648 445.9900 -4.1903 418.9005 423.0908 375.4499 447.5984 -4.1818 418.6816 422.8634 375.2256 449.1968 -4.1709 418.5056 422.6765 375.0029 450.8000 -4.1648 418.2816 422.4464 374.7716 452.3983 -4.1583 418.0503 422.2086 374.5441 454.0015 -4.1592 417.8255 421.9846 374.3364 455.6050 -4.1558 417.6128 421.7685 374.1334 457.2135 -4.1477 417.3959 421.5436 373.9077 458.8116 -4.1395 417.1628 421.3022 373.6317 460.4150 -4.1277 416.9695 421.0972 373.4199 462.0081 -4.1266 416.7748 420.9014 373.1920 463.6268 -4.1270 416.5680 420.6950 372.9886 465.2354 -4.1200 416.3875 420.5075 372.7537 466.8336 -4.1166 416.1800 420.2966 372.5229 468.4370 -4.1045 415.9700 420.0745 372.3193 470.0508 -4.1025 415.7197 419.8222 372.1057 471.6593 -4.0970 415.5053 419.6023 371.9296 473.2678 -4.0869 415.2707 419.3576 371.7581 474.8866 -4.0801 415.0492 419.1293 371.5780 476.4798 -4.0710 414.8581 418.9291 371.3834 478.0881 -4.0669 414.6652 418.7321 371.1818 479.7019 -4.0610 414.4729 418.5339 370.9824 481.3103 -4.0615 414.2485 418.3100 370.7866 482.9189 -4.0541 413.9975 418.0516 370.5748 484.5223 -4.0462 413.7449 417.7911 370.3511 486.1306 -4.0342 413.5424 417.5766 370.1345 487.7494 -4.0292 413.3668 417.3959 369.9343 489.3424 -4.0243 413.1697 417.1940 369.7366 490.9715 -4.0235 412.9129 416.9364 369.5318 492.5750 -4.0185 412.7223 416.7408 369.3330 494.1834 -4.0161 412.4932 416.5093 369.1057 495.7869 -4.0154 412.2875 416.3030 368.8836 497.3903 -4.0054 412.0964 416.1017 368.6766 498.9986 -3.9922 411.9044 415.8966 368.4351 500.6175 -3.9852 411.6764 415.6616 368.2143 502.2260 -3.9787 411.4529 415.4317 367.9778 503.8294 -3.9757 411.2251 415.2008 367.7722 505.4379 -3.9669 410.9791 414.9460 367.5513 507.0413 -3.9567 410.7601 414.7168 367.3161 508.6549 -3.9521 410.5506 414.5027 367.0879 510.2635 -3.9476 410.3617 414.3094 366.8676 511.8821 -3.9383 410.1365 414.0748 366.6176 513.4856 -3.9374 409.9192 413.8567 366.3972 515.0840 -3.9378 409.7174 413.6551 366.2034 516.6770 -3.9296 409.5064 413.4361 366.0161 518.2754 -3.9225 409.2794 413.2019 365.8204 519.8736 -3.9148 409.0811 412.9960 365.6351 521.4820 -3.9132 408.8350 412.7482 365.4440 523.0854 -3.9032 408.6182 412.5214 365.2448 524.7040 -3.8921 408.4000 412.2921 365.0449 526.3126 -3.8903 408.2174 412.1077 364.8151 527.9159 -3.8849 408.0049 411.8898 364.6169 529.5089 -3.8760 407.7932 411.6692 364.4112 531.1123 -3.8736 407.5720 411.4456 364.1871 532.7206 -3.8700 407.3967 411.2668 363.9897 534.3241 -3.8695 407.2014 411.0709 363.7974 535.9274 -3.8590 406.9613 410.8203 363.5901 537.5564 -3.8435 406.6993 410.5428 363.3807 539.1598 -3.8361 406.4916 410.3277 363.1567 540.7579 -3.8272 406.3108 410.1380 362.9583 542.3614 -3.8172 406.1017 409.9189 362.7469 543.9699 -3.8124 405.9104 409.7228 362.5212 545.5733 -3.8053 405.6844 409.4897 362.3161 547.1819 -3.7950 405.4616 409.2566 362.1061 548.7904 -3.7922 405.2541 409.0463 361.8888 550.4040 -3.7896 405.0387 408.8284 361.6506 552.0230 -3.7895 404.8284 408.6179 361.4249 553.6265 -3.7860 404.6224 408.4084 361.1923 555.2298 -3.7759 404.4143 408.1902 360.9964 556.8384 -3.7697 404.1832 407.9530 360.7832 558.4573 -3.7658 403.9831 407.7489 360.5858 560.0656 -3.7593 403.7741 407.5334 360.3636 561.6846 -3.7601 403.5204 407.2805 360.1370 563.2983 -3.7573 403.3341 407.0914 359.9549 564.9015 -3.7459 403.1326 406.8786 359.7692 566.5101 -3.7428 402.9239 406.6668 359.5655 568.1136 -3.7382 402.6696 406.4078 359.3556 569.7169 -3.7266 402.4733 406.1999 359.1353 571.4793 -3.7139 402.2144 405.9283 358.8881 573.1340 -3.7059 401.9600 405.6659 358.6626 574.7371 -3.7026 401.7683 405.4709 358.4707 576.3458 -3.6954 401.5673 405.2628 358.2315 577.9440 -3.6956 401.3564 405.0520 357.9888 579.5626 -3.6942 401.1377 404.8319 357.7612 581.1456 -3.6820 400.9055 404.5875 357.5539 582.7643 -3.6770 400.6690 404.3460 357.3655 584.3626 -3.6688 400.4538 404.1226 357.1150 585.9660 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