DTA measure 1gyors_le Date: 2024123:1414 Lower limit = 220.0 C Upper limit = 440.0 C Rate = 8.00 C/min Mtime = 1647.98 s Mass = 957.100 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3655 -4.5452 409.8306 414.3758 411.5426 3.9929 -4.5426 409.8643 414.4069 411.5138 5.5856 -4.5421 409.8937 414.4358 411.5065 7.1776 -4.5425 409.9381 414.4806 411.4969 8.7845 -4.5465 409.9901 414.5366 411.4799 10.3766 -4.5462 410.0320 414.5781 411.4565 11.9994 -4.5426 410.0657 414.6083 411.4114 13.5966 -4.5389 410.1272 414.6661 411.3731 15.1955 -4.5383 410.1486 414.6869 411.3066 16.8095 -4.5391 410.2005 414.7396 411.2039 18.4085 -4.5359 410.2343 414.7703 411.1237 20.0225 -4.5378 410.2697 414.8075 411.0007 21.6365 -4.5416 410.3063 414.8479 410.8675 23.2355 -4.5431 410.3392 414.8823 410.7365 24.8343 -4.5393 410.3701 414.9093 410.5752 26.4333 -4.5356 410.4125 414.9480 410.4137 28.0621 -4.5341 410.4462 414.9803 410.2205 29.6610 -4.5329 410.4707 415.0036 410.0225 31.2748 -4.5304 410.5013 415.0316 409.8110 32.8738 -4.5251 410.5403 415.0654 409.6013 34.4878 -4.5113 410.5571 415.0684 409.3908 36.1026 -4.5022 410.5794 415.0816 409.1671 37.7141 -4.4987 410.6149 415.1136 408.9423 39.3050 -4.4936 410.6265 415.1201 408.7152 40.8971 -4.4869 410.6405 415.1274 408.4974 42.5049 -4.4786 410.6589 415.1375 408.2444 44.1121 -4.4669 410.6772 415.1441 408.0223 45.7228 -4.4572 410.6896 415.1468 407.7788 47.3193 -4.4473 410.6884 415.1357 407.5569 48.9179 -4.4417 410.7001 415.1418 407.3228 50.5319 -4.4343 410.7037 415.1381 407.0927 52.1459 -4.4259 410.7158 415.1417 406.8803 53.7600 -4.4169 410.7262 415.1431 406.6473 55.3598 -4.4071 410.7110 415.1181 406.4211 56.9588 -4.4004 410.7175 415.1179 406.2003 58.5728 -4.3886 410.7094 415.0980 405.9745 60.1869 -4.3751 410.7082 415.0833 405.7559 61.8009 -4.3627 410.7074 415.0701 405.5389 63.3998 -4.3532 410.6947 415.0480 405.3228 65.0141 -4.3472 410.6996 415.0469 405.1154 66.6143 -4.3383 410.6657 415.0040 404.9169 68.2438 -4.3274 410.6764 415.0038 404.7049 69.8399 -4.3181 410.6526 414.9706 404.4963 71.4305 -4.3136 410.6354 414.9490 404.3032 73.0376 -4.3064 410.6061 414.9126 404.1143 74.6290 -4.2950 410.5835 414.8784 403.9115 76.2520 -4.2860 410.5553 414.8413 403.7157 77.8461 -4.2799 410.5435 414.8234 403.5365 79.4430 -4.2730 410.5281 414.8011 403.3641 81.0566 -4.2635 410.4826 414.7462 403.1597 82.6558 -4.2560 410.4516 414.7076 402.9730 84.2699 -4.2482 410.4349 414.6832 402.7834 85.8838 -4.2416 410.4002 414.6418 402.6163 87.4826 -4.2332 410.3595 414.5927 402.4465 89.0816 -4.2232 410.3182 414.5414 402.2718 90.6806 -4.2133 410.2900 414.5033 402.1092 92.3096 -4.2080 410.2454 414.4534 401.9347 93.9086 -4.1980 410.2123 414.4103 401.7706 95.5228 -4.1921 410.1531 414.3451 401.5920 97.1225 -4.1871 410.1157 414.3028 401.4277 98.7220 -4.1777 410.0638 414.2415 401.2387 100.3515 -4.1692 410.0225 414.1917 401.0554 101.9616 -4.1635 409.9577 414.1212 400.8738 103.5530 -4.1541 409.9295 414.0836 400.6942 105.1444 -4.1503 409.8658 414.0161 400.5161 106.7523 -4.1461 409.8112 413.9573 400.3246 108.3613 -4.1399 409.7485 413.8884 400.1553 109.9723 -4.1344 409.7043 413.8387 399.9617 111.5688 -4.1282 409.6363 413.7644 399.7591 113.1675 -4.1210 409.5906 413.7117 399.5803 114.7815 -4.1138 409.5255 413.6393 399.3712 116.3955 -4.1091 409.4703 413.5794 399.1916 118.0095 -4.1024 409.4036 413.5059 398.9839 119.6085 -4.0976 409.3253 413.4229 398.7989 121.2225 -4.0927 409.2641 413.3568 398.5893 122.8215 -4.0854 409.2021 413.2874 398.4073 124.4505 -4.0782 409.1372 413.2153 398.2080 126.0495 -4.0698 409.0818 413.1517 398.0142 127.6635 -4.0640 408.9985 413.0625 397.8303 129.2630 -4.0583 408.9163 412.9746 397.6414 130.8770 -4.0513 408.8305 412.8818 397.4187 132.4919 -4.0410 408.7544 412.7954 397.2305 134.0873 -4.0326 408.7072 412.7399 397.0402 135.6785 -4.0257 408.6050 412.6307 396.8297 137.2853 -4.0212 408.5265 412.5477 396.6160 138.8776 -4.0132 408.4388 412.4520 396.4279 140.5005 -4.0070 408.3505 412.3575 396.2196 142.0970 -3.9985 408.2800 412.2785 396.0114 143.6955 -3.9901 408.1948 412.1849 395.8093 145.2945 -3.9838 408.1054 412.0892 395.6032 146.9085 -3.9754 408.0198 411.9952 395.3878 148.5225 -3.9696 407.9372 411.9068 395.1868 150.1215 -3.9626 407.8484 411.8110 394.9764 151.7355 -3.9559 407.7470 411.7029 394.7761 153.3341 -3.9523 407.6670 411.6193 394.5609 154.9331 -3.9466 407.5766 411.5232 394.3765 156.5620 -3.9390 407.4683 411.4074 394.1531 158.1618 -3.9348 407.3710 411.3058 393.9651 159.7760 -3.9293 407.2762 411.2055 393.7709 161.3761 -3.9240 407.1746 411.0986 393.5727 162.9763 -3.9160 407.0619 410.9780 393.3705 164.6059 -3.9065 406.9662 410.8726 393.1684 166.2198 -3.9010 406.8668 410.7678 392.9739 167.8120 -3.8950 406.7546 410.6496 392.7838 169.4035 -3.8868 406.6546 410.5414 392.5808 171.0101 -3.8814 406.5565 410.4379 392.3894 172.6171 -3.8761 406.4609 410.3370 392.1933 174.2248 -3.8698 406.3251 410.1949 392.0097 175.8205 -3.8611 406.2333 410.0943 391.8100 177.4339 -3.8563 406.1195 409.9758 391.6151 179.0328 -3.8544 405.9920 409.8463 391.4273 180.6620 -3.8478 405.8985 409.7463 391.2338 182.2608 -3.8408 405.7891 409.6299 391.0321 183.8598 -3.8333 405.6815 409.5149 390.8550 185.4588 -3.8271 405.5529 409.3800 390.6451 187.0728 -3.8223 405.4521 409.2745 390.4548 188.6869 -3.8118 405.3177 409.1295 390.2564 190.3019 -3.8044 405.1977 409.0021 390.0540 191.9006 -3.7979 405.0793 408.8772 389.8577 193.4996 -3.7911 404.9732 408.7643 389.6533 195.1136 -3.7860 404.8582 408.6442 389.4568 196.7284 -3.7806 404.7280 408.5086 389.2454 198.3413 -3.7743 404.5967 408.3709 389.0425 199.9330 -3.7652 404.4823 408.2475 388.8602 201.5246 -3.7558 404.3446 408.1004 388.6739 203.1316 -3.7471 404.2332 407.9802 388.4583 204.7393 -3.7421 404.1046 407.8467 388.2839 206.3496 -3.7392 403.9724 407.7116 388.0841 207.9473 -3.7342 403.8378 407.5720 387.8947 209.5456 -3.7280 403.7027 407.4308 387.6917 211.1448 -3.7214 403.5848 407.3062 387.5072 212.7736 -3.7152 403.4524 407.1676 387.2987 214.3729 -3.7061 403.3239 407.0300 387.0900 215.9868 -3.7008 403.1807 406.8815 386.8760 217.5856 -3.6960 403.0485 406.7445 386.6663 219.1846 -3.6860 402.9268 406.6129 386.4527 220.8135 -3.6782 402.7866 406.4648 386.2463 222.4125 -3.6726 402.6488 406.3214 386.0383 224.0265 -3.6658 402.5013 406.1671 385.8288 225.6255 -3.6615 402.3651 406.0266 385.6303 227.2401 -3.6569 402.2314 405.8883 385.4141 228.8553 -3.6510 402.0978 405.7488 385.2088 230.4673 -3.6437 401.9478 405.5914 384.9804 232.0599 -3.6373 401.8028 405.4401 384.8038 233.6510 -3.6340 401.6767 405.3107 384.6029 235.2576 -3.6329 401.5480 405.1809 384.3935 236.8648 -3.6258 401.3961 405.0219 384.1967 238.4719 -3.6204 401.2452 404.8656 384.0147 240.0644 -3.6120 401.1174 404.7295 383.8049 241.6789 -3.6037 400.9737 404.5775 383.6102 243.2785 -3.6042 400.8239 404.4281 383.4055 244.8925 -3.5989 400.6821 404.2810 383.2186 246.4915 -3.5943 400.5464 404.1408 383.0210 248.1056 -3.5852 400.3854 403.9706 382.8310 249.7045 -3.5821 400.2398 403.8219 382.6431 251.3041 -3.5777 400.0877 403.6654 382.4484 252.9335 -3.5738 399.9472 403.5211 382.2545 254.5324 -3.5685 399.7890 403.3575 382.0532 256.1468 -3.5653 399.6304 403.1957 381.8527 257.7461 -3.5578 399.4994 403.0571 381.6424 259.3449 -3.5517 399.3584 402.9101 381.4494 260.9739 -3.5381 399.2137 402.7518 381.2332 262.5701 -3.5362 399.0376 402.5738 381.0400 264.1761 -3.5332 398.8765 402.4096 380.8125 265.7678 -3.5305 398.7230 402.2535 380.6101 267.3745 -3.5205 398.5826 402.1031 380.4022 268.9816 -3.5111 398.4289 401.9400 380.1885 270.5904 -3.5020 398.2878 401.7898 379.9845 272.1868 -3.4965 398.1227 401.6193 379.7839 273.7874 -3.4946 397.9775 401.4721 379.5708 275.4028 -3.4927 397.8073 401.2999 379.3626 277.0185 -3.4834 397.6544 401.1379 379.1497 278.6174 -3.4807 397.4877 400.9684 378.9564 280.2309 -3.4751 397.3328 400.8080 378.7435 281.8338 -3.4716 397.1766 400.6481 378.5396 283.4340 -3.4746 397.0217 400.4963 378.3243 285.0479 -3.4796 396.8537 400.3333 378.1154 286.6619 -3.4792 396.7035 400.1828 377.9151 288.2608 -3.4736 396.5307 400.0042 377.7147 289.8751 -3.4686 396.3751 399.8437 377.5001 291.4748 -3.4641 396.2266 399.6908 377.2984 293.0889 -3.4592 396.0493 399.5085 377.0850 294.7026 -3.4539 395.8905 399.3444 376.8960 296.2974 -3.4454 395.7247 399.1702 376.6868 297.9040 -3.4406 395.5541 398.9947 376.5012 299.4964 -3.4377 395.4042 398.8419 376.2920 301.1040 -3.4254 395.2450 398.6704 376.1103 302.7116 -3.4196 395.0585 398.4781 375.9017 304.3063 -3.4118 394.8973 398.3092 375.7006 305.9198 -3.4106 394.7361 398.1467 375.5099 307.5188 -3.4070 394.5570 397.9640 375.3049 309.1178 -3.4027 394.4107 397.8134 375.1151 310.7470 -3.3877 394.2361 397.6238 374.9266 312.3458 -3.3771 394.0873 397.4644 374.7146 313.9449 -3.3707 393.9100 397.2806 374.5270 315.5588 -3.3660 393.7340 397.1000 374.3355 317.1578 -3.3583 393.5646 396.9229 374.1151 318.7869 -3.3533 393.3907 396.7440 373.8970 320.3856 -3.3465 393.2342 396.5807 373.7003 321.9996 -3.3433 393.0633 396.4066 373.5057 323.5985 -3.3378 392.8901 396.2279 373.3022 325.2125 -3.3352 392.7052 396.0403 373.0883 326.8273 -3.3294 392.5445 395.8738 372.9081 328.4209 -3.3251 392.3746 395.6997 372.7042 330.0270 -3.3212 392.1962 395.5174 372.4954 331.6188 -3.3163 392.0331 395.3494 372.2850 333.2409 -3.3088 391.8699 395.1787 372.0836 334.8485 -3.3031 391.6909 394.9940 371.8808 336.4443 -3.2976 391.5024 394.8000 371.6738 338.0566 -3.2949 391.3335 394.6284 371.4741 339.6558 -3.2876 391.1633 394.4509 371.2795 341.2696 -3.2824 390.9802 394.2626 371.0723 342.8836 -3.2775 390.8186 394.0961 370.8717 344.4826 -3.2698 390.6393 393.9092 370.6781 346.0816 -3.2660 390.4594 393.7254 370.4770 347.6955 -3.2614 390.2922 393.5536 370.2858 349.3095 -3.2565 390.1062 393.3628 370.0862 350.9235 -3.2520 389.9457 393.1976 369.8834 352.5225 -3.2504 389.7731 393.0234 369.6773 354.1215 -3.2443 389.5799 392.8242 369.4907 355.7355 -3.2375 389.4128 392.6503 369.2848 357.3495 -3.2321 389.2369 392.4690 369.0992 358.9633 -3.2271 389.0654 392.2925 368.8968 360.5569 -3.2188 388.8798 392.0986 368.6981 362.1486 -3.2146 388.7066 391.9212 368.4920 363.7561 -3.2109 388.5139 391.7247 368.2792 365.3643 -3.2044 388.3521 391.5565 368.0770 366.9740 -3.1994 388.1789 391.3783 367.8719 368.5715 -3.1969 387.9876 391.1845 367.6603 370.1706 -3.1935 387.8179 391.0113 367.4685 371.7845 -3.1878 387.6321 390.8199 367.2440 373.4001 -3.1838 387.4414 390.6252 367.0494 375.0015 -3.1763 387.2647 390.4410 366.8483 376.6155 -3.1740 387.0922 390.2662 366.6381 378.2145 -3.1648 386.9134 390.0782 366.4253 379.8285 -3.1610 386.7410 389.9020 366.2134 381.4425 -3.1538 386.5608 389.7147 365.9916 383.0564 -3.1469 386.3660 389.5129 365.7816 384.6554 -3.1450 386.1824 389.3274 365.5642 386.2543 -3.1371 386.0149 389.1521 365.3619 387.8679 -3.1328 385.8396 388.9724 365.1582 389.4970 -3.1260 385.6412 388.7672 364.9519 391.0951 -3.1232 385.4574 388.5806 364.7384 392.6881 -3.1165 385.2628 388.3794 364.5437 394.2791 -3.1108 385.0851 388.1959 364.3378 395.8853 -3.1094 384.9167 388.0260 364.1351 397.4925 -3.1054 384.7342 387.8396 363.9176 399.1008 -3.0991 384.5460 387.6451 363.7308 400.6973 -3.0935 384.3782 387.4716 363.5250 402.2963 -3.0874 384.1821 387.2695 363.3038 403.9105 -3.0835 383.9988 387.0823 363.1034 405.5244 -3.0775 383.8048 386.8823 362.9123 407.1385 -3.0753 383.6288 386.7041 362.7255 408.7373 -3.0726 383.4416 386.5142 362.5150 410.3360 -3.0679 383.2632 386.3312 362.3164 411.9498 -3.0608 383.0659 386.1267 362.1201 413.5790 -3.0550 382.8951 385.9501 361.9104 415.1779 -3.0516 382.6994 385.7509 361.7057 416.7778 -3.0482 382.5105 385.5587 361.5083 418.3918 -3.0424 382.3408 385.3832 361.3249 420.0059 -3.0401 382.1512 385.1913 361.1368 421.6198 -3.0347 381.9597 384.9944 360.9221 423.2336 -3.0265 381.7792 384.8057 360.7234 424.8299 -3.0203 381.5906 384.6110 360.5165 426.4198 -3.0157 381.4051 384.4208 360.3148 428.0405 -3.0135 381.2023 384.2158 360.1045 429.6471 -3.0096 381.0157 384.0254 359.9046 431.2400 -3.0054 380.8371 383.8425 359.7031 432.8359 -3.0025 380.6373 383.6398 359.5079 434.4488 -2.9968 380.4519 383.4487 359.3075 436.0629 -2.9903 380.2696 383.2598 359.0848 437.6769 -2.9842 380.0892 383.0733 358.8756 439.2758 -2.9783 379.8967 382.8750 358.6663 440.8898 -2.9735 379.7112 382.6847 358.4681 442.4888 -2.9703 379.5179 382.4882 358.2624 444.1181 -2.9659 379.3316 382.2975 358.0493 445.7168 -2.9601 379.1393 382.0994 357.8211 447.3306 -2.9547 378.9551 381.9098 357.6218 448.9298 -2.9545 378.7561 381.7106 357.4171 450.5435 -2.9491 378.5560 381.5050 357.2084 452.1575 -2.9436 378.3768 381.3204 357.0037 453.7565 -2.9369 378.1929 381.1298 356.7984 455.3705 -2.9337 377.9972 380.9309 356.5944 456.9661 -2.9309 377.8121 380.7430 356.3786 458.5720 -2.9253 377.6281 380.5533 356.1783 460.1798 -2.9203 377.4334 380.3537 355.9648 461.7721 -2.9146 377.2369 380.1515 355.7714 463.3818 -2.9099 377.0599 379.9698 355.5686 464.9778 -2.9074 376.8826 379.7900 355.3718 466.5908 -2.9023 376.6779 379.5801 355.1518 468.2048 -2.8981 376.4855 379.3836 354.9506 469.8035 -2.8901 376.2989 379.1890 354.7644 471.4025 -2.8828 376.1115 378.9943 354.5653 473.0165 -2.8717 375.9088 378.7805 354.3606 474.6155 -2.8707 375.7352 378.6059 354.1419 476.2445 -2.8653 375.5267 378.3921 353.9439 477.8435 -2.8619 375.3285 378.1903 353.7433 479.4425 -2.8564 375.1477 378.0041 353.5434 481.0565 -2.8519 374.9610 377.8129 353.3390 482.6705 -2.8492 374.7704 377.6196 353.1203 484.2845 -2.8423 374.5781 377.4204 352.9028 485.8845 -2.8385 374.3800 377.2186 352.7053 487.4981 -2.8345 374.2033 377.0378 352.4916 489.0926 -2.8257 374.0101 376.8358 352.2851 490.6988 -2.8212 373.8109 376.6320 352.0735 492.3056 -2.8172 373.6165 376.4337 351.8478 493.9133 -2.8178 373.4258 376.2436 351.6504 495.5073 -2.8103 373.2277 376.0380 351.4257 497.1055 -2.8054 373.0275 375.8329 351.2244 498.7345 -2.7995 372.8286 375.6281 351.0126 500.3335 -2.7931 372.6459 375.4390 350.8113 501.9475 -2.7861 372.4719 375.2580 350.6002 503.5465 -2.7828 372.2589 375.0417 350.3846 505.1455 -2.7785 372.0687 374.8472 350.1783 506.7745 -2.7728 371.8762 374.6490 349.9862 508.3735 -2.7691 371.6971 374.4662 349.7726 509.9874 -2.7653 371.4934 374.2587 349.5708 511.5860 -2.7598 371.2998 374.0596 349.3790 513.2000 -2.7512 371.1042 373.8554 349.1696 514.8145 -2.7479 370.9169 373.6648 348.9649 516.4329 -2.7433 370.7257 373.4689 348.7594 518.0330 -2.7383 370.5262 373.2645 348.5676 519.6331 -2.7362 370.3354 373.0716 348.3580 521.2443 -2.7285 370.1378 372.8663 348.1721 522.8513 -2.7206 369.9454 372.6660 347.9747 524.4593 -2.7174 369.7573 372.4747 347.7581 526.0520 -2.7127 369.5642 372.2769 347.5714 527.6615 -2.7066 369.3573 372.0639 347.3854 529.2593 -2.7018 369.1695 371.8713 347.1792 530.8884 -2.6973 368.9702 371.6675 346.9833 532.4870 -2.6944 368.7842 371.4786 346.7994 534.0861 -2.6912 368.5873 371.2784 346.5928 535.6850 -2.6876 368.3987 371.0863 346.4002 537.2991 -2.6837 368.2075 370.8913 346.2117 538.9130 -2.6778 368.0053 370.6831 346.0258 540.5269 -2.6714 367.8077 370.4792 345.8237 542.1258 -2.6686 367.6148 370.2834 345.6254 543.7248 -2.6671 367.4275 370.0946 345.4148 545.3390 -2.6649 367.2339 369.8988 345.2220 546.9549 -2.6563 367.0316 369.6879 345.0095 548.5688 -2.6547 366.8312 369.4859 344.8235 550.1676 -2.6522 366.6346 369.2867 344.6225 551.7816 -2.6512 366.4518 369.1030 344.4095 553.3788 -2.6469 366.2633 368.9102 344.2225 554.9861 -2.6368 366.0599 368.6967 344.0135 556.5924 -2.6328 365.8543 368.4872 343.8021 558.1843 -2.6301 365.6692 368.2993 343.5951 559.7918 -2.6274 365.4758 368.1033 343.3951 561.3989 -2.6156 365.2900 367.9056 343.1768 563.0093 -2.6102 365.0873 367.6974 342.9768 564.6069 -2.6085 364.8911 367.4996 342.7835 566.2058 -2.6100 364.6950 367.3050 342.5701 567.8198 -2.6083 364.4942 367.1024 342.3611 569.4188 -2.6097 364.3041 366.9138 342.1544 571.0479 -2.6077 364.1161 366.7238 341.9439 572.6468 -2.6018 363.9224 366.5242 341.7515 574.2458 -2.5948 363.7379 366.3327 341.5403 575.8595 -2.5892 363.5335 366.1227 341.3413 577.4585 -2.5877 363.3212 365.9089 341.1233 579.0875 -2.5839 363.1319 365.7157 340.9084 580.6865 -2.5775 362.9410 365.5185 340.7006 582.2855 -2.5709 362.7288 365.2997 340.4933 583.8995 -2.5672 362.5441 365.1113 340.2769 585.5115 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