DTA measure 1lassufuteshutes Date: 2026331:1157 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.46 s Mass = 1156.200 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2000 -1.0811 218.1022 219.1834 249.0257 2.0280 -1.0875 218.2150 219.3025 248.9699 2.8038 -1.0892 218.3326 219.4218 248.9199 3.6420 -1.0910 218.4607 219.5517 248.8484 4.3983 -1.0953 218.5497 219.6450 248.7898 5.2358 -1.1001 218.6509 219.7510 248.7541 6.0328 -1.1062 218.7389 219.8450 248.6973 6.8300 -1.1064 218.8316 219.9380 248.6392 7.6468 -1.1037 218.9383 220.0420 248.6308 8.4235 -1.1026 219.0567 220.1592 248.6318 9.2728 -1.1059 219.2034 220.3093 248.5566 10.0395 -1.1072 219.2718 220.3790 248.4963 10.8675 -1.1031 219.3551 220.4582 248.4399 11.6648 -1.0964 219.4527 220.5492 248.4030 12.4620 -1.0906 219.5274 220.6180 248.3548 13.2798 -1.0890 219.5887 220.6777 248.3183 14.0565 -1.0877 219.6833 220.7710 248.2719 14.9153 -1.0881 219.7839 220.8720 248.2658 15.6818 -1.0852 219.8723 220.9575 248.2162 16.4995 -1.0817 220.0110 221.0927 248.1639 17.3070 -1.0777 220.1358 221.2135 248.1489 18.0940 -1.0733 220.2461 221.3194 248.1482 18.9220 -1.0720 220.3756 221.4475 248.1658 19.6888 -1.0717 220.4971 221.5688 248.1676 20.5380 -1.0741 220.6187 221.6929 248.1640 21.3045 -1.0759 220.7190 221.7950 248.1333 22.1325 -1.0777 220.7973 221.8750 248.0836 22.9195 -1.0735 220.8555 221.9290 248.0690 23.7065 -1.0682 220.9624 222.0307 248.0735 24.5140 -1.0659 221.0705 222.1364 248.0684 25.3010 -1.0680 221.2114 222.2795 248.1115 26.1188 -1.0667 221.3396 222.4063 248.1313 26.8955 -1.0611 221.4224 222.4835 248.1483 27.7448 -1.0587 221.5183 222.5770 248.1649 28.5115 -1.0617 221.6096 222.6713 248.1740 29.3395 -1.0608 221.7498 222.8106 248.1766 30.1368 -1.0584 221.8672 222.9256 248.1887 30.9340 -1.0522 221.9784 223.0306 248.2163 31.7210 -1.0497 222.0962 223.1458 248.2514 32.5285 -1.0439 222.1840 223.2279 248.3004 33.3463 -1.0461 222.2576 223.3037 248.3299 34.1128 -1.0438 222.3377 223.3815 248.3388 34.9715 -1.0429 222.4480 223.4910 248.4014 35.7380 -1.0390 222.5557 223.5947 248.4259 36.5558 -1.0382 222.6321 223.6703 248.4855 37.3530 -1.0392 222.7361 223.7754 248.5620 38.1513 -1.0381 222.8721 223.9101 248.6324 38.9793 -1.0359 222.9439 223.9797 248.7313 39.7355 -1.0256 223.0234 224.0490 248.7747 40.6045 -1.0225 223.1545 224.1770 248.8457 41.3608 -1.0198 223.2488 224.2686 248.9242 42.1888 -1.0163 223.3286 224.3449 249.0328 42.9860 -1.0114 223.4258 224.4372 249.1641 43.7935 -1.0143 223.5531 224.5674 249.2835 44.5805 -1.0087 223.6693 224.6780 249.4079 45.3778 -1.0045 223.7569 224.7614 249.5367 46.2058 -1.0029 223.8127 224.8156 249.6504 46.9723 -1.0024 223.9305 224.9328 249.7510 47.8310 -1.0039 224.0429 225.0468 249.8416 48.5875 -1.0020 224.1573 225.1593 249.9307 49.4265 -1.0047 224.2226 225.2274 250.0303 50.2135 -1.0009 224.3234 225.3243 250.1343 51.0108 -0.9931 224.4505 225.4436 250.2776 51.8388 -0.9908 224.5382 225.5290 250.4022 52.5950 -0.9902 224.6150 225.6052 250.5447 53.4435 -0.9912 224.7085 225.6997 250.6876 54.2100 -0.9900 224.8049 225.7949 250.8204 55.0380 -0.9880 224.9116 225.8996 250.9289 55.8250 -0.9913 224.9843 225.9756 251.0612 56.6223 -0.9891 225.0684 226.0575 251.2103 57.4503 -0.9884 225.1460 226.1344 251.2977 58.2065 -0.9902 225.2525 226.2427 251.4413 59.0653 -0.9934 225.3513 226.3448 251.6278 59.8318 -0.9941 225.4522 226.4463 251.8036 60.6505 -0.9904 225.5820 226.5723 251.9577 61.4580 -0.9894 225.6900 226.6794 252.1013 62.2450 -0.9868 225.8002 226.7870 252.2296 63.0730 -0.9833 225.9191 226.9025 252.4295 63.8498 -0.9856 225.9765 226.9621 252.6060 64.6778 -0.9858 226.0740 227.0598 252.7644 65.4443 -0.9861 226.1986 227.1848 252.8898 66.3030 -0.9874 226.3130 227.3004 253.0225 67.0593 -0.9898 226.3991 227.3889 253.1850 67.8975 -0.9897 226.5373 227.5270 253.3238 68.6845 -0.9893 226.6465 227.6358 253.4879 69.4820 -0.9903 226.7677 227.7580 253.6434 70.3108 -0.9901 226.8556 227.8457 253.7920 71.0773 -0.9896 226.9602 227.9498 253.9406 71.9360 -0.9888 227.0681 228.0569 254.1029 72.6923 -0.9944 227.1521 228.1465 254.2450 73.5305 -0.9961 227.2188 228.2149 254.3797 74.3175 -0.9999 227.3379 228.3379 254.5159 75.1148 -1.0044 227.4504 228.4547 254.6426 75.9428 -1.0002 227.5561 228.5563 254.7883 76.7093 -0.9999 227.6518 228.6517 254.9009 77.5680 -0.9979 227.7618 228.7597 255.0797 78.3245 -1.0071 227.8624 228.8695 255.2117 79.1635 -1.0112 227.9941 229.0053 255.3882 79.9505 -1.0123 228.0980 229.1103 255.5395 80.7580 -1.0124 228.1795 229.1919 255.6887 81.5758 -1.0112 228.2608 229.2719 255.8124 82.3525 -1.0093 228.3609 229.3701 255.9358 83.1703 -1.0058 228.4513 229.4571 256.0492 83.9265 -1.0092 228.5457 229.5549 256.1533 84.7853 -1.0081 228.6298 229.6379 256.2829 85.5415 -1.0065 228.7378 229.7444 256.3909 86.3695 -1.0036 228.8494 229.8530 256.5326 87.1668 -1.0007 228.9637 229.9644 256.6591 87.9538 -1.0015 229.0522 230.0537 256.7910 88.7818 -1.0042 229.1618 230.1660 256.9495 89.5380 -1.0048 229.2505 230.2554 257.0695 90.3968 -1.0067 229.3572 230.3640 257.1987 91.1643 -1.0110 229.4515 230.4625 257.3400 91.9820 -1.0105 229.5794 230.5899 257.5002 92.7485 -1.0094 229.6921 230.7014 257.5753 93.5765 -1.0077 229.7762 230.7839 257.7092 94.3738 -1.0054 229.8766 230.8820 257.8473 95.1710 -1.0074 229.9724 230.9798 257.9645 95.9888 -1.0154 230.0483 231.0637 258.0984 96.7655 -1.0157 230.1530 231.1686 258.2020 97.6140 -1.0179 230.2289 231.2468 258.3463 98.3805 -1.0206 230.3350 231.3556 258.4882 99.2085 -1.0250 230.4604 231.4854 258.5828 100.0058 -1.0310 230.5765 231.6076 258.6798 100.8030 -1.0345 230.6697 231.7041 258.7699 101.6208 -1.0300 230.7484 231.7784 258.8226 102.3975 -1.0295 230.8439 231.8734 258.8669 103.2468 -1.0304 230.9750 232.0054 258.9797 104.0135 -1.0327 231.1083 232.1410 259.0973 104.8415 -1.0329 231.2221 232.2550 259.2128 105.6183 -1.0343 231.2722 232.3065 259.2964 106.4360 -1.0308 231.3962 232.4269 259.3824 107.2333 -1.0344 231.4864 232.5207 259.4790 108.0305 -1.0382 231.5839 232.6221 259.5944 108.8585 -1.0441 231.7154 232.7594 259.6978 109.6250 -1.0418 231.8340 232.8757 259.7446 110.4735 -1.0400 231.9543 232.9944 259.8285 111.2505 -1.0400 232.0696 233.1096 259.9429 112.0690 -1.0391 232.1808 233.2199 260.0485 112.8663 -1.0360 232.2762 233.3122 260.1311 113.6635 -1.0393 232.3631 233.4025 260.2052 114.4915 -1.0412 232.4864 233.5276 260.2807 115.2580 -1.0461 232.5699 233.6160 260.3855 116.1168 -1.0494 232.6672 233.7166 260.4567 116.8833 -1.0496 232.7914 233.8410 260.5499 117.7010 -1.0496 232.9392 233.9888 260.6050 118.4880 -1.0526 233.0076 234.0603 260.6736 119.2860 -1.0502 233.0905 234.1407 260.7312 120.1143 -1.0506 233.2177 234.2683 260.8300 120.8705 -1.0526 233.3203 234.3729 260.9191 121.7293 -1.0529 233.4178 234.4707 261.0347 122.4855 -1.0514 233.5261 234.5775 261.1223 123.3135 -1.0503 233.6489 234.6992 261.1805 124.1108 -1.0516 233.7590 234.8106 261.2746 124.9080 -1.0482 233.9130 234.9612 261.3461 125.7258 -1.0466 234.0149 235.0615 261.4089 126.5025 -1.0472 234.0918 235.1391 261.4970 127.3510 -1.0471 234.2282 235.2753 261.6027 128.1178 -1.0466 234.2983 235.3449 261.6684 128.9465 -1.0514 234.3774 235.4288 261.7343 129.7130 -1.0562 234.4972 235.5535 261.8048 130.5308 -1.0549 234.5978 235.6527 261.9201 131.3280 -1.0540 234.6941 235.7481 262.0243 132.1253 -1.0531 234.8040 235.8572 262.1275 132.9533 -1.0515 234.8829 235.9344 262.2098 133.7095 -1.0527 234.9298 235.9825 262.2778 134.5785 -1.0481 235.0554 236.1035 262.3678 135.3348 -1.0493 235.1137 236.1630 262.4490 136.1628 -1.0496 235.1920 236.2416 262.5101 136.9600 -1.0520 235.2829 236.3349 262.6043 137.7573 -1.0565 235.3898 236.4463 262.7423 138.5860 -1.0618 235.5036 236.5654 262.8507 139.3418 -1.0588 235.6190 236.6778 262.9225 140.2115 -1.0608 235.7222 236.7830 263.0125 140.9370 -1.0587 235.8149 236.8736 263.1156 141.7958 -1.0608 235.9314 236.9923 263.2257 142.5623 -1.0615 236.0810 237.1425 263.3259 143.3903 -1.0626 236.1809 237.2435 263.4371 144.1875 -1.0601 236.3048 237.3649 263.5000 144.9745 -1.0570 236.3994 237.4564 263.5768 145.8128 -1.0558 236.5094 237.5653 263.6346 146.5690 -1.0584 236.6121 237.6705 263.7496 147.4278 -1.0599 236.6929 237.7528 263.8443 148.1943 -1.0598 236.7791 237.8389 263.9004 149.0223 -1.0562 236.9137 237.9699 264.0091 149.8093 -1.0534 237.0218 238.0752 264.1196 150.6065 -1.0551 237.1407 238.1959 264.2405 151.4250 -1.0526 237.2749 238.3275 264.3011 152.1918 -1.0520 237.3666 238.4186 264.3764 153.0505 -1.0506 237.4402 238.4908 264.5123 153.7760 -1.0492 237.5136 238.5628 264.5944 154.6348 -1.0485 237.5742 238.6228 264.6996 155.4013 -1.0452 237.6656 238.7108 264.8156 156.2190 -1.0453 237.7701 238.8154 264.9306 157.0165 -1.0465 237.8697 238.9161 265.0345 157.8135 -1.0480 237.9325 238.9804 265.1288 158.6423 -1.0506 238.0635 239.1141 265.2326 159.4085 -1.0597 238.1917 239.2514 265.3354 160.2575 -1.0619 238.2904 239.3523 265.4218 161.0340 -1.0603 238.3929 239.4532 265.5346 161.8520 -1.0559 238.5158 239.5717 265.6658 162.6490 -1.0582 238.6477 239.7059 265.7484 163.4465 -1.0558 238.7787 239.8345 265.8464 164.2745 -1.0561 238.8555 239.9117 265.9297 165.0410 -1.0625 238.9476 240.0101 265.9995 165.8895 -1.0637 239.0692 240.1329 266.0755 166.6663 -1.0642 239.1866 240.2508 266.1721 167.4840 -1.0644 239.2810 240.3454 266.2937 168.2813 -1.0680 239.4015 240.4695 266.3966 169.0785 -1.0657 239.4729 240.5386 266.5169 169.9065 -1.0644 239.5494 240.6138 266.6195 170.6730 -1.0650 239.6607 240.7257 266.7375 171.5215 -1.0666 239.7765 240.8430 266.8654 172.2675 -1.0659 239.8676 240.9335 266.9691 173.1168 -1.0697 239.9717 241.0414 267.0580 173.9143 -1.0697 240.0486 241.1182 267.2058 174.7115 -1.0748 240.1996 241.2743 267.3186 175.5088 -1.0743 240.3142 241.3885 267.4147 176.3060 -1.0776 240.3962 241.4738 267.4972 177.1238 -1.0794 240.4647 241.5441 267.5922 177.9005 -1.0798 240.5474 241.6272 267.6780 178.7490 -1.0818 240.6368 241.7186 267.7861 179.5155 -1.0848 240.7133 241.7981 267.8882 180.3445 -1.0898 240.7721 241.8619 267.9947 181.1418 -1.0864 240.9021 241.9885 268.1221 181.9288 -1.0829 241.0504 242.1333 268.2444 182.7568 -1.0782 241.1610 242.2392 268.3940 183.5130 -1.0770 241.2767 242.3537 268.5114 184.3615 -1.0782 241.4006 242.4788 268.6057 185.1383 -1.0847 241.5296 242.6143 268.7146 185.9560 -1.0861 241.6314 242.7175 268.8282 186.7533 -1.0855 241.7518 242.8373 268.9510 187.5505 -1.0851 241.8450 242.9302 269.0773 188.3375 -1.0846 241.9470 243.0316 269.1792 189.1348 -1.0851 242.0530 243.1381 269.2981 189.9635 -1.0767 242.1665 243.2432 269.4024 190.7303 -1.0714 242.2447 243.3161 269.4892 191.5890 -1.0730 242.3277 243.4007 269.5991 192.3453 -1.0705 242.4279 243.4983 269.6965 193.1733 -1.0703 242.5441 243.6143 269.7706 193.9705 -1.0708 242.6854 243.7562 269.8755 194.7575 -1.0794 242.7973 243.8767 270.0161 195.5958 -1.0816 242.8885 243.9701 270.1883 196.3520 -1.0841 242.9722 244.0563 270.3118 197.2108 -1.0840 243.0977 244.1817 270.4598 197.9465 -1.0858 243.2148 244.3006 270.5781 198.8053 -1.0829 243.3462 244.4291 270.6926 199.5720 -1.0815 243.4221 244.5036 270.8007 200.3905 -1.0853 243.5190 244.6042 270.9187 201.1980 -1.0897 243.6278 244.7175 271.0229 201.9850 -1.0922 243.7139 244.8061 271.1037 202.8130 -1.0938 243.8244 244.9182 271.2146 203.5795 -1.0952 243.9440 245.0392 271.3182 204.4383 -1.0971 244.0997 245.1968 271.4047 205.2048 -1.0997 244.1861 245.2858 271.4831 206.0328 -1.0992 244.3057 245.4049 271.5824 206.8300 -1.0996 244.4319 245.5315 271.7050 207.6273 -1.0996 244.5134 245.6130 271.8186 208.4553 -1.1014 244.5831 245.6844 271.8944 209.2115 -1.1020 244.6727 245.7747 271.9974 210.0805 -1.0997 244.7523 245.8520 272.1116 210.8368 -1.1025 244.8185 245.9210 272.2051 211.6760 -1.1063 244.8987 246.0049 272.2925 212.4630 -1.1045 244.9934 246.0979 272.3666 213.2500 -1.1054 245.0755 246.1809 272.5095 214.0678 -1.1078 245.1909 246.2987 272.6424 214.8445 -1.1100 245.3160 246.4261 272.7187 215.6930 -1.1095 245.4441 246.5536 272.8164 216.4185 -1.1116 245.5925 246.7041 272.8861 217.2875 -1.1126 245.7402 246.8528 273.0270 218.0438 -1.1118 245.8135 246.9254 273.1353 218.8615 -1.1113 245.9023 247.0136 273.2262 219.6690 -1.1081 246.0215 247.1296 273.3384 220.4663 -1.1087 246.1149 247.2236 273.4502 221.2945 -1.1078 246.2413 247.3491 273.5716 222.0515 -1.1071 246.3485 247.4556 273.6803 222.9103 -1.1049 246.4985 247.6034 273.8008 223.6768 -1.1045 246.6097 247.7142 273.8966 224.4945 -1.1076 246.7044 247.8120 273.9907 225.3020 -1.1106 246.7838 247.8944 274.0660 226.0890 -1.1137 246.8612 247.9750 274.1696 226.9170 -1.1155 246.9690 248.0845 274.2940 227.6835 -1.1136 247.0895 248.2031 274.3832 228.5218 -1.1124 247.2090 248.3215 274.4935 229.2885 -1.1171 247.2858 248.4029 274.5850 230.1480 -1.1281 247.4084 248.5366 274.6986 230.9043 -1.1282 247.5200 248.6482 274.7920 231.7425 -1.1241 247.6148 248.7389 274.8945 232.5295 -1.1233 247.7091 248.8324 274.9808 233.3268 -1.1238 247.8289 248.9527 275.0776 234.1548 -1.1258 247.9228 249.0485 275.1947 234.9213 -1.1290 248.0072 249.1362 275.3005 235.7800 -1.1288 248.1185 249.2473 275.4311 236.5363 -1.1285 248.2518 249.3803 275.5178 237.3745 -1.1314 248.3972 249.5285 275.5948 238.1308 -1.1279 248.4786 249.6065 275.6505 238.9695 -1.1265 248.5972 249.7237 275.7113 239.7570 -1.1281 248.6654 249.7936 275.8301 240.5645 -1.1324 248.7600 249.8924 275.9454 241.3823 -1.1337 248.8253 249.9590 276.0739 242.1488 -1.1342 248.8964 250.0306 276.2026 243.0075 -1.1330 249.0473 250.1803 276.3071 243.7740 -1.1339 249.1715 250.3055 276.3991 244.6020 -1.1338 249.2535 250.3873 276.4898 245.3890 -1.1341 249.3520 250.4861 276.5974 246.1863 -1.1318 249.4340 250.5659 276.7075 247.0040 -1.1309 249.5308 250.6616 276.7998 247.7705 -1.1349 249.6130 250.7480 276.9122 248.6200 -1.1365 249.7261 250.8626 277.0284 249.3865 -1.1366 249.8395 250.9761 277.1518 250.2145 -1.1389 249.9437 251.0826 277.2596 251.0015 -1.1411 250.0279 251.1690 277.3507 251.7988 -1.1425 250.1581 251.3006 277.4566 252.5960 -1.1447 250.2992 251.4439 277.5590 253.3933 -1.1440 250.4294 251.5735 277.6400 254.2110 -1.1465 250.5433 251.6898 277.7333 254.9775 -1.1512 250.6272 251.7784 277.8339 255.8363 -1.1502 250.7325 251.8828 277.9481 256.6030 -1.1452 250.8139 251.9591 278.0557 257.4215 -1.1424 250.9443 252.0867 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