DTA measure 1gyors Date: 2026922:151 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.34 s Mass = 1191.8 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2718 -3.8957 201.0757 204.9714 247.0903 2.0990 -3.8757 201.2509 205.1266 246.9600 2.8550 -3.8778 201.4520 205.3298 246.8726 3.6830 -3.8780 201.7216 205.5995 246.8486 4.4485 -3.8685 201.8967 205.7652 246.8329 5.3073 -3.8612 202.1590 206.0202 246.8006 6.0738 -3.8606 202.3171 206.1777 246.7367 6.8905 -3.8490 202.4467 206.2957 246.7213 7.6980 -3.8369 202.6938 206.5307 246.6279 8.4848 -3.8298 202.8522 206.6820 246.5508 9.3018 -3.8274 202.9216 206.7490 246.4685 10.0785 -3.8241 203.0914 206.9156 246.4677 10.9265 -3.8206 203.4109 207.2316 246.4138 11.6720 -3.8044 203.5624 207.3668 246.4206 12.5205 -3.8035 203.7484 207.5519 246.3977 13.2965 -3.7913 203.9103 207.7015 246.3256 14.1140 -3.7910 204.0606 207.8516 246.3539 14.9113 -3.7904 204.1985 207.9889 246.2310 15.7075 -3.7750 204.3938 208.1687 246.1552 16.5253 -3.7662 204.6541 208.4203 246.1964 17.2915 -3.7711 204.8433 208.6144 246.2321 18.1495 -3.7644 205.0188 208.7832 246.2355 18.9058 -3.7562 205.1807 208.9369 246.2458 19.7335 -3.7437 205.3508 209.0945 246.2567 20.5300 -3.7365 205.6267 209.3632 246.2886 21.3273 -3.7315 205.7949 209.5264 246.3812 22.1548 -3.7211 205.8703 209.5914 246.3843 22.9105 -3.7129 206.0093 209.7222 246.3420 23.7795 -3.7073 206.2145 209.9218 246.2338 24.5350 -3.7006 206.2848 209.9855 246.2109 25.3628 -3.6904 206.4291 210.1195 246.2954 26.1600 -3.6775 206.5987 210.2762 246.3585 26.9568 -3.6710 206.7701 210.4411 246.3508 27.7843 -3.6709 206.9372 210.6081 246.3523 28.5405 -3.6653 207.1303 210.7956 246.3186 29.4088 -3.6529 207.3296 210.9825 246.3950 30.1648 -3.6433 207.4684 211.1117 246.4801 30.9928 -3.6369 207.7201 211.3570 246.5066 31.7890 -3.6208 207.8845 211.5053 246.6938 32.6068 -3.6114 208.1815 211.7929 246.7526 33.3733 -3.5924 208.3985 211.9908 246.8176 34.2005 -3.5880 208.5340 212.1220 246.9206 34.9975 -3.5797 208.6328 212.2125 246.9643 35.7845 -3.5746 208.7704 212.3450 247.0580 36.6218 -3.5661 208.9229 212.4890 247.0679 37.3780 -3.5476 209.1251 212.6727 247.1717 38.2368 -3.5414 209.2364 212.7779 247.3546 39.0023 -3.5283 209.3928 212.9211 247.4802 39.8405 -3.5163 209.6626 213.1789 247.6142 40.6275 -3.5156 209.8646 213.3801 247.7163 41.4238 -3.5062 209.9950 213.5012 247.8308 42.2620 -3.4944 210.2234 213.7178 247.9224 43.0385 -3.4841 210.4278 213.9120 248.0441 43.8658 -3.4845 210.5393 214.0238 248.2209 44.6323 -3.4767 210.6360 214.1127 248.3976 45.4908 -3.4679 210.8578 214.3257 248.5700 46.2463 -3.4662 210.9554 214.4216 248.7228 47.0845 -3.4702 211.2027 214.6729 248.9410 47.8710 -3.4602 211.4782 214.9383 249.1341 48.6678 -3.4423 211.5801 215.0224 249.3159 49.4958 -3.4276 211.7051 215.1327 249.4435 50.2615 -3.4164 211.8911 215.3075 249.5817 51.1200 -3.4090 211.9728 215.3818 249.7495 51.8763 -3.4051 212.0951 215.5003 249.9227 52.7243 -3.3970 212.2508 215.6478 250.1066 53.4698 -3.3919 212.3821 215.7740 250.3087 54.3285 -3.3833 212.4689 215.8522 250.4541 55.0945 -3.3804 212.6586 216.0390 250.5214 55.9118 -3.3767 212.8416 216.2183 250.6928 56.7090 -3.3770 213.0201 216.3971 250.9235 57.5058 -3.3745 213.2924 216.6669 251.0908 58.2923 -3.3686 213.5693 216.9379 251.3185 59.0895 -3.3663 213.7714 217.1376 251.5876 59.9063 -3.3526 213.8855 217.2382 251.7906 60.6625 -3.3523 213.9877 217.3400 251.8774 61.5315 -3.3601 214.1010 217.4611 252.0458 62.2868 -3.3628 214.2913 217.6541 252.1364 63.1250 -3.3639 214.4734 217.8373 252.3287 63.8915 -3.3686 214.5715 217.9401 252.5471 64.7190 -3.3637 214.6198 217.9836 252.7761 65.5158 -3.3511 214.8258 218.1769 252.9661 66.3130 -3.3475 214.9598 218.3073 253.1106 67.1298 -3.3440 214.9983 218.3423 253.2740 67.8963 -3.3372 215.1420 218.4792 253.4862 68.7550 -3.3302 215.2825 218.6127 253.6203 69.4795 -3.3291 215.4879 218.8170 253.7924 70.3485 -3.3353 215.7741 219.1095 254.0239 71.1043 -3.3198 215.9038 219.2236 254.2174 71.9215 -3.3124 216.0543 219.3667 254.4443 72.7290 -3.3170 216.2490 219.5660 254.6484 73.5363 -3.3092 216.4440 219.7532 254.7634 74.3430 -3.3036 216.6145 219.9181 254.9918 75.1300 -3.3060 216.7231 220.0291 255.3121 75.9580 -3.2903 216.7871 220.0775 255.5099 76.7235 -3.2961 216.9021 220.1982 255.6830 77.5823 -3.2878 217.0862 220.3740 255.9414 78.3488 -3.2785 217.3529 220.6315 256.1687 79.1655 -3.2788 217.5308 220.8096 256.3425 79.9730 -3.2656 217.6818 220.9475 256.5215 80.7600 -3.2605 217.8356 221.0961 256.7492 81.5870 -3.2615 218.0652 221.3266 256.8189 82.3535 -3.2552 218.2533 221.5085 256.8882 83.2120 -3.2494 218.4125 221.6620 257.0038 83.9675 -3.2460 218.5470 221.7931 257.1513 84.7955 -3.2429 218.6788 221.9218 257.3268 85.5615 -3.2434 218.7317 221.9750 257.4858 86.4095 -3.2406 218.8460 222.0866 257.6805 87.1863 -3.2288 218.9790 222.2078 257.7991 88.0035 -3.2286 219.1921 222.4208 257.8996 88.8003 -3.2279 219.3204 222.5483 258.0488 89.5975 -3.2210 219.5049 222.7259 258.3021 90.4250 -3.2154 219.7209 222.9364 258.4197 91.1910 -3.2164 219.9149 223.1313 258.5159 92.0395 -3.2163 220.0577 223.2740 258.6478 92.8155 -3.2174 220.2528 223.4702 258.7408 93.6433 -3.2091 220.4518 223.6609 258.9414 94.4303 -3.2106 220.5960 223.8066 259.0487 95.2470 -3.2083 220.6707 223.8789 259.1022 96.0443 -3.2104 220.8124 224.0229 259.1270 96.8415 -3.2124 220.9092 224.1216 259.3152 97.6688 -3.2134 221.1731 224.3865 259.3732 98.4350 -3.2098 221.2806 224.4904 259.5174 99.2835 -3.2127 221.3830 224.5958 259.6053 100.0593 -3.2125 221.6579 224.8705 259.6647 100.8770 -3.2059 221.8758 225.0817 259.8288 101.6740 -3.2046 222.0035 225.2081 259.9679 102.4705 -3.2038 222.1673 225.3711 260.1249 103.2985 -3.1945 222.2840 225.4785 260.1882 104.0645 -3.2019 222.3715 225.5733 260.3048 104.9228 -3.1986 222.6115 225.8101 260.5118 105.6893 -3.1920 222.6449 225.8369 260.6864 106.5168 -3.1852 222.7647 225.9499 260.8465 107.3135 -3.1835 222.9117 226.0952 260.8647 108.1005 -3.1822 223.0933 226.2755 260.9723 108.9383 -3.1823 223.3308 226.5131 260.9956 109.6940 -3.1789 223.4843 226.6632 261.1425 110.5630 -3.1776 223.6469 226.8245 261.2701 111.3185 -3.1824 223.8645 227.0469 261.3760 112.1565 -3.1836 224.1138 227.2974 261.4946 112.9435 -3.1843 224.3889 227.5731 261.5099 113.7398 -3.1884 224.4579 227.6463 261.6369 114.5678 -3.1934 224.5170 227.7104 261.7832 115.3340 -3.1840 224.6879 227.8719 261.8712 116.1920 -3.1856 224.6990 227.8846 261.9989 116.9585 -3.1752 224.8343 228.0095 262.1353 117.7865 -3.1769 225.0104 228.1873 262.3267 118.5828 -3.1768 225.1079 228.2848 262.4772 119.3698 -3.1692 225.2244 228.3936 262.4996 120.1975 -3.1755 225.5406 228.7162 262.5693 120.9530 -3.1692 225.6386 228.8078 262.6663 121.8015 -3.1558 225.7990 228.9547 262.6293 122.5470 -3.1495 225.9306 229.0801 262.7370 123.3950 -3.1532 226.0894 229.2426 262.8759 124.1513 -3.1540 226.1824 229.3364 262.9225 124.9788 -3.1578 226.3985 229.5562 263.0832 125.7755 -3.1618 226.6009 229.7626 263.1939 126.5625 -3.1597 226.8033 229.9629 263.2763 127.3900 -3.1511 226.9667 230.1178 263.4353 128.1560 -3.1598 227.1939 230.3537 263.4853 128.9738 -3.1498 227.3128 230.4626 263.6471 129.7498 -3.1460 227.3842 230.5302 263.7323 130.5980 -3.1359 227.4575 230.5934 263.8068 131.3645 -3.1364 227.5400 230.6765 263.8763 132.1920 -3.1374 227.6838 230.8212 263.9792 132.9785 -3.1368 227.8338 230.9705 264.1015 133.7758 -3.1246 228.0369 231.1615 264.3393 134.6030 -3.1176 228.2473 231.3649 264.4331 135.3693 -3.1201 228.3468 231.4669 264.5804 136.2280 -3.1225 228.4292 231.5518 264.8117 136.9530 -3.1202 228.6020 231.7222 264.8668 137.8113 -3.1191 228.8396 231.9588 264.9494 138.5778 -3.1112 228.9154 232.0266 265.0199 139.3948 -3.1061 229.0627 232.1688 265.1127 140.2020 -3.0992 229.1775 232.2767 265.2785 140.9890 -3.1076 229.3847 232.4924 265.3908 141.8163 -3.1094 229.6503 232.7597 265.4872 142.5825 -3.0991 229.7685 232.8676 265.7029 143.4413 -3.0973 229.9259 233.0232 265.8455 144.2070 -3.0964 230.1269 233.2233 265.9513 145.0450 -3.0954 230.2136 233.3090 266.1028 145.8115 -3.0975 230.3741 233.4716 266.2425 146.6388 -3.0955 230.5240 233.6195 266.4742 147.4358 -3.1000 230.6180 233.7180 266.6292 148.2330 -3.0964 230.8086 233.9050 266.7960 149.0498 -3.0985 230.8982 233.9966 266.9130 149.8265 -3.0955 230.9786 234.0741 267.0395 150.6745 -3.0848 231.1729 234.2577 267.2351 151.4405 -3.0900 231.3460 234.4360 267.4261 152.2685 -3.0793 231.5937 234.6730 267.6022 153.0655 -3.0802 231.7456 234.8258 267.6575 153.8620 -3.0740 231.9769 235.0509 267.6866 154.6798 -3.0677 232.0825 235.1502 267.7747 155.4768 -3.0661 232.2820 235.3481 267.8263 156.2630 -3.0739 232.2795 235.3533 267.8382 157.0705 -3.0686 232.3945 235.4631 267.9280 157.8878 -3.0711 232.5776 235.6487 268.1476 158.6538 -3.0711 232.7309 235.8021 268.2920 159.5125 -3.0518 232.8736 235.9254 268.4262 160.2783 -3.0500 232.9960 236.0460 268.5359 161.1060 -3.0462 233.1302 236.1764 268.6415 161.8930 -3.0440 233.2714 236.3154 268.8446 162.6995 -3.0422 233.4709 236.5131 269.0164 163.5173 -3.0419 233.6081 236.6500 269.1957 164.2935 -3.0406 233.7313 236.7719 269.2947 165.1518 -3.0455 233.8962 236.9416 269.3655 165.9080 -3.0495 234.0285 237.0781 269.4654 166.7253 -3.0453 234.1577 237.2031 269.5387 167.5015 -3.0426 234.2484 237.2910 269.6725 168.3500 -3.0430 234.4083 237.4513 269.7628 169.1158 -3.0372 234.4953 237.5325 269.8493 169.9435 -3.0283 234.6607 237.6890 270.0797 170.7408 -3.0181 234.7734 237.7915 270.2556 171.5370 -3.0184 234.9695 237.9879 270.4273 172.3548 -3.0178 235.1107 238.1284 270.5656 173.1313 -3.0258 235.2934 238.3191 270.7100 173.9790 -3.0263 235.5364 238.5627 270.8766 174.7455 -3.0288 235.6800 238.7088 271.0706 175.5735 -3.0211 235.8019 238.8231 271.2092 176.3698 -3.0240 235.9182 238.9422 271.3410 177.1670 -3.0208 236.0712 239.0920 271.5003 177.9845 -3.0234 236.1520 239.1754 271.6647 178.7605 -3.0177 236.2823 239.3000 271.7837 179.6090 -3.0174 236.5828 239.6002 271.9959 180.3858 -3.0192 236.7200 239.7392 272.1236 181.2230 -3.0169 236.8266 239.8435 272.2358 182.0203 -3.0173 237.0350 240.0522 272.3933 182.8170 -3.0226 237.2613 240.2839 272.5861 183.6343 -3.0249 237.3594 240.3843 272.6868 184.4008 -3.0162 237.4483 240.4645 272.8896 185.2283 -3.0150 237.6064 240.6214 273.1192 185.9840 -3.0144 237.7696 240.7840 273.1654 186.8325 -3.0097 237.8435 240.8532 273.2498 187.6085 -3.0202 238.0612 241.0815 273.4457 188.4260 -3.0221 238.2001 241.2223 273.5714 189.2130 -3.0196 238.3944 241.4141 273.7233 190.0198 -3.0214 238.5216 241.5430 273.8092 190.8373 -3.0160 238.5811 241.5971 273.9441 191.5933 -3.0102 238.6881 241.6983 274.0787 192.4615 -3.0084 238.8256 241.8340 274.2251 193.2178 -3.0053 238.9113 241.9166 274.4015 194.0348 -2.9975 239.0953 242.0928 274.5063 194.8420 -2.9982 239.2310 242.2292 274.6144 195.6290 -2.9995 239.3989 242.3984 274.7314 196.4253 -2.9988 239.4928 242.4917 274.8399 197.2225 -3.0031 239.5978 242.6009 275.0559 198.0505 -2.9967 239.7753 242.7720 275.2394 198.8160 -2.9969 239.9529 242.9498 275.3718 199.6645 -2.9967 240.1337 243.1304 275.5276 200.4413 -3.0020 240.3774 243.3794 275.6473 201.2580 -2.9882 240.5448 243.5330 275.7178 202.0553 -2.9921 240.6744 243.6665 275.7868 202.8523 -2.9923 240.7270 243.7193 275.8509 203.6795 -2.9881 240.9054 243.8934 276.0229 204.4460 -2.9984 241.1312 244.1296 276.2196 205.2943 -3.0057 241.3318 244.3374 276.3930 206.0703 -3.0025 241.3717 244.3742 276.5700 206.8880 -3.0086 241.5370 244.5456 276.7409 207.6850 -2.9975 241.7284 244.7259 276.8127 208.4815 -2.9925 241.8700 244.8625 276.9451 209.3095 -2.9989 241.9673 244.9662 277.0096 210.0753 -2.9964 242.1531 245.1495 277.1464 210.9235 -2.9908 242.3452 245.3360 277.3640 211.7003 -2.9821 242.5746 245.5567 277.4255 212.5173 -2.9821 242.7400 245.7220 277.4565 213.3143 -2.9824 242.8762 245.8587 277.4621 214.1115 -2.9874 242.9925 245.9799 277.5927 214.9388 -2.9852 243.1432 246.1284 277.7815 215.7050 -2.9881 243.2505 246.2386 277.8904 216.5535 -2.9856 243.4875 246.4731 277.9731 217.3295 -2.9783 243.5997 246.5780 278.1050 218.1470 -2.9730 243.6941 246.6671 278.2752 218.9135 -2.9705 243.7937 246.7641 278.4254 219.7405 -2.9568 243.9735 246.9303 278.6150 220.5378 -2.9646 244.1273 247.0920 278.7451 221.3345 -2.9619 244.1853 247.1472 278.8477 222.1518 -2.9675 244.2085 247.1759 278.9495 222.9285 -2.9710 244.3419 247.3128 279.1168 223.7765 -2.9734 244.6405 247.6139 279.3254 224.5425 -2.9691 244.8536 247.8227 279.3925 225.3705 -2.9691 245.0535 248.0226 279.4274 226.1670 -2.9737 245.1889 248.1626 279.4863 226.9743 -2.9739 245.3581 248.3321 279.5491 227.7610 -2.9701 245.5193 248.4894 279.6990 228.5780 -2.9613 245.6866 248.6479 279.8276 229.3753 -2.9645 245.9350 248.8995 279.9136 230.1723 -2.9634 246.0193 248.9828 280.0195 230.9995 -2.9606 246.1995 249.1601 280.1624 231.7660 -2.9544 246.2384 249.1928 280.2496 232.6245 -2.9518 246.3197 249.2714 280.3848 233.3903 -2.9583 246.4260 249.3843 280.4545 234.2183 -2.9613 246.6240 249.5853 280.5318 235.0150 -2.9596 246.8431 249.8027 280.7035 235.8015 -2.9634 247.0627 250.0261 280.8697 236.6398 -2.9585 247.2173 250.1758 280.9492 237.4260 -2.9591 247.3650 250.3240 281.0062 238.2230 -2.9583 247.4581 250.4164 281.2059 239.0203 -2.9571 247.6688 250.6259 281.3882 239.8475 -2.9518 247.7580 250.7099 281.4434 240.6035 -2.9430 247.8487 250.7917 281.5318 241.4725 -2.9378 248.0553 250.9931 281.6708 242.2278 -2.9311 248.1807 251.1118 281.7879 243.0660 -2.9378 248.2699 251.2077 281.9488 243.8530 -2.9399 248.3615 251.3015 282.0534 244.6598 -2.9500 248.5009 251.4509 282.2187 245.4773 -2.9587 248.6687 251.6274 282.3538 246.2438 -2.9566 248.8393 251.7959 282.3549 247.1120 -2.9550 248.8764 251.8314 282.4452 247.8475 -2.9579 249.0058 251.9637 282.5644 248.7058 -2.9666 249.1782 252.1448 282.7685 249.4615 -2.9701 249.3184 252.2885 282.9233 250.2895 -2.9640 249.4902 252.4543 283.0966 251.0763 -2.9553 249.6262 252.5814 283.2418 251.8625 -2.9379 249.7705 252.7084 283.3865 252.6700 -2.9399 250.0254 252.9653 283.5243 253.4568 -2.9304 250.2027 253.1331 283.6721 254.2738 -2.9300 250.3479 253.2779 283.8324 255.0505 -2.9300 250.5201 253.4502 283.9554 255.8985 -2.9266 250.6158 253.5424 284.0136 256.6543 -2.9318 250.6903 253.6222 284.1659 257.5028 -2.9316 250.6302 253.5618 284.3359 258.2378 -2.9352 250.7555 253.6907 284.4751 259.1065 -2.9397 251.0124 253.9521 284.6002 259.8628 -2.9428 251.2351 254.1779 284.7409 260.6795 -2.9313 251.3870 254.3182 284.8576 261.4870 -2.9247 251.5204 254.4451 284.9552 262.2738 -2.9194 251.6730 254.5924 285.0275 263.0908 -2.9188 251.8502 254.7691 285.1081 263.8675 -2.9203 251.9966 254.9169 285.3117 264.7160 -2.9214 252.1562 255.0776 285.5081 265.4815 -2.9186 252.2950 255.2136 285.7277 266.3095 -2.9123 252.3504 255.2627 285.8449 267.1068 -2.9145 252.4433 255.3578 285.9683 267.9133 -2.9107 252.6928 255.6036 286.0604 268.6900 -2.9053 252.8696 255.7750 286.2461 269.5180 -2.9122 253.0016 255.9138 286.4375 270.3040 -2.9175 253.0416 255.9591 286.5682 271.1115 -2.9222 253.1124 256.0346 286.6491 271.9288 -2.9310 253.2010 256.1321 286.9055 272.6948 -2.9278 253.4087 256.3366 287.0364 273.5535 -2.9239 253.5893 256.5131 287.1665 274.3195 -2.9251 253.7775 256.7026 287.2246 275.1470 -2.9323 253.9064 256.8387 287.3694 275.9340 -2.9284 254.0588 256.9872 287.5248 276.7410 -2.9253 254.1619 257.0872 287.6437 277.5583 -2.9214 254.3019 257.2232 287.7346 278.3555 -2.9257 254.4969 257.4226 287.8372 279.1415 -2.9231 254.5379 257.4610 287.9954 279.9388 -2.9224 254.5866 257.5090 288.1491 280.7668 -2.9292 254.7755 257.7047 288.2478 281.5323 -2.9312 254.9648 257.8960 288.3720 282.3910 -2.9257 255.0918 258.0175 288.5214 283.1575 -2.9324 255.2938 258.2262 288.6433 283.9845 -2.9434 255.3972 258.3406 288.7350 284.7818 -2.9423 255.5023 258.4446 288.8472 285.5785 -2.9502 255.6481 258.5983 289.0238 286.3958 -2.9477 255.7658 258.7135 289.1926 287.1725 -2.9370 255.9106 258.8476 289.3851 288.0205 -2.9385 256.0591 258.9976 289.6592 288.7865 -2.9224 256.1753 259.0977 289.8141 289.6145 -2.9217 256.3743 259.2960 289.8953 290.3803 -2.9207 256.4947 259.4154 289.9817 291.2285 -2.9193 256.4989 259.4183 290.0846 292.0053 -2.9200 256.6418 259.5618 290.1893 292.8223 -2.9257 256.9024 259.8281 290.2956 293.6193 -2.9289 257.0220 259.9510 290.3322 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